#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/31/2013145.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013145_Fobs loop_ _publ_author_name 'Tsao, Jonglin F.' 'Faruqi, Sana R.' 'Thompson, Hugh W.' 'Lalancette, Roger A.' _publ_section_title ; Two new heterocyclic [3.3.3.0^1,5^]-propellanoid compounds: 2,8-dioxatricyclo[3.3.3.0^1,5^]undecane-3,7-dione and a related dimer ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o57 _journal_page_last o59 _journal_volume 59 _journal_year 2003 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.5710 _cell_length_b 27.0690 _cell_length_c 10.7540 _exptl_crystal_F_000 1488.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file fr1401IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' c:\xscans\012601 in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 354.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 29115.16 28181.21 963.80 o 8 0 0 3880.77 3965.56 262.04 o 12 0 0 0.92 5.50 99.15 o 2 2 0 18157.86 17515.88 492.25 o 4 2 0 2632.17 2666.35 118.85 o 6 2 0 566.10 535.03 60.81 o 8 2 0 31.60 124.46 84.20 o 10 2 0 906.58 831.14 106.33 o 12 2 0 2.60 -19.76 101.29 o 2 4 0 5581.23 5766.04 158.50 o 4 4 0 3741.77 3640.43 187.64 o 6 4 0 65.40 -3.17 57.01 o 8 4 0 356.17 302.11 192.15 o 10 4 0 0.15 -48.60 175.97 o 12 4 0 0.61 256.79 89.69 o 2 6 0 743.84 730.65 51.46 o 4 6 0 27302.88 27751.20 728.12 o 6 6 0 285.65 243.15 62.65 o 8 6 0 534.57 614.46 109.48 o 10 6 0 475.36 556.84 95.47 o 12 6 0 585.79 622.09 236.25 o 0 8 0 30.33 86.00 52.34 o 2 8 0 13576.62 13288.95 371.91 o 4 8 0 9743.12 9779.87 291.05 o 6 8 0 2711.36 2702.07 151.37 o 8 8 0 1411.66 1171.97 164.73 o 10 8 0 88.46 78.84 90.31 o 12 8 0 10.20 -107.68 107.68 o 2 10 0 18547.06 18510.73 1160.38 o 4 10 0 536.09 493.13 62.84 o 6 10 0 652.30 746.15 151.28 o 8 10 0 382.51 448.59 163.88 o 10 10 0 2252.05 2267.02 206.62 o 12 10 0 156.35 71.55 104.83 o 0 12 0 5459.33 5948.07 566.91 o 2 12 0 948.62 928.22 69.39 o 4 12 0 621.54 693.87 69.85 o 6 12 0 5270.61 5088.75 163.00 o 8 12 0 1459.49 1492.96 110.01 o 10 12 0 457.60 274.20 105.21 o 12 12 0 6.50 67.13 138.60 o 2 14 0 447.34 490.82 82.67 o 4 14 0 7510.43 7377.95 346.24 o 6 14 0 53.91 82.62 81.06 o 8 14 0 734.54 705.50 114.51 o 10 14 0 385.87 416.32 100.83 o 12 14 0 56.49 -18.39 170.78 o 0 16 0 3485.99 3540.80 160.14 o 2 16 0 3802.99 3772.09 184.74 o 4 16 0 3011.31 3051.35 123.71 o 6 16 0 4.52 -31.47 84.55 o 8 16 0 108.68 67.20 93.67 o 10 16 0 33.93 68.92 98.55 o 2 18 0 5071.25 4779.40 156.65 o 4 18 0 903.18 797.78 96.40 o 6 18 0 591.00 587.12 184.40 o 8 18 0 668.29 461.55 112.76 o 10 18 0 161.25 221.38 187.72 o 0 20 0 1484.19 1418.07 231.91 o 2 20 0 366.53 492.44 155.54 o 4 20 0 2401.84 2233.05 127.56 o 6 20 0 362.73 347.41 163.54 o 8 20 0 183.61 218.01 102.52 o 10 20 0 26.51 11.85 111.30 o 2 22 0 289.88 290.90 100.41 o 4 22 0 106.00 144.99 94.36 o 6 22 0 357.55 417.97 102.35 o 8 22 0 111.99 120.28 104.92 o 10 22 0 2.24 67.38 101.61 o 0 24 0 83.16 142.71 92.13 o 2 24 0 89.15 193.10 95.32 o 4 24 0 97.27 190.98 100.48 o 6 24 0 186.02 183.32 98.98 o 8 24 0 139.63 338.50 164.14 o 2 26 0 240.20 294.01 101.77 o 4 26 0 181.41 219.83 152.82 o 6 26 0 112.85 257.34 256.68 o 8 26 0 251.33 409.53 117.17 o 0 28 0 1.09 10.03 102.15 o 2 28 0 876.51 859.03 120.74 o 4 28 0 60.97 181.36 106.06 o 6 28 0 29.89 -35.25 111.25 o 2 30 0 42.88 -23.77 106.90 o 4 30 0 69.11 135.60 115.31 o 0 32 0 311.05 279.81 211.81 o 1 1 1 39819.49 39417.96 774.81 o 3 1 1 16126.50 15836.10 439.08 o 5 1 1 9260.30 9671.74 467.13 o 7 1 1 1312.95 1168.22 83.23 o 9 1 1 1240.00 1245.66 102.08 o 11 1 1 493.47 500.76 105.23 o 13 1 1 51.88 52.02 105.88 o 1 3 1 39002.69 36767.77 493.38 o 3 3 1 12339.82 12313.77 413.00 o 5 3 1 4019.96 4294.65 172.74 o 7 3 1 173.53 277.52 79.94 o 9 3 1 174.55 289.62 83.66 o 11 3 1 182.98 33.74 113.74 o 13 3 1 16.97 94.36 125.23 o 1 5 1 89407.66 85798.59 880.59 o 3 5 1 1635.84 1640.71 102.93 o 5 5 1 6358.21 6583.50 213.18 o 7 5 1 980.62 1005.16 84.68 o 9 5 1 272.01 294.28 90.06 o 11 5 1 154.92 156.80 97.73 o 13 5 1 9.84 -26.58 111.04 o 1 7 1 3265.38 3538.03 121.87 o 3 7 1 6280.72 7048.82 240.50 o 5 7 1 488.14 503.52 58.85 o 7 7 1 273.05 376.60 99.61 o 9 7 1 1599.85 1507.55 116.43 o 11 7 1 149.16 116.62 95.07 o 13 7 1 43.56 41.83 109.97 o 1 9 1 30847.54 31046.35 712.89 o 3 9 1 6192.00 6082.73 393.49 o 5 9 1 2716.66 2841.21 175.89 o 7 9 1 147.43 211.12 79.26 o 9 9 1 2235.41 2247.85 127.92 o 11 9 1 249.48 200.74 158.18 o 13 9 1 7.58 155.56 109.48 o 1 11 1 7455.93 7464.43 272.77 o 3 11 1 2239.24 2274.91 85.36 o 5 11 1 9435.10 9786.28 299.15 o 7 11 1 467.58 372.55 88.76 o 9 11 1 1624.21 1725.12 115.23 o 11 11 1 428.57 526.25 108.99 o 1 13 1 432.20 417.12 66.18 o 3 13 1 501.80 524.86 69.69 o 5 13 1 1085.72 1150.81 87.67 o 7 13 1 931.36 1119.63 108.04 o 9 13 1 243.77 406.23 92.62 o 11 13 1 172.10 293.04 106.33 o 1 15 1 1394.12 1459.71 84.40 o 3 15 1 1270.20 1249.13 91.75 o 5 15 1 1431.55 1537.32 101.46 o 7 15 1 701.16 686.03 100.23 o 9 15 1 132.16 -5.25 97.70 o 11 15 1 66.37 246.10 199.13 o 1 17 1 6064.68 6195.84 250.38 o 3 17 1 1261.65 1250.92 96.92 o 5 17 1 1784.45 1842.60 134.26 o 7 17 1 3440.03 3571.66 142.96 o 9 17 1 16.10 -112.15 116.04 o 11 17 1 70.01 -23.24 106.15 o 1 19 1 1138.96 1153.37 103.89 o 3 19 1 333.45 307.67 96.50 o 5 19 1 39.74 157.44 169.76 o 7 19 1 428.53 543.33 105.52 o 9 19 1 52.62 48.37 182.10 o 11 19 1 101.04 93.41 116.25 o 1 21 1 474.62 588.34 98.29 o 3 21 1 324.95 313.68 118.00 o 5 21 1 1643.28 1568.11 127.38 o 7 21 1 13.16 27.00 194.70 o 9 21 1 4.68 117.88 187.47 o 1 23 1 193.88 127.79 99.02 o 3 23 1 2109.07 2119.67 134.18 o 5 23 1 21.31 116.20 129.91 o 7 23 1 37.82 42.83 99.96 o 9 23 1 152.31 143.56 117.87 o 1 25 1 62.01 -41.88 96.66 o 3 25 1 454.16 448.20 107.86 o 5 25 1 110.17 155.41 102.69 o 7 25 1 26.18 -74.02 107.82 o 1 27 1 656.84 707.62 115.09 o 3 27 1 547.33 539.91 211.22 o 5 27 1 112.52 146.90 108.64 o 7 27 1 77.46 119.12 139.71 o 1 29 1 68.54 108.43 154.26 o 3 29 1 10.51 67.11 179.46 o 5 29 1 12.70 -141.71 267.07 o 1 31 1 63.41 229.49 133.41 o 3 31 1 48.98 11.82 118.58 o 2 0 2 15526.63 16269.97 426.50 o 6 0 2 2453.10 2414.76 93.49 o 10 0 2 2586.66 2438.06 132.85 o 0 2 2 125670.15 117874.02 2270.53 o 2 2 2 7851.74 7796.33 204.61 o 4 2 2 5147.40 5200.50 164.40 o 6 2 2 2744.77 2675.34 94.44 o 8 2 2 235.54 202.89 81.25 o 10 2 2 48.06 138.26 91.38 o 12 2 2 81.38 20.12 100.54 o 2 4 2 37924.28 39234.64 695.15 o 4 4 2 1536.68 1348.34 106.42 o 6 4 2 1174.92 1137.81 74.56 o 8 4 2 2069.94 2228.54 107.02 o 10 4 2 231.18 362.27 86.43 o 12 4 2 34.51 292.85 179.46 o 0 6 2 1517.60 1463.20 80.71 o 2 6 2 34056.57 33975.21 713.93 o 4 6 2 12926.91 13687.39 355.20 o 6 6 2 6709.07 6679.29 213.65 o 8 6 2 672.90 650.08 87.87 o 10 6 2 83.76 83.57 93.48 o 12 6 2 294.72 426.07 126.34 o 2 8 2 2307.44 2502.83 82.95 o 4 8 2 1206.76 1279.28 68.40 o 6 8 2 337.45 383.22 91.60 o 8 8 2 239.75 353.03 79.86 o 10 8 2 423.56 470.94 136.81 o 12 8 2 125.41 279.00 131.45 o 0 10 2 5930.20 5859.34 185.81 o 2 10 2 8709.91 8815.01 284.52 o 4 10 2 2043.36 2175.15 97.41 o 6 10 2 1578.99 1519.54 89.75 o 8 10 2 205.34 79.96 137.15 o 10 10 2 49.71 -57.76 95.78 o 12 10 2 14.63 -104.36 104.36 o 2 12 2 5058.14 5204.32 255.66 o 4 12 2 2427.88 2307.39 146.18 o 6 12 2 2131.07 1992.85 117.93 o 8 12 2 1007.50 859.67 102.22 o 10 12 2 264.42 159.62 96.58 o 12 12 2 68.47 7.48 273.20 o 0 14 2 4311.17 4487.90 334.49 o 2 14 2 881.37 1035.97 78.94 o 4 14 2 3247.66 3173.41 122.24 o 6 14 2 910.53 990.45 144.81 o 8 14 2 122.83 132.13 148.47 o 10 14 2 42.03 -0.66 128.21 o 12 14 2 59.68 195.70 113.92 o 2 16 2 831.62 775.66 86.38 o 4 16 2 77.78 39.49 83.46 o 6 16 2 2419.66 2206.03 138.43 o 8 16 2 332.64 281.46 96.52 o 10 16 2 184.58 379.24 100.25 o 0 18 2 302.07 384.59 88.43 o 2 18 2 877.16 813.63 96.44 o 4 18 2 686.39 635.92 100.95 o 6 18 2 891.15 976.01 109.67 o 8 18 2 103.58 142.54 91.97 o 10 18 2 287.12 379.68 105.09 o 2 20 2 2076.98 2179.11 178.02 o 4 20 2 283.96 353.50 171.55 o 6 20 2 349.10 397.06 99.78 o 8 20 2 478.89 287.52 110.16 o 10 20 2 155.18 132.93 108.07 o 0 22 2 34.63 -76.84 102.64 o 2 22 2 1327.25 1055.00 113.46 o 4 22 2 617.24 682.22 105.88 o 6 22 2 1059.84 1422.38 111.59 o 8 22 2 302.69 515.64 107.35 o 2 24 2 224.94 208.18 128.47 o 4 24 2 200.48 68.73 101.75 o 6 24 2 12.22 -91.08 107.45 o 8 24 2 39.09 125.92 98.84 o 0 26 2 225.41 270.51 114.93 o 2 26 2 1598.07 1594.82 128.10 o 4 26 2 256.64 142.67 113.32 o 6 26 2 3.03 26.69 168.23 o 2 28 2 44.23 126.40 108.38 o 4 28 2 13.46 109.96 101.43 o 6 28 2 29.01 -116.54 116.54 o 0 30 2 490.13 482.82 124.75 o 2 30 2 90.21 154.71 114.42 o 4 30 2 23.63 138.27 112.63 o 1 1 3 1584.60 1665.50 89.14 o 3 1 3 955.12 966.46 58.26 o 5 1 3 1416.95 1464.08 101.31 o 7 1 3 3878.59 3820.06 122.99 o 9 1 3 333.70 277.64 87.92 o 11 1 3 8.75 188.12 154.77 o 13 1 3 106.94 233.30 114.47 o 1 3 3 2362.41 2348.75 94.63 o 3 3 3 6951.08 6845.81 208.09 o 5 3 3 10017.17 10175.10 288.16 o 7 3 3 3660.23 3746.05 408.30 o 9 3 3 1093.13 921.43 99.42 o 11 3 3 705.64 726.89 104.21 o 13 3 3 5.43 22.30 109.65 o 1 5 3 24103.38 24554.66 605.78 o 3 5 3 9051.19 8978.36 317.30 o 5 5 3 11510.77 11546.54 372.97 o 7 5 3 164.49 66.03 73.74 o 9 5 3 317.42 290.08 90.40 o 11 5 3 218.75 117.95 100.57 o 13 5 3 104.38 -61.29 115.31 o 1 7 3 3349.18 3525.37 113.28 o 3 7 3 3755.22 3939.48 114.90 o 5 7 3 632.88 667.62 71.59 o 7 7 3 301.66 373.81 165.76 o 9 7 3 182.04 101.84 86.32 o 11 7 3 63.39 0.32 92.10 o 13 7 3 25.33 104.51 118.21 o 1 9 3 3544.02 3541.33 127.31 o 3 9 3 11659.61 12170.47 331.62 o 5 9 3 6340.63 6309.76 391.79 o 7 9 3 261.23 264.57 95.61 o 9 9 3 317.50 283.32 92.94 o 11 9 3 48.42 44.14 217.69 o 1 11 3 17524.44 18079.37 463.54 o 3 11 3 1875.18 1980.01 225.52 o 5 11 3 343.84 322.32 214.11 o 7 11 3 1873.84 1832.80 112.45 o 9 11 3 258.79 304.00 169.25 o 11 11 3 94.21 257.35 134.60 o 1 13 3 1900.72 1716.51 156.65 o 3 13 3 1841.26 1713.19 95.12 o 5 13 3 771.11 628.76 155.63 o 7 13 3 909.88 1050.52 125.74 o 9 13 3 236.32 210.50 88.19 o 11 13 3 15.08 174.29 135.70 o 1 15 3 497.17 492.55 81.56 o 3 15 3 465.17 552.51 81.53 o 5 15 3 758.96 760.65 152.90 o 7 15 3 2551.99 2636.24 129.68 o 9 15 3 388.25 577.59 97.33 o 11 15 3 147.44 267.75 100.70 o 1 17 3 576.57 596.29 90.85 o 3 17 3 826.55 885.56 89.63 o 5 17 3 797.30 631.74 99.56 o 7 17 3 224.70 152.07 100.98 o 9 17 3 11.18 -95.81 95.81 o 11 17 3 33.06 -42.30 126.25 o 1 19 3 43.94 102.91 87.30 o 3 19 3 10.42 91.82 125.66 o 5 19 3 598.02 691.17 101.56 o 7 19 3 173.55 282.08 92.27 o 9 19 3 54.27 200.22 95.43 o 1 21 3 647.16 534.72 104.50 o 3 21 3 1792.14 1807.83 120.53 o 5 21 3 82.24 -31.41 96.12 o 7 21 3 178.65 391.95 118.25 o 9 21 3 124.41 59.19 112.81 o 1 23 3 166.95 57.09 99.93 o 3 23 3 200.31 196.70 102.06 o 5 23 3 132.26 245.73 96.44 o 7 23 3 188.56 309.90 104.78 o 9 23 3 30.28 172.71 194.79 o 1 25 3 565.74 575.84 105.76 o 3 25 3 719.79 849.08 111.64 o 5 25 3 104.17 200.98 101.24 o 7 25 3 0.27 43.73 107.71 o 1 27 3 29.03 240.40 133.06 o 3 27 3 50.01 -21.43 105.63 o 5 27 3 106.88 64.36 110.11 o 1 29 3 43.35 -118.17 130.85 o 3 29 3 49.24 212.37 214.54 o 5 29 3 34.86 -55.56 116.62 o 1 31 3 228.60 294.30 273.20 o 0 0 4 28679.51 27384.77 1239.30 o 4 0 4 4368.36 4507.99 137.82 o 8 0 4 329.27 357.54 85.59 o 12 0 4 130.34 59.79 106.82 o 2 2 4 3335.07 3430.50 111.63 o 4 2 4 1328.21 1374.29 106.50 o 6 2 4 42.87 35.00 110.08 o 8 2 4 1223.74 1074.89 143.88 o 10 2 4 1177.37 1179.33 110.42 o 12 2 4 76.52 214.11 118.08 o 0 4 4 11137.84 11586.29 312.60 o 2 4 4 1193.64 1241.95 83.52 o 4 4 4 22656.90 23093.80 1402.59 o 6 4 4 334.96 356.21 69.03 o 8 4 4 525.85 471.52 116.38 o 10 4 4 213.15 329.79 103.35 o 12 4 4 117.02 224.86 103.78 o 2 6 4 2919.91 3002.74 94.83 o 4 6 4 7899.19 8057.16 296.10 o 6 6 4 1776.82 1754.54 146.52 o 8 6 4 707.63 624.88 91.46 o 10 6 4 338.17 312.93 92.45 o 12 6 4 11.23 157.54 95.25 o 0 8 4 3010.65 3040.38 107.23 o 2 8 4 8858.08 8691.28 319.17 o 4 8 4 1209.66 1093.98 95.01 o 6 8 4 149.74 129.17 76.73 o 8 8 4 1092.22 1122.27 98.78 o 10 8 4 475.99 343.25 101.54 o 12 8 4 2.63 34.12 106.07 o 2 10 4 810.42 804.75 105.48 o 4 10 4 3803.56 3802.18 121.55 o 6 10 4 968.62 927.30 94.52 o 8 10 4 374.58 346.97 89.43 o 10 10 4 32.25 125.34 100.88 o 12 10 4 36.14 82.50 98.49 o 0 12 4 4297.31 4092.12 133.18 o 2 12 4 1050.77 893.08 100.29 o 4 12 4 457.67 546.69 82.05 o 6 12 4 777.81 682.93 95.03 o 8 12 4 1054.05 1004.69 154.09 o 10 12 4 62.70 408.88 176.40 o 12 12 4 33.20 107.70 135.02 o 2 14 4 2920.46 3077.60 113.70 o 4 14 4 433.09 525.96 87.86 o 6 14 4 1199.29 1210.07 135.02 o 8 14 4 315.63 362.61 103.01 o 10 14 4 15.37 73.83 97.40 o 0 16 4 12367.88 12861.72 424.99 o 2 16 4 722.18 679.89 92.25 o 4 16 4 10.78 151.21 87.13 o 6 16 4 207.47 127.81 88.91 o 8 16 4 66.99 190.77 95.97 o 10 16 4 40.69 -103.46 103.46 o 2 18 4 108.62 180.41 86.85 o 4 18 4 364.72 299.40 92.83 o 6 18 4 30.79 198.50 91.07 o 8 18 4 19.92 -56.88 177.08 o 10 18 4 24.91 -15.65 103.53 o 0 20 4 1027.54 944.16 109.44 o 2 20 4 300.11 358.55 218.37 o 4 20 4 78.16 80.55 134.94 o 6 20 4 1445.24 1310.38 119.34 o 8 20 4 486.71 597.12 109.21 o 2 22 4 691.47 532.15 122.85 o 4 22 4 806.01 789.54 107.83 o 6 22 4 125.23 126.32 103.85 o 8 22 4 2.46 187.13 103.65 o 0 24 4 1186.47 1038.11 118.29 o 2 24 4 40.59 42.53 149.16 o 4 24 4 286.08 228.69 179.97 o 6 24 4 41.13 90.37 99.40 o 8 24 4 21.60 -11.95 108.81 o 2 26 4 270.34 257.30 110.31 o 4 26 4 43.21 -60.34 111.92 o 6 26 4 6.32 17.53 110.25 o 0 28 4 424.98 332.16 121.00 o 2 28 4 22.63 150.66 105.36 o 4 28 4 58.43 26.58 110.91 o 2 30 4 21.97 -118.83 118.83 o 1 1 5 3177.49 3193.22 211.98 o 3 1 5 38.92 52.93 66.15 o 5 1 5 1257.20 1339.11 88.12 o 7 1 5 888.55 888.18 226.20 o 9 1 5 504.14 591.44 95.86 o 11 1 5 129.64 63.89 99.80 o 1 3 5 641.76 751.38 100.46 o 3 3 5 555.41 497.80 70.41 o 5 3 5 966.73 1075.19 84.10 o 7 3 5 76.76 80.74 214.54 o 9 3 5 1234.09 1262.75 193.60 o 11 3 5 40.90 112.11 96.62 o 1 5 5 5421.02 5421.84 328.70 o 3 5 5 1388.56 1448.48 81.98 o 5 5 5 1262.35 1305.62 88.48 o 7 5 5 224.72 274.42 78.02 o 9 5 5 482.22 348.10 100.51 o 11 5 5 73.43 122.59 93.75 o 1 7 5 3112.96 3205.65 102.39 o 3 7 5 3998.99 3897.26 114.90 o 5 7 5 1973.72 2036.12 150.35 o 7 7 5 705.81 601.38 99.09 o 9 7 5 1158.73 1060.72 184.40 o 11 7 5 66.08 86.73 97.48 o 1 9 5 7366.90 7186.37 436.74 o 3 9 5 1097.38 1170.29 83.18 o 5 9 5 231.67 19.68 83.54 o 7 9 5 908.65 817.51 97.10 o 9 9 5 491.56 530.16 101.24 o 11 9 5 53.55 -45.81 101.60 o 1 11 5 3145.34 3082.13 112.61 o 3 11 5 842.41 778.35 81.85 o 5 11 5 2695.53 2655.09 233.61 o 7 11 5 633.06 703.46 129.83 o 9 11 5 227.78 293.60 90.90 o 11 11 5 86.18 59.83 99.51 o 1 13 5 805.73 769.80 146.26 o 3 13 5 3197.53 3223.66 136.56 o 5 13 5 404.19 395.34 112.12 o 7 13 5 78.50 95.38 91.81 o 9 13 5 233.83 377.93 98.56 o 11 13 5 45.35 114.42 112.04 o 1 15 5 1384.09 1472.83 103.27 o 3 15 5 1030.82 1032.59 150.77 o 5 15 5 706.64 790.93 140.73 o 7 15 5 312.35 383.58 165.25 o 9 15 5 24.99 61.15 97.18 o 1 17 5 115.61 -90.64 90.64 o 3 17 5 169.97 4.12 96.71 o 5 17 5 1212.37 1132.85 150.52 o 7 17 5 346.99 433.55 101.36 o 9 17 5 9.31 -12.69 100.14 o 1 19 5 1715.58 1545.74 216.41 o 3 19 5 390.70 512.09 101.59 o 5 19 5 74.21 150.44 126.85 o 7 19 5 42.33 -43.81 93.92 o 9 19 5 173.16 279.70 225.86 o 1 21 5 1113.17 935.52 158.95 o 3 21 5 827.79 864.31 112.01 o 5 21 5 274.41 249.70 101.85 o 7 21 5 136.68 146.80 353.56 o 1 23 5 254.47 282.30 103.03 o 3 23 5 36.97 141.52 250.38 o 5 23 5 29.06 67.29 118.17 o 7 23 5 104.68 50.11 143.54 o 1 25 5 148.88 147.67 154.35 o 3 25 5 225.69 176.78 112.10 o 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