#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012370.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012370_Fobs loop_ _publ_author_name 'Abboud, Khalil A.' 'Nickias, Peter N.' 'Chen, Eugene Y.-X.' _publ_section_title ; {N-[Dimethyl(\h^5^-2,3,4,6-tetramethylindenyl)silyl]cyclobutylamido-\kN}(\h^4^-1,4-diphenyl-1,3-butadiene)titanium(II) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1408 _journal_page_last 1409 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.020 _cell_angle_gamma 90.000 _cell_length_a 11.0726 _cell_length_b 20.5095 _cell_length_c 13.9311 _exptl_crystal_F_000 1176.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file fr1316Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ec04t in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 433.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14.34 30.73 24.02 o 4 0 0 8693.98 8234.70 226.14 o 6 0 0 218.12 281.32 46.96 o 8 0 0 280.93 275.91 59.08 o 10 0 0 831.66 872.31 84.18 o 12 0 0 115.98 223.54 82.45 o 1 1 0 651.39 635.35 11.52 o 2 1 0 15558.31 14883.39 190.57 o 3 1 0 56.94 72.70 17.93 o 4 1 0 4374.47 4231.31 90.05 o 5 1 0 1881.62 2182.88 58.83 o 6 1 0 6322.44 6594.08 138.64 o 7 1 0 481.90 527.18 40.70 o 8 1 0 4490.49 4420.42 109.79 o 9 1 0 85.02 74.46 42.15 o 10 1 0 157.79 177.70 47.44 o 11 1 0 1.81 22.40 49.73 o 12 1 0 50.30 105.84 82.56 o 13 1 0 7.49 -49.56 62.16 o 0 2 0 37345.28 39530.17 993.06 o 1 2 0 1584.00 1528.84 22.66 o 2 2 0 12227.33 12379.61 159.48 o 3 2 0 258.44 316.58 16.52 o 4 2 0 5512.12 5591.31 79.61 o 5 2 0 2.80 28.00 22.36 o 6 2 0 122.46 195.67 32.13 o 7 2 0 417.23 473.47 40.29 o 8 2 0 313.38 357.06 43.05 o 9 2 0 37.51 10.96 58.10 o 10 2 0 614.19 712.94 55.55 o 11 2 0 0.51 17.15 54.42 o 12 2 0 477.13 472.32 64.19 o 13 2 0 29.93 -93.39 62.44 o 1 3 0 1472.72 1463.24 20.49 o 2 3 0 1374.49 1385.48 25.13 o 3 3 0 1901.02 1779.25 31.61 o 4 3 0 351.34 271.60 17.48 o 5 3 0 81.07 88.14 17.65 o 6 3 0 1220.85 1153.79 65.38 o 7 3 0 0.19 13.21 37.22 o 8 3 0 3840.08 3748.68 105.17 o 9 3 0 1.84 3.49 56.70 o 10 3 0 16.85 19.29 43.99 o 11 3 0 3.94 9.14 48.42 o 12 3 0 20.36 -11.87 57.24 o 13 3 0 24.46 34.72 65.87 o 0 4 0 3174.00 3198.57 61.21 o 1 4 0 2439.80 2681.57 38.74 o 2 4 0 5843.74 5618.63 68.38 o 3 4 0 1961.83 1879.34 32.78 o 4 4 0 308.89 295.98 20.71 o 5 4 0 195.26 199.27 18.74 o 6 4 0 863.35 835.55 43.71 o 7 4 0 53.53 30.00 26.41 o 8 4 0 1383.98 1430.27 59.45 o 9 4 0 125.78 185.11 43.38 o 10 4 0 395.62 414.79 82.77 o 11 4 0 25.58 20.78 49.86 o 12 4 0 240.70 191.39 57.50 o 13 4 0 180.50 192.18 66.73 o 1 5 0 6.55 17.41 24.40 o 2 5 0 1134.98 1199.05 29.07 o 3 5 0 75.96 75.30 18.99 o 4 5 0 11.97 31.07 15.73 o 5 5 0 21.69 15.28 17.13 o 6 5 0 1376.03 1415.87 34.22 o 7 5 0 354.94 393.90 44.97 o 8 5 0 578.50 627.19 57.09 o 9 5 0 609.54 586.85 49.42 o 10 5 0 0.40 18.90 45.77 o 11 5 0 49.28 66.12 50.46 o 12 5 0 66.25 46.25 55.59 o 13 5 0 50.29 73.24 67.02 o 0 6 0 1055.37 1038.79 27.27 o 1 6 0 7360.64 7713.04 229.97 o 2 6 0 16.93 22.91 12.13 o 3 6 0 406.67 369.06 15.59 o 4 6 0 180.11 174.82 17.66 o 5 6 0 1230.99 1264.65 33.67 o 6 6 0 2.46 -27.37 19.13 o 7 6 0 1392.50 1470.94 37.77 o 8 6 0 78.41 110.87 30.61 o 9 6 0 7.29 -26.21 39.71 o 10 6 0 428.91 458.18 50.88 o 11 6 0 24.21 45.97 49.42 o 12 6 0 7.96 25.83 55.92 o 1 7 0 6876.33 7279.55 196.80 o 2 7 0 455.42 468.34 15.67 o 3 7 0 457.50 497.36 19.38 o 4 7 0 283.09 311.26 17.13 o 5 7 0 0.05 -11.88 17.66 o 6 7 0 115.99 114.74 21.05 o 7 7 0 13.49 14.19 21.98 o 8 7 0 454.30 438.44 47.95 o 9 7 0 1311.66 1274.82 48.57 o 10 7 0 43.82 40.18 44.53 o 11 7 0 294.80 291.80 55.59 o 12 7 0 0.27 1.88 57.54 o 0 8 0 1976.86 2053.69 44.65 o 1 8 0 1011.32 978.96 20.33 o 2 8 0 53.73 62.62 12.67 o 3 8 0 2855.73 2921.37 47.37 o 4 8 0 456.05 512.61 19.42 o 5 8 0 1884.48 1878.81 34.64 o 6 8 0 1061.33 1107.41 31.92 o 7 8 0 779.86 830.13 30.81 o 8 8 0 503.62 469.70 29.27 o 9 8 0 205.30 191.60 34.48 o 10 8 0 62.90 34.05 46.59 o 11 8 0 160.04 111.77 54.01 o 12 8 0 15.64 65.22 59.45 o 1 9 0 2.26 16.70 15.25 o 2 9 0 213.30 225.21 13.88 o 3 9 0 323.08 306.62 17.02 o 4 9 0 1098.95 1241.66 26.66 o 5 9 0 45.41 56.60 17.45 o 6 9 0 101.50 80.60 19.50 o 7 9 0 1.24 0.84 20.85 o 8 9 0 0.61 12.10 24.52 o 9 9 0 2227.39 2373.80 64.63 o 10 9 0 4.76 -6.04 51.82 o 11 9 0 88.10 95.14 53.23 o 12 9 0 82.62 100.16 86.13 o 0 10 0 474.25 496.73 17.76 o 1 10 0 1289.77 1159.42 36.48 o 2 10 0 329.60 312.69 23.49 o 3 10 0 3678.00 3660.48 51.53 o 4 10 0 1389.40 1421.02 29.22 o 5 10 0 2879.50 2673.23 44.21 o 6 10 0 0.28 -23.75 19.07 o 7 10 0 1914.22 1898.03 39.90 o 8 10 0 17.30 11.79 26.33 o 9 10 0 335.32 325.06 32.90 o 10 10 0 353.30 345.24 41.07 o 11 10 0 7.81 -51.89 43.05 o 12 10 0 88.54 42.80 50.73 o 1 11 0 5021.08 4829.85 68.48 o 2 11 0 31.16 91.15 16.34 o 3 11 0 2934.76 2864.44 43.42 o 4 11 0 193.39 194.96 19.03 o 5 11 0 14.23 4.55 18.13 o 6 11 0 418.38 354.69 23.26 o 7 11 0 191.51 216.44 23.43 o 8 11 0 760.40 767.49 35.10 o 9 11 0 192.41 159.35 31.64 o 10 11 0 17.25 37.00 34.43 o 11 11 0 301.95 317.99 42.04 o 12 11 0 43.32 5.35 52.41 o 0 12 0 2219.00 2125.49 87.43 o 1 12 0 110.12 95.70 11.28 o 2 12 0 591.99 616.87 20.06 o 3 12 0 5246.67 5314.01 70.94 o 4 12 0 590.55 606.08 22.95 o 5 12 0 1994.84 1929.27 38.02 o 6 12 0 0.12 -15.80 20.41 o 7 12 0 1547.37 1610.89 37.82 o 8 12 0 160.89 159.86 29.03 o 9 12 0 232.87 249.21 32.68 o 10 12 0 8.07 24.63 34.59 o 11 12 0 162.08 173.06 42.28 o 1 13 0 5289.17 4943.89 119.78 o 2 13 0 7.14 10.90 41.01 o 3 13 0 1164.51 1157.13 30.68 o 4 13 0 2.92 13.06 21.27 o 5 13 0 260.07 224.23 25.38 o 6 13 0 2.24 16.04 25.99 o 7 13 0 182.82 175.98 30.65 o 8 13 0 2.15 21.75 32.66 o 9 13 0 17.09 35.81 35.44 o 10 13 0 35.01 30.59 40.87 o 11 13 0 468.13 544.11 53.69 o 0 14 0 490.53 529.75 56.70 o 1 14 0 47.36 41.52 35.71 o 2 14 0 194.82 194.95 33.91 o 3 14 0 1473.75 1329.63 41.92 o 4 14 0 8.68 16.40 27.42 o 5 14 0 1928.18 1856.12 52.60 o 6 14 0 196.50 211.59 30.98 o 7 14 0 549.88 563.39 48.91 o 8 14 0 57.71 82.68 38.93 o 9 14 0 655.03 579.29 57.13 o 10 14 0 86.19 56.03 47.85 o 11 14 0 56.12 13.58 56.23 o 1 15 0 1339.94 1366.11 55.06 o 2 15 0 685.22 723.26 59.73 o 3 15 0 325.58 345.96 30.40 o 4 15 0 27.01 29.30 29.27 o 5 15 0 379.97 351.54 33.77 o 6 15 0 9.75 6.65 35.49 o 7 15 0 52.58 69.72 39.93 o 8 15 0 40.42 68.70 44.87 o 9 15 0 80.92 90.48 50.21 o 10 15 0 107.58 81.46 59.73 o 11 15 0 343.57 372.74 63.58 o 0 16 0 1355.69 1333.46 80.93 o 1 16 0 635.61 597.34 44.73 o 2 16 0 201.55 257.90 40.69 o 3 16 0 8.54 -2.67 26.94 o 4 16 0 113.61 138.12 30.62 o 5 16 0 187.00 250.24 33.31 o 6 16 0 806.92 697.87 48.48 o 7 16 0 390.92 468.95 47.60 o 8 16 0 65.76 104.71 45.41 o 9 16 0 121.40 126.48 64.92 o 10 16 0 54.57 39.67 56.04 o 1 17 0 581.93 541.29 47.43 o 2 17 0 162.53 140.50 53.78 o 3 17 0 332.27 325.18 31.54 o 4 17 0 52.29 42.52 30.47 o 5 17 0 129.51 116.77 39.70 o 6 17 0 116.99 116.53 39.41 o 7 17 0 58.23 42.03 41.72 o 8 17 0 0.52 38.39 45.56 o 9 17 0 92.33 29.08 53.99 o 10 17 0 2.67 4.61 58.36 o 0 18 0 3.71 38.95 58.64 o 1 18 0 12.96 39.44 40.70 o 2 18 0 81.59 57.89 41.16 o 3 18 0 55.14 38.55 29.01 o 4 18 0 222.48 143.60 32.71 o 5 18 0 4.26 -43.54 38.40 o 6 18 0 121.47 54.52 41.11 o 7 18 0 11.20 9.69 43.28 o 8 18 0 281.67 244.51 50.25 o 9 18 0 18.35 14.83 51.62 o 1 19 0 217.20 347.80 56.16 o 2 19 0 40.33 31.53 39.47 o 3 19 0 3.14 33.91 31.23 o 4 19 0 107.64 59.83 40.05 o 5 19 0 517.83 466.84 48.42 o 6 19 0 38.53 15.63 42.73 o 7 19 0 14.33 65.47 45.56 o 8 19 0 11.24 53.91 80.61 o 9 19 0 56.29 80.07 56.78 o 0 20 0 198.36 173.12 64.70 o 1 20 0 156.62 201.96 44.76 o 2 20 0 50.49 35.16 43.19 o 3 20 0 29.57 13.56 32.44 o 4 20 0 31.26 31.86 40.54 o 5 20 0 37.06 53.01 43.00 o 6 20 0 92.97 29.89 46.08 o 7 20 0 39.77 57.66 47.31 o 8 20 0 13.76 61.51 56.70 o 1 21 0 9.05 48.69 44.90 o 2 21 0 86.29 61.20 46.59 o 3 21 0 76.02 15.21 44.01 o 4 21 0 22.89 25.63 44.06 o 5 21 0 62.58 27.97 55.29 o 6 21 0 209.71 208.79 51.02 o 7 21 0 2.42 23.79 65.89 o 8 21 0 28.18 3.81 69.14 o 0 22 0 177.57 188.05 72.49 o 1 22 0 33.94 14.21 46.20 o 2 22 0 131.03 153.43 38.91 o 3 22 0 303.41 321.11 51.25 o 4 22 0 29.22 12.71 46.53 o 5 22 0 311.87 285.95 51.61 o 6 22 0 8.29 -16.75 49.24 o 7 22 0 19.78 23.28 51.28 o 1 23 0 19.91 36.61 48.88 o 2 23 0 232.76 339.57 53.50 o 3 23 0 20.33 7.93 47.83 o 4 23 0 305.10 397.33 56.26 o 5 23 0 164.96 166.56 54.38 o 6 23 0 220.94 189.91 56.48 o 0 24 0 1096.74 1344.50 103.87 o 1 24 0 5.15 4.90 52.47 o 2 24 0 696.63 921.43 66.15 o 3 24 0 65.42 24.03 51.85 o 4 24 0 35.40 59.93 56.10 o 5 24 0 76.85 99.54 56.05 o 1 25 0 15.53 -11.73 55.83 o 2 25 0 153.53 162.99 55.82 o 3 25 0 12.25 42.61 56.13 o 4 25 0 324.48 378.92 64.18 o 0 26 0 165.77 250.16 86.56 o 1 26 0 0.83 -22.83 58.05 o 2 26 0 408.45 435.81 65.41 o -13 0 1 62.55 99.54 85.26 o -11 0 1 14.65 166.20 72.28 o -9 0 1 580.22 622.59 70.76 o -7 0 1 756.97 856.51 62.97 o -5 0 1 4914.10 4981.12 149.97 o -3 0 1 10248.37 9942.11 263.14 o -1 0 1 36036.31 35597.05 639.57 o 1 0 1 4483.18 4777.44 73.42 o 3 0 1 776.92 650.07 41.98 o 5 0 1 2733.14 2310.51 85.91 o 7 0 1 2522.76 2416.12 101.71 o 9 0 1 2815.02 2794.60 122.27 o 11 0 1 174.68 162.95 77.04 o 13 0 1 10.66 20.13 91.97 o -13 1 1 0.57 9.99 61.64 o -12 1 1 1.70 -11.90 54.32 o -11 1 1 265.52 247.51 52.87 o -10 1 1 22.66 47.88 44.60 o -9 1 1 2816.68 2917.89 87.81 o -8 1 1 62.00 -50.90 37.63 o -7 1 1 2521.67 2600.48 73.68 o -6 1 1 1543.90 1787.16 55.61 o -5 1 1 2095.92 2113.53 98.68 o -4 1 1 1530.86 1643.42 49.46 o -3 1 1 3307.12 3039.20 48.66 o -2 1 1 214.16 261.08 12.20 o -1 1 1 20549.86 19875.06 267.98 o 0 1 1 101.59 115.44 6.03 o 1 1 1 15488.92 15793.92 256.88 o 2 1 1 1065.73 1277.85 50.64 o 3 1 1 15075.74 15647.52 255.39 o 4 1 1 517.01 581.24 29.67 o 5 1 1 2523.24 2405.81 62.51 o 6 1 1 262.57 269.46 30.36 o 7 1 1 987.11 1138.92 50.96 o 8 1 1 453.27 557.11 60.16 o 9 1 1 123.41 140.06 43.92 o 10 1 1 19.18 15.60 44.89 o 11 1 1 133.41 149.29 53.13 o 12 1 1 6.85 38.04 79.09 o 13 1 1 222.51 273.31 97.60 o -13 2 1 1.81 -8.14 62.54 o -12 2 1 159.21 215.83 57.07 o -11 2 1 59.89 136.16 50.25 o -10 2 1 42.47 5.39 43.30 o -9 2 1 782.46 827.35 53.78 o -8 2 1 15.03 -36.46 37.77 o -7 2 1 22.52 22.13 37.22 o -6 2 1 810.47 847.84 41.07 o -5 2 1 4927.89 4566.90 68.89 o -4 2 1 651.93 670.50 22.74 o -3 2 1 3664.61 3494.64 51.46 o -2 2 1 2009.35 2155.65 41.76 o -1 2 1 19086.65 19228.05 244.13 o 0 2 1 6778.20 6913.60 88.77 o 1 2 1 567.56 641.42 16.25 o 2 2 1 20452.41 21529.72 245.58 o 3 2 1 2265.78 2422.18 92.78 o 4 2 1 218.98 281.23 26.40 o 5 2 1 283.65 236.37 22.53 o 6 2 1 551.13 491.81 35.11 o 7 2 1 1966.81 2101.25 75.63 o 8 2 1 73.19 79.58 38.86 o 9 2 1 2762.45 2882.03 88.50 o 10 2 1 0.13 -4.33 44.74 o 11 2 1 133.08 55.44 52.55 o 12 2 1 1.28 11.04 59.36 o -13 3 1 39.13 3.14 61.67 o -12 3 1 528.95 600.05 64.80 o -11 3 1 326.67 322.66 88.62 o -10 3 1 336.87 332.93 48.50 o -9 3 1 3202.25 3039.00 98.90 o -8 3 1 105.00 120.89 38.84 o -7 3 1 155.68 123.11 35.33 o -6 3 1 172.27 204.00 20.61 o -5 3 1 6.73 1.89 16.82 o -4 3 1 137.22 129.95 16.47 o -3 3 1 377.36 404.93 17.51 o -2 3 1 15393.74 15266.81 175.00 o -1 3 1 633.81 711.39 13.13 o 0 3 1 1069.44 1171.67 18.82 o 1 3 1 8730.80 9302.04 120.04 o 2 3 1 7659.31 7476.40 88.92 o 3 3 1 8424.36 8278.78 125.00 o 4 3 1 667.98 768.29 27.03 o 5 3 1 3735.62 3712.81 69.53 o 6 3 1 45.84 48.47 27.24 o 7 3 1 29.29 59.08 33.94 o 8 3 1 206.16 218.14 40.85 o 9 3 1 36.17 20.24 41.69 o 10 3 1 4.44 10.03 55.40 o 11 3 1 103.31 111.01 52.41 o 12 3 1 0.89 64.85 59.98 o -13 4 1 93.62 100.37 62.97 o -12 4 1 2.27 -40.64 53.31 o -11 4 1 59.25 27.02 55.83 o -10 4 1 412.67 429.05 50.42 o -9 4 1 289.76 333.67 45.45 o -8 4 1 47.99 111.40 38.74 o -7 4 1 366.59 384.88 33.28 o -6 4 1 2244.43 2036.13 40.93 o -5 4 1 31.17 48.63 17.22 o -4 4 1 3977.38 4002.51 67.42 o -3 4 1 377.13 339.01 16.94 o -2 4 1 14.85 19.53 12.02 o -1 4 1 1072.85 1146.58 43.88 o 0 4 1 14679.17 14615.16 185.13 o 1 4 1 17.26 34.11 11.90 o 2 4 1 1105.35 1058.87 21.06 o 3 4 1 412.36 503.30 18.23 o 4 4 1 62.08 75.24 16.12 o 5 4 1 1296.13 1445.03 38.37 o 6 4 1 537.81 588.31 30.20 o 7 4 1 1406.44 1346.64 43.22 o 8 4 1 260.75 240.83 41.39 o 9 4 1 1196.08 1319.82 61.66 o 10 4 1 44.49 49.74 45.13 o 11 4 1 133.06 108.00 51.41 o 12 4 1 1.27 -10.53 56.85 o -13 5 1 80.29 59.86 65.42 o -12 5 1 937.35 981.92 75.09 o -11 5 1 539.57 563.23 58.22 o -10 5 1 1265.03 1238.17 63.87 o -9 5 1 1106.89 1139.20 58.30 o -8 5 1 202.30 249.19 30.72 o -7 5 1 270.73 278.59 28.14 o -6 5 1 40.12 49.12 19.14 o -5 5 1 342.84 383.25 20.70 o -4 5 1 2417.58 2566.29 50.57 o -3 5 1 35.23 36.08 13.23 o -2 5 1 6391.62 6197.13 75.99 o -1 5 1 113.34 160.57 14.21 o 0 5 1 3342.97 3207.45 112.43 o 1 5 1 5316.96 5292.81 114.53 o 2 5 1 1052.65 916.42 18.28 o 3 5 1 3853.70 3733.93 55.69 o 4 5 1 4.85 -4.34 15.68 o 5 5 1 722.35 657.49 24.55 o 6 5 1 159.32 151.67 25.03 o 7 5 1 11.62 35.04 27.00 o 8 5 1 6.42 55.76 46.96 o 9 5 1 2.82 -26.60 39.86 o 10 5 1 100.36 71.93 45.60 o 11 5 1 10.37 -16.84 49.65 o 12 5 1 30.06 -35.65 56.82 o -13 6 1 114.48 84.16 66.12 o -12 6 1 50.17 112.91 58.36 o -11 6 1 346.06 367.92 54.30 o -10 6 1 364.15 383.87 50.27 o -9 6 1 100.58 99.24 42.13 o -8 6 1 1221.28 1349.63 38.66 o -7 6 1 2.24 -6.95 21.20 o -6 6 1 121.27 124.67 20.08 o -5 6 1 372.85 376.81 20.41 o -4 6 1 5012.15 5111.10 68.81 o -3 6 1 3065.94 2786.19 39.60 o -2 6 1 129.37 187.47 18.78 o -1 6 1 2684.74 2627.17 38.68 o 0 6 1 1093.31 1016.26 24.69 o 1 6 1 96.12 117.22 13.65 o 2 6 1 299.91 284.45 11.78 o 3 6 1 63.05 98.41 15.40 o 4 6 1 5.93 -0.46 16.22 o 5 6 1 42.57 41.34 17.76 o 6 6 1 922.73 982.93 29.80 o 7 6 1 19.37 22.17 34.81 o 8 6 1 0.37 33.65 30.01 o 9 6 1 100.03 67.53 41.28 o 10 6 1 15.69 32.83 44.83 o 11 6 1 55.71 -1.29 51.02 o 12 6 1 71.94 101.60 58.46 o -13 7 1 8.08 71.74 66.47 o -12 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3334.28 3259.42 85.09 o -2 8 1 3050.95 3265.43 44.25 o -1 8 1 2.79 21.35 15.87 o 0 8 1 94.59 230.53 40.41 o 1 8 1 1033.80 999.61 21.70 o 2 8 1 1283.13 1155.17 19.92 o 3 8 1 643.70 647.88 19.26 o 4 8 1 5821.57 5595.47 77.60 o 5 8 1 803.84 839.91 26.66 o 6 8 1 1109.65 1156.07 32.56 o 7 8 1 177.58 205.98 24.48 o 8 8 1 108.68 106.21 32.79 o 9 8 1 591.99 629.79 55.56 o 10 8 1 235.29 194.88 48.97 o 11 8 1 18.53 31.51 68.38 o 12 8 1 518.25 469.49 67.40 o -12 9 1 150.88 175.09 49.35 o -11 9 1 18.14 -2.67 41.27 o -10 9 1 182.61 163.56 32.88 o -9 9 1 239.33 291.61 35.57 o -8 9 1 18.80 -19.92 21.88 o -7 9 1 530.63 520.37 24.96 o -6 9 1 139.99 149.16 19.66 o -5 9 1 460.54 489.69 20.83 o -4 9 1 3024.15 2865.69 43.93 o -3 9 1 830.49 951.65 31.06 o -2 9 1 21.46 21.31 13.63 o -1 9 1 588.97 636.81 22.31 o 0 9 1 1903.69 1788.40 36.70 o 1 9 1 333.19 348.76 15.08 o 2 9 1 2096.57 2053.48 42.14 o 3 9 1 1746.09 1940.68 32.60 o 4 9 1 4943.76 5244.48 70.31 o 5 9 1 24.52 45.35 17.60 o 6 9 1 565.35 612.72 26.98 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