#------------------------------------------------------------------------------
#$Date: 2016-04-02 21:36:46 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180792 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/23/2012386.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2012386_Fobs
loop_
_publ_author_name
'Miyashita, Yoshitaro'
'Arai, Satoshi'
'Yamada, Yasunori'
'Fujisawa, Kiyoshi'
'Okamoto, Ken-ichi'
_publ_section_title
;
 <i>anti</i>-Bis(\m-2-ammonioethanethiolato-\k^2^<i>S</i>:<i>S</i>)bis[dichloropalladium(II)]
 dihydrate
;
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1393
_journal_page_last               1394
_journal_volume                  57
_journal_year                    2001
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cod_data_source_file            oa1118Isup2.hkl
_cod_data_source_block           I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_calc
_refln_observed_status
1 0 0 4197.74 160.25 4210.91 o
0 1 1 27414.77 865.15 28895.86 o
0 0 2 8998.60 266.40 7729.24 o
1 1 0 3806.66 163.81 3716.14 o
1 1 -1 285.31 55.32 330.49 o
1 1 1 18558.51 603.67 18927.31 o
0 1 2 447.80 43.88 394.28 o
1 0 -2 4408.45 198.63 4717.57 o
1 0 2 21627.34 707.20 22292.01 o
0 2 0 26949.66 817.80 25181.22 o
0 2 1 2824.46 129.03 2809.19 o
1 1 -2 3339.82 176.00 3410.58 o
1 1 2 9418.37 336.59 9187.36 o
1 2 0 11143.33 382.13 10571.67 o
2 0 0 19198.40 634.93 19405.94 o
1 2 -1 8445.86 313.30 8203.28 o
0 1 3 -69.54 88.21 19.22 o
1 2 1 18881.45 609.54 18214.87 o
0 2 2 149.11 82.39 40.52 o
2 1 0 606.08 75.62 669.97 o
2 1 -1 1679.38 154.78 2084.69 o
1 1 -3 9874.04 372.27 10338.26 o
2 1 1 1946.42 163.27 2080.04 o
1 2 -2 575.05 76.00 403.59 o
1 1 3 4971.32 233.65 5047.13 o
1 2 2 19649.56 643.65 19190.81 o
2 0 -2 32.86 127.87 85.36 o
2 0 2 3465.99 195.75 3477.05 o
2 1 -2 3919.67 204.47 3811.16 o
0 0 4 6347.28 226.33 5838.13 o
0 2 3 1573.31 113.07 1572.89 o
2 1 2 469.11 76.42 363.90 o
0 3 1 68.66 69.45 39.60 o
2 2 0 22465.55 723.13 21450.38 o
0 1 4 4281.33 183.56 4461.63 o
1 0 -4 44807.17 1427.28 45635.57 o
2 2 -1 112.27 119.83 38.64 o
1 2 -3 362.36 79.44 416.70 o
2 2 1 16942.45 581.45 17175.45 o
1 3 0 9830.15 367.18 9805.87 o
1 0 4 5781.86 270.33 5915.40 o
1 2 3 819.45 85.28 841.35 o
1 3 -1 5990.00 252.27 5434.54 o
1 3 1 9020.32 343.80 8775.74 o
1 1 -4 1128.77 110.42 1186.85 o
0 3 2 1758.34 122.02 1872.48 o
2 1 -3 9849.59 379.23 10065.25 o
1 1 4 1554.37 151.74 1265.83 o
2 2 -2 9397.73 360.41 9375.32 o
2 1 3 10190.79 381.46 9682.32 o
2 2 2 1132.30 108.98 1049.65 o
1 3 -2 3697.35 203.89 3808.82 o
1 3 2 617.18 84.00 709.47 o
0 2 4 257.05 54.02 158.33 o
3 0 0 6507.31 294.52 7078.69 o
3 1 0 2117.31 169.97 1976.49 o
0 3 3 610.88 58.78 519.82 o
1 2 -4 5741.66 264.50 5791.19 o
2 0 -4 17510.86 615.38 17893.92 o
3 1 -1 1031.98 107.49 1139.75 o
2 2 -3 3301.80 194.30 3343.39 o
1 2 4 10814.74 414.47 11002.47 o
3 1 1 15901.68 563.81 16036.63 o
2 3 0 16187.97 568.39 16281.65 o
3 0 -2 4313.68 231.95 4352.64 o
0 1 5 8592.97 304.01 8422.55 o
2 2 3 10874.06 413.82 10857.85 o
2 0 4 1730.74 127.73 1859.78 o
2 3 -1 2397.02 176.18 2262.91 o
2 1 -4 5956.35 271.69 5891.49 o
1 3 -3 70.58 141.68 281.06 o
2 3 1 3816.74 226.73 3868.84 o
3 0 2 18955.04 666.42 19652.57 o
1 3 3 790.49 87.23 899.12 o
3 1 -2 787.43 81.28 671.76 o
0 4 0 820.72 83.52 704.57 o
2 1 4 68.15 135.53 6.03 o
1 1 -5 29667.18 977.73 29976.13 o
3 1 2 8480.81 342.99 8180.98 o
0 4 1 755.01 62.27 823.65 o
1 1 5 4243.99 234.09 4450.40 o
2 3 -2 120.96 134.42 92.64 o
3 2 0 6787.49 301.55 6734.23 o
2 3 2 25215.36 854.11 25870.29 o
3 2 -1 785.72 85.07 825.91 o
1 4 0 3305.12 201.45 3318.63 o
3 2 1 1707.61 169.46 1695.64 o
0 3 4 4445.86 188.80 4177.79 o
0 2 5 3663.37 179.18 3957.00 o
1 4 -1 12814.67 477.38 12955.90 o
1 4 1 7215.84 313.61 7009.23 o
0 4 2 98.97 97.35 93.95 o
2 2 -4 17652.79 617.37 17434.76 o
3 1 -3 370.13 80.81 408.96 o
3 2 -2 1300.53 113.49 1203.19 o
2 2 4 1128.27 116.05 1005.64 o
1 2 -5 576.52 92.27 716.87 o
1 3 -4 98.58 137.33 20.82 o
3 1 3 1197.93 120.72 1166.87 o
2 3 -3 6277.77 280.73 5740.16 o
3 2 2 11199.58 434.45 11216.61 o
1 4 -2 2058.01 176.86 2156.98 o
1 3 4 4120.17 225.16 3844.64 o
1 2 5 1749.64 179.64 1944.36 o
1 4 2 -48.84 136.54 5.22 o
0 0 6 17675.63 584.29 17983.05 o
2 3 3 4062.16 242.43 4292.81 o
2 1 -5 349.91 83.82 309.45 o
0 4 3 9425.45 337.90 9468.75 o
0 1 6 1952.52 145.40 2069.22 o
1 0 -6 20464.14 709.74 20473.22 o
2 1 5 2533.82 200.38 2890.39 o
3 0 -4 3169.10 215.82 3439.92 o
3 2 -3 11154.48 429.27 11293.21 o
2 4 0 2150.27 181.57 2049.50 o
1 0 6 131.70 101.04 47.31 o
3 3 0 1663.23 128.91 1844.98 o
1 1 -6 1396.82 131.55 1420.78 o
2 4 -1 3980.10 225.13 3852.79 o
3 1 -4 414.50 87.60 571.54 o
1 4 -3 4448.48 241.41 4512.27 o
3 3 -1 46.54 143.74 128.95 o
2 4 1 17337.06 612.30 16971.37 o
3 2 3 8737.28 367.06 8778.33 o
3 0 4 1732.35 179.22 1596.10 o
1 4 3 74.41 143.02 187.74 o
3 3 1 4204.98 233.10 4061.97 o
1 1 6 1132.89 96.71 1142.67 o
0 3 5 291.44 60.36 371.10 o
4 0 0 47.95 147.58 139.94 o
2 2 -5 11297.12 450.18 11562.18 o
2 3 -4 10177.49 397.85 9636.99 o
3 1 4 2531.09 220.26 2684.13 o
2 4 -2 249.49 78.76 85.73 o
3 3 -2 16353.62 589.59 16196.81 o
0 2 6 11849.45 421.23 12304.80 o
4 1 0 2757.00 218.23 3059.83 o
2 3 4 7259.62 334.06 7311.96 o
1 3 -5 3027.42 208.90 3092.69 o
2 4 2 568.04 87.63 501.82 o
2 2 5 29.28 147.29 59.15 o
4 1 -1 879.32 94.19 781.45 o
3 3 2 2323.42 192.77 2359.12 o
1 3 5 4320.84 246.89 4108.39 o
4 1 1 39.89 153.34 160.37 o
4 0 -2 6587.00 303.66 6431.30 o
0 4 4 4459.26 200.53 4532.95 o
1 2 -6 683.59 94.35 709.93 o
2 0 -6 3318.31 234.66 3582.44 o
3 2 -4 5158.39 274.94 5209.29 o
0 5 1 1705.25 111.81 1517.39 o
4 0 2 15105.26 545.64 14332.83 o
1 2 6 34.65 155.53 205.27 o
4 1 -2 2556.73 197.93 2562.20 o
1 4 -4 734.92 93.05 644.56 o
2 1 -6 1713.84 134.45 1720.86 o
1 5 0 13371.53 512.86 13584.16 o
2 0 6 3891.70 256.64 3972.77 o
2 4 -3 3005.89 209.84 2720.37 o
3 3 -3 415.26 84.86 385.00 o
3 2 4 1100.41 99.99 1037.64 o
1 4 4 536.81 85.53 378.72 o
4 1 2 686.52 93.76 599.36 o
1 5 -1 6284.54 299.60 6045.44 o
1 5 1 580.57 94.87 616.54 o
4 2 0 897.86 98.53 938.22 o
2 4 3 10814.18 434.74 10689.26 o
3 1 -5 6697.38 319.68 6707.44 o
0 5 2 7672.46 302.79 8147.81 o
4 2 -1 3122.74 223.73 3225.31 o
2 1 6 2271.02 197.37 2209.07 o
3 3 3 6.39 149.97 7.92 o
4 2 1 1812.50 140.68 1805.16 o
2 3 -5 -5.50 151.63 57.44 o
0 1 7 16793.96 562.33 16715.41 o
4 1 -3 17965.10 653.46 18454.65 o
1 5 -2 4751.57 267.99 4687.89 o
3 1 5 109.83 161.19 472.02 o
1 5 2 200.76 156.70 122.55 o
4 2 -2 2378.91 198.97 2049.04 o
3 4 0 306.01 86.79 301.02 o
0 3 6 904.10 73.88 923.33 o
2 2 -6 276.34 84.51 76.82 o
2 3 5 1870.25 146.93 2030.58 o
1 1 -7 1269.52 110.45 1422.64 o
3 4 -1 6849.91 325.82 6623.87 o
3 4 1 116.99 144.62 0.11 o
4 1 3 20294.00 732.15 20568.20 o
4 2 2 3029.71 223.14 3137.40 o
0 4 5 5096.83 226.36 5130.89 o
0 5 3 121.72 103.74 90.00 o
1 1 7 7320.01 350.54 7574.42 o
3 2 -5 3475.64 240.30 3466.72 o
1 3 -6 2155.97 211.58 2336.36 o
2 4 -4 -271.12 160.81 0.24 o
3 3 -4 15250.39 566.36 15027.68 o
2 2 6 8820.20 398.32 9130.71 o
2 5 0 1593.39 133.54 1494.58 o
1 3 6 15856.94 596.59 15967.77 o
3 4 -2 2363.31 210.67 2555.79 o
2 4 4 137.58 85.55 5.87 o
1 4 -5 238.23 90.21 258.10 o
4 0 -4 21166.68 765.38 21672.19 o
2 5 -1 161.24 169.03 485.27 o
1 5 -3 826.26 98.21 772.41 o
0 2 7 1520.04 105.44 1379.33 o
2 5 1 102.03 155.10 2.71 o
4 2 -3 3737.47 244.38 3585.95 o
3 4 2 225.44 90.03 232.75 o
3 3 4 4357.85 265.11 4607.67 o
1 5 3 2870.05 226.53 2926.30 o
1 4 5 7239.15 346.89 7218.87 o
3 2 5 3856.90 267.44 3897.49 o
4 3 0 1723.01 140.61 1764.16 o
3 0 -6 399.00 97.01 387.04 o
4 1 -4 2350.16 198.51 2089.24 o
1 2 -7 2201.72 209.92 2048.45 o
4 3 -1 918.80 105.03 899.79 o
4 2 3 229.65 160.36 222.88 o
2 5 -2 186.81 89.51 152.84 o
4 0 4 22934.16 810.74 22810.13 o
4 3 1 173.00 148.52 131.40 o
3 1 -6 238.35 161.82 98.73 o
1 2 7 5597.25 299.53 5616.12 o
2 5 2 2774.02 209.72 2666.82 o
2 1 -7 1299.67 119.38 1455.62 o
3 4 -3 12001.86 491.67 12294.85 o
4 1 4 8.44 167.74 8.20 o
4 3 -2 1499.91 136.55 1334.43 o
0 5 4 11477.63 412.07 11528.86 o
3 0 6 2039.05 205.38 1858.48 o
2 3 -6 8393.91 375.42 8022.60 o
3 4 3 4064.95 267.25 4251.06 o
4 3 2 310.61 94.90 277.46 o
2 1 7 7325.52 354.39 7107.52 o
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3 3 -5 5719.58 308.72 6145.66 o
1 5 -4 1788.79 138.95 1518.14 o
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2 4 -5 7523.17 349.70 7206.22 o
2 3 6 208.68 176.19 356.60 o
2 5 -3 378.79 98.06 357.83 o
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1 1 8 221.59 170.17 194.93 o
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2 5 -4 4322.96 277.19 4101.46 o
4 4 -1 3550.98 254.66 3555.27 o
1 6 -2 833.12 111.64 878.09 o
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1 6 2 952.52 100.83 738.59 o
5 1 2 414.21 103.36 381.03 o
4 4 1 4829.03 296.57 4762.93 o
3 5 -2 1749.08 150.44 1758.90 o
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4 3 -4 108.04 153.97 79.05 o
3 1 -7 2098.54 171.07 2204.19 o
5 2 -1 20.71 183.38 182.67 o
3 5 2 1827.83 138.36 1602.16 o
2 0 -8 2625.90 232.63 2219.84 o
1 5 5 396.94 104.81 412.14 o
1 2 -8 -216.17 176.54 41.79 o
5 2 1 226.71 182.43 332.02 o
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0 6 3 8468.57 340.08 8634.42 o
3 3 -6 1025.97 114.20 1063.31 o
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2 3 -7 720.10 112.88 758.33 o
1 2 8 1953.30 165.56 2016.12 o
2 1 -8 0.89 178.22 0.31 o
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3 4 -5 3230.98 268.41 3565.74 o
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3 5 -3 1529.19 125.40 1446.89 o
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1 5 -6 3695.41 272.34 3516.06 o
3 5 -4 2999.09 265.69 3157.66 o
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5 3 3 0.38 188.45 10.87 o
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3 6 -2 127.60 191.55 58.55 o
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1 7 -1 192.56 182.23 66.45 o
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1 7 1 172.87 197.53 249.65 o
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1 6 -5 79.01 182.58 8.69 o
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1 6 5 801.32 125.67 780.05 o
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