#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/27/2012715.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012715_Fobs loop_ _publ_author_name 'Aragoni, M. Carla' 'Arca, Massimiliano' 'Blake, Alexander J.' 'Lippolis, Vito' 'Schr\"oder, Martin' 'Wilson, Claire' _publ_section_title ; 4-Methoxyphenylphosphonic acid: reactivity of Lawesson's reagent ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o260 _journal_page_last o262 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.5819 _cell_length_b 10.0867 _cell_length_c 18.0870 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.7372 _[local]_cod_data_source_file na1560IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' MEBZPS #1465 for VL in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 122.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2525.50 2803.74 49.60 o 4 0 0 900.92 993.64 43.11 o 1 1 0 1555.50 1727.73 27.85 o 2 1 0 136.81 159.65 9.86 o 3 1 0 260.38 240.02 11.18 o 4 1 0 3.31 11.21 6.08 o 5 1 0 17.75 15.87 13.56 o 0 2 0 14965.31 14969.61 81.73 o 1 2 0 464.45 484.25 8.58 o 2 2 0 1245.84 1388.38 47.09 o 3 2 0 391.44 438.26 12.90 o 4 2 0 31.63 34.31 7.32 o 5 2 0 117.57 122.86 16.72 o 1 3 0 4538.46 5059.92 299.77 o 2 3 0 35.51 44.91 6.67 o 3 3 0 1163.85 1183.00 46.32 o 4 3 0 12.87 5.83 7.92 o 5 3 0 0.00 -7.12 10.98 o 6 3 0 4.80 24.61 21.04 o 0 4 0 1503.20 1417.05 23.51 o 1 4 0 30.96 34.75 4.71 o 2 4 0 73.30 85.64 14.15 o 3 4 0 1.19 -5.16 5.67 o 4 4 0 82.97 71.27 13.33 o 5 4 0 79.97 83.15 18.98 o 1 5 0 380.14 399.36 24.09 o 2 5 0 78.13 74.43 7.49 o 3 5 0 284.41 297.48 16.14 o 4 5 0 12.02 15.35 11.78 o 5 5 0 0.10 15.41 13.74 o 0 6 0 530.70 491.84 23.23 o 1 6 0 199.08 194.33 8.56 o 2 6 0 151.53 144.67 9.65 o 3 6 0 87.05 79.80 8.61 o 4 6 0 22.44 20.36 11.93 o 5 6 0 25.66 22.14 15.07 o 1 7 0 44.43 39.45 8.36 o 2 7 0 29.44 33.42 7.81 o 3 7 0 3.28 2.76 10.39 o 4 7 0 33.67 26.21 12.94 o 5 7 0 31.41 32.85 25.85 o 0 8 0 1193.48 1100.28 37.45 o 1 8 0 36.72 33.69 8.23 o 2 8 0 115.87 100.25 11.65 o 3 8 0 118.83 112.11 22.25 o 4 8 0 104.17 109.98 18.75 o 1 9 0 17.07 -0.96 8.12 o 2 9 0 58.68 66.78 11.24 o 3 9 0 20.55 16.28 19.59 o 4 9 0 5.66 -3.29 13.88 o 0 10 0 775.23 805.79 46.57 o 1 10 0 225.96 224.46 20.48 o 2 10 0 28.19 11.18 14.62 o 3 10 0 7.31 12.31 14.29 o 1 11 0 22.02 23.96 13.46 o 2 11 0 69.41 61.58 15.86 o 3 11 0 69.25 55.32 23.19 o 0 12 0 47.34 18.51 20.89 o 1 12 0 227.31 237.01 23.01 o 2 12 0 0.28 16.74 23.16 o 1 13 0 79.10 76.44 18.86 o 1 0 1 95.43 98.99 6.72 o 2 0 1 39.61 63.95 8.14 o 3 0 1 337.77 369.99 16.70 o 4 0 1 307.08 321.74 15.23 o 0 1 1 1987.20 1927.10 152.56 o 1 1 1 5168.31 5666.56 97.54 o 2 1 1 224.46 235.91 9.77 o 3 1 1 598.64 625.17 21.71 o 4 1 1 404.14 404.30 11.12 o 5 1 1 52.80 66.89 14.30 o 0 2 1 5462.74 4915.10 88.17 o 1 2 1 788.50 927.93 28.22 o 2 2 1 731.33 854.39 34.95 o 3 2 1 284.66 271.81 7.04 o 4 2 1 278.59 285.96 9.80 o 5 2 1 13.91 30.74 9.87 o 0 3 1 71.15 89.46 8.33 o 1 3 1 326.76 314.73 18.02 o 2 3 1 1105.23 1202.43 41.55 o 3 3 1 69.30 72.41 5.51 o 4 3 1 102.16 102.72 8.62 o 5 3 1 146.15 136.11 12.52 o 6 3 1 35.84 31.42 14.96 o 0 4 1 28.39 29.61 5.20 o 1 4 1 2266.42 2490.57 102.11 o 2 4 1 287.89 317.56 8.46 o 3 4 1 757.55 783.35 21.00 o 4 4 1 62.22 67.21 8.35 o 5 4 1 8.82 4.84 8.30 o 0 5 1 921.88 866.56 36.15 o 1 5 1 313.65 333.71 13.74 o 2 5 1 515.42 540.73 14.26 o 3 5 1 84.06 91.35 6.15 o 4 5 1 46.74 44.66 8.92 o 5 5 1 59.43 50.72 10.68 o 0 6 1 7.38 4.52 5.03 o 1 6 1 69.82 72.06 4.33 o 2 6 1 91.41 88.42 5.99 o 3 6 1 131.71 124.90 8.35 o 4 6 1 14.63 15.24 8.28 o 5 6 1 49.69 52.39 11.41 o 0 7 1 1637.96 1603.01 28.26 o 1 7 1 494.87 444.15 12.19 o 2 7 1 193.22 185.54 8.87 o 3 7 1 168.34 149.41 9.51 o 4 7 1 39.41 53.80 10.78 o 5 7 1 9.10 -10.96 15.37 o 0 8 1 186.07 180.96 10.21 o 1 8 1 214.58 205.29 9.55 o 2 8 1 66.95 68.76 7.11 o 3 8 1 64.06 58.41 9.95 o 4 8 1 7.32 -0.37 9.11 o 0 9 1 375.30 391.81 23.02 o 1 9 1 143.19 127.30 8.62 o 2 9 1 37.59 33.70 7.22 o 3 9 1 96.61 100.77 12.26 o 4 9 1 63.45 56.28 11.98 o 0 10 1 3.00 3.81 11.18 o 1 10 1 52.50 46.98 8.43 o 2 10 1 107.91 95.17 9.93 o 3 10 1 142.55 152.77 14.81 o 0 11 1 68.66 84.05 16.28 o 1 11 1 167.44 146.21 12.99 o 2 11 1 122.62 136.88 11.81 o 3 11 1 78.34 75.50 12.83 o 0 12 1 22.90 15.97 14.38 o 1 12 1 49.99 56.85 11.29 o 2 12 1 18.07 27.04 16.74 o 0 13 1 44.42 65.15 17.65 o 1 13 1 11.09 5.84 16.23 o 0 0 2 1.03 4.26 2.03 o 1 0 2 31.69 25.81 4.74 o 2 0 2 252.01 267.22 9.70 o 3 0 2 119.76 113.15 8.82 o 4 0 2 3.40 8.00 7.16 o 5 0 2 1.71 6.45 16.71 o 0 1 2 371.59 371.04 13.59 o 1 1 2 9115.33 9787.47 245.69 o 2 1 2 266.40 287.64 7.60 o 3 1 2 160.04 155.80 5.35 o 4 1 2 280.64 276.39 9.48 o 5 1 2 133.00 140.76 13.62 o 0 2 2 57.97 65.25 4.75 o 1 2 2 5321.67 6140.47 155.84 o 2 2 2 262.07 244.02 7.32 o 3 2 2 147.58 157.53 5.67 o 4 2 2 463.36 472.25 14.52 o 5 2 2 28.32 18.20 9.54 o 6 2 2 9.42 18.87 20.28 o 0 3 2 155.39 123.44 7.26 o 1 3 2 1148.22 1181.94 47.62 o 2 3 2 872.68 931.05 26.31 o 3 3 2 390.04 392.51 12.07 o 4 3 2 231.07 222.09 10.98 o 5 3 2 0.44 9.76 12.45 o 6 3 2 67.75 23.57 22.69 o 0 4 2 206.12 195.81 7.55 o 1 4 2 642.21 713.99 25.90 o 2 4 2 2701.29 2923.15 93.81 o 3 4 2 27.99 24.57 5.43 o 4 4 2 162.43 154.60 10.17 o 5 4 2 52.01 39.81 10.46 o 0 5 2 24.87 28.50 5.29 o 1 5 2 192.22 190.55 7.60 o 2 5 2 101.85 120.04 5.69 o 3 5 2 397.63 386.57 19.20 o 4 5 2 19.88 27.95 7.47 o 5 5 2 26.55 31.00 10.70 o 0 6 2 99.82 118.39 7.69 o 1 6 2 712.07 693.38 27.57 o 2 6 2 657.33 725.74 29.32 o 3 6 2 286.17 265.50 16.35 o 4 6 2 31.43 33.96 9.25 o 5 6 2 73.99 69.56 12.61 o 0 7 2 14.90 16.54 5.74 o 1 7 2 643.90 594.45 18.09 o 2 7 2 179.51 190.39 8.64 o 3 7 2 10.56 19.44 6.86 o 4 7 2 42.32 34.32 9.87 o 5 7 2 49.17 55.47 17.61 o 0 8 2 1.45 6.71 7.56 o 1 8 2 111.93 104.68 7.84 o 2 8 2 5.45 2.81 5.52 o 3 8 2 82.09 93.39 9.14 o 4 8 2 9.64 5.42 9.35 o 0 9 2 451.06 455.68 24.38 o 1 9 2 607.72 595.18 15.42 o 2 9 2 46.48 43.03 8.60 o 3 9 2 66.64 76.52 11.28 o 4 9 2 72.40 66.84 12.07 o 0 10 2 184.37 187.75 19.14 o 1 10 2 39.25 33.28 7.84 o 2 10 2 36.06 24.19 8.28 o 3 10 2 25.43 19.67 10.10 o 0 11 2 244.48 254.50 43.31 o 1 11 2 18.62 29.19 9.65 o 2 11 2 28.70 14.79 10.19 o 3 11 2 10.68 15.05 11.11 o 0 12 2 71.79 84.12 19.67 o 1 12 2 14.63 8.20 11.95 o 2 12 2 133.93 136.74 16.84 o 0 13 2 15.65 17.50 15.29 o 1 13 2 8.91 3.42 16.36 o 1 0 3 826.21 794.00 24.49 o 2 0 3 221.25 266.89 9.65 o 3 0 3 0.23 6.16 5.50 o 4 0 3 18.27 25.00 9.28 o 5 0 3 262.54 264.62 16.93 o 0 1 3 2.55 2.85 3.03 o 1 1 3 1.35 0.87 2.21 o 2 1 3 538.61 625.45 13.31 o 3 1 3 199.14 182.20 5.80 o 4 1 3 112.59 112.86 7.68 o 5 1 3 20.07 31.49 8.20 o 6 1 3 37.34 57.48 22.49 o 0 2 3 4770.21 4409.38 380.89 o 1 2 3 784.50 796.86 21.89 o 2 2 3 713.81 816.61 9.60 o 3 2 3 66.11 66.90 4.45 o 4 2 3 369.05 355.86 11.90 o 5 2 3 216.80 218.46 16.67 o 6 2 3 2.65 -7.94 17.94 o 0 3 3 4.99 3.58 4.69 o 1 3 3 497.36 510.78 21.59 o 2 3 3 244.58 245.08 5.80 o 3 3 3 352.09 376.50 17.32 o 4 3 3 333.93 348.74 13.51 o 5 3 3 55.91 57.52 12.64 o 0 4 3 1224.25 997.84 49.50 o 1 4 3 84.49 95.24 5.14 o 2 4 3 383.60 392.99 10.77 o 3 4 3 116.03 123.02 8.61 o 4 4 3 171.11 176.09 11.04 o 5 4 3 27.12 37.99 14.30 o 0 5 3 0.78 -0.65 4.49 o 1 5 3 829.59 850.09 19.41 o 2 5 3 922.55 915.94 39.34 o 3 5 3 271.16 260.29 17.39 o 4 5 3 248.11 251.61 16.84 o 5 5 3 63.71 66.96 16.26 o 0 6 3 874.94 886.82 16.47 o 1 6 3 861.35 880.45 48.80 o 2 6 3 479.81 460.02 21.53 o 3 6 3 229.31 216.37 11.48 o 4 6 3 76.99 81.17 9.61 o 5 6 3 55.73 69.57 12.30 o 0 7 3 77.82 70.39 7.29 o 1 7 3 201.93 197.35 7.81 o 2 7 3 33.37 26.42 6.27 o 3 7 3 224.50 214.26 10.77 o 4 7 3 31.37 26.00 9.75 o 5 7 3 7.07 2.14 23.17 o 0 8 3 51.89 50.33 9.68 o 1 8 3 1387.91 1250.19 32.78 o 2 8 3 227.15 227.00 15.80 o 3 8 3 13.40 12.90 7.16 o 4 8 3 18.08 25.12 10.08 o 0 9 3 67.11 63.30 10.88 o 1 9 3 50.82 46.60 7.34 o 2 9 3 135.90 144.64 10.76 o 3 9 3 17.77 13.19 7.78 o 4 9 3 101.87 106.15 13.74 o 0 10 3 63.63 60.21 14.00 o 1 10 3 109.46 109.37 10.36 o 2 10 3 19.43 19.82 8.39 o 3 10 3 13.30 7.32 11.16 o 0 11 3 0.00 -4.20 11.22 o 1 11 3 12.14 18.12 10.87 o 2 11 3 72.33 71.41 11.72 o 3 11 3 3.87 18.59 16.56 o 0 12 3 1.66 -0.16 13.17 o 1 12 3 37.09 49.80 13.40 o 2 12 3 6.11 3.35 12.47 o 0 13 3 2.00 -15.10 17.25 o 1 13 3 4.01 17.53 16.98 o 0 0 4 1790.25 1753.63 115.69 o 1 0 4 28.34 33.85 4.25 o 2 0 4 105.87 120.76 7.52 o 3 0 4 31.36 42.63 7.08 o 4 0 4 134.97 136.99 15.03 o 5 0 4 11.35 10.04 8.72 o 6 0 4 28.14 -15.51 19.11 o 0 1 4 483.90 472.93 14.45 o 1 1 4 1685.46 1690.33 57.16 o 2 1 4 637.69 624.15 22.85 o 3 1 4 254.61 250.76 8.25 o 4 1 4 340.07 335.85 12.81 o 5 1 4 97.74 97.82 11.27 o 6 1 4 7.43 -3.25 20.79 o 0 2 4 815.30 698.88 22.00 o 1 2 4 59.64 48.92 3.12 o 2 2 4 464.33 484.08 14.67 o 3 2 4 243.77 240.04 8.00 o 4 2 4 248.88 256.55 11.74 o 5 2 4 48.43 48.98 10.03 o 0 3 4 11.90 3.02 4.93 o 1 3 4 407.80 418.75 16.61 o 2 3 4 679.61 737.68 15.25 o 3 3 4 767.79 787.62 30.59 o 4 3 4 456.88 499.93 20.43 o 5 3 4 34.85 25.16 11.60 o 0 4 4 310.81 322.20 9.95 o 1 4 4 205.48 240.29 9.03 o 2 4 4 116.91 111.54 5.32 o 3 4 4 26.13 23.81 6.29 o 4 4 4 301.99 306.11 19.10 o 5 4 4 153.90 144.69 15.26 o 0 5 4 421.43 422.06 13.83 o 1 5 4 989.30 1020.09 42.16 o 2 5 4 258.36 266.14 8.62 o 3 5 4 1213.61 1241.55 56.09 o 4 5 4 186.78 195.54 11.86 o 5 5 4 4.77 10.28 14.71 o 0 6 4 77.43 69.72 7.05 o 1 6 4 126.78 126.30 6.42 o 2 6 4 99.11 93.96 7.02 o 3 6 4 108.63 104.40 9.39 o 4 6 4 118.81 103.01 10.21 o 5 6 4 84.99 81.30 21.84 o 0 7 4 33.29 38.11 6.53 o 1 7 4 22.51 18.79 4.59 o 2 7 4 392.28 420.18 14.44 o 3 7 4 102.76 115.84 10.23 o 4 7 4 175.82 146.14 11.53 o 0 8 4 646.62 648.06 22.43 o 1 8 4 110.00 104.33 9.87 o 2 8 4 81.59 80.62 8.02 o 3 8 4 67.77 67.91 8.56 o 4 8 4 117.68 110.30 13.19 o 0 9 4 30.69 29.74 9.22 o 1 9 4 71.34 59.37 7.88 o 2 9 4 47.82 48.90 7.80 o 3 9 4 77.88 75.75 9.79 o 4 9 4 64.85 50.41 13.92 o 0 10 4 8.12 9.47 11.66 o 1 10 4 129.98 119.71 12.02 o 2 10 4 8.68 3.44 8.12 o 3 10 4 23.06 30.11 8.74 o 0 11 4 7.09 8.76 12.94 o 1 11 4 22.28 22.43 10.76 o 2 11 4 13.64 12.21 9.77 o 3 11 4 63.42 72.35 20.51 o 0 12 4 32.15 47.53 15.20 o 1 12 4 12.39 9.76 11.64 o 2 12 4 69.80 64.34 15.05 o 1 13 4 38.27 57.87 25.46 o 1 0 5 227.59 255.44 7.43 o 2 0 5 48.31 33.83 6.59 o 3 0 5 105.14 107.86 8.64 o 4 0 5 215.96 228.15 17.10 o 5 0 5 13.92 11.95 9.88 o 6 0 5 32.78 45.92 23.86 o 0 1 5 3648.55 3234.36 148.34 o 1 1 5 298.04 287.59 12.69 o 2 1 5 421.29 463.44 14.08 o 3 1 5 108.96 105.24 5.92 o 4 1 5 221.53 224.68 11.66 o 5 1 5 40.69 35.29 9.87 o 6 1 5 75.52 107.78 35.29 o 0 2 5 292.76 281.23 15.71 o 1 2 5 330.01 329.40 8.63 o 2 2 5 467.21 492.36 15.04 o 3 2 5 532.54 525.10 21.33 o 4 2 5 130.16 122.58 10.48 o 5 2 5 43.01 49.10 10.24 o 6 2 5 76.97 49.19 17.00 o 0 3 5 1689.33 1791.06 75.67 o 1 3 5 304.06 272.35 9.87 o 2 3 5 119.60 122.19 5.39 o 3 3 5 157.24 161.07 11.77 o 4 3 5 48.97 47.91 8.09 o 5 3 5 131.38 150.18 13.54 o 0 4 5 581.08 682.37 41.79 o 1 4 5 733.77 678.66 37.24 o 2 4 5 136.12 151.35 9.59 o 3 4 5 1366.62 1410.35 80.05 o 4 4 5 32.08 29.55 7.77 o 5 4 5 5.09 -0.14 10.89 o 0 5 5 865.70 917.96 57.67 o 1 5 5 362.14 358.48 10.49 o 2 5 5 318.55 298.06 15.26 o 3 5 5 294.68 274.12 13.32 o 4 5 5 4.25 -1.42 7.20 o 5 5 5 139.74 153.38 16.56 o 0 6 5 724.13 753.19 19.48 o 1 6 5 15.03 12.83 4.54 o 2 6 5 302.88 297.21 17.18 o 3 6 5 334.89 353.09 16.85 o 4 6 5 129.09 118.67 10.86 o 5 6 5 32.20 42.31 17.09 o 0 7 5 477.33 432.74 13.38 o 1 7 5 340.10 320.21 11.67 o 2 7 5 617.16 630.19 41.75 o 3 7 5 100.31 85.02 9.45 o 4 7 5 13.86 20.42 8.69 o 0 8 5 15.11 11.01 8.04 o 1 8 5 25.11 22.44 6.30 o 2 8 5 81.99 89.11 8.26 o 3 8 5 2.71 4.58 6.66 o 4 8 5 145.35 131.32 12.08 o 0 9 5 350.45 360.23 17.75 o 1 9 5 22.15 19.94 8.38 o 2 9 5 179.39 161.90 10.53 o 3 9 5 40.78 38.11 8.41 o 4 9 5 29.55 28.69 11.33 o 0 10 5 37.89 31.78 12.47 o 1 10 5 5.42 -2.21 7.92 o 2 10 5 97.85 92.48 12.69 o 3 10 5 60.80 74.83 9.77 o 0 11 5 2.14 12.89 13.01 o 1 11 5 62.17 64.66 11.55 o 2 11 5 13.50 6.78 9.80 o 3 11 5 18.54 22.64 14.14 o 0 12 5 20.71 32.03 21.90 o 1 12 5 52.75 49.72 13.36 o 2 12 5 2.84 1.58 12.80 o 1 13 5 9.83 5.42 25.47 o 0 0 6 8092.02 7573.22 699.46 o 1 0 6 350.35 439.48 20.45 o 2 0 6 1599.48 1692.44 59.99 o 3 0 6 209.49 210.00 14.64 o 4 0 6 192.86 161.89 12.75 o 5 0 6 198.94 185.67 16.15 o 6 0 6 51.06 93.75 26.52 o 0 1 6 384.85 331.82 12.20 o 1 1 6 564.11 593.36 24.11 o 2 1 6 37.33 31.31 2.61 o 3 1 6 437.60 444.72 17.01 o 4 1 6 204.46 215.70 11.39 o 5 1 6 324.46 318.04 15.32 o 6 1 6 37.89 27.00 14.45 o 0 2 6 997.49 921.86 18.02 o 1 2 6 102.16 112.55 6.63 o 2 2 6 696.47 717.23 34.39 o 3 2 6 203.10 208.29 9.70 o 4 2 6 34.93 32.10 7.83 o 5 2 6 311.28 299.50 16.74 o 0 3 6 17.67 10.38 4.37 o 1 3 6 178.83 169.48 6.08 o 2 3 6 378.56 387.97 18.42 o 3 3 6 629.74 591.59 31.68 o 4 3 6 87.91 99.65 10.64 o 5 3 6 102.36 112.34 12.63 o 0 4 6 10.44 15.33 5.47 o 1 4 6 103.34 101.77 5.45 o 2 4 6 491.83 523.56 15.35 o 3 4 6 38.89 36.98 6.15 o 4 4 6 227.12 219.40 19.84 o 5 4 6 140.70 136.09 13.49 o 0 5 6 60.63 83.02 8.64 o 1 5 6 187.23 165.28 8.30 o 2 5 6 50.85 50.16 5.97 o 3 5 6 119.30 132.16 9.89 o 4 5 6 111.84 105.85 10.36 o 5 5 6 17.96 28.17 12.04 o 0 6 6 166.12 158.74 11.12 o 1 6 6 14.42 6.01 4.56 o 2 6 6 38.16 41.86 6.33 o 3 6 6 309.53 299.89 22.77 o 4 6 6 169.87 160.95 14.27 o 5 6 6 54.27 69.32 17.26 o 0 7 6 35.29 34.01 8.17 o 1 7 6 238.71 220.25 8.63 o 2 7 6 30.44 30.18 7.49 o 3 7 6 12.60 21.60 7.65 o 4 7 6 93.54 78.70 10.17 o 0 8 6 536.59 524.65 19.53 o 1 8 6 30.15 32.29 6.97 o 2 8 6 109.36 97.83 9.70 o 3 8 6 111.56 112.37 10.97 o 4 8 6 34.74 43.28 9.35 o 0 9 6 2.32 5.53 8.66 o 1 9 6 113.52 110.99 11.27 o 2 9 6 32.10 31.14 7.52 o 3 9 6 20.05 28.00 8.98 o 4 9 6 18.64 6.18 13.31 o 0 10 6 20.12 9.48 12.63 o 1 10 6 38.79 40.25 9.88 o 2 10 6 73.72 72.40 10.11 o 3 10 6 49.97 46.06 9.28 o 0 11 6 72.85 96.22 24.84 o 1 11 6 22.02 11.64 9.64 o 2 11 6 46.73 44.15 11.33 o 3 11 6 71.78 78.39 19.10 o 0 12 6 57.06 79.71 25.28 o 1 12 6 47.31 54.63 14.14 o 2 12 6 17.11 -1.48 13.66 o 1 0 7 4475.31 4400.13 249.53 o 2 0 7 665.51 664.28 25.40 o 3 0 7 69.61 58.12 7.64 o 4 0 7 4.90 4.01 8.30 o 5 0 7 584.97 639.98 47.41 o 0 1 7 2228.89 2301.68 67.13 o 1 1 7 189.31 221.79 6.94 o 2 1 7 270.10 276.50 8.28 o 3 1 7 386.08 418.44 11.65 o 4 1 7 457.36 437.57 15.33 o 5 1 7 45.07 45.88 9.32 o 0 2 7 140.76 123.81 6.02 o 1 2 7 355.06 346.47 13.16 o 2 2 7 329.32 344.78 14.66 o 3 2 7 38.88 29.12 6.15 o 4 2 7 148.31 150.01 11.86 o 5 2 7 110.46 108.58 14.17 o 0 3 7 73.19 73.41 5.89 o 1 3 7 772.43 796.93 22.38 o 2 3 7 1565.02 1536.76 78.95 o 3 3 7 66.66 71.02 7.74 o 4 3 7 370.79 373.69 17.08 o 5 3 7 14.51 5.95 9.63 o 0 4 7 15.37 14.93 5.92 o 1 4 7 898.54 900.82 23.29 o 2 4 7 297.07 296.37 14.92 o 3 4 7 77.10 70.39 7.01 o 4 4 7 4.90 3.23 7.88 o 5 4 7 17.65 23.44 10.24 o 0 5 7 344.58 322.08 33.64 o 1 5 7 24.83 28.62 4.48 o 2 5 7 597.42 615.01 30.09 o 3 5 7 113.94 114.99 8.51 o 4 5 7 42.16 39.29 9.53 o 5 5 7 0.05 10.30 10.20 o 0 6 7 569.72 485.55 33.22 o 1 6 7 233.43 237.21 11.72 o 2 6 7 65.76 60.70 6.69 o 3 6 7 11.59 11.41 7.29 o 4 6 7 10.56 13.19 8.84 o 5 6 7 28.85 47.92 16.20 o 0 7 7 253.92 232.63 13.52 o 1 7 7 231.68 230.65 10.01 o 2 7 7 16.52 17.62 7.23 o 3 7 7 148.18 164.07 11.37 o 4 7 7 44.25 44.10 9.74 o 0 8 7 26.13 26.04 8.76 o 1 8 7 266.35 264.15 11.23 o 2 8 7 26.48 20.07 7.48 o 3 8 7 27.00 29.99 9.27 o 4 8 7 5.29 8.48 8.98 o 0 9 7 69.88 76.87 11.59 o 1 9 7 59.45 66.07 9.82 o 2 9 7 9.50 16.19 7.00 o 3 9 7 122.04 145.21 11.33 o 4 9 7 16.96 28.28 14.40 o 0 10 7 221.92 224.45 20.40 o 1 10 7 64.68 52.82 10.06 o 2 10 7 0.16 4.30 9.19 o 3 10 7 18.14 15.79 9.07 o 0 11 7 2.60 1.75 17.46 o 1 11 7 8.20 2.14 9.07 o 2 11 7 67.07 85.11 12.45 o 3 11 7 72.87 85.91 23.39 o 0 12 7 35.77 73.86 25.64 o 1 12 7 5.37 10.33 12.66 o 2 12 7 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6.37 10.82 o 0 4 21 353.24 385.93 40.43 o 1 4 21 53.16 64.99 11.99 o 2 4 21 4.80 19.86 13.10 o 0 5 21 9.07 16.87 18.29 o 1 5 21 30.49 14.98 13.91 o 1 6 21 4.91 0.93 20.81 o 0 0 22 6.14 29.05 20.45 o 1 0 22 121.97 135.71 19.15 o 0 1 22 213.29 262.57 23.82 o 1 1 22 15.01 23.93 11.32 o 2 1 22 13.84 18.33 16.91 o 0 2 22 16.71 12.91 13.72 o 1 2 22 59.08 60.15 13.48 o 2 2 22 3.61 1.53 12.78 o 1 3 22 25.86 13.55 11.28 o 2 3 22 22.87 35.55 14.25 o 0 4 22 1.38 4.70 17.14 o 1 0 23 38.10 56.79 17.36 o 0 1 23 77.11 99.30 18.87 o 1 1 23 16.31 25.47 11.79 o 0 2 23 43.39 53.00 22.57 o 1 2 23 53.41 72.19 17.73 o 1 3 23 53.69 101.32 26.05 o 0 0 24 7.30 8.77 21.23 o 0 1 24 1.70 30.95 22.45 o 1 1 24 49.21 45.59 23.85 o