#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:39:39 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180796 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/27/2012736.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012736_Fobs loop_ _publ_author_name 'Jones, Peter G.' 'Hartig, Thorsten' 'Hopf, Henning' _publ_section_title ; Three ruthenocene derivatives: (\h^5^-4,7-dimethylindenyl)(\h^5^-pentamethylcyclopentadienyl)ruthenium(II), [\h^5^-[2](4,7)indeno[2]paracyclophanyl](\h^5^-pentamethylcyclopentadienyl)ruthenium(II) and bis[\h^5^-[2](4,7)indeno[2]paracyclophanyl]ruthenium(II) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m347 _journal_page_last m350 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.920 _cell_angle_gamma 90.000 _cell_length_a 12.6200 _cell_length_b 17.0260 _cell_length_c 13.0050 _exptl_crystal_F_000 1224.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file bm1496Vsup4.hkl _cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' ruebe in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 277.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 257.02 214.72 5.28 o 4 0 0 165.14 179.58 6.82 o 6 0 0 1054.96 1075.95 26.56 o 8 0 0 3663.24 3561.50 56.01 o 10 0 0 2966.20 3146.76 55.96 o 12 0 0 2790.63 3068.93 66.60 o 14 0 0 102.52 79.85 23.26 o 2 1 0 205.26 166.83 4.75 o 3 1 0 4171.80 4507.69 114.72 o 4 1 0 1437.25 1617.10 17.88 o 5 1 0 164.69 137.73 9.82 o 6 1 0 4748.48 4799.73 77.92 o 7 1 0 3307.84 3649.54 49.92 o 8 1 0 900.95 923.57 27.95 o 9 1 0 3548.32 3676.49 64.89 o 10 1 0 107.95 89.79 16.13 o 11 1 0 482.51 454.03 26.89 o 12 1 0 1196.55 1287.98 43.16 o 13 1 0 460.25 486.52 32.15 o 14 1 0 445.72 497.97 34.61 o 2 2 0 2356.25 2447.52 74.34 o 3 2 0 855.27 879.71 11.79 o 4 2 0 11445.09 12299.30 121.26 o 5 2 0 15618.69 16006.75 196.04 o 6 2 0 199.96 215.60 13.21 o 7 2 0 6999.80 6582.87 96.08 o 8 2 0 4.49 -1.17 9.59 o 9 2 0 51.23 64.53 13.56 o 10 2 0 152.27 147.07 17.65 o 11 2 0 118.10 146.25 19.52 o 12 2 0 40.92 36.24 17.77 o 13 2 0 970.10 1043.40 42.10 o 14 2 0 0.01 1.40 20.93 o 1 3 0 14308.75 15085.46 124.79 o 2 3 0 6501.14 6664.28 60.73 o 3 3 0 5691.14 5946.64 54.83 o 4 3 0 2441.33 2411.17 26.60 o 5 3 0 144.35 152.23 10.64 o 6 3 0 7572.21 8274.31 113.82 o 7 3 0 1911.75 1843.09 35.82 o 8 3 0 863.95 857.33 27.60 o 9 3 0 2253.55 2101.75 44.36 o 10 3 0 538.33 495.68 26.19 o 11 3 0 2189.39 2075.89 50.32 o 12 3 0 346.51 320.94 26.77 o 13 3 0 667.24 654.59 36.13 o 14 3 0 737.70 767.08 40.58 o 0 4 0 40923.20 38021.66 588.63 o 1 4 0 27.01 28.22 4.27 o 2 4 0 405.76 483.19 9.10 o 3 4 0 9695.65 10772.95 217.73 o 4 4 0 1677.04 1719.98 21.57 o 5 4 0 2029.99 2194.71 39.11 o 6 4 0 1841.19 1758.82 32.89 o 7 4 0 301.97 300.73 17.07 o 8 4 0 3767.71 3838.44 59.63 o 9 4 0 0.52 6.08 11.92 o 10 4 0 2399.37 2385.22 50.68 o 11 4 0 17.63 8.07 15.31 o 12 4 0 1215.34 1224.70 43.16 o 13 4 0 157.03 155.25 23.97 o 14 4 0 230.36 212.43 28.41 o 1 5 0 1939.27 1818.10 21.25 o 2 5 0 7045.66 7896.54 202.29 o 3 5 0 74.51 113.27 6.20 o 4 5 0 35183.94 38903.39 457.66 o 5 5 0 4796.97 5456.90 79.68 o 6 5 0 10059.77 10699.92 124.90 o 7 5 0 250.70 272.19 17.42 o 8 5 0 3099.31 3391.63 57.03 o 9 5 0 1787.49 1804.75 42.36 o 10 5 0 279.77 276.04 22.10 o 11 5 0 625.05 595.89 30.52 o 12 5 0 1016.78 1100.27 41.75 o 13 5 0 29.63 -10.52 18.70 o 14 5 0 678.05 661.36 39.41 o 0 6 0 27.53 16.02 5.73 o 1 6 0 650.98 622.24 11.29 o 2 6 0 5290.38 5776.27 54.42 o 3 6 0 16899.12 17090.03 269.49 o 4 6 0 5418.59 6640.00 73.19 o 5 6 0 8415.75 8586.44 112.92 o 6 6 0 8645.07 8667.94 129.21 o 7 6 0 10627.96 10935.03 132.11 o 8 6 0 682.50 698.75 27.01 o 9 6 0 248.36 274.64 20.46 o 10 6 0 148.78 133.74 18.47 o 11 6 0 1165.77 1126.56 40.00 o 12 6 0 209.29 152.34 22.91 o 13 6 0 1675.25 1672.52 54.86 o 14 6 0 4.59 -1.17 21.39 o 1 7 0 14163.20 13385.67 120.39 o 2 7 0 1481.48 1460.95 18.71 o 3 7 0 4619.17 4344.45 61.84 o 4 7 0 1093.69 1131.94 18.45 o 5 7 0 1701.84 1787.99 33.94 o 6 7 0 8060.58 8639.19 113.26 o 7 7 0 1711.76 1761.67 38.62 o 8 7 0 738.84 839.09 29.94 o 9 7 0 1132.14 1226.50 37.31 o 10 7 0 25.39 9.94 14.15 o 11 7 0 768.87 766.07 34.85 o 12 7 0 310.10 299.66 27.59 o 13 7 0 0.38 5.96 19.64 o 14 7 0 219.42 180.04 28.99 o 0 8 0 18076.62 17310.48 202.04 o 1 8 0 1.20 -1.76 9.47 o 2 8 0 9994.82 9699.75 90.96 o 3 8 0 781.48 851.48 30.47 o 4 8 0 1822.26 1787.97 23.96 o 5 8 0 522.45 461.92 20.00 o 6 8 0 1816.98 1856.04 38.38 o 7 8 0 1888.19 2055.37 42.83 o 8 8 0 823.91 796.55 30.17 o 9 8 0 239.72 204.60 19.88 o 10 8 0 979.67 1113.85 39.06 o 11 8 0 199.45 166.13 22.21 o 12 8 0 1131.96 1161.69 44.91 o 13 8 0 38.04 32.15 21.63 o 1 9 0 3171.55 3483.60 58.18 o 2 9 0 2191.65 1869.19 1139.86 o 3 9 0 1224.34 1359.21 47.50 o 4 9 0 9414.32 8967.39 86.08 o 5 9 0 1213.36 1266.02 31.94 o 6 9 0 2099.09 1938.27 40.73 o 7 9 0 2578.93 2511.95 48.58 o 8 9 0 1176.68 1168.86 36.26 o 9 9 0 406.92 446.30 26.19 o 10 9 0 127.36 110.48 19.29 o 11 9 0 705.30 723.48 35.78 o 12 9 0 557.64 609.30 35.90 o 13 9 0 117.05 114.45 24.90 o 0 10 0 226.05 224.48 14.38 o 1 10 0 69.78 45.09 7.06 o 2 10 0 1044.38 1124.78 22.99 o 3 10 0 3459.40 3556.76 38.18 o 4 10 0 158.76 161.70 10.37 o 5 10 0 2555.69 2445.91 44.95 o 6 10 0 195.51 182.27 17.07 o 7 10 0 799.77 775.36 30.29 o 8 10 0 20.33 9.70 13.91 o 9 10 0 5.37 -13.79 13.79 o 10 10 0 60.19 80.78 18.94 o 11 10 0 36.16 23.38 18.70 o 12 10 0 33.78 42.90 21.39 o 1 11 0 4006.44 4134.74 41.54 o 2 11 0 1150.21 1122.48 21.13 o 3 11 0 4071.36 4053.75 106.34 o 4 11 0 463.82 482.30 18.48 o 5 11 0 35.30 31.91 12.39 o 6 11 0 556.13 540.94 25.73 o 7 11 0 2920.69 2934.53 56.19 o 8 11 0 353.63 277.57 22.68 o 9 11 0 739.87 842.42 35.90 o 10 11 0 750.09 654.38 34.61 o 11 11 0 2678.34 2714.89 65.53 o 12 11 0 3.03 21.74 21.28 o 0 12 0 3856.16 3723.42 58.58 o 1 12 0 67.45 47.28 8.64 o 2 12 0 4065.04 4378.97 44.28 o 3 12 0 1036.11 1025.17 36.14 o 4 12 0 898.73 958.65 22.24 o 5 12 0 587.99 523.29 25.61 o 6 12 0 347.42 357.66 23.38 o 7 12 0 1293.50 1279.53 40.00 o 8 12 0 699.08 652.97 31.57 o 9 12 0 12.44 -4.56 15.66 o 10 12 0 4948.74 4625.57 93.12 o 11 12 0 394.72 406.18 32.27 o 12 12 0 762.89 711.66 41.16 o 1 13 0 28.62 12.72 8.18 o 2 13 0 1959.69 2016.13 41.25 o 3 13 0 1052.12 1103.73 24.03 o 4 13 0 1584.49 1654.98 29.49 o 5 13 0 4.19 -8.53 12.63 o 6 13 0 1529.55 1569.43 43.40 o 7 13 0 0.11 -11.92 14.50 o 8 13 0 1223.93 1110.66 40.47 o 9 13 0 252.61 201.09 24.32 o 10 13 0 198.56 135.03 24.08 o 11 13 0 133.53 109.66 24.32 o 0 14 0 1920.08 1961.22 44.46 o 1 14 0 68.18 74.48 13.97 o 2 14 0 969.37 906.73 34.15 o 3 14 0 2919.72 3029.37 70.12 o 4 14 0 84.24 83.45 11.57 o 5 14 0 1455.34 1462.56 42.35 o 6 14 0 168.81 169.87 20.34 o 7 14 0 1336.63 1316.57 43.63 o 8 14 0 778.51 779.97 36.95 o 9 14 0 109.37 99.49 21.51 o 10 14 0 469.29 473.07 33.91 o 1 15 0 1301.78 1333.23 28.04 o 2 15 0 15.41 -5.46 9.63 o 3 15 0 1930.58 1982.28 34.13 o 4 15 0 737.32 723.28 22.82 o 5 15 0 14.25 9.24 14.73 o 6 15 0 91.50 57.99 17.65 o 7 15 0 784.10 788.75 36.95 o 8 15 0 115.18 78.56 20.69 o 9 15 0 1197.92 1259.47 48.42 o 10 15 0 51.71 38.23 22.21 o 0 16 0 553.33 507.71 28.06 o 1 16 0 33.57 17.94 11.03 o 2 16 0 642.44 680.23 22.70 o 3 16 0 1303.84 1284.10 29.82 o 4 16 0 744.28 713.97 28.01 o 5 16 0 281.86 280.95 24.90 o 6 16 0 168.20 148.24 21.98 o 7 16 0 269.63 290.06 27.47 o 8 16 0 147.50 141.58 23.85 o 9 16 0 3.22 -8.42 19.41 o 1 17 0 1.55 -10.86 10.86 o 2 17 0 1966.95 2044.15 43.17 o 3 17 0 75.02 55.29 13.51 o 4 17 0 2091.31 2221.54 40.58 o 5 17 0 0.50 -3.74 16.37 o 6 17 0 779.77 764.18 38.12 o 7 17 0 110.95 113.75 23.85 o 8 17 0 514.51 471.20 34.26 o 0 18 0 566.57 557.98 32.74 o 1 18 0 747.94 674.80 24.76 o 2 18 0 371.41 400.13 21.04 o 3 18 0 879.38 856.13 27.86 o 4 18 0 8.42 -4.98 13.27 o 5 18 0 384.78 364.55 29.46 o 6 18 0 42.57 32.50 20.22 o 1 19 0 757.26 768.21 27.33 o 2 19 0 43.25 33.43 14.01 o 3 19 0 234.21 221.35 18.93 o 4 19 0 15.73 7.11 14.09 o 5 19 0 3.53 -18.47 18.47 o 0 20 0 650.74 643.81 37.77 o 1 20 0 210.45 207.17 19.10 o 2 20 0 106.12 64.43 15.91 o -13 0 1 1987.03 1902.33 54.29 o -11 0 1 1415.89 1388.41 41.29 o -9 0 1 776.58 771.88 27.95 o -7 0 1 164.08 178.88 13.80 o -5 0 1 10764.89 10574.38 138.20 o -3 0 1 17939.78 19278.42 167.53 o 3 0 1 5942.05 6083.35 90.40 o 5 0 1 8547.33 9164.90 120.66 o 7 0 1 3899.76 3261.96 61.54 o 9 0 1 1785.47 1815.14 41.07 o 11 0 1 116.88 92.12 18.24 o 13 0 1 77.36 67.10 20.69 o -14 1 1 628.83 610.84 37.07 o -13 1 1 44.97 37.29 19.76 o -12 1 1 1985.77 2005.75 52.65 o -11 1 1 144.64 136.67 19.29 o -10 1 1 50.28 36.82 14.03 o -9 1 1 1959.53 2008.56 43.65 o -8 1 1 154.54 110.95 13.56 o -7 1 1 7141.18 7355.79 95.63 o -6 1 1 3519.36 3952.58 65.42 o -5 1 1 3508.05 3330.40 54.43 o -4 1 1 9686.81 9384.74 122.38 o -3 1 1 2461.13 2371.03 24.51 o -2 1 1 18727.58 18839.13 167.95 o 2 1 1 511.43 505.75 25.16 o 3 1 1 13814.52 14777.54 212.70 o 4 1 1 3127.06 3237.89 31.10 o 5 1 1 7571.52 7925.83 99.83 o 6 1 1 8978.79 8994.53 118.31 o 7 1 1 382.19 401.66 18.36 o 8 1 1 579.32 560.74 22.80 o 9 1 1 324.41 326.80 20.58 o 10 1 1 489.45 456.14 25.14 o 11 1 1 1885.86 1994.65 49.26 o 12 1 1 48.32 33.43 18.35 o 13 1 1 1119.11 1137.84 44.21 o 14 1 1 44.69 -1.64 20.58 o -14 2 1 42.63 33.08 21.98 o -13 2 1 150.54 157.59 23.97 o -12 2 1 13.41 14.50 16.60 o -11 2 1 101.06 122.52 18.82 o -10 2 1 1024.67 1000.02 33.45 o -9 2 1 51.61 46.65 13.21 o -8 2 1 9541.61 9403.72 147.68 o -7 2 1 61.93 71.31 10.99 o -6 2 1 6557.36 6392.74 85.78 o -5 2 1 113.29 114.93 9.70 o -4 2 1 13042.01 14377.83 128.72 o -3 2 1 2144.52 2257.18 23.21 o -2 2 1 319.06 303.54 6.45 o -1 2 1 30324.22 30121.27 282.82 o 1 2 1 29384.53 29084.79 311.44 o 2 2 1 21529.83 23134.81 275.98 o 3 2 1 10810.95 11660.89 125.30 o 4 2 1 547.10 457.07 10.09 o 5 2 1 353.38 403.79 15.20 o 6 2 1 6065.53 6627.55 107.46 o 7 2 1 48.33 51.79 10.64 o 8 2 1 2701.35 2801.62 47.30 o 9 2 1 1.16 -0.23 11.81 o 10 2 1 2488.32 2552.74 54.54 o 11 2 1 0.01 2.81 14.61 o 12 2 1 2197.18 2342.76 57.57 o 13 2 1 2.56 -8.42 18.59 o 14 2 1 968.67 973.20 44.44 o -14 3 1 243.37 186.83 27.24 o -13 3 1 14.28 9.94 19.17 o -12 3 1 2587.57 2571.84 58.75 o -11 3 1 24.38 3.74 15.31 o -10 3 1 99.40 123.34 17.19 o -9 3 1 1755.12 1715.05 40.25 o -8 3 1 235.46 243.89 17.77 o -7 3 1 2922.66 3070.37 46.97 o -6 3 1 518.16 448.26 17.54 o -5 3 1 92.55 56.00 8.42 o -4 3 1 18.09 -3.28 8.36 o -3 3 1 35130.84 35243.57 325.65 o -2 3 1 22379.72 22999.08 194.96 o -1 3 1 1209.26 1114.73 12.38 o 0 3 1 16877.72 17702.21 174.41 o 1 3 1 6161.38 6227.73 59.16 o 2 3 1 1511.43 1530.83 17.20 o 3 3 1 11702.03 13085.03 109.59 o 4 3 1 683.18 565.69 11.77 o 5 3 1 3734.93 3718.32 53.01 o 6 3 1 2616.17 2495.69 41.00 o 7 3 1 222.21 237.11 15.78 o 8 3 1 3594.16 3783.30 69.23 o 9 3 1 435.66 430.65 23.15 o 10 3 1 2349.93 2307.58 49.86 o 11 3 1 777.95 806.78 34.03 o 12 3 1 15.77 0.94 17.18 o 13 3 1 315.37 345.37 29.58 o 14 3 1 137.70 141.81 25.84 o -14 4 1 28.79 24.32 21.98 o -13 4 1 1388.09 1384.17 48.07 o -12 4 1 97.61 78.33 19.64 o -11 4 1 1944.43 1831.11 47.97 o -10 4 1 623.37 610.88 28.18 o -9 4 1 1180.05 1229.17 34.98 o -8 4 1 663.23 665.08 25.38 o -7 4 1 2307.17 2316.84 44.14 o -6 4 1 21.50 19.64 8.77 o -5 4 1 24838.57 26927.21 321.33 o -4 4 1 622.10 643.34 12.37 o -3 4 1 9.34 50.27 6.31 o -2 4 1 14920.04 16651.48 132.84 o -1 4 1 16144.92 15783.21 171.83 o 0 4 1 1373.68 1465.13 15.69 o 1 4 1 34.33 31.14 4.00 o 2 4 1 7515.97 7587.49 67.28 o 3 4 1 6891.77 7506.03 68.30 o 4 4 1 1347.80 1672.19 20.04 o 5 4 1 13924.14 14903.83 231.13 o 6 4 1 3.65 -0.94 8.07 o 7 4 1 22070.53 21989.27 260.54 o 8 4 1 6.03 15.55 11.34 o 9 4 1 5127.67 5332.97 100.33 o 10 4 1 1442.13 1477.48 41.53 o 11 4 1 89.55 85.34 18.94 o 12 4 1 295.16 255.81 25.37 o 13 4 1 167.83 146.60 24.32 o 14 4 1 0.23 -20.22 20.22 o -14 5 1 572.93 604.98 37.65 o -13 5 1 131.27 145.67 24.67 o -12 5 1 577.09 497.07 30.87 o -11 5 1 310.24 313.92 24.90 o -10 5 1 27.09 24.67 14.61 o -9 5 1 1358.29 1417.49 38.02 o -8 5 1 87.43 87.10 14.26 o -7 5 1 11970.78 12365.65 149.69 o -6 5 1 3225.28 3493.75 50.03 o -5 5 1 9540.96 9308.34 128.85 o -4 5 1 5623.52 6026.22 94.75 o -3 5 1 3.21 11.80 4.30 o -2 5 1 832.32 849.69 12.62 o -1 5 1 1982.27 1998.95 22.82 o 0 5 1 322.54 286.90 7.44 o 1 5 1 5347.34 5469.76 72.19 o 2 5 1 1272.72 1460.00 25.17 o 3 5 1 6600.58 6301.45 62.22 o 4 5 1 4605.35 4751.68 44.15 o 5 5 1 4851.90 4849.20 66.88 o 6 5 1 6255.81 6503.43 101.55 o 7 5 1 2795.66 2849.91 49.18 o 8 5 1 2176.08 2318.15 44.94 o 9 5 1 667.84 748.31 29.47 o 10 5 1 1412.16 1440.24 41.29 o 11 5 1 1556.87 1604.39 46.09 o 12 5 1 28.34 45.12 18.94 o 13 5 1 521.82 472.84 33.09 o 14 5 1 650.28 668.37 39.52 o -14 6 1 282.15 232.54 29.35 o -13 6 1 375.13 412.72 31.80 o -12 6 1 144.96 126.61 22.33 o -11 6 1 556.29 551.67 30.52 o -10 6 1 865.55 921.91 34.62 o -9 6 1 26.40 6.55 13.44 o -8 6 1 6874.96 7442.47 92.11 o -7 6 1 76.43 79.15 12.63 o -6 6 1 6124.96 5790.24 92.73 o -5 6 1 100.85 113.05 11.34 o -4 6 1 1387.75 1341.71 19.24 o -3 6 1 933.40 1001.15 15.43 o -2 6 1 73.14 86.14 5.83 o -1 6 1 8.77 7.04 3.92 o 0 6 1 9250.74 8995.59 76.45 o 1 6 1 5.75 5.52 8.01 o 2 6 1 13595.92 12646.89 119.39 o 3 6 1 3266.92 3823.23 34.93 o 4 6 1 3663.17 3154.47 31.69 o 5 6 1 623.84 632.14 21.05 o 6 6 1 1410.08 1468.57 32.65 o 7 6 1 149.40 155.61 15.32 o 8 6 1 12.76 0.82 11.34 o 9 6 1 57.15 41.97 15.08 o 10 6 1 734.57 780.81 32.63 o 11 6 1 10.81 -4.44 16.13 o 12 6 1 1644.10 1646.01 50.65 o 13 6 1 0.04 -18.94 18.94 o 14 6 1 178.75 208.68 29.11 o -14 7 1 786.78 727.22 41.63 o -13 7 1 26.85 27.24 21.16 o -12 7 1 1873.86 1843.16 53.58 o -11 7 1 0.57 16.72 17.42 o -10 7 1 679.77 754.25 32.63 o -9 7 1 1739.16 1828.37 44.58 o -8 7 1 52.90 49.80 14.15 o -7 7 1 1095.20 1099.80 31.23 o -6 7 1 3852.25 4026.53 61.64 o -5 7 1 41.13 43.14 9.70 o -4 7 1 5433.08 5417.88 56.60 o -3 7 1 106.21 132.53 7.56 o -2 7 1 12536.95 11905.38 105.58 o -1 7 1 537.31 537.66 23.33 o 0 7 1 4446.31 4486.51 43.46 o 1 7 1 1931.97 1809.78 42.57 o 2 7 1 62.77 73.87 6.32 o 3 7 1 1151.44 1081.34 18.72 o 4 7 1 16614.26 17666.05 146.99 o 5 7 1 3659.30 3872.28 54.96 o 6 7 1 8208.10 8125.50 101.04 o 7 7 1 184.64 189.98 16.72 o 8 7 1 1413.63 1496.50 38.49 o 9 7 1 466.87 449.70 25.49 o 10 7 1 686.40 659.76 30.99 o 11 7 1 259.59 238.62 24.20 o 12 7 1 15.53 20.93 19.17 o 13 7 1 23.64 18.24 20.46 o -13 8 1 1150.49 1166.59 47.37 o -12 8 1 18.71 4.68 18.70 o -11 8 1 1919.80 1972.88 52.88 o -10 8 1 196.99 183.08 21.04 o -9 8 1 0.72 7.60 14.15 o -8 8 1 2.21 33.32 14.03 o -7 8 1 29.64 12.51 11.46 o -6 8 1 3779.51 3972.62 60.10 o -5 8 1 18035.66 17780.87 210.11 o -4 8 1 138.26 168.78 9.26 o -3 8 1 5758.07 5753.68 52.08 o -2 8 1 925.66 1036.02 21.12 o -1 8 1 14414.02 15093.32 285.71 o 0 8 1 759.49 933.37 21.06 o 1 8 1 124.14 90.65 7.54 o 2 8 1 1895.73 1904.47 24.05 o 3 8 1 2.00 5.78 16.42 o 4 8 1 1744.07 1736.45 23.83 o 5 8 1 7977.06 7960.08 99.16 o 6 8 1 6.03 -8.88 10.17 o 7 8 1 2535.21 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