#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012726.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012726_Fobs loop_ _publ_author_name 'Horne, Keri T.' 'Powell, Gregory L.' 'Daniels, Lee M.' _publ_section_title ; Tetrakis(\m-benzothiazole-2-thiolato)-1:2\k^4^N:S^2^;1:2\k^4^S^2^:N-dichloro-1\kCl,2\kCl-dirhenium(III)(Re---Re) dichloromethane solvate: a bridged complex with a long Re---Re quadruple bond ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m292 _journal_page_last m294 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.092 _cell_angle_gamma 90.000 _cell_length_a 12.9408 _cell_length_b 15.5347 _cell_length_c 17.5303 _exptl_crystal_F_000 2264.00 _reflns_d_resolution_high 0.7691 _[local]_cod_data_source_file ta1364Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xl in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 588.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 50366.11 49250.76 827.18 o 3 0 0 857.87 1488.63 335.86 o 4 0 0 134339.22 136839.13 1633.82 o 5 0 0 176108.36 181213.34 1957.95 o 6 0 0 321119.50 306948.63 2691.26 o 7 0 0 85724.21 86588.13 1503.29 o 8 0 0 5979.43 6063.47 340.67 o 9 0 0 691.43 384.53 202.59 o 10 0 0 674.75 267.68 223.77 o 11 0 0 2223.40 1983.34 285.60 o 12 0 0 13951.47 14236.32 568.79 o 13 0 0 5285.00 5230.22 385.77 o 14 0 0 426.73 708.01 404.79 o 15 0 0 83.50 298.32 266.19 o 16 0 0 51.39 -171.60 338.79 o 1 1 0 2277.78 2474.32 64.86 o 2 1 0 561.17 619.98 72.56 o 3 1 0 520.61 686.63 141.58 o 4 1 0 9307.62 9727.43 493.13 o 5 1 0 37249.59 35315.07 553.84 o 6 1 0 72130.13 72218.73 795.57 o 7 1 0 49551.50 50450.18 1174.92 o 8 1 0 9182.03 8989.48 337.32 o 9 1 0 40.31 73.73 168.99 o 10 1 0 2344.37 2516.91 244.43 o 11 1 0 23325.32 24100.42 497.51 o 12 1 0 29808.91 30240.20 568.30 o 13 1 0 21391.94 22068.30 512.69 o 14 1 0 10094.25 10274.21 368.91 o 15 1 0 626.45 765.00 196.67 o 16 1 0 5804.64 5537.17 440.39 o 0 2 0 314708.53 318407.19 1237.27 o 1 2 0 267034.03 264514.34 908.89 o 2 2 0 8276.68 8643.12 235.06 o 3 2 0 4469.47 4868.52 161.85 o 4 2 0 16273.06 17044.58 307.42 o 5 2 0 153240.19 155909.19 1247.82 o 6 2 0 103321.59 102967.09 3357.24 o 7 2 0 106216.67 101461.17 1786.16 o 8 2 0 27666.24 26228.97 581.49 o 9 2 0 313.74 323.74 188.43 o 10 2 0 7742.11 8116.30 362.39 o 11 2 0 24623.85 26381.44 654.09 o 12 2 0 17125.86 18026.80 520.99 o 13 2 0 6367.52 6339.57 347.86 o 14 2 0 314.94 310.64 182.22 o 15 2 0 10.73 4.18 173.45 o 16 2 0 89.70 311.89 192.43 o 1 3 0 644.20 802.99 56.68 o 2 3 0 146.48 185.81 60.82 o 3 3 0 3207.73 3450.69 131.63 o 4 3 0 5700.24 6080.19 186.06 o 5 3 0 10982.55 10408.96 300.33 o 6 3 0 10841.18 10184.95 479.99 o 7 3 0 36404.56 36148.32 608.21 o 8 3 0 8632.80 8309.32 354.10 o 9 3 0 1.62 -90.59 179.92 o 10 3 0 27050.01 26274.09 613.64 o 11 3 0 56752.57 58560.48 1483.59 o 12 3 0 42334.03 41754.89 1812.02 o 13 3 0 36604.06 37421.21 973.79 o 14 3 0 14924.30 15533.56 527.95 o 15 3 0 11.65 95.40 172.68 o 16 3 0 11744.88 12305.38 514.47 o 0 4 0 3310.04 3784.94 295.40 o 1 4 0 3392.54 3376.91 86.93 o 2 4 0 33850.14 35622.11 326.54 o 3 4 0 47.33 153.22 98.01 o 4 4 0 160576.66 173133.20 2169.07 o 5 4 0 49374.95 48812.00 628.40 o 6 4 0 32089.23 30584.59 475.98 o 7 4 0 25877.15 26268.74 897.06 o 8 4 0 5029.76 5326.95 331.82 o 9 4 0 1678.67 1749.09 228.35 o 10 4 0 49630.63 46229.81 1011.41 o 11 4 0 27374.09 25965.05 823.64 o 12 4 0 12575.85 13667.64 624.80 o 13 4 0 4526.53 3875.99 389.24 o 14 4 0 798.73 748.65 275.71 o 15 4 0 72.92 29.89 181.88 o 16 4 0 901.83 933.70 266.40 o 1 5 0 378.59 341.25 58.81 o 2 5 0 7710.11 7907.44 135.46 o 3 5 0 35.99 54.06 63.18 o 4 5 0 9118.51 8891.94 183.64 o 5 5 0 15499.99 15561.98 298.91 o 6 5 0 17474.25 17171.76 352.04 o 7 5 0 12618.05 12163.68 485.22 o 8 5 0 3557.83 3720.86 241.76 o 9 5 0 1047.69 1107.21 204.45 o 10 5 0 23040.83 23613.36 808.84 o 11 5 0 40633.13 36167.55 1007.21 o 12 5 0 20315.26 19648.67 760.79 o 13 5 0 14113.72 14209.84 669.65 o 14 5 0 6941.08 7574.29 514.88 o 15 5 0 65.95 285.75 261.84 o 16 5 0 7544.28 7696.47 447.92 o 0 6 0 103112.41 104509.50 524.78 o 1 6 0 124823.68 126426.13 956.95 o 2 6 0 34049.57 35807.50 406.24 o 3 6 0 6600.18 6384.85 179.87 o 4 6 0 64570.75 68189.72 1466.28 o 5 6 0 108809.66 110953.12 2299.15 o 6 6 0 30466.10 29725.92 449.87 o 7 6 0 14399.70 14475.26 355.30 o 8 6 0 133.25 157.97 146.17 o 9 6 0 6892.39 6728.52 483.35 o 10 6 0 9877.39 9532.33 554.64 o 11 6 0 13534.03 13118.20 935.71 o 12 6 0 2375.88 1721.29 332.85 o 13 6 0 1103.01 982.32 285.77 o 14 6 0 111.09 -241.47 241.47 o 15 6 0 575.15 190.33 264.43 o 16 6 0 861.31 804.90 305.19 o 1 7 0 4502.74 4765.98 132.49 o 2 7 0 1613.12 1516.58 88.12 o 3 7 0 5191.69 5258.57 198.66 o 4 7 0 351.90 415.20 86.93 o 5 7 0 6066.78 5978.72 182.67 o 6 7 0 21285.79 20296.95 469.37 o 7 7 0 24535.45 24290.04 689.90 o 8 7 0 9131.11 8820.79 513.52 o 9 7 0 3770.28 3573.29 405.24 o 10 7 0 334.70 591.37 267.54 o 11 7 0 9553.40 10356.62 580.84 o 12 7 0 9669.48 8806.35 562.55 o 13 7 0 7309.35 6273.91 1058.17 o 14 7 0 726.45 811.39 289.86 o 15 7 0 848.00 1448.31 324.28 o 0 8 0 70907.77 72653.67 1216.79 o 1 8 0 31558.81 32795.71 257.21 o 2 8 0 17002.52 17707.97 239.51 o 3 8 0 12865.32 13692.46 216.00 o 4 8 0 4001.86 4176.56 155.30 o 5 8 0 7028.17 6772.11 230.32 o 6 8 0 82274.02 79987.67 1147.49 o 7 8 0 32214.92 31573.65 800.94 o 8 8 0 8823.81 8742.77 668.05 o 9 8 0 57.79 -162.89 263.29 o 10 8 0 4327.14 3735.59 404.06 o 11 8 0 3380.76 3556.10 495.72 o 12 8 0 4633.64 5221.34 457.24 o 13 8 0 256.42 622.85 294.64 o 14 8 0 2698.21 3088.59 854.31 o 15 8 0 2507.30 2477.68 398.41 o 1 9 0 3773.62 3862.90 109.58 o 2 9 0 11552.97 11481.85 267.40 o 3 9 0 8995.45 8996.25 191.82 o 4 9 0 13910.56 13758.38 237.97 o 5 9 0 346.29 256.46 153.01 o 6 9 0 13877.33 14314.56 421.32 o 7 9 0 12792.54 11921.65 542.12 o 8 9 0 13476.16 13617.75 626.48 o 9 9 0 6461.13 7187.48 507.08 o 10 9 0 722.90 839.16 271.39 o 11 9 0 1127.92 1086.55 285.74 o 12 9 0 9656.88 10246.02 609.96 o 13 9 0 7331.09 6788.93 526.84 o 14 9 0 714.67 813.33 477.39 o 15 9 0 145.46 -416.52 419.45 o 0 10 0 17347.40 17768.02 339.72 o 1 10 0 6869.03 6908.10 148.28 o 2 10 0 220.14 292.08 80.21 o 3 10 0 308.66 138.49 121.95 o 4 10 0 486.06 598.46 135.86 o 5 10 0 9001.21 8831.33 335.45 o 6 10 0 5446.23 5488.50 293.81 o 7 10 0 2730.80 2916.86 338.98 o 8 10 0 317.43 205.52 239.16 o 9 10 0 1259.50 1358.02 308.11 o 10 10 0 884.35 805.57 288.04 o 11 10 0 1308.75 1410.94 308.96 o 12 10 0 696.57 685.08 282.30 o 13 10 0 21.28 47.98 257.92 o 14 10 0 997.98 695.15 344.66 o 1 11 0 6080.69 6054.47 150.26 o 2 11 0 6762.23 6627.32 154.58 o 3 11 0 9569.90 9415.51 321.91 o 4 11 0 3936.63 3885.26 205.05 o 5 11 0 12.11 -152.76 152.76 o 6 11 0 318.23 298.88 187.29 o 7 11 0 1280.43 1407.97 276.43 o 8 11 0 718.55 796.36 264.91 o 9 11 0 207.88 103.42 255.18 o 10 11 0 12.52 -173.68 253.80 o 11 11 0 397.86 323.46 256.65 o 12 11 0 956.66 837.11 299.17 o 13 11 0 562.00 412.71 291.90 o 14 11 0 302.97 111.46 478.12 o 0 12 0 357.94 312.04 172.56 o 1 12 0 160.17 332.83 133.15 o 2 12 0 145.69 122.63 123.81 o 3 12 0 5279.64 5169.13 281.20 o 4 12 0 14577.52 14349.16 551.79 o 5 12 0 2694.70 2626.90 259.31 o 6 12 0 1090.46 988.93 188.56 o 7 12 0 9922.88 9372.86 435.83 o 8 12 0 4627.54 4771.64 427.87 o 9 12 0 4317.37 4520.51 450.40 o 10 12 0 3549.53 3457.93 406.05 o 11 12 0 969.50 821.85 286.51 o 12 12 0 162.49 171.71 258.24 o 13 12 0 1605.78 1615.64 348.29 o 1 13 0 1700.46 1648.07 192.98 o 2 13 0 5996.46 6202.77 297.49 o 3 13 0 7587.66 7492.08 330.74 o 4 13 0 5339.84 5464.42 296.80 o 5 13 0 1646.24 1610.62 207.27 o 6 13 0 1128.01 968.26 197.78 o 7 13 0 73.70 290.34 178.72 o 8 13 0 2754.44 2791.70 398.19 o 9 13 0 2629.23 2180.65 632.12 o 10 13 0 720.27 857.43 310.04 o 11 13 0 501.23 325.60 262.92 o 12 13 0 397.67 640.36 334.39 o 0 14 0 41460.24 41996.83 1270.10 o 1 14 0 9409.43 9252.21 442.30 o 2 14 0 131.43 113.50 152.38 o 3 14 0 118.51 137.68 163.03 o 4 14 0 587.04 678.16 180.96 o 5 14 0 2278.63 2132.38 232.34 o 6 14 0 10184.83 9365.23 411.15 o 7 14 0 3514.73 3250.97 286.19 o 8 14 0 1014.66 947.81 349.79 o 9 14 0 1329.78 1240.63 335.28 o 10 14 0 2545.13 1832.14 354.33 o 11 14 0 270.10 307.97 300.21 o 1 15 0 3504.46 3456.51 310.22 o 2 15 0 8198.06 8494.54 451.49 o 3 15 0 13000.85 12236.82 436.63 o 4 15 0 9339.66 9232.17 394.54 o 5 15 0 4703.46 4342.08 302.50 o 6 15 0 2472.56 2164.33 242.09 o 7 15 0 17.03 -143.98 176.78 o 8 15 0 2289.46 2023.43 358.27 o 9 15 0 5125.85 4872.67 482.84 o 10 15 0 4710.04 4831.43 498.27 o 11 15 0 3802.11 3917.41 446.45 o 0 16 0 11283.54 11083.29 733.31 o 1 16 0 7220.06 6937.53 442.92 o 2 16 0 4850.87 5038.52 378.81 o 3 16 0 2198.24 1758.97 268.01 o 4 16 0 186.04 282.00 184.21 o 5 16 0 3989.35 3757.74 295.51 o 6 16 0 8732.27 8764.31 426.61 o 7 16 0 8578.31 8742.08 444.91 o 8 16 0 9445.07 9656.67 632.68 o 9 16 0 3117.61 2678.38 406.47 o 10 16 0 74.35 538.25 574.92 o 1 17 0 2838.45 3029.03 317.32 o 2 17 0 3345.56 2984.73 321.56 o 3 17 0 3604.56 3813.26 352.05 o 4 17 0 5578.90 5560.93 411.71 o 5 17 0 3119.59 3502.04 352.60 o 6 17 0 1133.75 1321.78 236.21 o 7 17 0 307.61 319.48 213.85 o 8 17 0 13.72 -290.21 324.86 o 9 17 0 659.30 978.24 586.65 o 0 18 0 6015.54 6596.88 629.18 o 1 18 0 8055.07 8484.35 494.51 o 2 18 0 7209.22 6744.35 445.09 o 3 18 0 2010.44 1998.25 379.86 o 4 18 0 1558.29 1723.60 279.45 o 5 18 0 3916.58 3981.15 378.18 o 6 18 0 2707.68 3433.98 370.74 o 7 18 0 9837.97 9775.59 498.91 o 1 19 0 658.90 594.72 248.89 o 2 19 0 216.58 45.73 256.66 o 3 19 0 535.20 278.30 239.23 o 4 19 0 3007.80 2853.61 352.72 o 5 19 0 3431.80 3637.15 389.41 o 0 20 0 16251.59 17784.30 1058.90 o 1 20 0 12970.39 13217.91 649.16 o 2 20 0 2619.98 3188.44 504.52 o -16 1 1 1119.78 990.85 217.27 o -15 1 1 208.78 463.31 191.15 o -14 1 1 10.53 241.57 150.46 o -13 1 1 351.79 326.84 158.01 o -12 1 1 553.75 837.70 170.64 o -11 1 1 405.46 505.22 162.79 o -10 1 1 275.43 140.03 147.78 o -9 1 1 533.75 684.34 183.10 o -8 1 1 115.34 -11.72 154.67 o -7 1 1 86.00 -28.71 149.24 o -6 1 1 10932.10 10787.51 581.33 o -5 1 1 26693.22 27888.24 499.43 o -4 1 1 10436.57 10985.41 267.44 o -3 1 1 78.89 50.41 141.86 o -2 1 1 2501.35 2833.40 124.77 o -1 1 1 48.51 72.42 26.88 o 0 1 1 304.36 296.56 28.72 o 1 1 1 544.76 656.28 41.41 o 2 1 1 200.97 299.54 74.64 o 3 1 1 25.62 142.73 146.03 o 4 1 1 979.38 1204.50 161.85 o 5 1 1 5588.87 5553.29 285.00 o 6 1 1 3133.92 3246.27 230.96 o 7 1 1 3609.29 3797.81 280.87 o 8 1 1 3969.90 3983.14 251.87 o 9 1 1 1594.58 1536.70 215.41 o 10 1 1 45.04 122.76 181.05 o 11 1 1 4773.74 4961.67 263.45 o 12 1 1 475.99 251.53 153.97 o 13 1 1 584.53 475.08 160.11 o 14 1 1 71.25 118.52 170.54 o 15 1 1 633.92 689.55 192.02 o 16 1 1 868.07 828.04 263.38 o -16 2 1 273.55 209.96 196.91 o -15 2 1 456.01 170.42 177.41 o -14 2 1 789.95 746.69 195.03 o -13 2 1 38.78 -83.02 152.49 o -12 2 1 143.04 40.17 147.45 o -11 2 1 4038.18 4121.00 294.56 o -10 2 1 267.04 228.40 193.25 o -9 2 1 2704.51 2672.25 249.75 o -8 2 1 2243.30 2702.60 240.68 o -7 2 1 143.23 207.34 156.75 o -6 2 1 8507.81 9203.82 294.83 o -5 2 1 27243.11 28606.32 434.90 o -4 2 1 16986.93 17406.80 302.77 o -3 2 1 252.86 346.50 107.45 o -2 2 1 18702.83 19089.54 176.72 o -1 2 1 486.86 434.23 46.17 o 0 2 1 168.16 331.03 46.36 o 1 2 1 1152.01 1185.73 61.77 o 2 2 1 23225.04 23856.70 884.38 o 3 2 1 720.12 860.77 154.14 o 4 2 1 68948.46 71036.38 3644.84 o 5 2 1 60457.52 62375.00 726.43 o 6 2 1 37002.48 37493.71 719.17 o 7 2 1 555.63 166.19 178.51 o 8 2 1 1433.29 1388.38 208.59 o 9 2 1 2761.37 2978.11 250.52 o 10 2 1 6045.95 6391.62 329.08 o 11 2 1 2629.83 2692.67 255.56 o 12 2 1 2201.95 2357.37 247.17 o 13 2 1 1916.87 1734.88 228.50 o 14 2 1 618.44 496.64 189.56 o 15 2 1 811.87 772.59 200.96 o 16 2 1 624.39 672.72 214.22 o -16 3 1 142.47 282.83 205.65 o -15 3 1 339.61 352.62 187.93 o -14 3 1 2042.43 2020.35 240.29 o -13 3 1 131.45 431.85 239.59 o -12 3 1 863.49 1219.09 217.09 o -11 3 1 2238.56 2517.01 297.01 o -10 3 1 13405.07 13687.94 557.96 o -9 3 1 3867.89 3543.02 274.97 o -8 3 1 11959.23 12066.24 383.69 o -7 3 1 4558.14 4017.63 259.05 o -6 3 1 7810.44 8828.03 275.66 o -5 3 1 35395.68 35966.38 471.36 o -4 3 1 56163.13 55629.13 565.55 o -3 3 1 11954.57 12007.23 172.47 o -2 3 1 22029.87 22298.81 280.15 o -1 3 1 2005.67 2287.31 96.27 o 0 3 1 339.34 378.51 55.03 o 1 3 1 466.28 494.57 62.27 o 2 3 1 6102.41 6261.10 237.09 o 3 3 1 11471.19 12192.70 219.87 o 4 3 1 20316.21 20837.72 357.76 o 5 3 1 10832.05 11365.48 282.57 o 6 3 1 769.44 756.23 151.34 o 7 3 1 152.44 186.49 167.83 o 8 3 1 225.52 251.00 190.02 o 9 3 1 4.47 -186.46 186.46 o 10 3 1 1006.87 697.55 218.10 o 11 3 1 866.58 938.22 215.14 o 12 3 1 34.39 58.44 226.86 o 13 3 1 17.82 50.24 263.99 o 14 3 1 238.49 261.03 178.76 o 15 3 1 251.29 236.97 186.51 o 16 3 1 147.45 -50.56 192.69 o -16 4 1 109.58 231.01 204.41 o -15 4 1 1496.17 1797.09 306.86 o -14 4 1 5820.09 5363.01 431.52 o -13 4 1 12103.13 11887.50 628.45 o -12 4 1 5855.41 5909.50 454.75 o -11 4 1 2183.37 1533.48 249.58 o -10 4 1 168.99 -117.45 205.58 o -9 4 1 7067.14 7269.77 452.57 o -8 4 1 3054.76 2795.43 224.39 o -7 4 1 4724.39 4752.25 278.19 o -6 4 1 9709.91 10563.15 294.38 o -5 4 1 2811.35 3015.55 167.69 o -4 4 1 11392.79 10878.05 381.96 o -3 4 1 4459.33 4370.50 118.41 o -2 4 1 14171.89 14147.41 223.19 o -1 4 1 24254.89 25294.47 217.69 o 0 4 1 3406.77 3276.28 82.70 o 1 4 1 28547.25 31340.93 355.26 o 2 4 1 28301.78 27163.06 438.41 o 3 4 1 48490.79 49272.37 517.16 o 4 4 1 14745.45 15323.91 276.35 o 5 4 1 16189.29 17466.56 312.07 o 6 4 1 1772.67 1512.33 227.06 o 7 4 1 15178.32 15463.94 388.12 o 8 4 1 15088.46 14465.24 553.77 o 9 4 1 18752.94 18584.64 535.25 o 10 4 1 17034.17 15421.29 503.65 o 11 4 1 3882.49 3636.95 385.54 o 12 4 1 432.33 428.12 247.79 o 13 4 1 4233.95 4133.80 451.72 o 14 4 1 7205.38 7609.62 500.20 o 15 4 1 3890.86 4515.70 414.30 o 16 4 1 2092.29 2109.77 269.38 o -16 5 1 8763.43 8806.47 448.07 o -15 5 1 13091.30 13554.48 657.84 o -14 5 1 7798.20 7586.54 512.65 o -13 5 1 3191.45 3025.82 376.79 o -12 5 1 535.40 519.54 258.05 o -11 5 1 6964.04 6047.31 769.98 o -10 5 1 29465.51 28840.86 1085.03 o -9 5 1 67854.71 68702.82 1143.83 o -8 5 1 39229.50 40662.82 642.29 o -7 5 1 24837.32 24939.63 473.13 o -6 5 1 6425.01 6309.49 245.29 o -5 5 1 8860.55 9702.59 258.19 o -4 5 1 33332.08 34440.37 798.16 o -3 5 1 70261.03 69672.84 494.62 o -2 5 1 18424.69 18363.80 227.46 o -1 5 1 4415.44 4221.66 110.32 o 0 5 1 69.89 93.71 52.65 o 1 5 1 503.97 355.79 52.39 o 2 5 1 10807.61 11142.21 138.02 o 3 5 1 37654.68 37551.23 774.57 o 4 5 1 20604.75 21781.46 318.38 o 5 5 1 4181.18 4325.70 168.98 o 6 5 1 2345.44 2515.09 156.49 o 7 5 1 4003.74 3958.66 215.16 o 8 5 1 3116.03 3023.95 231.50 o 9 5 1 8030.30 7328.96 516.55 o 10 5 1 768.98 602.29 452.45 o 11 5 1 77.99 -47.71 241.55 o 12 5 1 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