#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012898.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012898_Fobs loop_ _publ_author_name 'Usman, Anwar' 'Razak, Ibrahim Abdul' 'Fun, Hoong-Kun' 'Chantrapromma, Suchada' 'Zhang, Yan' 'Xu, Jian-Hua' _publ_section_title ; 11-Methyl-12a-phenyl-9a,12a-dihydrophenanthro[9',10':5,6][1,4]dioxino[2,3-d]oxazole and 9a-(10-hydroxyphenanthren-9-yl)-11,12a-diphenyl-9a,12a-dihydrophenanthro[9',10':5,6][1,4]dioxino[2,3-d]oxazole ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o477 _journal_page_last o479 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 102.607 _cell_angle_beta 99.511 _cell_angle_gamma 94.529 _cell_length_a 12.4812 _cell_length_b 14.3317 _cell_length_c 18.5727 _exptl_crystal_F_000 1328.00 _reflns_d_resolution_high 0.7481 _[local]_cod_data_source_file sk1563IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title 'sk1563II in P-1 (-60 degrees Celsius, 10 sec)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 301.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2415.76 2866.04 255.40 o 3 0 0 1437.49 1682.25 158.66 o 4 0 0 10741.51 13040.49 1130.06 o 5 0 0 47.65 55.74 18.68 o 6 0 0 8162.98 9444.68 601.35 o 7 0 0 215.89 332.30 41.72 o 8 0 0 443.86 455.65 80.10 o 9 0 0 13.35 17.78 35.82 o 10 0 0 63.79 52.33 44.28 o 11 0 0 27.03 22.88 55.88 o 12 0 0 988.77 957.99 148.80 o 13 0 0 2.43 73.19 95.53 o 14 0 0 30.50 29.85 111.56 o 15 0 0 122.65 56.69 117.27 o 16 0 0 183.11 198.64 133.17 o -16 1 0 108.21 134.71 128.94 o -15 1 0 0.41 14.56 83.92 o -14 1 0 71.81 158.12 126.86 o -13 1 0 23.31 28.31 88.49 o -12 1 0 97.79 94.12 75.47 o -11 1 0 149.45 107.40 71.45 o -10 1 0 400.36 381.38 80.17 o -9 1 0 66.86 28.58 40.86 o -8 1 0 110.86 115.32 43.87 o -7 1 0 1140.05 1133.08 131.76 o -6 1 0 1001.62 1079.48 120.35 o -5 1 0 383.67 280.15 47.77 o -4 1 0 3890.20 3487.39 314.83 o -3 1 0 18359.06 15028.51 1291.54 o -2 1 0 300.45 318.12 39.45 o 2 1 0 8546.83 9559.81 878.09 o 3 1 0 201.16 205.42 42.53 o 4 1 0 228.23 253.09 29.41 o 5 1 0 3053.58 3282.78 219.03 o 6 1 0 3215.77 4160.55 276.69 o 7 1 0 600.94 699.56 67.68 o 8 1 0 290.33 390.71 69.64 o 9 1 0 178.09 260.83 78.96 o 10 1 0 172.55 131.42 61.45 o 11 1 0 294.27 279.35 73.66 o 12 1 0 9.29 11.40 74.87 o 13 1 0 12.18 -19.59 90.83 o 14 1 0 195.60 165.64 115.45 o 15 1 0 123.28 76.34 117.87 o -16 2 0 17.16 66.62 118.07 o -15 2 0 112.55 -22.07 86.67 o -14 2 0 337.50 403.99 142.96 o -13 2 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113.78 o -11 3 0 38.90 43.67 51.79 o -10 3 0 21.70 28.18 39.92 o -9 3 0 53.00 19.59 33.21 o -8 3 0 435.58 505.63 79.03 o -7 3 0 1733.31 1512.45 160.80 o -6 3 0 243.88 298.40 52.53 o -5 3 0 74.25 105.19 37.37 o -4 3 0 0.01 6.31 17.78 o -3 3 0 998.25 1005.95 73.53 o -2 3 0 2187.77 1799.53 121.19 o -1 3 0 7151.02 6497.28 413.14 o 0 3 0 369.15 319.58 30.91 o 1 3 0 11790.16 2271.90 5002.23 o 2 3 0 978.01 706.35 86.67 o 3 3 0 2183.19 1727.60 180.86 o 4 3 0 1.99 -0.74 23.28 o 5 3 0 826.69 980.05 81.93 o 6 3 0 2434.40 2396.08 169.19 o 7 3 0 4264.54 4526.76 306.90 o 8 3 0 506.91 547.49 73.43 o 9 3 0 1121.48 1131.27 144.77 o 10 3 0 255.38 313.10 64.72 o 11 3 0 0.01 25.36 77.62 o 13 3 0 13.63 86.81 86.61 o 14 3 0 6.55 -40.92 87.08 o 15 3 0 116.55 136.18 132.29 o -16 4 0 79.52 64.13 133.77 o -15 4 0 4.78 75.87 99.96 o -14 4 0 502.41 444.27 92.12 o -13 4 0 268.44 233.65 75.63 o -12 4 0 1580.73 1739.07 218.23 o -11 4 0 0.91 46.69 49.78 o -10 4 0 58.63 67.22 49.78 o -9 4 0 376.69 377.83 76.41 o -8 4 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11 0 432.90 231.87 257.58 o 3 11 0 119.22 172.61 80.44 o 4 11 0 48.44 37.84 62.99 o 5 11 0 357.90 480.47 133.30 o 6 11 0 904.87 1139.25 193.95 o 7 11 0 483.98 548.29 140.01 o 8 11 0 61.19 54.34 98.28 o 9 11 0 427.70 500.93 161.27 o -13 12 0 53.19 -5.03 78.02 o -12 12 0 23.66 12.14 79.56 o -11 12 0 159.96 181.40 99.09 o -10 12 0 713.37 763.10 145.24 o -9 12 0 398.83 341.27 104.65 o -8 12 0 37.74 64.27 74.73 o -7 12 0 0.26 19.05 40.72 o -6 12 0 9.92 5.90 41.32 o -5 12 0 284.97 231.77 51.17 o -4 12 0 369.05 340.16 57.40 o -3 12 0 1496.22 1138.72 106.28 o -2 12 0 2680.65 2333.08 178.82 o -1 12 0 19.54 2.56 31.45 o 0 12 0 44.59 61.34 38.50 o 1 12 0 610.87 707.79 85.13 o 2 12 0 965.80 653.97 572.81 o 3 12 0 21.23 27.51 78.22 o 4 12 0 107.16 161.54 95.53 o 5 12 0 39.67 99.09 92.44 o 6 12 0 5.52 28.51 78.96 o 7 12 0 226.63 199.45 109.69 o 8 12 0 79.05 227.42 127.13 o 9 12 0 21.04 25.02 104.25 o -12 13 0 279.61 363.67 129.61 o -11 13 0 183.70 158.59 103.11 o -10 13 0 0.32 21.60 75.20 o -9 13 0 6.88 -39.45 49.64 o -8 13 0 91.68 77.89 60.71 o -7 13 0 0.08 39.51 53.00 o -6 13 0 272.24 281.02 74.87 o -5 13 0 396.32 349.11 74.87 o -4 13 0 643.27 672.00 81.57 o -3 13 0 2067.23 1717.28 147.46 o -2 13 0 322.05 313.48 57.52 o -1 13 0 14.89 23.73 34.43 o 0 13 0 289.26 219.41 52.13 o 1 13 0 1814.81 1977.91 167.77 o 2 13 0 330.67 238.98 139.67 o 3 13 0 47.71 87.01 83.86 o 4 13 0 9.23 3.89 77.01 o 5 13 0 0.96 2.35 67.35 o 6 13 0 161.22 147.52 108.01 o 7 13 0 1.56 43.34 103.45 o 8 13 0 0.72 -14.83 101.37 o 9 13 0 19.18 171.61 127.06 o -11 14 0 23.10 73.19 84.33 o -10 14 0 90.62 70.57 70.37 o -9 14 0 184.31 196.49 89.63 o -8 14 0 11.32 90.16 100.09 o -7 14 0 27.57 18.31 44.81 o -6 14 0 89.62 65.88 54.94 o -5 14 0 43.45 25.96 44.08 o -4 14 0 572.83 488.32 74.68 o -3 14 0 93.29 107.77 43.20 o -2 14 0 4.06 -8.58 33.96 o -1 14 0 15.69 0.15 32.64 o 0 14 0 92.54 108.09 41.98 o 1 14 0 118.28 110.92 50.90 o 2 14 0 762.07 730.83 147.99 o 3 14 0 8.98 112.30 87.08 o 4 14 0 40.98 -4.09 72.59 o 5 14 0 191.09 295.98 127.53 o 6 14 0 11.95 22.47 97.61 o 7 14 0 30.49 63.26 108.28 o 8 14 0 3.73 -56.42 98.08 o 9 14 0 19.56 32.40 123.84 o -10 15 0 386.82 384.34 149.60 o -9 15 0 303.92 327.71 114.38 o -8 15 0 86.28 87.88 68.23 o -7 15 0 98.12 82.72 67.02 o -6 15 0 13.87 36.09 50.78 o -5 15 0 19.43 23.28 45.35 o -4 15 0 0.38 20.66 39.47 o -3 15 0 1.72 -12.02 41.72 o -2 15 0 25.96 36.35 38.54 o -1 15 0 0.73 -3.20 39.21 o 0 15 0 0.63 11.16 41.48 o 2 15 0 14.72 10.47 84.66 o 3 15 0 0.01 24.35 89.63 o 4 15 0 30.67 92.98 100.29 o 5 15 0 55.39 93.99 117.80 o 6 15 0 5.48 70.37 118.74 o 7 15 0 159.98 172.41 123.97 o 8 15 0 134.26 171.14 126.79 o -9 16 0 84.27 70.71 94.19 o -8 16 0 8.71 -14.96 60.31 o -7 16 0 190.49 193.61 85.00 o -6 16 0 57.90 21.53 53.67 o -5 16 0 212.21 219.64 72.45 o -4 16 0 30.29 52.60 94.12 o -3 16 0 2.43 -9.85 42.73 o -2 16 0 1.76 -4.85 38.41 o -1 16 0 3.73 29.67 44.38 o 0 16 0 0.63 27.73 48.05 o 1 16 0 17.35 29.12 95.73 o 2 16 0 0.03 -44.08 74.93 o 3 16 0 0.54 50.38 108.61 o 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