#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:40:12 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180797 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/28/2012888.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012888_Fobs loop_ _publ_author_name 'Sethu Sankar, K.' 'Kannadasan, S.' 'Velmurugan, D.' 'Srinivasan, P. C.' 'Moon, Jib-Kim' _publ_section_title ; Diethyl {3-[\b-(2,4-dichlorophenyl)vinyl]-N-(phenylsulfonyl)indol-2-ylmethyl}phosphonate and diethyl {3-[\b-(4-bromophenyl)vinyl]-N-(phenylsulfonyl)indol-2-ylmethyl}phosphonate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o450 _journal_page_last o454 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.296 _cell_angle_gamma 90.000 _cell_length_a 16.6080 _cell_length_b 8.3571 _cell_length_c 19.6470 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.8415 _cod_data_source_file na1565Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' vel1 in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 260.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 379.77 325.36 7.01 o 4 0 0 5941.72 5571.99 45.87 o 6 0 0 6357.70 6744.28 58.81 o 8 0 0 150.65 120.24 9.91 o 10 0 0 2530.45 2689.74 39.45 o 12 0 0 2.71 -6.46 17.70 o 14 0 0 20.08 14.43 12.34 o 16 0 0 780.76 769.35 35.57 o 18 0 0 79.32 102.86 19.30 o 1 1 0 31583.74 38421.80 1563.39 o 2 1 0 1426.47 1324.47 21.92 o 3 1 0 2006.15 2117.30 21.59 o 4 1 0 10.47 14.59 7.47 o 5 1 0 148.89 154.13 9.84 o 6 1 0 179.54 171.97 10.54 o 7 1 0 316.91 289.06 21.37 o 8 1 0 1864.33 2072.83 33.27 o 9 1 0 82.15 79.44 9.88 o 10 1 0 61.00 62.23 9.98 o 11 1 0 653.46 651.03 22.13 o 12 1 0 161.50 193.71 14.14 o 13 1 0 138.95 130.88 15.08 o 14 1 0 199.12 159.52 16.81 o 15 1 0 554.00 583.98 30.75 o 16 1 0 4.65 4.76 15.72 o 17 1 0 200.25 201.25 21.86 o 18 1 0 2.14 -9.03 15.49 o 19 1 0 76.00 46.79 23.65 o 0 2 0 35954.39 42755.66 456.20 o 1 2 0 3953.50 4195.66 51.13 o 2 2 0 13598.28 13618.15 243.83 o 3 2 0 19869.09 20623.66 208.76 o 4 2 0 29.90 35.61 8.16 o 5 2 0 13.10 20.06 8.14 o 6 2 0 428.63 407.56 14.31 o 7 2 0 0.26 8.43 7.70 o 8 2 0 392.55 378.72 15.73 o 9 2 0 1688.36 1543.19 29.84 o 10 2 0 16.06 27.11 8.71 o 11 2 0 19.33 10.86 9.63 o 12 2 0 626.55 569.26 23.27 o 13 2 0 273.81 294.12 18.14 o 14 2 0 107.47 86.12 14.61 o 15 2 0 79.26 106.80 18.24 o 16 2 0 761.56 888.56 38.54 o 17 2 0 0.18 3.08 44.67 o 18 2 0 0.12 -21.42 25.38 o 19 2 0 12.80 5.68 29.81 o 1 3 0 691.13 756.83 16.78 o 2 3 0 673.95 803.11 17.55 o 3 3 0 49.81 45.14 7.75 o 4 3 0 45.46 76.82 13.65 o 5 3 0 1455.48 1444.00 25.31 o 6 3 0 2810.75 3166.70 38.29 o 7 3 0 83.06 54.55 8.99 o 8 3 0 36.60 34.53 20.06 o 9 3 0 23.12 -4.59 10.50 o 10 3 0 290.60 253.78 17.32 o 11 3 0 99.11 109.24 13.28 o 12 3 0 50.98 39.09 12.32 o 13 3 0 751.20 728.90 28.20 o 14 3 0 43.98 10.76 15.26 o 15 3 0 319.32 289.31 28.44 o 16 3 0 38.45 31.57 20.94 o 17 3 0 2.81 7.87 17.51 o 18 3 0 3.18 2.37 21.17 o 0 4 0 1729.39 1465.51 36.61 o 1 4 0 3.14 -8.56 10.03 o 2 4 0 397.11 474.88 16.16 o 3 4 0 3056.53 3129.19 45.16 o 4 4 0 31.08 31.22 8.41 o 5 4 0 2407.79 2354.82 35.26 o 6 4 0 239.57 282.99 15.27 o 7 4 0 1209.66 1255.96 54.15 o 8 4 0 1.25 8.75 7.92 o 9 4 0 601.75 596.63 24.17 o 10 4 0 1237.52 1268.68 32.82 o 11 4 0 26.39 -7.17 16.44 o 12 4 0 36.70 3.27 17.06 o 13 4 0 4.64 22.94 14.52 o 14 4 0 176.80 130.89 21.16 o 15 4 0 132.17 134.07 21.39 o 16 4 0 2.58 -18.86 18.86 o 17 4 0 9.19 29.91 21.70 o 18 4 0 13.44 48.07 24.88 o 1 5 0 1074.44 1158.80 26.58 o 2 5 0 56.64 44.05 10.69 o 3 5 0 5164.65 4891.55 99.86 o 4 5 0 12.50 11.28 11.40 o 5 5 0 470.28 468.51 20.00 o 6 5 0 2.11 1.84 11.35 o 7 5 0 1314.66 1300.81 32.13 o 8 5 0 447.15 418.64 20.68 o 9 5 0 43.19 28.52 14.57 o 10 5 0 6.99 13.60 14.21 o 11 5 0 120.00 137.89 17.28 o 12 5 0 95.58 90.50 18.18 o 13 5 0 152.06 170.68 19.20 o 14 5 0 5.57 -2.76 17.54 o 15 5 0 9.36 -5.37 19.66 o 16 5 0 14.54 7.02 19.80 o 17 5 0 35.59 40.78 20.79 o 0 6 0 189.26 167.82 20.39 o 1 6 0 97.24 95.13 11.32 o 2 6 0 365.00 371.59 18.39 o 3 6 0 1.00 -2.00 11.08 o 4 6 0 128.09 140.78 14.22 o 5 6 0 8.78 12.58 9.81 o 6 6 0 1130.46 1107.07 31.89 o 7 6 0 268.75 272.65 26.42 o 8 6 0 57.25 82.76 33.05 o 9 6 0 30.27 27.44 15.73 o 10 6 0 5.41 -8.35 17.46 o 11 6 0 45.98 47.27 33.16 o 12 6 0 235.34 215.17 24.18 o 13 6 0 0.49 -20.58 20.58 o 14 6 0 59.13 65.46 34.36 o 15 6 0 3.69 48.26 30.58 o 1 7 0 164.53 170.19 17.81 o 2 7 0 14.93 35.31 18.96 o 3 7 0 69.17 84.10 13.52 o 4 7 0 106.74 83.50 40.50 o 5 7 0 1.21 15.20 12.08 o 6 7 0 186.12 164.43 20.09 o 7 7 0 81.60 50.77 31.95 o 8 7 0 33.13 20.07 19.91 o 9 7 0 22.39 -20.46 20.46 o 10 7 0 297.70 266.10 26.35 o 11 7 0 0.14 -0.44 20.53 o 12 7 0 57.03 65.19 18.37 o 13 7 0 199.93 199.63 40.56 o 0 8 0 11.04 -6.14 23.24 o 1 8 0 10.24 10.78 15.95 o 2 8 0 0.16 -9.30 17.65 o 3 8 0 4.96 32.60 13.37 o 4 8 0 41.50 24.92 18.83 o 5 8 0 74.96 46.33 17.75 o 6 8 0 124.57 76.38 21.01 o 7 8 0 3.70 -18.85 29.21 o 8 8 0 7.04 -9.79 30.20 o 9 8 0 128.94 166.54 22.50 o 10 8 0 23.12 6.51 21.00 o 11 8 0 10.76 -6.88 32.55 o 1 9 0 47.65 59.19 25.21 o 2 9 0 8.01 4.73 14.69 o 3 9 0 5.26 -10.39 27.40 o 4 9 0 21.32 23.45 16.58 o 5 9 0 2.76 31.13 22.80 o 6 9 0 0.35 -2.64 16.10 o 7 9 0 86.22 77.02 19.54 o 8 9 0 4.57 -18.61 26.47 o -19 0 1 4.06 25.54 21.37 o -17 0 1 256.49 281.48 39.13 o -15 0 1 680.78 637.61 39.35 o -13 0 1 136.74 108.41 21.05 o -11 0 1 62.17 40.45 16.77 o -9 0 1 322.77 378.60 21.37 o -7 0 1 5201.29 5724.92 64.67 o -5 0 1 1892.25 1713.56 30.91 o -3 0 1 8975.37 8819.38 66.97 o 3 0 1 28132.54 29596.21 123.53 o 5 0 1 28.80 35.84 11.40 o 7 0 1 1710.48 1792.48 37.38 o 9 0 1 2.16 -3.07 13.70 o 11 0 1 1447.97 1302.63 42.42 o 13 0 1 451.64 480.54 30.14 o 15 0 1 352.77 364.57 37.05 o 17 0 1 48.90 53.82 23.68 o 19 0 1 23.59 54.26 24.44 o -19 1 1 131.92 151.37 27.84 o -18 1 1 13.23 21.16 18.74 o -17 1 1 0.05 -27.29 27.29 o -16 1 1 631.18 607.47 47.57 o -15 1 1 169.49 213.96 27.51 o -14 1 1 516.66 537.76 35.40 o -13 1 1 21.29 5.59 15.46 o -12 1 1 245.75 222.73 22.03 o -11 1 1 1405.86 1488.42 44.50 o -10 1 1 4.66 19.51 12.17 o -9 1 1 3879.45 4115.49 64.89 o -8 1 1 1234.90 1244.86 34.42 o -7 1 1 1245.79 1284.21 32.88 o -6 1 1 179.87 148.74 13.15 o -5 1 1 5862.59 6265.64 65.77 o -4 1 1 7105.42 7015.82 63.57 o -3 1 1 420.61 363.69 14.25 o -2 1 1 4207.87 4628.03 41.87 o -1 1 1 255.84 219.11 10.19 o 0 1 1 494.24 467.60 11.95 o 1 1 1 1294.22 1211.65 17.10 o 2 1 1 3251.12 3169.87 31.46 o 3 1 1 5202.26 5613.34 51.74 o 4 1 1 31146.73 31103.37 153.35 o 5 1 1 446.28 467.39 19.62 o 6 1 1 33.35 32.99 11.07 o 7 1 1 881.82 860.34 26.96 o 8 1 1 852.98 1098.86 32.66 o 9 1 1 91.39 65.11 14.36 o 10 1 1 215.67 212.43 19.40 o 11 1 1 942.27 942.99 36.06 o 12 1 1 270.44 322.04 24.01 o 13 1 1 776.98 835.79 39.90 o 14 1 1 2.43 -17.98 21.59 o 15 1 1 3.94 8.33 21.05 o 16 1 1 371.60 289.16 35.84 o 17 1 1 48.57 66.64 22.25 o 18 1 1 12.26 -14.25 18.09 o 19 1 1 29.40 51.85 29.92 o -19 2 1 78.80 61.38 33.21 o -18 2 1 19.51 10.85 27.29 o -17 2 1 328.99 362.27 39.02 o -16 2 1 0.11 -15.46 25.43 o -15 2 1 22.83 42.97 20.61 o -14 2 1 0.94 13.15 21.26 o -13 2 1 598.33 616.13 36.72 o -12 2 1 146.50 214.73 21.48 o -11 2 1 617.57 665.34 32.34 o -10 2 1 79.83 81.00 16.22 o -9 2 1 417.81 433.73 23.90 o -8 2 1 1436.02 1576.88 39.57 o -7 2 1 647.65 664.03 25.76 o -6 2 1 2683.51 2589.80 45.05 o -5 2 1 857.13 777.92 25.10 o -4 2 1 278.45 250.57 16.00 o -3 2 1 11683.71 11335.30 98.43 o -2 2 1 167.17 189.74 13.37 o -1 2 1 1824.74 1834.25 26.53 o 0 2 1 2143.03 2329.47 29.38 o 1 2 1 2546.52 2681.33 35.08 o 2 2 1 51039.01 61967.78 644.63 o 3 2 1 167.32 156.75 14.80 o 4 2 1 2241.73 2462.87 38.80 o 5 2 1 1996.04 2118.47 38.80 o 6 2 1 1424.39 1519.66 35.19 o 7 2 1 2325.73 2752.03 49.33 o 8 2 1 1364.55 1383.41 38.25 o 9 2 1 334.01 358.43 22.91 o 10 2 1 463.15 462.45 26.42 o 11 2 1 186.18 191.16 18.74 o 12 2 1 22.27 33.65 14.80 o 13 2 1 0.33 -14.69 18.96 o 14 2 1 178.50 195.33 27.29 o 15 2 1 372.88 334.86 38.69 o 16 2 1 53.02 61.27 21.05 o 17 2 1 104.97 89.11 29.16 o 18 2 1 75.09 76.95 30.58 o 19 2 1 192.15 221.74 32.77 o -18 3 1 75.15 70.37 24.01 o -17 3 1 38.76 -17.43 36.50 o -16 3 1 13.73 12.93 27.07 o -15 3 1 16.24 58.53 19.40 o -14 3 1 58.47 41.65 23.02 o -13 3 1 4.02 -17.98 18.63 o -12 3 1 1301.05 1271.28 47.79 o -11 3 1 218.46 196.97 23.57 o -10 3 1 1291.06 1247.16 43.74 o -9 3 1 0.57 -5.48 18.20 o -8 3 1 268.32 247.28 21.37 o -7 3 1 75.09 75.85 12.82 o -6 3 1 2257.31 2582.57 49.43 o -5 3 1 345.09 312.94 19.29 o -4 3 1 326.81 314.59 17.76 o -3 3 1 661.88 699.43 23.24 o -2 3 1 1879.14 1869.32 35.95 o -1 3 1 1632.50 1751.49 33.87 o 0 3 1 7.10 1.97 12.61 o 1 3 1 720.35 687.60 22.58 o 2 3 1 18.49 26.31 10.52 o 3 3 1 2555.65 2442.26 42.31 o 4 3 1 2198.18 2533.46 44.61 o 5 3 1 9971.05 10916.14 105.23 o 6 3 1 99.98 133.84 14.36 o 7 3 1 49.91 27.62 11.95 o 8 3 1 69.19 51.52 13.70 o 9 3 1 2.00 9.21 16.77 o 10 3 1 14.68 10.08 16.22 o 11 3 1 715.38 709.52 34.97 o 12 3 1 133.39 120.24 23.57 o 13 3 1 10.55 0.00 21.92 o 14 3 1 30.02 40.23 20.17 o 15 3 1 2.74 -9.21 24.22 o 16 3 1 355.34 343.41 38.36 o 17 3 1 97.34 69.17 27.95 o 18 3 1 281.43 251.56 42.42 o -18 4 1 71.09 133.62 26.75 o -17 4 1 37.62 83.20 25.43 o -16 4 1 7.50 28.50 18.85 o -15 4 1 50.00 60.29 25.21 o -14 4 1 0.44 2.96 26.64 o -13 4 1 0.06 -24.88 24.88 o -12 4 1 50.71 51.19 16.77 o -11 4 1 151.44 160.03 20.17 o -10 4 1 62.46 80.24 15.35 o -9 4 1 219.87 204.86 20.94 o -8 4 1 1053.87 1077.05 39.90 o -7 4 1 1752.18 1868.99 48.23 o -6 4 1 0.03 -18.63 18.63 o -5 4 1 1247.94 1372.23 38.80 o -4 4 1 903.94 776.16 29.38 o -3 4 1 119.94 92.29 14.47 o -2 4 1 325.81 323.68 20.39 o -1 4 1 1581.34 1815.94 39.90 o 0 4 1 200.97 183.05 15.78 o 1 4 1 3165.21 3161.76 52.50 o 2 4 1 738.09 816.61 28.39 o 3 4 1 1931.11 2114.19 44.72 o 4 4 1 1932.97 1987.15 45.16 o 5 4 1 1199.94 970.83 33.87 o 6 4 1 26.93 13.48 21.48 o 7 4 1 118.12 123.20 17.76 o 8 4 1 0.05 7.78 17.54 o 9 4 1 1184.16 1153.34 42.42 o 10 4 1 1228.08 1190.60 45.82 o 11 4 1 437.54 410.83 30.36 o 12 4 1 954.33 929.29 44.83 o 13 4 1 0.09 23.57 17.21 o 14 4 1 3.97 -2.30 23.79 o 15 4 1 93.25 74.10 24.99 o 16 4 1 5.44 0.00 25.98 o 17 4 1 91.44 125.07 31.35 o -17 5 1 5.23 -16.11 30.14 o -16 5 1 8.36 7.56 31.13 o -15 5 1 8.83 7.12 29.27 o -14 5 1 0.03 22.36 19.73 o -13 5 1 17.86 32.66 22.36 o -12 5 1 11.60 -11.62 27.07 o -11 5 1 1.83 -5.48 21.81 o -10 5 1 306.43 315.13 28.50 o -9 5 1 33.58 41.87 17.65 o -8 5 1 128.85 119.59 20.94 o -7 5 1 3.97 4.27 18.41 o -6 5 1 997.32 1099.52 40.45 o -5 5 1 273.90 304.83 23.35 o -4 5 1 22.17 33.21 13.26 o -3 5 1 417.56 435.27 24.77 o -2 5 1 506.16 465.41 26.64 o -1 5 1 4.96 -18.74 18.74 o 0 5 1 124.21 116.96 16.77 o 1 5 1 17.23 23.57 12.28 o 2 5 1 584.51 471.77 27.84 o 3 5 1 266.35 273.04 22.36 o 4 5 1 745.80 708.64 32.77 o 5 5 1 120.34 112.57 17.76 o 6 5 1 848.66 837.44 35.51 o 7 5 1 117.44 139.32 19.73 o 8 5 1 886.24 906.82 39.90 o 9 5 1 70.78 97.44 18.85 o 10 5 1 1787.31 1726.61 57.33 o 11 5 1 422.36 364.90 31.02 o 12 5 1 14.49 -28.94 28.94 o 13 5 1 6.75 9.43 22.80 o 14 5 1 191.48 193.14 32.45 o 15 5 1 16.55 -3.62 30.03 o 16 5 1 11.23 15.24 24.11 o -15 6 1 13.82 -19.40 33.10 o -14 6 1 54.76 71.25 27.07 o -13 6 1 0.99 -6.91 24.88 o -12 6 1 22.58 48.78 21.05 o -11 6 1 94.85 76.07 27.40 o -10 6 1 2.38 -2.96 28.39 o -9 6 1 238.10 215.28 27.73 o -8 6 1 700.93 711.49 39.24 o -7 6 1 115.70 114.11 21.92 o -6 6 1 46.53 11.95 26.09 o -5 6 1 5.68 5.48 13.81 o -4 6 1 0.80 -11.18 21.92 o -3 6 1 353.18 334.43 25.87 o -2 6 1 661.08 702.94 34.97 o -1 6 1 425.48 470.24 28.83 o 0 6 1 23.54 8.33 20.94 o 1 6 1 51.69 18.96 17.87 o 2 6 1 205.48 216.05 21.70 o 3 6 1 358.04 407.10 27.29 o 4 6 1 70.93 53.71 16.33 o 5 6 1 57.97 41.65 17.32 o 6 6 1 236.53 259.89 25.54 o 7 6 1 5.65 0.00 16.55 o 8 6 1 103.06 95.03 21.92 o 9 6 1 82.69 59.96 21.59 o 10 6 1 393.04 397.56 36.61 o 11 6 1 24.38 30.14 22.14 o 12 6 1 7.04 63.90 21.16 o 13 6 1 1.28 -20.83 28.17 o 14 6 1 42.14 49.65 28.72 o 15 6 1 43.18 55.57 26.96 o -14 7 1 37.74 -4.17 36.06 o -13 7 1 12.73 11.73 29.49 o -12 7 1 48.34 61.27 26.09 o -11 7 1 25.76 7.12 33.87 o -10 7 1 36.00 30.36 26.31 o -9 7 1 26.27 -12.93 33.76 o -8 7 1 6.77 -9.32 27.84 o -7 7 1 177.36 231.50 29.49 o -6 7 1 23.59 -28.83 28.83 o -5 7 1 3.13 24.99 17.10 o -4 7 1 112.55 124.85 22.03 o -3 7 1 166.86 166.61 22.14 o -2 7 1 583.97 626.65 36.28 o -1 7 1 452.49 483.06 33.10 o 0 7 1 94.58 89.55 18.74 o 1 7 1 0.14 -7.78 19.51 o 2 7 1 127.12 156.53 22.91 o 3 7 1 0.97 2.63 22.69 o 4 7 1 0.01 -18.96 23.79 o 5 7 1 152.68 162.12 24.66 o 6 7 1 30.33 14.36 27.07 o 7 7 1 88.33 29.05 28.06 o 8 7 1 61.83 44.17 28.61 o 9 7 1 148.12 171.76 30.36 o 10 7 1 174.41 147.32 31.68 o 11 7 1 124.98 107.42 31.35 o 12 7 1 15.81 14.69 27.95 o 13 7 1 4.19 -31.57 31.57 o -11 8 1 1.52 -27.95 32.23 o -10 8 1 52.84 54.59 28.28 o -9 8 1 6.73 3.73 25.76 o -8 8 1 3.50 10.63 20.28 o -7 8 1 25.43 20.61 20.28 o -6 8 1 489.02 460.48 46.91 o -5 8 1 150.00 187.77 32.12 o -4 8 1 27.94 31.02 19.51 o -3 8 1 49.89 84.40 19.07 o -2 8 1 0.41 9.21 22.03 o -1 8 1 0.32 -30.14 30.14 o 0 8 1 273.46 265.81 33.32 o 1 8 1 0.05 -3.07 25.87 o 2 8 1 70.39 97.34 27.18 o 3 8 1 70.47 86.92 26.42 o 4 8 1 56.34 88.46 26.31 o 5 8 1 29.09 36.72 20.28 o 6 8 1 146.64 158.17 31.02 o 7 8 1 104.62 85.39 27.95 o 8 8 1 0.09 34.86 23.79 o 9 8 1 3.86 7.45 22.80 o 10 8 1 9.61 31.79 23.35 o 11 8 1 27.79 -16.11 33.10 o -8 9 1 27.15 24.44 27.29 o -7 9 1 196.22 195.99 34.09 o -6 9 1 14.63 11.62 25.21 o -5 9 1 86.92 87.80 24.22 o -4 9 1 40.47 47.24 24.44 o -2 9 1 19.52 10.85 30.03 o -1 9 1 18.07 37.71 17.87 o 0 9 1 4.35 0.00 19.62 o 1 9 1 15.53 7.23 25.43 o 2 9 1 39.26 0.00 28.06 o 3 9 1 0.05 7.34 24.22 o 4 9 1 70.33 11.18 28.06 o 5 9 1 133.30 88.02 27.95 o 6 9 1 2.71 0.00 25.10 o 7 9 1 6.02 20.83 24.44 o 8 9 1 0.72 12.28 21.26 o -18 0 2 20.67 21.05 33.21 o -16 0 2 305.66 300.12 41.87 o -14 0 2 535.40 521.97 32.12 o -12 0 2 25.52 26.31 13.92 o -10 0 2 493.11 404.58 25.43 o -8 0 2 1042.44 1014.68 30.91 o -6 0 2 1020.63 1094.80 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