#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:34:15 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180790 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/21/2012165.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012165_Fobs loop_ _publ_author_name 'Lu, Ying-Hong' 'Fun, Hoong-Kun' 'Chantrapromma, Suchada' 'Razak, Ibrahim Abdul' 'Shen, Zhen' 'Zuo, Jing-Lin' 'You, Xiao-Zeng' _publ_section_title ; A mixed-valence manganese(III)--manganese(IV) di-\m-oxo complex, [(cyclam)MnO]~2~(ClO~4~)~2~(NO~3~) ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 911 _journal_page_last 913 _journal_volume 57 _journal_year 2001 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.508 _cell_angle_gamma 90.000 _cell_length_a 19.9616 _cell_length_b 13.8047 _cell_length_c 12.1531 _exptl_crystal_F_000 1676.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file sk1485Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sz038 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 325.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 81953.70 82315.25 2346.48 o 6 0 0 6302.97 5941.00 141.47 o 8 0 0 41.03 87.21 14.33 o 10 0 0 5228.27 5348.50 160.29 o 12 0 0 44.04 77.72 26.78 o 14 0 0 4788.40 4151.43 283.09 o 16 0 0 17417.06 17069.36 496.79 o 18 0 0 1542.86 1676.70 60.94 o 20 0 0 2.37 23.36 15.21 o 22 0 0 595.95 493.75 30.39 o 24 0 0 354.74 269.70 37.99 o 3 1 0 718.67 596.51 13.77 o 5 1 0 44341.42 45121.25 914.01 o 7 1 0 194.24 194.08 9.41 o 9 1 0 513.43 458.91 13.29 o 11 1 0 582.57 640.12 22.51 o 13 1 0 4.40 11.83 7.56 o 15 1 0 30.20 55.95 12.53 o 17 1 0 36.08 16.44 10.48 o 19 1 0 102.08 68.16 19.87 o 21 1 0 241.28 295.87 17.34 o 23 1 0 0.36 -7.19 12.81 o 25 1 0 5.12 21.56 19.32 o 2 2 0 11779.18 13989.14 279.73 o 4 2 0 28812.37 28964.97 575.95 o 6 2 0 5542.96 5328.86 99.13 o 8 2 0 1282.04 1807.59 41.64 o 10 2 0 6285.71 6610.37 139.01 o 12 2 0 1082.81 1281.42 32.35 o 14 2 0 1493.31 1394.90 41.55 o 16 2 0 9242.76 9075.41 233.11 o 18 2 0 1882.01 1801.21 66.23 o 20 2 0 4.21 5.71 30.83 o 22 2 0 149.69 170.11 18.03 o 24 2 0 375.90 308.33 22.65 o 1 3 0 19639.62 19842.41 907.07 o 3 3 0 15583.89 17235.36 344.36 o 5 3 0 35369.01 36037.57 715.97 o 7 3 0 12691.10 13959.38 280.70 o 9 3 0 16.15 6.68 7.64 o 11 3 0 8143.48 7825.03 235.36 o 13 3 0 193.84 232.75 21.18 o 15 3 0 138.94 123.11 14.14 o 17 3 0 5.94 12.19 11.02 o 19 3 0 44.54 33.55 12.35 o 21 3 0 853.60 1029.62 44.42 o 23 3 0 197.96 180.37 19.07 o 25 3 0 44.85 46.15 16.44 o 0 4 0 1944.19 1458.64 38.03 o 2 4 0 24662.68 26815.70 439.07 o 4 4 0 589.72 383.10 14.47 o 6 4 0 24221.20 24720.22 493.02 o 8 4 0 10682.60 11672.85 236.02 o 10 4 0 73.05 115.09 9.85 o 12 4 0 214.29 298.02 16.22 o 14 4 0 2093.32 2232.82 74.63 o 16 4 0 1542.46 1289.31 71.01 o 18 4 0 1025.35 1024.24 48.89 o 20 4 0 72.19 74.81 13.66 o 22 4 0 50.27 35.87 14.41 o 24 4 0 228.86 208.42 20.09 o 1 5 0 421.28 595.27 13.19 o 3 5 0 1035.95 1368.21 25.74 o 5 5 0 26413.37 24428.08 434.56 o 7 5 0 29951.92 28003.04 558.65 o 9 5 0 17638.79 17862.08 492.45 o 11 5 0 17534.82 18387.21 369.84 o 13 5 0 1275.83 1245.86 32.38 o 15 5 0 3.70 -6.23 13.02 o 17 5 0 35.46 9.46 13.01 o 19 5 0 43.19 52.64 13.15 o 21 5 0 1121.21 1043.90 66.02 o 23 5 0 1342.40 1335.45 57.61 o 0 6 0 5304.15 5344.36 127.95 o 2 6 0 5044.87 5263.01 89.17 o 4 6 0 5163.17 6116.22 103.16 o 6 6 0 1424.20 1462.68 30.34 o 8 6 0 6433.38 6386.81 132.17 o 10 6 0 4532.90 4153.42 94.13 o 12 6 0 1.56 15.12 9.92 o 14 6 0 231.04 274.18 19.82 o 16 6 0 54.09 25.65 20.87 o 18 6 0 3.35 1.97 12.86 o 20 6 0 98.38 118.22 15.84 o 22 6 0 0.17 -1.09 12.97 o 24 6 0 159.92 180.79 19.34 o 1 7 0 430.20 407.40 10.85 o 3 7 0 532.90 595.93 19.92 o 5 7 0 8164.14 6230.32 105.40 o 7 7 0 5425.51 6091.44 126.40 o 9 7 0 1577.86 1839.86 43.10 o 11 7 0 6120.03 5608.54 172.52 o 13 7 0 4520.71 4136.37 133.86 o 15 7 0 2213.42 2084.57 58.00 o 17 7 0 27.98 15.85 18.06 o 19 7 0 595.33 566.36 34.88 o 21 7 0 1532.94 1437.76 58.32 o 23 7 0 603.60 542.54 27.88 o 0 8 0 6604.44 7809.96 185.33 o 2 8 0 2.18 7.75 7.99 o 4 8 0 1587.21 1984.81 36.65 o 6 8 0 67.33 75.24 6.30 o 8 8 0 6161.28 5469.32 114.66 o 10 8 0 1878.11 2042.91 47.84 o 12 8 0 990.63 1127.79 53.48 o 14 8 0 85.53 54.11 14.20 o 16 8 0 948.34 947.18 40.34 o 18 8 0 545.35 508.83 32.08 o 20 8 0 15.36 36.11 15.96 o 22 8 0 40.60 25.03 17.80 o 1 9 0 523.41 445.56 14.56 o 3 9 0 5490.56 6200.79 105.26 o 5 9 0 8345.00 8045.66 156.09 o 7 9 0 254.46 271.15 11.16 o 9 9 0 39.40 40.16 8.38 o 11 9 0 1061.18 1210.09 37.98 o 13 9 0 1976.54 1767.74 50.63 o 15 9 0 2278.16 2163.93 59.91 o 17 9 0 1.17 -4.62 13.63 o 19 9 0 986.29 904.38 59.79 o 21 9 0 1209.03 1233.60 58.55 o 0 10 0 5795.81 5281.64 128.20 o 2 10 0 115.93 42.79 6.36 o 4 10 0 1785.15 1987.77 37.40 o 6 10 0 83.91 100.47 8.48 o 8 10 0 185.22 178.07 11.61 o 10 10 0 304.67 326.43 13.90 o 12 10 0 169.86 148.89 21.39 o 14 10 0 0.91 -6.23 16.82 o 16 10 0 840.79 857.53 42.98 o 18 10 0 1.93 -1.87 20.55 o 20 10 0 7.78 34.88 22.42 o 1 11 0 359.43 587.89 16.76 o 3 11 0 2893.65 2861.26 51.76 o 5 11 0 3165.93 3116.41 68.92 o 7 11 0 2610.39 2284.52 52.98 o 9 11 0 28.27 32.72 9.26 o 11 11 0 382.48 394.53 18.61 o 13 11 0 1643.69 1807.09 49.63 o 15 11 0 829.09 767.42 29.18 o 17 11 0 22.29 19.80 11.28 o 19 11 0 836.46 848.92 57.10 o 0 12 0 1812.44 1705.08 46.91 o 2 12 0 143.61 71.95 8.76 o 4 12 0 9.92 50.50 12.05 o 6 12 0 62.16 58.75 9.88 o 8 12 0 1140.24 1048.47 34.14 o 10 12 0 1995.96 1805.00 44.43 o 12 12 0 115.01 120.57 14.33 o 14 12 0 307.87 295.11 23.09 o 16 12 0 297.07 331.01 19.99 o 18 12 0 78.75 68.50 14.23 o 1 13 0 597.85 616.33 20.34 o 3 13 0 1794.05 2022.72 47.93 o 5 13 0 910.10 763.30 23.65 o 7 13 0 574.95 595.39 24.66 o 9 13 0 161.48 154.57 12.61 o 11 13 0 568.76 606.17 25.07 o 13 13 0 901.87 871.80 31.76 o 15 13 0 135.09 133.05 16.17 o 17 13 0 10.52 23.93 12.40 o 0 14 0 54.13 7.47 15.57 o 2 14 0 611.33 572.44 23.71 o 4 14 0 54.34 84.77 13.05 o 6 14 0 1159.99 1116.45 35.71 o 8 14 0 3194.40 3194.39 115.78 o 10 14 0 1000.31 945.01 32.62 o 12 14 0 83.54 83.65 13.74 o 14 14 0 47.06 14.98 12.55 o 16 14 0 103.36 123.09 16.18 o 1 15 0 8.50 -3.85 11.79 o 3 15 0 101.93 55.91 14.27 o 5 15 0 262.74 251.19 21.36 o 7 15 0 63.46 119.12 17.36 o 9 15 0 23.51 22.73 13.65 o 11 15 0 302.37 251.32 21.53 o 13 15 0 437.00 482.16 23.86 o 2 16 0 588.60 671.96 43.60 o 4 16 0 5.44 1.87 17.44 o 6 16 0 710.45 668.85 48.89 o 8 16 0 1321.09 1458.72 77.86 o 10 16 0 665.91 641.84 74.74 o 1 17 0 63.99 73.64 17.02 o 3 17 0 93.19 99.28 17.36 o 5 17 0 4.31 13.18 14.07 o 7 17 0 5.41 14.33 20.55 o -25 1 1 949.57 995.76 47.33 o -23 1 1 450.93 583.22 35.40 o -21 1 1 15.39 45.45 17.61 o -19 1 1 425.19 416.26 26.82 o -17 1 1 2635.90 2526.08 68.41 o -15 1 1 7788.88 7676.86 162.10 o -13 1 1 933.58 1127.00 30.11 o -11 1 1 130.18 217.08 13.04 o -9 1 1 15116.91 12040.01 313.79 o -7 1 1 1346.15 1263.25 102.15 o -5 1 1 3315.20 2844.43 87.15 o -3 1 1 2278.81 2156.96 53.43 o -1 1 1 40359.02 38998.07 1512.29 o 1 1 1 44358.39 41600.00 1352.53 o 3 1 1 2084.96 2040.11 39.43 o 5 1 1 78663.07 78881.34 1416.61 o 7 1 1 2096.80 1529.64 31.36 o 9 1 1 1631.28 1254.90 24.49 o 11 1 1 6864.66 6849.08 121.03 o 13 1 1 34.71 48.43 8.04 o 15 1 1 6566.80 6826.33 128.54 o 17 1 1 6035.69 5606.74 126.17 o 19 1 1 795.90 584.45 21.78 o 21 1 1 731.92 1023.71 31.92 o 23 1 1 215.27 224.66 16.76 o 25 1 1 619.12 728.66 31.98 o -24 2 1 15.75 12.70 19.36 o -22 2 1 308.44 314.32 60.73 o -20 2 1 254.92 227.67 18.03 o -18 2 1 683.98 753.48 71.63 o -16 2 1 2.43 4.25 23.36 o -14 2 1 2029.60 2149.39 58.06 o -12 2 1 82.62 66.83 13.12 o -10 2 1 343.16 219.73 15.40 o -8 2 1 23.92 47.75 12.46 o -6 2 1 6510.54 7924.34 329.68 o -4 2 1 27174.08 28541.52 2455.63 o -2 2 1 30858.77 37364.08 859.77 o 0 2 1 47052.55 48372.07 1682.95 o 2 2 1 16384.40 16470.23 328.74 o 4 2 1 2544.09 3106.34 58.97 o 6 2 1 4070.23 4457.46 83.54 o 8 2 1 1617.15 1620.32 33.22 o 10 2 1 489.70 445.72 17.57 o 12 2 1 538.15 422.14 15.51 o 14 2 1 20.78 20.56 7.75 o 16 2 1 1369.69 1650.32 40.94 o 18 2 1 449.66 463.16 19.66 o 20 2 1 1753.87 1831.50 47.17 o 22 2 1 411.61 313.52 17.84 o 24 2 1 10.54 19.67 16.51 o -25 3 1 805.40 847.28 135.78 o -23 3 1 183.32 206.09 19.77 o -21 3 1 56.60 44.38 14.30 o -19 3 1 21.43 5.25 12.18 o -17 3 1 5429.36 5236.71 130.16 o -15 3 1 6297.27 6064.08 267.33 o -13 3 1 983.49 860.78 49.83 o -11 3 1 160.83 153.06 15.34 o -9 3 1 5897.17 4737.99 115.21 o -7 3 1 36146.37 32453.11 1026.33 o -5 3 1 1766.70 2049.68 79.25 o -3 3 1 9438.96 6662.16 157.03 o -1 3 1 11481.67 11600.40 210.41 o 1 3 1 657.29 454.53 12.83 o 3 3 1 65669.06 64165.42 1271.40 o 5 3 1 3675.38 3603.83 68.24 o 7 3 1 19502.70 20146.20 364.42 o 9 3 1 16210.16 15366.02 279.56 o 11 3 1 4309.29 3601.10 78.67 o 13 3 1 208.77 157.29 14.76 o 15 3 1 2640.19 2732.45 55.82 o 17 3 1 2140.62 2001.88 49.01 o 19 3 1 1101.96 1039.32 30.74 o 21 3 1 46.71 32.93 12.97 o 23 3 1 179.50 158.42 18.77 o 25 3 1 508.24 506.28 27.50 o -24 4 1 57.68 28.76 15.50 o -22 4 1 127.99 110.70 16.81 o -20 4 1 613.12 471.60 39.81 o -18 4 1 602.60 715.84 82.22 o -16 4 1 16.16 32.30 16.01 o -14 4 1 3598.46 3861.85 636.56 o -12 4 1 2342.09 2366.81 144.50 o -10 4 1 8429.90 9174.84 283.10 o -8 4 1 416.59 445.46 29.27 o -6 4 1 225.24 324.68 13.73 o -4 4 1 15.22 19.15 4.95 o -2 4 1 26768.63 27928.24 457.25 o 0 4 1 5814.68 5185.14 106.32 o 2 4 1 7210.49 7423.18 150.75 o 4 4 1 25813.22 27679.16 551.24 o 6 4 1 16618.44 19203.89 384.29 o 8 4 1 918.49 1217.60 38.66 o 10 4 1 297.64 361.59 12.57 o 12 4 1 26.24 33.95 11.51 o 14 4 1 2804.45 2548.80 58.71 o 16 4 1 1867.42 2077.07 57.41 o 18 4 1 338.68 354.32 20.15 o 20 4 1 1409.18 1197.20 39.57 o 22 4 1 1161.48 1016.51 52.85 o 24 4 1 95.21 101.53 22.75 o -23 5 1 147.73 105.48 26.52 o -21 5 1 114.16 89.89 16.71 o -19 5 1 53.90 55.49 17.78 o -17 5 1 4299.37 4476.26 347.24 o -15 5 1 3369.80 3112.28 455.62 o -13 5 1 414.01 451.37 20.15 o -11 5 1 2953.22 2971.88 116.48 o -9 5 1 711.40 524.29 19.86 o -7 5 1 5355.08 3820.99 71.81 o -5 5 1 26.95 12.95 5.15 o -3 5 1 8.09 65.37 5.17 o -1 5 1 1886.10 2010.32 36.08 o 1 5 1 11801.21 10931.51 220.29 o 3 5 1 34.29 45.91 6.45 o 5 5 1 12196.62 13222.76 266.00 o 7 5 1 13189.85 13295.82 267.95 o 9 5 1 1049.12 1307.63 31.96 o 11 5 1 538.26 295.78 13.81 o 13 5 1 2168.01 1952.80 53.78 o 15 5 1 293.62 288.25 27.86 o 17 5 1 1566.23 1460.73 44.17 o 19 5 1 558.07 514.43 24.22 o 21 5 1 29.58 28.48 12.68 o 23 5 1 163.08 97.72 16.80 o -24 6 1 0.69 9.60 13.94 o -22 6 1 1383.83 1180.73 41.15 o -20 6 1 1721.22 1712.28 64.96 o -18 6 1 601.93 611.95 32.37 o -16 6 1 140.53 130.35 18.11 o -14 6 1 347.05 296.67 20.92 o -12 6 1 3648.55 4155.08 209.50 o -10 6 1 6281.45 6275.44 165.21 o -8 6 1 74.85 38.00 6.47 o -6 6 1 8274.64 10820.96 195.35 o -4 6 1 1534.12 1875.44 36.81 o -2 6 1 2924.73 2229.13 39.97 o 0 6 1 45.30 30.89 5.43 o 2 6 1 2530.34 2368.01 51.57 o 4 6 1 6146.63 6093.99 113.19 o 6 6 1 12468.43 13659.05 275.23 o 8 6 1 167.55 102.28 8.86 o 10 6 1 1790.15 1958.89 53.20 o 12 6 1 1113.62 1146.98 30.32 o 14 6 1 5839.03 6458.38 176.03 o 16 6 1 684.21 600.15 25.04 o 18 6 1 1.45 13.03 15.21 o 20 6 1 376.64 298.53 19.55 o 22 6 1 1033.82 923.11 37.43 o 24 6 1 171.04 150.43 21.36 o -23 7 1 159.40 107.29 17.08 o -21 7 1 172.60 134.92 22.26 o -19 7 1 15.05 6.71 16.19 o -17 7 1 265.11 260.10 22.60 o -15 7 1 1691.92 1729.19 49.95 o -13 7 1 1118.53 1154.89 43.94 o -11 7 1 5856.75 5530.70 224.85 o -9 7 1 1925.81 1897.61 148.13 o -7 7 1 878.13 783.57 40.42 o -5 7 1 2518.81 2488.83 44.69 o -3 7 1 16779.82 19026.50 313.32 o -1 7 1 629.38 586.16 13.62 o 1 7 1 5704.11 5622.68 95.27 o 3 7 1 3610.64 3560.37 68.00 o 5 7 1 5717.36 6015.59 112.18 o 7 7 1 2298.37 2187.23 49.33 o 9 7 1 6.81 18.40 9.38 o 11 7 1 929.11 886.80 25.52 o 13 7 1 3313.67 2836.45 63.99 o 15 7 1 128.64 125.70 21.99 o 17 7 1 1114.04 1120.10 37.34 o 19 7 1 0.70 3.66 14.01 o 21 7 1 209.61 134.64 15.90 o 23 7 1 271.98 211.51 20.06 o -22 8 1 596.38 549.14 35.11 o -20 8 1 2242.76 2233.03 128.00 o -18 8 1 739.67 693.56 36.04 o -16 8 1 82.58 33.17 14.87 o -14 8 1 792.20 861.42 36.87 o -12 8 1 3744.30 3710.72 181.99 o -10 8 1 11426.71 11075.55 394.32 o -8 8 1 1009.97 1235.90 91.57 o -6 8 1 2170.14 2372.52 56.81 o -4 8 1 16273.05 16857.08 278.34 o -2 8 1 4247.78 3937.59 68.20 o 0 8 1 272.62 525.13 13.00 o 2 8 1 3931.62 3294.14 63.52 o 4 8 1 10758.36 11722.86 214.41 o 6 8 1 18252.20 18403.62 334.20 o 8 8 1 780.75 828.99 26.75 o 10 8 1 871.24 910.78 29.59 o 12 8 1 8795.03 8193.01 169.53 o 14 8 1 2709.17 2925.85 77.50 o 16 8 1 298.48 276.60 16.38 o 18 8 1 65.82 95.75 14.57 o 20 8 1 502.23 509.65 31.47 o 22 8 1 729.03 715.58 38.75 o -21 9 1 27.51 -15.64 15.25 o -19 9 1 6.74 30.90 16.72 o -17 9 1 248.61 202.12 17.32 o -15 9 1 633.88 609.27 37.76 o -13 9 1 106.96 103.87 13.41 o -11 9 1 1322.83 1247.98 38.10 o -9 9 1 48.52 45.19 11.51 o -7 9 1 86.18 54.16 6.77 o -5 9 1 7.11 12.70 6.36 o -3 9 1 598.89 378.86 11.33 o -1 9 1 419.62 530.47 14.64 o 1 9 1 692.21 512.67 16.70 o 3 9 1 632.92 597.37 15.77 o 5 9 1 298.34 160.18 9.61 o 7 9 1 44.64 4.39 7.94 o 9 9 1 1284.18 1300.22 60.51 o 11 9 1 583.62 574.39 23.32 o 13 9 1 161.89 186.97 13.54 o 15 9 1 59.31 46.45 11.65 o 17 9 1 3.48 -0.86 11.96 o 19 9 1 17.69 -3.88 14.75 o 21 9 1 69.31 46.60 19.93 o -20 10 1 899.35 770.39 39.17 o -18 10 1 295.94 309.42 20.01 o -16 10 1 18.33 1.90 15.26 o -14 10 1 76.95 84.81 13.21 o -12 10 1 765.00 853.25 81.28 o -10 10 1 5130.61 5219.05 191.85 o -8 10 1 166.77 149.47 10.84 o -6 10 1 10886.37 10071.91 408.47 o -4 10 1 15309.45 16253.09 269.07 o -2 10 1 3791.35 3386.58 61.37 o 0 10 1 4.56 11.06 5.86 o 2 10 1 36.03 74.88 7.11 o 4 10 1 591.35 500.42 16.27 o 6 10 1 6388.73 6718.86 139.76 o 8 10 1 1970.27 1730.78 42.01 o 10 10 1 3355.00 3040.22 67.99 o 12 10 1 4534.95 4243.22 92.35 o 14 10 1 470.72 493.96 30.97 o 16 10 1 22.36 20.06 9.49 o 18 10 1 21.76 4.70 12.99 o 20 10 1 302.52 321.92 26.41 o -19 11 1 24.03 26.51 13.38 o -17 11 1 33.38 24.64 14.89 o -15 11 1 669.88 626.20 27.51 o -13 11 1 3.46 -10.48 12.57 o -11 11 1 847.06 736.65 27.01 o -9 11 1 815.02 931.80 26.24 o -7 11 1 100.64 96.02 8.55 o -5 11 1 263.04 280.20 12.58 o -3 11 1 466.36 451.29 15.75 o -1 11 1 2330.63 2491.69 50.11 o 1 11 1 2639.07 2798.28 55.57 o 3 11 1 1147.37 1123.94 29.48 o 5 11 1 96.47 97.57 10.53 o 7 11 1 22.55 12.47 9.08 o 9 11 1 36.60 63.38 12.59 o 11 11 1 87.28 163.78 13.33 o 13 11 1 15.76 12.56 11.99 o 15 11 1 127.65 131.60 15.29 o 17 11 1 223.70 246.81 24.11 o 19 11 1 7.19 -6.63 11.11 o -18 12 1 112.51 132.01 16.21 o -16 12 1 0.60 0.51 12.41 o -14 12 1 4.96 -5.36 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