#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012441.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012441_Fobs loop_ _publ_author_name 'Coles, Simon J.' 'Davies, David B.' 'Hursthouse, Michael B.' '\.Ibi\,so\(glu, Han\?ife' 'K\?il\?i\,c, Adem' 'Shaw, Robert A.' _publ_section_title ; Conformational polymorphism in a chiral spiro-cis-ansa-bridged cyclotriphosphazene derivative ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o51 _journal_page_last o54 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 95.645 _cell_angle_beta 96.981 _cell_angle_gamma 92.074 _cell_length_a 10.0832 _cell_length_b 12.7699 _cell_length_c 25.8156 _exptl_crystal_F_000 1464.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file na1540Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 01SRC160R in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 241.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' 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120.14 o 5 4 0 0.04 24.61 18.99 o 6 4 0 5.82 26.88 19.72 o 7 4 0 8686.23 8727.26 289.08 o 8 4 0 77.88 94.71 33.23 o 9 4 0 278.48 356.29 62.20 o 10 4 0 132.65 96.54 49.57 o 11 4 0 335.55 245.52 70.11 o -11 5 0 455.07 553.81 113.28 o -10 5 0 78.13 11.49 121.82 o -9 5 0 23.33 -50.88 67.78 o -8 5 0 812.87 950.01 113.25 o -7 5 0 2322.28 2294.85 86.50 o -6 5 0 1151.90 1125.77 48.80 o -5 5 0 175.60 125.13 39.15 o -4 5 0 46.99 106.59 28.05 o -3 5 0 86.90 56.46 20.68 o -2 5 0 32.05 61.55 19.55 o -1 5 0 3003.74 2848.25 81.79 o 0 5 0 15849.52 16314.17 398.18 o 1 5 0 2662.68 2752.41 73.51 o 2 5 0 2698.39 2873.79 72.41 o 3 5 0 2053.11 1978.54 60.55 o 4 5 0 131.46 102.80 16.24 o 5 5 0 1852.13 1756.30 63.08 o 6 5 0 277.54 298.17 25.71 o 7 5 0 5274.35 5882.02 362.19 o 8 5 0 41.69 19.97 25.64 o 9 5 0 10.77 -0.55 47.89 o 10 5 0 1374.66 1456.05 155.81 o 11 5 0 121.07 328.70 111.48 o 12 5 0 5.76 -82.17 93.67 o -12 6 0 4.36 132.08 119.66 o -10 6 0 170.38 39.62 114.07 o -9 6 0 1093.52 1325.13 255.72 o -8 6 0 2370.14 2523.31 110.08 o -7 6 0 2896.19 2984.84 136.80 o -6 6 0 18.94 52.71 33.59 o -5 6 0 26.63 0.10 29.57 o -4 6 0 4331.32 4406.21 134.23 o -3 6 0 4634.35 4114.69 109.87 o -2 6 0 5878.99 5530.07 156.25 o -1 6 0 4320.22 4678.86 125.92 o 0 6 0 1534.04 1466.08 47.52 o 1 6 0 75.58 35.05 12.98 o 2 6 0 504.24 474.59 22.20 o 3 6 0 916.33 864.26 58.61 o 4 6 0 1350.80 1161.85 88.87 o 5 6 0 109.44 141.51 19.41 o 6 6 0 54.53 97.88 17.43 o 7 6 0 2122.28 2287.87 86.67 o 8 6 0 3.37 26.66 44.48 o 9 6 0 4.06 42.87 25.12 o 10 6 0 658.47 624.76 66.90 o -11 7 0 129.05 68.75 98.31 o -9 7 0 897.19 1049.85 128.21 o -8 7 0 123.29 126.96 36.99 o -7 7 0 629.29 565.57 46.44 o -6 7 0 390.74 380.39 51.26 o -5 7 0 119.49 152.78 36.19 o -4 7 0 5387.44 4843.26 157.79 o -3 7 0 343.11 321.51 32.50 o -2 7 0 211.81 157.03 24.30 o -1 7 0 6343.89 6586.73 164.77 o 0 7 0 1933.84 2031.10 58.86 o 1 7 0 3591.25 3892.55 103.49 o 2 7 0 705.54 772.12 30.13 o 3 7 0 896.36 1006.22 42.30 o 4 7 0 2362.08 870.21 1242.38 o 5 7 0 580.28 431.18 122.86 o 6 7 0 66.13 62.97 15.42 o 7 7 0 530.84 480.50 38.42 o 8 7 0 40.42 22.01 25.54 o 9 7 0 0.93 30.73 35.63 o 10 7 0 129.42 23.56 64.36 o 11 7 0 52.17 93.67 75.85 o -11 8 0 145.71 114.41 97.05 o -10 8 0 155.66 117.90 97.24 o -9 8 0 490.69 616.73 105.12 o -8 8 0 2813.13 2794.32 135.83 o -7 8 0 1117.67 1143.18 84.90 o -6 8 0 7.18 16.72 31.99 o -5 8 0 2.31 -12.62 28.97 o -4 8 0 280.23 267.65 37.32 o -3 8 0 1545.18 1540.91 74.11 o -2 8 0 233.44 183.31 29.20 o -1 8 0 5326.88 5535.48 162.45 o 0 8 0 11.16 20.91 18.36 o 1 8 0 823.85 783.92 35.95 o 2 8 0 411.20 483.34 26.84 o 3 8 0 3097.13 3115.86 114.70 o 4 8 0 63.76 50.01 15.56 o 5 8 0 233.18 292.68 23.99 o 6 8 0 140.08 108.29 18.36 o 7 8 0 342.67 400.56 32.66 o 8 8 0 869.09 468.15 273.91 o 9 8 0 86.53 48.58 44.56 o 10 8 0 2.10 93.09 75.85 o 11 8 0 127.80 145.38 87.35 o -10 9 0 836.30 821.19 146.35 o -9 9 0 7.05 -13.92 75.82 o -8 9 0 1350.87 1219.28 109.69 o -7 9 0 126.41 73.08 71.08 o -6 9 0 9.37 -74.14 49.42 o -5 9 0 952.23 942.15 74.90 o -4 9 0 130.31 143.19 41.57 o -3 9 0 1677.16 1557.28 82.51 o -2 9 0 549.19 482.23 38.12 o -1 9 0 2091.38 2024.53 77.32 o 0 9 0 29.74 30.04 21.33 o 1 9 0 2481.95 2559.55 94.24 o 2 9 0 996.93 1032.37 48.69 o 3 9 0 412.56 470.27 30.30 o 4 9 0 411.57 389.98 24.27 o 5 9 0 52.23 44.20 13.74 o 6 9 0 585.14 591.63 36.99 o 7 9 0 115.66 131.80 20.65 o 8 9 0 674.21 484.31 77.18 o 9 9 0 499.76 576.37 87.35 o -10 10 0 35.75 174.18 125.70 o -9 10 0 23.95 55.53 84.27 o -8 10 0 97.44 92.52 52.29 o -7 10 0 0.08 61.98 63.45 o -6 10 0 308.76 219.44 80.78 o -5 10 0 0.44 -13.91 90.79 o -4 10 0 984.48 878.52 65.17 o -3 10 0 287.71 354.36 52.68 o -2 10 0 171.78 199.11 33.87 o -1 10 0 1332.21 1245.04 60.58 o 0 10 0 2563.81 2769.97 105.35 o 1 10 0 5431.46 5711.08 200.75 o 2 10 0 581.62 593.36 33.31 o 3 10 0 14.90 6.69 14.22 o 4 10 0 0.87 18.84 13.39 o 5 10 0 64.49 41.61 12.98 o 6 10 0 850.09 876.54 55.96 o 7 10 0 19.44 32.02 18.32 o -10 11 0 113.84 93.67 181.59 o -9 11 0 1148.35 1184.54 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242.58 282.51 31.20 o -1 -12 1 13.57 5.67 22.91 o 0 -12 1 194.64 205.13 37.11 o 1 -12 1 1955.58 1984.44 101.97 o 2 -12 1 3471.72 4245.65 195.66 o 3 -12 1 86.75 135.55 60.38 o 4 -12 1 260.78 318.16 74.04 o 5 -12 1 417.52 548.62 187.33 o 6 -12 1 124.84 253.86 81.44 o 7 -12 1 132.64 249.46 102.41 o 8 -12 1 117.21 191.85 109.65 o 9 -12 1 190.05 192.16 121.62 o -7 -11 1 371.84 629.23 180.44 o -4 -11 1 22.31 36.97 9.95 o -3 -11 1 269.61 260.86 25.88 o -2 -11 1 10.74 -0.94 20.22 o -1 -11 1 174.32 199.16 36.98 o 0 -11 1 1316.79 1489.39 78.74 o 1 -11 1 15.12 34.46 39.56 o 2 -11 1 35.36 20.60 26.65 o 3 -11 1 224.57 303.92 49.70 o 4 -11 1 1387.35 1491.75 88.67 o 5 -11 1 532.85 487.36 74.54 o 6 -11 1 854.04 836.44 108.92 o 8 -11 1 8.10 1.97 84.85 o 9 -11 1 0.12 80.67 113.46 o 10 -11 1 157.32 14.95 111.02 o -7 -10 1 50.02 -58.04 116.65 o -4 -10 1 1652.94 1510.61 89.68 o -3 -10 1 344.89 382.58 23.20 o -2 -10 1 56.04 54.93 15.63 o -1 -10 1 1987.78 2148.30 76.12 o 0 -10 1 5.46 7.59 24.57 o 1 -10 1 325.42 339.38 34.61 o 2 -10 1 470.10 365.14 40.50 o 3 -10 1 3.38 1.07 31.92 o 4 -10 1 25.27 68.62 42.15 o 5 -10 1 74.09 -34.45 36.96 o 6 -10 1 4.63 23.27 70.39 o 7 -10 1 1265.35 1348.86 144.27 o 8 -10 1 400.79 296.52 40.80 o 9 -10 1 5.55 -15.74 77.31 o 10 -10 1 10.44 -16.13 122.97 o -9 -9 1 117.07 233.31 64.36 o -8 -9 1 8.92 9.77 20.24 o -7 -9 1 148.43 160.19 18.88 o -6 -9 1 26.68 17.53 8.62 o -5 -9 1 188.97 197.04 22.23 o -4 -9 1 44.68 55.45 11.78 o -3 -9 1 6.14 3.76 12.34 o -2 -9 1 14.41 14.74 18.93 o -1 -9 1 285.18 308.64 29.90 o 0 -9 1 1827.15 1775.10 68.92 o 1 -9 1 7.71 25.42 20.68 o 2 -9 1 8008.98 8715.65 294.84 o 3 -9 1 13.42 17.71 25.86 o 4 -9 1 2931.04 3273.34 132.51 o 5 -9 1 1640.26 1841.46 129.56 o 6 -9 1 508.11 610.69 74.98 o 7 -9 1 542.38 512.90 76.49 o 8 -9 1 22.36 23.56 23.56 o 9 -9 1 83.51 201.09 95.00 o 10 -9 1 394.99 536.14 136.53 o -9 -8 1 118.67 116.65 75.85 o -8 -8 1 0.11 -5.75 26.28 o -7 -8 1 477.55 502.27 30.33 o -6 -8 1 28.29 12.32 13.74 o -5 -8 1 1.41 4.91 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