#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:39:39 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180796 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/27/2012741.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012741_Fobs loop_ _publ_author_name 'Assaaoudi, Hassane' 'Ennaciri, Abdelaziz' 'Harcharras, Mohamed' 'El Bali, Brahim' 'Reinauer, Felix' 'Glaum, Robert' 'Rulmont, Andr\'e' 'Spirlet, Marie-Rose' _publ_section_title ; KZn(HP~2~O~7~)·2H~2~O and KMn(HP~2~O~7~)·2H~2~O: acid pyrophosphate metallates(II) with layer structures ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i79 _journal_page_last i81 _journal_volume 58 _journal_year 2002 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cod_data_source_file br1366Isup2.hkl _cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5754.14 5428.58 75.14 o 4 0 0 6928.19 7035.47 118.99 o 6 0 0 1169.47 1462.39 68.02 o 8 0 0 371.27 382.79 16.76 o 10 0 0 2312.78 2367.36 109.01 o 12 0 0 14073.48 14367.07 282.61 o 14 0 0 149.90 132.26 18.31 o 16 0 0 779.86 755.62 31.26 o 18 0 0 4219.50 4298.62 119.55 o 2 1 0 8.62 23.29 9.15 o 4 1 0 11751.36 12020.33 349.43 o 6 1 0 156.59 189.92 32.35 o 8 1 0 4753.51 4548.85 95.97 o 10 1 0 6250.82 5948.51 126.54 o 12 1 0 5745.39 5474.86 123.12 o 14 1 0 2973.63 2889.32 83.40 o 16 1 0 702.79 717.24 21.84 o 18 1 0 0.53 6.63 8.95 o 0 2 0 2923.55 2660.50 58.97 o 2 2 0 1077.36 991.10 39.47 o 4 2 0 10909.02 9928.46 152.33 o 6 2 0 4228.53 4587.83 118.27 o 8 2 0 12555.70 11982.88 233.87 o 10 2 0 9008.45 8139.82 215.17 o 12 2 0 2972.57 2817.30 122.62 o 14 2 0 4984.70 5095.42 155.08 o 16 2 0 155.30 156.06 19.26 o 2 3 0 8515.64 8398.55 138.65 o 4 3 0 17602.15 16654.31 225.30 o 6 3 0 321.80 389.77 15.42 o 8 3 0 1971.51 2129.88 97.68 o 10 3 0 528.75 602.13 28.57 o 12 3 0 925.82 837.65 37.25 o 14 3 0 2243.59 2295.88 102.04 o 16 3 0 6159.43 5852.21 149.21 o 0 4 0 45229.98 49372.64 440.60 o 2 4 0 475.12 505.53 18.88 o 4 4 0 127.18 93.77 9.30 o 6 4 0 52.02 30.82 10.52 o 8 4 0 3963.62 3961.40 132.55 o 10 4 0 4074.01 3894.58 140.59 o 12 4 0 3591.04 3490.09 123.34 o 14 4 0 411.96 418.86 24.62 o 16 4 0 67.69 56.41 16.40 o 2 5 0 1044.48 1076.94 39.96 o 4 5 0 4869.02 4897.09 140.60 o 6 5 0 1020.52 1007.24 39.04 o 8 5 0 2864.53 2957.41 114.71 o 10 5 0 4667.95 4694.20 143.67 o 12 5 0 8964.86 8457.02 189.40 o 14 5 0 1820.05 1806.92 86.72 o 0 6 0 32302.10 32962.12 398.59 o 2 6 0 2822.08 2526.11 103.33 o 4 6 0 191.95 173.24 14.90 o 6 6 0 841.73 818.95 34.36 o 8 6 0 20.88 40.19 11.18 o 10 6 0 962.91 1011.74 39.42 o 12 6 0 6404.99 6370.43 150.28 o 14 6 0 58.15 53.09 16.87 o 2 7 0 2128.30 2107.78 88.48 o 4 7 0 3677.09 3581.13 114.63 o 6 7 0 348.13 338.35 19.86 o 8 7 0 919.56 843.74 33.20 o 10 7 0 908.00 900.40 37.28 o 12 7 0 10.90 15.73 14.31 o 0 8 0 228.68 233.13 17.28 o 2 8 0 35.01 56.59 13.55 o 4 8 0 3017.71 3033.24 97.16 o 6 8 0 132.13 113.25 16.50 o 8 8 0 6801.86 6771.91 140.60 o 2 9 0 398.88 381.29 21.85 o 4 9 0 3436.91 3321.85 94.43 o 1 0 1 16.90 19.33 2.09 o 2 0 1 13516.81 15168.99 341.77 o 3 0 1 95.70 114.64 5.95 o 4 0 1 7864.90 8150.62 93.33 o 5 0 1 15897.41 15851.38 197.03 o 6 0 1 11070.31 11530.44 253.31 o 7 0 1 1876.13 1486.56 43.47 o 8 0 1 225.75 243.12 16.78 o 9 0 1 22.12 35.77 7.77 o 10 0 1 1766.88 1780.46 57.55 o 11 0 1 3862.83 3601.92 98.13 o 12 0 1 136.16 121.49 30.93 o 13 0 1 13903.36 13435.62 190.00 o 14 0 1 2714.63 2811.07 93.61 o 15 0 1 13.40 8.08 10.22 o 16 0 1 737.88 807.84 40.87 o 17 0 1 618.09 625.20 20.84 o 18 0 1 794.77 837.42 24.21 o 0 1 1 1461.59 1494.67 92.08 o 1 1 1 16218.51 17012.59 476.60 o 2 1 1 179.01 160.79 5.07 o 3 1 1 1896.09 1926.16 46.16 o 4 1 1 9554.34 9320.82 245.03 o 5 1 1 3544.78 3351.22 46.79 o 6 1 1 836.13 849.76 20.70 o 7 1 1 9.13 11.06 4.46 o 8 1 1 4807.37 4914.76 72.10 o 9 1 1 6912.64 6738.51 155.20 o 10 1 1 229.42 234.51 8.63 o 11 1 1 1337.72 1282.32 25.58 o 12 1 1 680.41 667.12 17.60 o 13 1 1 841.13 853.80 18.48 o 14 1 1 178.92 189.83 9.22 o 15 1 1 216.94 225.75 11.97 o 16 1 1 95.29 89.92 9.26 o 17 1 1 2640.10 2690.50 76.79 o 18 1 1 279.20 276.25 21.80 o 1 2 1 20560.56 22697.78 334.16 o 2 2 1 6053.50 6272.92 83.87 o 3 2 1 6847.11 6902.02 83.58 o 4 2 1 775.55 739.09 20.38 o 5 2 1 8522.38 8305.33 130.04 o 6 2 1 1244.57 1179.78 30.20 o 7 2 1 6358.16 6323.29 112.12 o 8 2 1 828.99 787.92 47.56 o 9 2 1 28.34 43.33 11.38 o 10 2 1 6719.05 6350.02 132.38 o 11 2 1 254.87 247.04 15.29 o 12 2 1 859.31 858.51 25.69 o 13 2 1 1148.35 1246.60 37.07 o 14 2 1 43.93 45.62 10.82 o 15 2 1 1898.88 1839.05 64.43 o 16 2 1 86.42 99.81 18.11 o 17 2 1 1463.56 1417.60 37.75 o 0 3 1 6633.79 6243.45 88.25 o 1 3 1 295.51 414.52 13.07 o 2 3 1 2742.83 3090.56 59.01 o 3 3 1 5619.15 5466.65 83.57 o 4 3 1 3999.21 4454.75 143.93 o 5 3 1 1328.97 1455.25 55.36 o 6 3 1 3200.63 3331.90 77.54 o 7 3 1 2990.33 2858.79 77.75 o 8 3 1 496.30 516.36 17.00 o 9 3 1 14133.59 13096.13 191.40 o 10 3 1 1392.73 1366.21 39.98 o 11 3 1 1475.81 1351.74 37.51 o 12 3 1 1975.10 1851.14 118.37 o 13 3 1 319.58 321.31 15.45 o 14 3 1 1353.88 1319.44 35.61 o 15 3 1 847.43 805.85 24.17 o 16 3 1 14.60 13.83 10.05 o 17 3 1 444.47 433.40 23.90 o 1 4 1 1533.23 1564.15 34.76 o 2 4 1 32.61 38.13 5.52 o 3 4 1 2438.86 2453.18 61.94 o 4 4 1 1955.46 1979.33 100.25 o 5 4 1 9087.54 8660.66 129.66 o 6 4 1 350.39 350.22 12.11 o 7 4 1 1180.03 1063.82 30.24 o 8 4 1 352.30 364.36 13.67 o 9 4 1 61.83 73.99 12.94 o 10 4 1 286.95 309.88 25.60 o 11 4 1 111.29 134.46 15.56 o 12 4 1 205.21 190.03 17.80 o 13 4 1 5012.36 5055.05 105.21 o 14 4 1 604.32 575.75 19.78 o 15 4 1 247.39 254.34 24.16 o 16 4 1 119.98 111.00 12.77 o 0 5 1 134.21 127.00 13.33 o 1 5 1 15704.35 15901.38 204.17 o 2 5 1 49.96 59.13 7.07 o 3 5 1 163.88 155.13 8.99 o 4 5 1 3158.85 3142.94 81.87 o 5 5 1 1550.31 1539.32 39.76 o 6 5 1 4.63 8.67 8.62 o 7 5 1 204.91 189.78 11.04 o 8 5 1 3946.49 3827.43 90.53 o 9 5 1 1866.82 1812.00 51.74 o 10 5 1 1288.61 1363.23 65.86 o 11 5 1 595.05 592.06 18.39 o 12 5 1 82.61 89.48 11.62 o 13 5 1 1670.80 1581.21 64.86 o 14 5 1 895.90 908.75 25.59 o 15 5 1 17.26 27.74 10.84 o 1 6 1 1197.29 1181.17 22.77 o 2 6 1 2280.46 2087.99 65.51 o 3 6 1 189.91 178.02 10.83 o 4 6 1 1322.64 1311.27 33.85 o 5 6 1 3441.52 3278.26 80.65 o 6 6 1 1270.55 1187.00 32.09 o 7 6 1 3020.83 2908.74 76.55 o 8 6 1 137.30 160.44 11.00 o 9 6 1 91.90 97.06 10.86 o 10 6 1 84.23 96.57 10.82 o 11 6 1 1698.78 1706.49 57.33 o 12 6 1 41.39 45.05 10.65 o 13 6 1 3171.43 3263.42 74.90 o 0 7 1 1096.91 1178.50 32.41 o 1 7 1 296.84 300.14 8.96 o 2 7 1 418.28 480.81 16.45 o 3 7 1 2347.34 2389.60 65.63 o 4 7 1 777.60 739.17 20.80 o 5 7 1 458.65 470.06 15.67 o 6 7 1 809.90 815.72 23.01 o 7 7 1 734.60 729.30 45.16 o 8 7 1 350.59 332.85 14.54 o 9 7 1 3367.95 3298.86 75.02 o 10 7 1 110.69 108.05 12.29 o 11 7 1 866.73 823.41 46.18 o 1 8 1 2053.08 1957.15 41.62 o 2 8 1 1771.10 1786.93 53.50 o 3 8 1 2861.33 2836.78 82.75 o 4 8 1 142.46 158.72 11.30 o 5 8 1 2236.56 2225.58 60.00 o 6 8 1 996.79 992.71 26.51 o 7 8 1 216.42 213.19 13.22 o 8 8 1 344.67 329.32 15.31 o 0 9 1 1053.64 1017.44 26.03 o 1 9 1 745.90 696.17 14.81 o 2 9 1 130.10 143.66 11.36 o 3 9 1 173.34 189.52 12.14 o 0 0 2 1785.06 1790.13 56.17 o 1 0 2 2742.25 2917.87 123.17 o 2 0 2 2613.37 2619.10 69.18 o 3 0 2 1043.52 838.66 41.27 o 4 0 2 10079.80 10801.04 163.44 o 5 0 2 173.42 195.65 10.45 o 6 0 2 80.15 86.24 8.73 o 7 0 2 680.55 644.90 28.01 o 8 0 2 11516.53 12336.99 231.02 o 9 0 2 24464.40 24023.44 362.79 o 10 0 2 408.69 454.55 21.69 o 11 0 2 112.91 82.44 14.51 o 12 0 2 168.64 188.57 17.46 o 13 0 2 1016.73 1060.53 42.14 o 14 0 2 346.09 301.49 22.52 o 15 0 2 891.30 813.80 34.34 o 16 0 2 169.97 172.87 18.22 o 17 0 2 352.79 315.17 20.90 o 1 1 2 10648.31 11006.10 102.17 o 2 1 2 1374.41 1386.02 37.18 o 3 1 2 3651.64 3876.24 78.53 o 4 1 2 7463.37 7744.11 156.74 o 5 1 2 8832.32 9206.36 117.27 o 6 1 2 2903.63 2907.81 69.61 o 7 1 2 759.90 812.47 23.67 o 8 1 2 362.97 362.73 20.56 o 9 1 2 199.95 225.22 11.05 o 10 1 2 70.11 83.32 19.58 o 11 1 2 1283.24 1291.13 36.71 o 12 1 2 1012.04 1017.72 29.51 o 13 1 2 3291.75 3223.14 107.53 o 14 1 2 1911.88 1962.40 65.20 o 15 1 2 438.42 469.87 17.73 o 16 1 2 891.86 921.76 27.35 o 17 1 2 980.81 997.68 27.95 o 0 2 2 22.36 53.56 9.29 o 1 2 2 3674.49 3454.15 73.45 o 2 2 2 1970.27 1776.46 78.36 o 3 2 2 9165.13 8884.96 179.10 o 4 2 2 20.28 18.11 9.19 o 5 2 2 7039.91 6388.64 161.09 o 6 2 2 5790.99 5604.13 157.44 o 7 2 2 116.80 142.06 13.29 o 8 2 2 1212.70 1182.88 46.47 o 9 2 2 403.45 386.70 20.93 o 10 2 2 878.15 881.95 38.99 o 11 2 2 5.64 -7.11 14.12 o 12 2 2 1354.56 1537.28 56.45 o 13 2 2 2673.95 2694.98 114.46 o 14 2 2 132.27 136.69 16.13 o 15 2 2 21.06 25.12 13.74 o 16 2 2 784.46 811.33 33.34 o 17 2 2 3567.36 3696.03 111.78 o 1 3 2 55.37 49.83 10.38 o 2 3 2 5564.71 6086.65 133.99 o 3 3 2 2956.85 3239.31 96.08 o 4 3 2 3090.62 3163.32 101.67 o 5 3 2 12235.96 11947.77 227.89 o 6 3 2 3510.77 3593.88 128.51 o 7 3 2 8905.25 8492.33 215.38 o 8 3 2 3767.33 3616.86 141.44 o 9 3 2 1900.34 1752.41 63.85 o 10 3 2 1.56 7.01 13.65 o 11 3 2 3446.22 3218.07 130.92 o 12 3 2 798.68 825.42 37.96 o 13 3 2 3115.08 3272.67 121.33 o 14 3 2 838.39 889.80 37.85 o 15 3 2 179.80 196.12 20.68 o 16 3 2 80.38 64.19 17.35 o 0 4 2 1913.25 1829.68 79.55 o 1 4 2 867.55 870.35 31.21 o 2 4 2 694.46 665.35 24.74 o 3 4 2 1862.79 1851.31 82.91 o 4 4 2 632.71 618.61 23.00 o 5 4 2 932.08 982.46 36.27 o 6 4 2 507.74 531.77 22.38 o 7 4 2 102.22 113.83 13.85 o 8 4 2 3985.45 3929.38 143.42 o 9 4 2 4879.14 4702.63 156.76 o 10 4 2 556.89 595.68 27.04 o 11 4 2 6.02 8.24 14.50 o 12 4 2 39.88 37.35 14.60 o 13 4 2 174.02 206.94 19.64 o 14 4 2 92.86 96.82 17.45 o 15 4 2 47.02 47.40 16.30 o 1 5 2 7440.21 7630.16 127.75 o 2 5 2 253.06 234.56 15.11 o 3 5 2 6714.88 6838.06 168.11 o 4 5 2 4419.79 4435.09 135.28 o 5 5 2 2298.68 2418.14 100.44 o 6 5 2 945.89 1013.75 38.70 o 7 5 2 231.28 224.28 16.43 o 8 5 2 3.55 -10.33 12.51 o 9 5 2 885.99 893.07 35.12 o 10 5 2 30.56 40.38 13.46 o 11 5 2 3582.12 3683.63 125.15 o 12 5 2 760.85 802.33 34.39 o 13 5 2 2089.06 2040.59 89.87 o 14 5 2 1531.83 1451.13 51.98 o 0 6 2 103.21 100.45 14.42 o 1 6 2 173.76 173.63 10.84 o 2 6 2 1556.72 1610.81 55.89 o 3 6 2 2244.53 2239.24 93.96 o 4 6 2 1704.40 1685.07 58.25 o 5 6 2 85.42 77.19 12.99 o 6 6 2 687.28 656.43 25.82 o 7 6 2 493.37 479.26 22.17 o 8 6 2 2077.91 2044.48 92.20 o 9 6 2 6037.44 6096.20 154.95 o 10 6 2 382.01 425.04 23.95 o 11 6 2 143.02 151.01 18.50 o 12 6 2 59.72 64.37 17.16 o 13 6 2 180.48 188.99 22.30 o 1 7 2 335.43 343.93 13.80 o 2 7 2 1714.84 1725.39 80.55 o 3 7 2 67.69 85.62 13.27 o 4 7 2 881.90 846.80 34.44 o 5 7 2 3189.38 3260.48 104.64 o 6 7 2 1160.15 1171.77 43.00 o 7 7 2 2451.03 2302.45 88.89 o 8 7 2 1014.84 975.22 37.22 o 9 7 2 274.35 260.90 20.22 o 10 7 2 41.57 65.60 15.17 o 11 7 2 486.31 516.47 26.24 o 0 8 2 705.32 749.76 30.95 o 1 8 2 2832.43 2887.33 68.21 o 2 8 2 188.85 186.74 16.70 o 3 8 2 480.76 498.88 24.06 o 4 8 2 55.72 38.58 14.88 o 5 8 2 1974.23 2182.69 79.70 o 6 8 2 642.83 677.42 27.31 o 7 8 2 2.39 -12.13 13.65 o 1 0 3 1376.99 1587.89 45.71 o 2 0 3 1605.47 1394.47 61.49 o 3 0 3 5455.54 5352.45 125.32 o 4 0 3 25043.37 26818.35 309.15 o 5 0 3 634.78 667.59 29.32 o 6 0 3 1243.04 1356.63 49.61 o 7 0 3 3543.15 3644.25 122.52 o 8 0 3 1984.51 2010.73 99.88 o 9 0 3 252.54 258.87 17.38 o 10 0 3 197.78 303.89 18.51 o 11 0 3 193.39 187.66 17.75 o 12 0 3 22.64 -11.56 14.50 o 13 0 3 1.83 15.45 11.66 o 14 0 3 1830.26 1715.19 60.21 o 15 0 3 4287.53 4351.47 124.79 o 16 0 3 1585.54 1616.65 76.81 o 0 1 3 13484.95 13423.99 141.74 o 1 1 3 467.12 441.02 9.37 o 2 1 3 30.58 23.04 8.20 o 3 1 3 3095.20 3195.33 96.13 o 4 1 3 338.80 386.37 11.81 o 5 1 3 3536.59 3601.55 78.66 o 6 1 3 824.38 865.72 23.97 o 7 1 3 5219.12 5489.24 107.91 o 8 1 3 4670.30 5002.58 213.12 o 9 1 3 974.42 1012.26 29.71 o 10 1 3 3085.52 3100.55 85.49 o 11 1 3 306.74 320.07 14.23 o 12 1 3 1752.65 1783.94 92.83 o 13 1 3 2.15 23.37 19.05 o 14 1 3 1177.31 1167.89 31.79 o 15 1 3 7.99 6.52 15.78 o 16 1 3 136.52 155.41 39.17 o 1 2 3 195.74 183.69 9.36 o 2 2 3 547.77 555.65 25.39 o 3 2 3 151.20 176.41 10.82 o 4 2 3 3719.33 3698.23 110.71 o 5 2 3 25.00 0.76 9.67 o 6 2 3 2361.46 2474.12 105.34 o 7 2 3 2936.99 3070.06 126.39 o 8 2 3 3656.83 3791.92 136.83 o 9 2 3 11.10 23.31 13.93 o 10 2 3 5186.27 4902.41 159.52 o 11 2 3 3632.26 3684.00 134.75 o 12 2 3 2177.78 2107.89 69.58 o 13 2 3 91.31 88.57 16.60 o 14 2 3 1576.59 1682.64 82.51 o 15 2 3 65.67 57.64 17.54 o 16 2 3 1379.13 1419.01 47.91 o 0 3 3 28279.33 25294.13 385.73 o 1 3 3 6470.88 5783.35 121.85 o 2 3 3 3061.06 2855.58 121.02 o 3 3 3 141.66 118.93 14.33 o 4 3 3 11.75 91.74 12.13 o 5 3 3 1541.29 1528.17 59.99 o 6 3 3 914.50 945.61 37.01 o 7 3 3 676.34 653.53 28.42 o 8 3 3 27.02 48.53 14.50 o 9 3 3 1722.17 1731.06 65.11 o 10 3 3 842.66 822.18 36.07 o 11 3 3 1771.88 1796.98 67.16 o 12 3 3 4780.62 4917.16 151.32 o 13 3 3 2034.43 2061.65 98.27 o 14 3 3 276.19 303.07 23.64 o 15 3 3 24.40 -11.66 16.11 o 1 4 3 939.89 984.39 29.49 o 2 4 3 242.13 218.21 16.24 o 3 4 3 977.77 1003.59 41.34 o 4 4 3 9075.94 9134.02 199.79 o 5 4 3 509.40 540.67 22.76 o 6 4 3 1131.16 1144.01 45.96 o 7 4 3 9.07 13.08 14.22 o 8 4 3 1273.50 1393.62 55.94 o 9 4 3 6.61 26.82 12.60 o 10 4 3 378.00 361.64 24.14 o 11 4 3 455.62 457.09 25.48 o 12 4 3 633.22 724.54 33.03 o 13 4 3 107.34 89.24 18.02 o 14 4 3 1568.97 1525.83 54.87 o 0 5 3 2612.31 2585.13 111.56 o 1 5 3 86.27 87.72 9.97 o 2 5 3 76.38 78.52 14.70 o 3 5 3 3031.90 3064.88 109.07 o 4 5 3 517.85 571.54 24.94 o 5 5 3 5505.43 5621.01 151.26 o 6 5 3 291.75 270.73 19.57 o 7 5 3 4165.37 4153.30 137.35 o 8 5 3 5987.25 6176.66 165.99 o 9 5 3 3005.82 2963.22 116.66 o 10 5 3 2664.28 2727.67 105.29 o 11 5 3 3.70 -16.87 16.87 o 12 5 3 299.03 318.87 23.17 o 13 5 3 373.93 373.72 24.98 o 1 6 3 39.77 36.40 8.62 o 2 6 3 1409.40 1563.05 54.25 o 3 6 3 1812.22 1955.86 85.65 o 4 6 3 4995.99 5404.50 141.64 o 5 6 3 7.61 29.19 10.99 o 6 6 3 842.23 870.33 35.57 o 7 6 3 238.30 232.68 19.75 o 8 6 3 1218.07 1126.96 43.97 o 9 6 3 45.39 67.49 15.36 o 10 6 3 117.21 128.70 17.83 o 11 6 3 1.03 12.13 14.31 o 12 6 3 7.93 0.57 17.25 o 0 7 3 5749.32 5645.04 140.45 o 1 7 3 1108.03 1112.97 41.56 o 2 7 3 821.12 894.79 34.22 o 3 7 3 41.05 35.45 13.27 o 4 7 3 16.15 31.66 12.98 o 5 7 3 157.14 139.74 16.98 o 6 7 3 694.87 781.49 32.38 o 7 7 3 494.41 489.49 23.87 o 8 7 3 159.41 164.12 18.88 o 9 7 3 185.89 203.99 18.50 o 1 8 3 508.55 507.08 17.71 o 2 8 3 16.22 27.77 12.13 o 3 8 3 23.57 36.11 11.94 o 4 8 3 1279.04 1314.16 42.62 o 5 8 3 266.83 254.60 20.03 o 0 0 4 6463.80 6141.33 150.29 o 1 0 4 6585.00 6430.48 109.12 o 2 0 4 75.76 95.89 10.24 o 3 0 4 25.33 30.81 9.19 o 4 0 4 148.74 124.34 11.86 o 5 0 4 578.29 607.06 25.83 o 6 0 4 1291.67 1444.43 52.78 o 7 0 4 2301.77 2217.56 96.90 o 8 0 4 1854.92 1947.88 90.17 o 9 0 4 5926.45 5887.73 155.00 o 10 0 4 2799.18 2883.77 107.78 o 11 0 4 866.96 888.91 38.26 o 12 0 4 2561.75 2395.80 99.95 o 13 0 4 871.74 964.54 37.09 o 14 0 4 136.30 183.54 16.98 o 15 0 4 17.15 13.08 14.31 o 1 1 4 281.46 272.18 10.48 o 2 1 4 827.18 881.81 25.83 o 3 1 4 1866.01 1833.58 59.06 o 4 1 4 138.60 148.07 8.82 o 5 1 4 5639.91 5444.96 109.34 o 6 1 4 607.04 618.83 19.76 o 7 1 4 2244.00 2346.20 71.03 o 8 1 4 1607.27 1558.78 41.28 o 9 1 4 2.29 -8.70 8.70 o 10 1 4 1080.56 1078.24 29.69 o 11 1 4 1139.55 1170.06 31.64 o 12 1 4 24.63 45.06 9.28 o 13 1 4 1935.48 1962.63 61.23 o 14 1 4 19.87 24.35 9.67 o 15 1 4 452.13 420.30 17.43 o 0 2 4 141.68 152.52 14.33 o 1 2 4 9962.14 10052.33 151.67 o 2 2 4 1943.63 2015.00 89.34 o 3 2 4 3701.60 3667.38 122.41 o 4 2 4 4633.84 4639.73 137.43 o 5 2 4 77.79 80.42 11.48 o 6 2 4 132.47 151.05 14.52 o 7 2 4 82.35 94.74 12.42 o 8 2 4 2430.07 2685.92 109.60 o 9 2 4 3228.73 3575.77 127.71 o 10 2 4 0.13 4.45 12.98 o 11 2 4 5652.64 5639.64 155.05 o 12 2 4 79.90 69.50 14.51 o 13 2 4 20.27 26.35 12.98 o 14 2 4 969.89 946.58 39.30 o 15 2 4 867.87 862.26 34.50 o 1 3 4 4156.46 4091.91 109.92 o 2 3 4 1469.21 1494.60 57.00 o 3 3 4 4121.21 3928.03 129.36 o 4 3 4 1371.39 1511.44 53.65 o 5 3 4 118.09 129.59 13.38 o 6 3 4 5804.70 6070.33 162.10 o 7 3 4 52.26 75.94 15.17 o 8 3 4 37.63 28.06 13.56 o 9 3 4 8.06 9.76 13.55 o 10 3 4 454.95 449.31 24.91 o 11 3 4 907.59 936.20 38.25 o 12 3 4 1197.42 1197.80 47.11 o 13 3 4 3532.39 3403.95 117.78 o 14 3 4 323.28 352.13 22.70 o 0 4 4 225.63 194.09 20.80 o 1 4 4 6321.07 5714.85 128.95 o 2 4 4 447.18 476.57 25.88 o 3 4 4 323.69 327.59 22.71 o 4 4 4 492.83 462.52 26.93 o 5 4 4 2.88 -3.03 13.55 o 6 4 4 168.62 168.63 18.69 o 7 4 4 482.51 434.84 25.69 o 8 4 4 6.15 26.25 14.03 o 9 4 4 4441.16 4518.14 147.79 o 10 4 4 308.04 274.10 23.46 o 11 4 4 1496.97 1595.00 55.83 o 12 4 4 343.57 342.52 24.98 o 13 4 4 156.81 143.34 20.30 o 1 5 4 74.57 70.26 15.22 o 2 5 4 1838.29 2000.57 99.45 o 3 5 4 597.92 702.16 29.90 o 4 5 4 24.77 43.70 12.99 o 5 5 4 6333.39 5941.41 149.50 o 6 5 4 58.10 74.80 13.84 o 7 5 4 2146.20 2026.85 97.33 o 8 5 4 1991.76 1980.67 93.82 o 9 5 4 0.09 -0.95 14.69 o 10 5 4 1979.90 1832.84 88.07 o 11 5 4 659.35 627.05 32.74 o 12 5 4 386.41 385.80 26.03 o 0 6 4 2254.33 2447.83 102.53 o 1 6 4 2799.01 2767.74 121.94 o 2 6 4 170.30 187.87 17.74 o 3 6 4 347.62 371.10 21.57 o 4 6 4 26.11 17.91 13.46 o 5 6 4 650.22 626.37 25.80 o 6 6 4 153.32 190.59 16.41 o 7 6 4 756.03 738.75 31.82 o 8 6 4 193.88 185.13 18.60 o 9 6 4 1375.58 1389.57 51.64 o 10 6 4 885.94 1015.51 38.70 o 1 7 4 1201.46 1179.19 31.01 o 2 7 4 81.29 120.23 16.12 o 3 7 4 1234.19 1286.73 45.58 o 4 7 4 358.28 330.39 21.56 o 5 7 4 296.12 335.47 20.22 o 6 7 4 1368.11 1371.52 64.06 o 7 7 4 431.93 418.23 24.04 o 1 0 5 30.79 27.57 8.21 o 2 0 5 302.75 328.43 17.11 o 3 0 5 1404.66 1323.29 51.73 o 4 0 5 3351.09 3216.38 112.69 o 5 0 5 1685.81 1744.82 82.02 o 6 0 5 13333.03 13309.54 236.11 o 7 0 5 440.35 442.82 21.21 o 8 0 5 1400.05 1588.97 75.88 o 9 0 5 1409.97 1381.32 50.29 o 10 0 5 49.93 57.16 14.41 o 11 0 5 359.70 345.07 20.14 o 12 0 5 4081.93 4288.28 121.95 o 13 0 5 711.53 713.15 29.80 o 14 0 5 91.75 70.07 17.07 o 0 1 5 2199.05 2191.71 92.91 o 1 1 5 283.52 268.68 8.45 o 2 1 5 2543.42 2545.94 71.16 o 3 1 5 2839.04 2738.37 75.46 o 4 1 5 350.22 361.75 32.56 o 5 1 5 256.89 268.47 16.24 o 6 1 5 969.85 1026.77 28.64 o 7 1 5 25.38 31.75 8.04 o 8 1 5 1450.92 1397.39 99.82 o 9 1 5 956.19 901.75 25.58 o 10 1 5 1394.91 1413.64 34.66 o 11 1 5 68.97 83.76 10.22 o 12 1 5 189.58 190.61 12.75 o 13 1 5 512.62 456.25 17.53 o 1 2 5 1858.86 1765.84 51.33 o 2 2 5 11813.76 11375.23 221.24 o 3 2 5 214.03 212.10 16.33 o 4 2 5 796.01 783.31 33.11 o 5 2 5 242.33 234.26 16.33 o 6 2 5 313.94 345.83 18.81 o 7 2 5 48.07 60.48 12.13 o 8 2 5 7.12 2.84 11.37 o 9 2 5 30.28 35.26 12.32 o 10 2 5 146.16 133.95 15.65 o 11 2 5 428.77 397.30 24.33 o 12 2 5 538.41 525.86 26.44 o 13 2 5 1066.55 1141.66 41.32 o 0 3 5 39.61 41.62 14.03 o 1 3 5 1.71 -3.05 9.75 o 2 3 5 3606.64 3743.00 127.36 o 3 3 5 877.95 893.83 35.89 o 4 3 5 2475.72 2413.38 99.18 o 5 3 5 185.75 186.68 15.47 o 6 3 5 9.41 -8.25 12.51 o 7 3 5 10.20 15.45 10.90 o 8 3 5 3473.59 3522.33 113.89 o 9 3 5 2214.37 2311.91 92.90 o 10 3 5 4679.09 4821.53 131.76 o 11 3 5 26.71 23.51 16.11 o 12 3 5 39.99 42.94 14.12 o 1 4 5 498.36 511.18 34.16 o 2 4 5 1228.69 1265.75 51.28 o 3 4 5 66.09 118.42 16.40 o 4 4 5 2209.02 2292.41 96.65 o 5 4 5 556.94 540.15 24.36 o 6 4 5 2423.81 2392.46 91.92 o 7 4 5 80.67 106.29 13.84 o 8 4 5 74.69 108.75 16.69 o 9 4 5 149.75 156.14 18.78 o 10 4 5 131.96 178.41 17.74 o 11 4 5 2.31 19.05 15.07 o 0 5 5 3781.39 3405.05 130.21 o 1 5 5 400.55 420.14 18.99 o 2 5 5 1006.96 1084.02 46.01 o 3 5 5 1937.67 1809.91 65.44 o 4 5 5 1632.12 1553.19 59.44 o 5 5 5 204.52 224.73 21.26 o 6 5 5 976.12 1035.49 39.69 o 7 5 5 26.74 46.63 13.55 o 8 5 5 518.37 514.94 28.53 o 9 5 5 207.48 207.25 21.45 o 1 6 5 41.69 56.87 16.40 o 2 6 5 214.01 221.98 22.21 o 3 6 5 211.32 223.59 20.97 o 4 6 5 496.08 512.78 25.77 o 5 6 5 549.91 525.69 25.78 o 6 6 5 4722.77 4445.92 115.06 o 7 6 5 59.47 60.58 15.45 o 0 7 5 39.10 66.83 18.01 o 1 7 5 24.51 23.65 11.83 o 0 0 6 182.74 169.31 16.23 o 1 0 6 4701.99 4475.86 105.08 o 2 0 6 668.09 683.52 29.44 o 3 0 6 1510.36 1480.94 72.68 o 4 0 6 2571.06 2578.11 92.47 o 5 0 6 232.47 233.72 17.85 o 6 0 6 6.81 -12.23 12.23 o 7 0 6 1495.69 1584.84 72.80 o 8 0 6 2358.65 2175.88 84.49 o 9 0 6 170.94 205.03 17.27 o 10 0 6 696.11 664.08 27.71 o 11 0 6 517.80 511.94 23.68 o 1 1 6 382.40 360.81 9.84 o 2 1 6 240.31 255.74 18.18 o 3 1 6 1989.27 1736.86 57.64 o 4 1 6 2214.30 2126.08 62.00 o 5 1 6 1190.18 1175.75 74.53 o 6 1 6 754.20 707.79 35.88 o 7 1 6 1352.58 1341.59 33.26 o 8 1 6 57.29 87.39 9.48 o 9 1 6 278.17 292.21 13.90 o 10 1 6 102.56 100.53 10.86 o 11 1 6 1412.83 1460.60 96.45 o 0 2 6 2386.75 2378.81 96.21 o 1 2 6 9.77 5.02 12.37 o 2 2 6 101.00 93.13 13.94 o 3 2 6 2556.78 2439.95 92.34 o 4 2 6 522.04 481.00 22.74 o 5 2 6 1487.65 1366.28 47.90 o 6 2 6 851.05 870.70 36.14 o 7 2 6 4542.89 4469.86 119.67 o 8 2 6 81.80 85.34 15.17 o 9 2 6 598.74 623.89 26.17 o 10 2 6 238.82 233.20 19.74 o 1 3 6 217.57 195.47 13.01 o 2 3 6 6.84 20.94 12.60 o 3 3 6 4900.56 4968.83 128.13 o 4 3 6 1402.80 1322.21 47.86 o 5 3 6 110.26 154.68 15.55 o 6 3 6 2531.65 2629.43 89.78 o 7 3 6 3.81 1.14 13.36 o 8 3 6 1469.95 1351.56 66.99 o 9 3 6 19.34 53.45 13.65 o 0 4 6 818.60 917.97 37.74 o 1 4 6 906.76 856.95 25.73 o 2 4 6 202.58 227.57 19.83 o 3 4 6 1.87 16.77 12.79 o 4 4 6 43.13 33.27 14.60 o 5 4 6 300.34 359.90 20.51 o 6 4 6 267.10 258.51 19.94 o 7 4 6 2150.39 2232.46 80.92 o 8 4 6 582.69 612.88 26.73 o 1 5 6 932.87 943.08 26.60 o 2 5 6 232.81 245.44 23.54 o 3 5 6 476.85 476.75 28.80 o 4 5 6 1593.87 1615.34 76.22 o 5 5 6 1578.09 1523.37 72.47 o 1 0 7 556.91 555.15 17.52 o 2 0 7 19.02 24.83 14.12 o 3 0 7 4926.65 4883.06 120.46 o 4 0 7 96.21 100.61 15.27 o 5 0 7 209.18 225.86 18.41 o 6 0 7 683.71 646.37 26.65 o 7 0 7 542.04 577.07 24.82 o 0 1 7 114.28 104.42 11.24 o 1 1 7 1340.89 1312.63 26.37 o 2 1 7 1234.88 1137.99 68.91 o 3 1 7 249.78 272.41 12.95 o 4 1 7 73.98 90.36 19.20 o 5 1 7 307.08 304.48 14.50 o 6 1 7 5.47 5.76 20.56 o 7 1 7 699.01 712.97 20.30 o 1 2 7 186.81 180.41 12.69 o 2 2 7 173.83 146.68 17.55 o 3 2 7 253.21 248.71 19.55 o 4 2 7 21.25 23.41 14.03 o 5 2 7 2250.94 2311.13 80.20 o 6 2 7 1362.13 1365.79 64.44 o 0 3 7 290.50 282.47 21.84 o 1 3 7 2869.59 2909.35 117.75 o 2 3 7 1403.36 1385.85 46.67 o 3 3 7 257.66 259.24 19.46 o 4 3 7 146.25 148.35 16.98 o 5 3 7 1332.65 1366.17 63.46 o