#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/27/2012744.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012744_Fobs loop_ _publ_author_name 'Vojnovi\'c, Marija' 'Peri\'c, Berislav' 'Planini\'c, Pavica' 'Giester, Gerald' 'Brni\octahedro-hexatantalum bromide chloride octahydrate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i71 _journal_page_last i73 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.920 _cell_angle_beta 80.280 _cell_angle_gamma 80.340 _cell_length_a 9.7290 _cell_length_b 9.8230 _cell_length_c 19.3920 _exptl_crystal_F_000 2078.40 _reflns_d_resolution_high 0.7013 _[local]_cod_data_source_file br1370Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BERO6 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 831.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 543647.63 531459.88 9470.42 o 2 0 0 1852.19 1276.83 49.67 o 3 0 0 6224.85 7353.91 159.31 o 4 0 0 177347.05 174174.55 2490.79 o 5 0 0 234522.22 233157.63 6103.99 o 6 0 0 28126.59 27752.21 456.12 o 7 0 0 166321.39 176246.53 3028.45 o 8 0 0 72639.52 75404.16 1542.28 o 9 0 0 100383.89 107349.63 2777.74 o 10 0 0 13139.27 13572.35 752.80 o 11 0 0 20033.43 21699.85 1625.98 o 12 0 0 14552.54 15458.08 1193.11 o 13 0 0 3093.81 3610.06 880.36 o -13 1 0 3880.98 2943.77 1323.04 o -12 1 0 30121.21 33015.81 4702.54 o -11 1 0 53147.02 59521.59 2525.39 o -10 1 0 269.45 709.99 268.04 o -9 1 0 62115.50 63655.57 1962.16 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