#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:40:12 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180797 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/28/2012889.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012889_Fobs loop_ _publ_author_name 'Sethu Sankar, K.' 'Kannadasan, S.' 'Velmurugan, D.' 'Srinivasan, P. C.' 'Moon, Jib-Kim' _publ_section_title ; Diethyl {3-[\b-(2,4-dichlorophenyl)vinyl]-N-(phenylsulfonyl)indol-2-ylmethyl}phosphonate and diethyl {3-[\b-(4-bromophenyl)vinyl]-N-(phenylsulfonyl)indol-2-ylmethyl}phosphonate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o450 _journal_page_last o454 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.113 _cell_angle_gamma 90.000 _cell_length_a 16.8372 _cell_length_b 8.3234 _cell_length_c 19.6105 _exptl_crystal_F_000 1208.00 _reflns_d_resolution_high 0.8417 _cod_data_source_file na1565IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' vel40 in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 294.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9215.26 8675.46 52.46 o 4 0 0 14052.11 13874.48 111.30 o 6 0 0 87.08 49.77 7.27 o 8 0 0 1360.46 1266.34 26.36 o 10 0 0 266.99 222.96 12.21 o 12 0 0 1822.28 1825.97 38.11 o 14 0 0 3435.87 3476.94 146.07 o 16 0 0 232.54 285.32 21.44 o 18 0 0 20.30 22.11 48.29 o 1 1 0 5993.90 5064.77 568.63 o 2 1 0 60.30 83.91 4.59 o 3 1 0 17885.48 17781.77 272.28 o 4 1 0 7182.32 7010.56 72.37 o 5 1 0 4242.54 3761.38 39.60 o 6 1 0 2755.44 2722.57 44.58 o 7 1 0 6718.37 6669.09 60.62 o 8 1 0 371.66 336.08 11.02 o 9 1 0 293.39 203.67 11.27 o 10 1 0 0.96 25.81 22.97 o 11 1 0 247.46 295.30 26.77 o 12 1 0 601.75 628.38 18.12 o 13 1 0 9.25 8.09 19.78 o 14 1 0 0.57 14.43 29.12 o 15 1 0 6.08 -37.26 37.26 o 16 1 0 76.95 -1.13 42.95 o 17 1 0 185.60 229.35 36.58 o 18 1 0 70.10 46.74 24.08 o 19 1 0 32.95 57.33 31.31 o 0 2 0 552.93 448.79 12.75 o 1 2 0 830.88 757.90 53.54 o 2 2 0 14095.22 12346.96 1578.12 o 3 2 0 51.84 46.53 6.50 o 4 2 0 2738.06 2879.62 89.82 o 5 2 0 11.50 30.72 11.19 o 6 2 0 6189.35 6090.91 452.04 o 7 2 0 202.92 175.93 10.41 o 8 2 0 44.25 51.28 9.49 o 9 2 0 293.19 293.45 19.07 o 10 2 0 853.05 878.07 20.01 o 11 2 0 420.72 388.66 18.83 o 12 2 0 1329.33 1337.22 91.20 o 13 2 0 1316.25 1368.77 64.49 o 14 2 0 114.55 146.42 17.57 o 15 2 0 57.68 26.28 24.10 o 16 2 0 11.99 28.23 45.06 o 17 2 0 9.83 11.93 45.46 o 18 2 0 1.71 -16.65 30.55 o 1 3 0 133.64 159.45 8.08 o 2 3 0 167.31 155.64 26.29 o 3 3 0 80.04 80.00 14.74 o 4 3 0 295.98 296.48 19.25 o 5 3 0 2633.63 2479.23 61.12 o 6 3 0 111.89 106.54 9.53 o 7 3 0 1879.62 2003.27 50.29 o 8 3 0 676.28 718.96 50.53 o 9 3 0 3168.58 3201.67 133.01 o 10 3 0 66.75 75.38 13.86 o 11 3 0 1.09 -14.24 31.63 o 12 3 0 23.71 24.39 34.14 o 13 3 0 482.09 462.94 20.76 o 14 3 0 0.08 -19.13 56.67 o 15 3 0 62.71 132.92 20.89 o 16 3 0 28.37 16.10 42.67 o 17 3 0 7.92 7.02 29.55 o 18 3 0 0.99 -27.99 50.66 o 0 4 0 5610.61 4806.54 76.40 o 1 4 0 1244.52 1103.27 36.64 o 2 4 0 113.48 92.04 15.28 o 3 4 0 188.47 189.96 26.89 o 4 4 0 1760.08 1532.00 256.40 o 5 4 0 1071.69 1080.11 24.18 o 6 4 0 171.90 183.31 11.49 o 7 4 0 1188.93 1203.68 29.36 o 8 4 0 243.88 207.76 15.82 o 9 4 0 221.13 258.97 21.36 o 10 4 0 1854.92 1831.52 205.75 o 11 4 0 3.29 4.79 24.61 o 12 4 0 21.74 33.75 48.61 o 13 4 0 15.31 7.06 36.03 o 14 4 0 725.98 672.59 60.04 o 15 4 0 324.26 255.12 50.53 o 16 4 0 12.57 -13.29 45.32 o 17 4 0 42.57 68.75 33.99 o 1 5 0 146.38 180.42 18.65 o 2 5 0 144.63 105.56 17.15 o 3 5 0 3173.30 2813.01 359.70 o 4 5 0 273.51 230.03 27.73 o 5 5 0 7.50 3.89 33.33 o 6 5 0 90.96 103.95 13.91 o 7 5 0 2188.34 2312.94 83.02 o 8 5 0 2.05 -5.50 19.31 o 9 5 0 453.31 409.87 19.05 o 10 5 0 45.64 12.99 34.15 o 11 5 0 416.62 425.03 20.33 o 12 5 0 232.81 171.28 37.00 o 13 5 0 453.44 389.08 24.18 o 14 5 0 32.01 -27.47 28.65 o 15 5 0 63.54 38.36 29.91 o 16 5 0 9.48 15.55 30.70 o 0 6 0 892.77 846.09 26.71 o 1 6 0 211.10 181.57 15.18 o 2 6 0 318.09 309.39 26.05 o 3 6 0 1250.23 1079.09 79.41 o 4 6 0 88.61 75.87 15.27 o 5 6 0 0.61 14.90 35.61 o 6 6 0 1684.05 1376.52 184.75 o 7 6 0 32.55 5.73 34.50 o 8 6 0 75.36 17.83 35.78 o 9 6 0 0.60 -4.03 35.84 o 10 6 0 187.49 201.21 19.78 o 11 6 0 238.59 229.39 21.78 o 12 6 0 12.90 25.37 42.53 o 13 6 0 1.02 -5.58 28.17 o 14 6 0 46.65 26.33 34.59 o 15 6 0 8.25 34.02 50.53 o 1 7 0 52.61 117.56 25.33 o 2 7 0 51.25 53.01 23.54 o 3 7 0 45.23 33.80 31.28 o 4 7 0 20.72 -43.74 43.74 o 5 7 0 283.64 340.58 21.35 o 6 7 0 491.47 491.57 123.51 o 7 7 0 19.38 45.33 47.04 o 8 7 0 96.42 121.41 25.51 o 9 7 0 0.51 7.59 56.97 o 10 7 0 80.43 151.31 47.65 o 11 7 0 0.53 32.62 57.26 o 12 7 0 6.37 -60.30 60.30 o 13 7 0 38.29 157.84 87.65 o 0 8 0 11.75 45.72 53.30 o 1 8 0 40.30 -38.61 38.61 o 2 8 0 75.75 54.07 54.44 o 3 8 0 128.70 41.16 32.31 o 4 8 0 1.19 38.51 75.44 o 5 8 0 19.04 -13.20 43.08 o 6 8 0 7.28 14.62 41.63 o 7 8 0 42.13 31.31 21.91 o 8 8 0 1.57 -3.92 44.84 o 9 8 0 0.34 -26.98 45.95 o 10 8 0 5.52 2.87 31.26 o 11 8 0 31.72 -3.85 63.39 o 1 9 0 43.36 45.00 23.31 o 2 9 0 3.13 11.55 47.65 o 3 9 0 19.55 6.80 46.83 o 4 9 0 24.23 28.29 66.06 o 5 9 0 3.91 -5.69 49.00 o 6 9 0 7.11 -44.08 55.11 o 7 9 0 30.75 31.84 40.13 o 8 9 0 13.36 -21.20 51.35 o -19 0 1 0.84 -34.53 68.46 o -17 0 1 770.75 801.93 39.46 o -15 0 1 402.98 379.97 28.52 o -13 0 1 48.66 -34.05 46.92 o -11 0 1 10397.25 10797.75 138.37 o -9 0 1 1576.49 1566.81 46.92 o -7 0 1 3025.12 2878.89 56.79 o -5 0 1 5160.62 5726.26 64.01 o -3 0 1 19100.58 19920.88 87.95 o -1 0 1 269.70 425.93 9.63 o 1 0 1 48.87 38.38 4.09 o 3 0 1 86928.99 93813.66 785.45 o 5 0 1 30407.28 30262.38 148.47 o 7 0 1 4716.46 4488.41 71.95 o 9 0 1 992.72 1329.29 41.39 o 11 0 1 74.76 63.17 19.13 o 13 0 1 212.88 209.96 24.18 o 15 0 1 5.29 23.10 51.98 o 17 0 1 135.56 117.07 31.64 o 19 0 1 18.88 39.71 36.22 o -19 1 1 10.90 74.24 33.21 o -18 1 1 25.93 11.19 68.34 o -17 1 1 8.35 -20.70 59.80 o -16 1 1 45.39 92.04 26.23 o -15 1 1 60.49 8.78 56.07 o -14 1 1 2796.34 2628.03 80.37 o -13 1 1 858.67 910.22 29.60 o -12 1 1 561.64 560.21 25.39 o -11 1 1 35.52 27.19 34.89 o -10 1 1 16.36 8.18 31.04 o -9 1 1 34.83 11.19 28.76 o -8 1 1 928.23 911.18 25.51 o -7 1 1 1886.87 2181.88 51.74 o -6 1 1 3620.65 3756.51 60.28 o -5 1 1 6239.93 6186.49 69.30 o -4 1 1 2374.91 2351.77 40.79 o -3 1 1 454.74 553.71 16.72 o -2 1 1 90.06 73.64 6.50 o -1 1 1 22719.93 22819.15 82.90 o 0 1 1 13774.73 13743.78 62.93 o 1 1 1 9342.25 10159.21 58.11 o 2 1 1 12078.35 12210.90 71.59 o 3 1 1 11851.89 10923.60 77.00 o 4 1 1 6.08 18.89 8.78 o 5 1 1 291.42 273.01 11.19 o 6 1 1 3376.03 3582.89 61.48 o 7 1 1 425.71 377.44 15.16 o 8 1 1 372.19 277.46 15.28 o 9 1 1 16.61 25.87 30.32 o 10 1 1 4296.53 4165.11 86.39 o 11 1 1 220.47 213.57 20.94 o 12 1 1 13.15 -44.28 44.28 o 13 1 1 1020.20 1063.03 31.64 o 14 1 1 160.41 142.82 25.03 o 15 1 1 74.79 35.01 54.87 o 16 1 1 5.46 35.49 57.63 o 17 1 1 0.03 -5.53 59.68 o 18 1 1 1.57 30.44 33.21 o 19 1 1 39.67 51.26 70.51 o -19 2 1 37.40 9.26 71.11 o -18 2 1 1.05 -63.29 67.74 o -17 2 1 122.97 113.34 32.25 o -16 2 1 61.17 4.93 61.60 o -15 2 1 3.05 16.00 24.91 o -14 2 1 99.85 139.45 23.22 o -13 2 1 876.87 885.92 30.92 o -12 2 1 10.09 -1.68 20.82 o -11 2 1 8.90 -15.88 39.34 o -10 2 1 872.26 954.02 26.83 o -9 2 1 2893.39 3119.65 73.03 o -8 2 1 1817.28 1889.62 53.78 o -7 2 1 2903.30 2663.64 58.84 o -6 2 1 237.43 259.89 12.99 o -5 2 1 5350.68 5194.81 69.30 o -4 2 1 5228.95 5259.54 64.85 o -3 2 1 8036.85 8307.49 75.92 o -2 2 1 5149.21 5164.85 57.75 o -1 2 1 4503.71 4237.55 50.65 o 0 2 1 45.44 56.07 8.54 o 1 2 1 32789.36 33588.38 137.04 o 2 2 1 9638.91 11473.58 85.55 o 3 2 1 4277.33 4332.60 58.23 o 4 2 1 293.29 263.74 11.91 o 5 2 1 46.46 47.89 10.83 o 6 2 1 1735.92 1862.31 50.17 o 7 2 1 2078.71 1835.72 54.14 o 8 2 1 347.57 321.86 16.72 o 9 2 1 1196.02 1006.96 27.07 o 10 2 1 1902.93 1775.68 53.54 o 11 2 1 64.79 23.34 39.46 o 12 2 1 71.75 26.23 22.62 o 13 2 1 50.02 39.95 51.02 o 14 2 1 81.16 86.63 24.91 o 15 2 1 382.96 368.18 30.68 o 16 2 1 223.03 244.25 31.88 o 17 2 1 44.15 41.51 60.04 o 18 2 1 7.11 -70.87 70.87 o -18 3 1 32.04 65.69 34.65 o -17 3 1 11.27 -59.92 65.69 o -16 3 1 12.96 97.82 28.88 o -15 3 1 107.70 114.66 27.43 o -14 3 1 63.36 37.78 25.51 o -13 3 1 13.79 -6.26 47.89 o -12 3 1 665.64 720.84 28.64 o -11 3 1 43.71 29.96 19.61 o -10 3 1 204.12 288.53 21.30 o -9 3 1 202.54 180.00 17.45 o -8 3 1 1503.49 1541.18 45.48 o -7 3 1 793.66 801.93 22.86 o -6 3 1 3069.65 2758.57 63.77 o -5 3 1 129.82 129.22 12.99 o -4 3 1 10946.07 11289.74 106.24 o -3 3 1 3685.60 3606.23 60.64 o -2 3 1 4929.00 4401.18 64.01 o -1 3 1 66.06 46.20 10.59 o 0 3 1 1270.96 1034.63 31.64 o 1 3 1 2682.05 2557.52 51.14 o 2 3 1 39.31 4.09 10.59 o 3 3 1 120.20 113.70 11.43 o 4 3 1 1834.32 1767.74 49.09 o 5 3 1 227.16 223.43 14.20 o 6 3 1 51.85 37.78 12.99 o 7 3 1 773.92 596.06 19.49 o 8 3 1 15.95 -22.02 32.25 o 9 3 1 109.44 92.41 17.33 o 10 3 1 336.05 319.57 21.78 o 11 3 1 235.59 185.41 23.22 o 12 3 1 125.50 163.51 23.94 o 13 3 1 0.51 -16.97 49.69 o 14 3 1 272.08 297.55 28.15 o 15 3 1 137.86 104.20 29.48 o 16 3 1 9.67 -5.41 64.13 o 17 3 1 3.47 18.77 33.45 o 18 3 1 33.71 5.41 36.34 o -17 4 1 5.03 29.00 68.46 o -16 4 1 73.50 -35.25 68.94 o -15 4 1 5.76 50.41 56.07 o -14 4 1 174.93 197.08 27.91 o -13 4 1 62.50 2.17 50.17 o -12 4 1 640.18 646.12 29.36 o -11 4 1 402.31 392.72 26.35 o -10 4 1 955.35 874.61 28.03 o -9 4 1 81.79 99.38 19.73 o -8 4 1 325.81 347.00 20.09 o -7 4 1 1329.22 1568.25 44.64 o -6 4 1 8.93 18.65 14.32 o -5 4 1 584.28 516.17 18.17 o -4 4 1 336.64 255.32 15.88 o -3 4 1 616.90 603.89 17.81 o -2 4 1 606.89 624.10 17.69 o -1 4 1 4656.34 4758.29 76.40 o 0 4 1 988.88 914.43 27.43 o 1 4 1 317.60 321.13 15.04 o 2 4 1 14.65 -10.83 27.79 o 3 4 1 5779.58 5359.65 84.22 o 4 4 1 4650.60 5118.65 84.22 o 5 4 1 2561.07 2634.76 67.62 o 6 4 1 21.22 33.09 15.40 o 7 4 1 854.24 710.97 22.74 o 8 4 1 801.64 656.59 24.42 o 9 4 1 425.06 351.09 23.10 o 10 4 1 312.61 366.25 24.91 o 11 4 1 189.56 151.60 24.55 o 12 4 1 0.32 17.09 47.89 o 13 4 1 342.45 277.94 28.28 o 14 4 1 21.12 -58.23 58.23 o 15 4 1 5.28 7.94 62.81 o 16 4 1 26.09 8.54 67.74 o 17 4 1 39.96 87.71 35.25 o -16 5 1 4.20 80.25 33.21 o -15 5 1 3.03 -8.54 67.74 o -14 5 1 69.56 93.97 32.61 o -13 5 1 43.37 47.05 28.76 o -12 5 1 39.81 -53.78 53.78 o -11 5 1 132.82 121.64 25.39 o -10 5 1 372.93 373.83 27.07 o -9 5 1 695.32 726.37 29.24 o -8 5 1 2263.41 2444.30 71.95 o -7 5 1 671.35 612.07 26.35 o -6 5 1 310.16 236.43 22.02 o -5 5 1 737.27 690.03 24.06 o -4 5 1 2638.92 2825.59 75.44 o -3 5 1 175.51 187.10 18.05 o -2 5 1 277.72 283.11 18.41 o -1 5 1 4.87 -4.21 31.64 o 0 5 1 1384.36 1238.33 37.78 o 1 5 1 555.66 569.35 20.09 o 2 5 1 292.05 249.90 17.45 o 3 5 1 1291.03 1140.75 32.97 o 4 5 1 369.27 375.52 19.85 o 5 5 1 0.31 4.69 38.50 o 6 5 1 725.37 848.13 27.55 o 7 5 1 440.75 344.96 24.55 o 8 5 1 416.29 326.79 25.03 o 9 5 1 1242.17 1210.66 35.37 o 10 5 1 665.11 590.77 30.44 o 11 5 1 43.05 11.07 53.66 o 12 5 1 106.12 105.16 27.79 o 13 5 1 26.51 -64.13 64.13 o 14 5 1 2.30 17.45 31.52 o 15 5 1 10.35 2.89 69.18 o 16 5 1 0.19 61.96 34.89 o -15 6 1 6.98 9.14 71.35 o -14 6 1 0.11 31.52 68.82 o -13 6 1 17.78 -24.30 63.41 o -12 6 1 10.13 30.68 29.36 o -11 6 1 40.02 69.79 26.11 o -10 6 1 132.51 120.20 26.71 o -9 6 1 227.21 320.29 27.31 o -8 6 1 1151.52 1108.75 33.45 o -7 6 1 623.65 591.25 28.88 o -6 6 1 86.99 35.61 49.21 o -5 6 1 552.72 575.97 26.47 o -4 6 1 1460.74 1414.12 40.55 o -3 6 1 197.38 232.10 21.42 o -2 6 1 357.16 313.55 22.26 o -1 6 1 1.48 11.43 39.59 o 0 6 1 533.41 526.76 23.46 o 1 6 1 210.63 257.24 22.02 o 2 6 1 126.83 108.05 20.09 o 3 6 1 306.15 299.36 23.22 o 4 6 1 82.67 88.56 21.66 o 5 6 1 1091.95 1158.68 36.58 o 6 6 1 1640.26 1801.19 54.75 o 7 6 1 538.03 552.51 29.36 o 8 6 1 426.63 342.07 27.79 o 9 6 1 133.73 116.59 26.23 o 10 6 1 511.86 436.76 30.80 o 11 6 1 59.82 -64.73 64.73 o 12 6 1 210.93 171.22 32.97 o 13 6 1 2.36 -67.98 67.98 o 14 6 1 0.35 -76.04 76.04 o 15 6 1 1.01 -63.05 76.76 o -13 7 1 20.79 -5.17 118.27 o -12 7 1 25.77 58.72 115.03 o -11 7 1 70.63 48.85 56.79 o -10 7 1 168.50 293.94 56.43 o -9 7 1 24.77 67.86 102.63 o -8 7 1 7.96 56.79 84.58 o -7 7 1 49.48 -50.77 89.52 o -6 7 1 151.95 275.41 43.68 o -5 7 1 451.76 375.28 32.13 o -4 7 1 41.23 18.53 55.71 o -3 7 1 89.66 119.00 25.87 o -2 7 1 250.36 326.67 28.03 o -1 7 1 592.07 625.66 31.04 o 0 7 1 120.65 163.51 27.79 o 1 7 1 175.50 165.80 27.79 o 2 7 1 145.07 158.22 27.19 o 3 7 1 80.67 -43.07 56.79 o 4 7 1 52.10 37.66 27.43 o 5 7 1 98.07 112.86 27.55 o 6 7 1 4.51 32.13 57.75 o 7 7 1 122.41 191.79 29.72 o 8 7 1 244.25 367.70 33.81 o 9 7 1 73.04 7.70 61.48 o 10 7 1 25.54 -13.36 62.93 o 11 7 1 13.10 -8.42 68.70 o 12 7 1 1.42 -41.39 68.22 o 13 7 1 129.80 96.50 37.42 o -11 8 1 28.97 73.64 130.43 o -10 8 1 1.49 5.05 118.03 o -9 8 1 192.38 186.26 34.89 o -8 8 1 5.93 37.30 63.29 o -7 8 1 2.12 10.35 63.89 o -6 8 1 148.75 95.53 31.28 o -5 8 1 123.30 55.95 61.84 o -4 8 1 0.58 13.72 28.64 o -3 8 1 1.27 18.77 54.14 o -2 8 1 1.45 -9.26 25.75 o -1 8 1 0.47 -2.29 56.19 o 0 8 1 105.65 54.99 58.11 o 1 8 1 314.41 293.94 28.52 o 2 8 1 48.60 54.02 25.99 o 3 8 1 33.61 -57.75 57.75 o 4 8 1 87.63 117.67 28.76 o 5 8 1 17.70 -17.21 57.99 o 6 8 1 16.65 -27.79 58.48 o 7 8 1 0.12 -61.60 64.37 o 8 8 1 16.31 -30.56 66.66 o 9 8 1 48.50 77.13 34.53 o 10 8 1 0.82 63.05 67.14 o 11 8 1 2.35 -18.77 68.22 o -8 9 1 12.05 -72.07 72.43 o -7 9 1 31.44 32.01 36.10 o -6 9 1 8.88 -53.42 69.79 o -5 9 1 30.33 -29.00 69.79 o -4 9 1 87.21 76.28 34.89 o -3 9 1 51.01 -19.61 69.79 o -2 9 1 31.00 -41.75 68.94 o -1 9 1 40.24 -5.53 65.94 o 0 9 1 6.52 -11.07 60.64 o 1 9 1 3.94 -30.44 67.26 o 2 9 1 25.37 2.05 34.05 o 3 9 1 42.31 0.00 71.23 o 4 9 1 1.33 31.52 32.61 o 5 9 1 54.67 46.92 70.87 o 6 9 1 80.24 -23.94 71.47 o 7 9 1 37.49 21.54 72.07 o -18 0 2 3.87 25.87 66.18 o -16 0 2 22.27 2.41 52.58 o -14 0 2 421.38 517.38 27.91 o -12 0 2 341.94 332.80 22.62 o -10 0 2 19.45 23.34 15.16 o -8 0 2 2209.37 2211.96 54.14 o -6 0 2 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