#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013151.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013151_Fobs loop_ _publ_author_name 'B\"uy\"ukg\"ung\"or, Orhan' 'Odabasundefinedogundefinedlu, Mustafa' _publ_section_title ; Bis(2-aminopyridinium) maleate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o105 _journal_page_last o106 _journal_volume 59 _journal_year 2003 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 21.7560 _cell_length_b 23.5310 _cell_length_c 5.6280 _exptl_crystal_F_000 1280.00 _reflns_d_resolution_high 0.7826 _[local]_cod_data_source_file fr1408Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' samsun21 Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 343.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/4, y+1/4, z+1/4' 'x+3/4, -y+3/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x+1/4, y+3/4, z+3/4' 'x+3/4, -y+5/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+3/4, y+1/4, z+3/4' 'x+5/4, -y+3/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+3/4, y+3/4, z+1/4' 'x+5/4, -y+5/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3966.52 3633.32 20.62 o 8 0 0 53333.04 56840.92 129.61 o 12 0 0 1.75 5.42 4.09 o 16 0 0 4.84 25.70 6.51 o 20 0 0 3059.31 2892.30 44.16 o 24 0 0 150.45 142.79 15.11 o 2 2 0 1943.72 2149.57 13.00 o 4 2 0 55469.49 56716.57 108.48 o 6 2 0 2167.29 2146.15 19.87 o 8 2 0 6295.08 5884.38 37.62 o 10 2 0 21.15 13.60 4.34 o 12 2 0 5922.17 6118.92 47.41 o 14 2 0 2426.14 2486.86 32.77 o 16 2 0 72.70 74.60 7.93 o 18 2 0 12.39 0.83 6.01 o 20 2 0 17.30 18.36 7.01 o 22 2 0 0.64 16.27 7.18 o 24 2 0 681.96 676.65 25.22 o 26 2 0 441.78 457.22 22.54 o 0 4 0 5047.01 4345.27 21.85 o 2 4 0 7302.76 6198.04 28.06 o 4 4 0 3402.81 3120.76 22.30 o 6 4 0 11691.60 10417.43 47.33 o 8 4 0 1534.29 1520.77 19.87 o 10 4 0 1434.43 1429.71 21.44 o 12 4 0 1519.47 1711.99 25.61 o 14 4 0 1524.84 1441.55 25.35 o 16 4 0 39.79 32.21 6.51 o 18 4 0 53.14 56.24 8.18 o 20 4 0 2249.90 2105.58 38.08 o 22 4 0 994.47 965.09 28.07 o 24 4 0 68.45 77.52 10.85 o 26 4 0 121.20 135.61 14.69 o 2 6 0 3994.32 3357.89 24.28 o 4 6 0 33747.56 32978.29 90.56 o 6 6 0 7229.56 6864.97 40.80 o 8 6 0 1440.60 1516.82 20.94 o 10 6 0 730.79 654.27 15.30 o 12 6 0 12222.88 12754.13 72.32 o 14 6 0 17.70 27.20 5.92 o 16 6 0 9.58 3.59 5.67 o 18 6 0 36.95 16.52 7.09 o 20 6 0 3756.28 3731.74 51.32 o 22 6 0 334.70 345.16 17.61 o 24 6 0 6.21 -7.68 7.68 o 26 6 0 16.08 9.43 8.59 o 0 8 0 43927.96 46391.77 115.79 o 2 8 0 5958.33 5641.80 36.01 o 4 8 0 1538.28 1420.34 18.78 o 6 8 0 1575.51 1403.20 19.95 o 8 8 0 11397.92 11700.91 62.58 o 10 8 0 4041.95 4184.34 39.56 o 12 8 0 1674.55 1786.09 28.04 o 14 8 0 151.85 145.55 9.68 o 16 8 0 478.44 425.68 16.62 o 18 8 0 3229.74 3246.67 45.77 o 20 8 0 896.26 981.55 27.40 o 22 8 0 241.00 221.93 17.19 o 24 8 0 8.02 -5.84 8.09 o 26 8 0 81.17 112.74 13.85 o 2 10 0 10995.15 10772.36 55.79 o 4 10 0 168.34 145.25 7.43 o 6 10 0 77.65 88.21 7.09 o 8 10 0 4560.99 4467.42 40.70 o 10 10 0 1020.23 1106.53 21.74 o 12 10 0 3624.11 3932.58 43.08 o 14 10 0 795.55 852.50 21.81 o 16 10 0 821.76 853.36 23.22 o 18 10 0 210.09 186.96 18.70 o 20 10 0 238.28 291.87 16.61 o 22 10 0 2434.16 2326.22 44.69 o 24 10 0 328.45 345.73 19.78 o 26 10 0 4.93 -2.50 8.26 o 0 12 0 3285.37 3311.09 33.13 o 2 12 0 18569.87 17947.90 80.15 o 4 12 0 848.18 800.79 17.14 o 6 12 0 35.94 43.39 5.67 o 8 12 0 691.57 757.48 18.30 o 10 12 0 7.13 9.09 5.17 o 12 12 0 2678.85 2722.11 37.63 o 14 12 0 74.02 79.03 8.93 o 16 12 0 9.85 7.68 6.42 o 18 12 0 1401.03 1343.58 31.35 o 20 12 0 476.45 437.31 19.87 o 22 12 0 422.36 397.61 20.29 o 24 12 0 0.15 -8.01 8.01 o 2 14 0 5300.27 5285.12 46.05 o 4 14 0 219.49 187.73 9.68 o 6 14 0 254.68 225.22 10.85 o 8 14 0 277.39 285.17 12.44 o 10 14 0 17.40 15.19 5.84 o 12 14 0 60.02 58.58 7.93 o 14 14 0 127.88 138.45 16.27 o 16 14 0 311.48 333.48 16.36 o 18 14 0 14.51 16.85 7.93 o 20 14 0 321.28 310.26 17.61 o 22 14 0 33.98 42.30 9.43 o 24 14 0 54.71 79.02 12.18 o 0 16 0 393.83 445.21 14.86 o 2 16 0 982.09 985.23 21.73 o 4 16 0 10.52 5.01 5.17 o 6 16 0 29.63 23.45 5.92 o 8 16 0 642.86 667.03 19.46 o 10 16 0 3275.58 3148.96 42.77 o 12 16 0 0.75 -1.75 5.92 o 14 16 0 277.88 270.36 15.02 o 16 16 0 6.21 -1.59 6.84 o 18 16 0 814.95 843.65 26.98 o 20 16 0 54.88 49.40 10.68 o 22 16 0 7.71 9.35 8.51 o 2 18 0 455.23 463.84 16.37 o 4 18 0 200.38 231.45 12.44 o 6 18 0 1694.76 1708.94 31.54 o 8 18 0 4.75 7.84 6.26 o 10 18 0 1568.22 1591.12 32.45 o 12 18 0 460.91 442.17 18.28 o 14 18 0 0.89 1.75 6.59 o 16 18 0 794.85 786.59 26.14 o 18 18 0 700.85 701.37 26.05 o 20 18 0 198.17 190.53 19.53 o 22 18 0 73.11 46.73 11.27 o 0 20 0 1250.94 1371.43 29.26 o 2 20 0 1046.23 1057.79 25.66 o 4 20 0 293.04 287.99 14.36 o 6 20 0 51.54 57.66 8.43 o 8 20 0 0.85 -6.34 6.34 o 10 20 0 62.67 56.83 9.01 o 12 20 0 2110.66 2082.69 40.41 o 14 20 0 719.16 679.03 24.47 o 16 20 0 14.15 15.19 8.34 o 18 20 0 67.02 44.23 10.93 o 20 20 0 230.98 251.30 24.54 o 2 22 0 1849.90 1906.92 36.64 o 4 22 0 245.79 242.47 14.11 o 6 22 0 914.27 987.01 27.23 o 8 22 0 1084.98 1098.91 29.58 o 10 22 0 3893.67 3976.33 56.34 o 12 22 0 48.23 43.89 9.68 o 14 22 0 18.12 18.11 8.26 o 16 22 0 77.77 96.30 12.68 o 18 22 0 105.19 121.75 13.77 o 0 24 0 397.23 432.51 19.45 o 2 24 0 14.26 7.26 7.43 o 4 24 0 239.47 249.47 15.44 o 6 24 0 212.34 222.25 17.36 o 8 24 0 20.10 -5.67 8.01 o 10 24 0 416.96 422.57 20.29 o 12 24 0 126.65 136.86 14.27 o 14 24 0 161.76 170.41 18.11 o 16 24 0 89.26 99.72 13.43 o 2 26 0 190.00 167.83 20.28 o 4 26 0 4.58 15.02 7.59 o 6 26 0 5.44 0.42 7.76 o 8 26 0 201.70 207.31 22.28 o 10 26 0 9.34 8.18 8.76 o 12 26 0 90.25 91.37 11.93 o 0 28 0 339.89 314.35 19.20 o 2 28 0 27.41 23.70 9.35 o 4 28 0 37.94 55.74 10.43 o 6 28 0 108.77 105.65 13.02 o 8 28 0 203.15 211.65 25.12 o 10 28 0 203.06 216.40 22.78 o 1 1 1 2539.51 2695.38 28.83 o 3 1 1 16506.88 15765.20 170.24 o 5 1 1 5476.35 5168.70 48.92 o 7 1 1 2761.78 2507.36 43.44 o 9 1 1 6156.21 6602.10 71.16 o 11 1 1 2441.94 2616.95 39.22 o 13 1 1 555.85 585.55 11.31 o 15 1 1 1704.48 1682.70 30.46 o 17 1 1 612.34 593.11 13.29 o 19 1 1 1896.75 1841.61 24.52 o 21 1 1 45.04 47.52 6.28 o 23 1 1 594.13 615.63 32.19 o 25 1 1 67.80 75.19 8.55 o 27 1 1 20.40 24.38 7.23 o 1 3 1 30190.69 30811.64 568.17 o 3 3 1 13671.37 12970.22 120.02 o 5 3 1 1965.36 1930.56 13.97 o 7 3 1 2238.74 2375.04 22.77 o 9 3 1 3309.74 3343.03 24.78 o 11 3 1 80.23 91.59 7.55 o 13 3 1 4984.53 5285.63 33.45 o 15 3 1 1222.26 1131.13 16.94 o 17 3 1 861.91 848.66 15.89 o 19 3 1 2969.77 2857.47 35.99 o 21 3 1 573.40 616.71 40.16 o 23 3 1 309.49 293.83 12.12 o 25 3 1 550.58 571.60 18.03 o 27 3 1 247.20 301.06 31.34 o 1 5 1 118045.92 116089.22 2183.58 o 3 5 1 21851.65 20551.29 194.16 o 5 5 1 18459.24 18005.53 78.26 o 7 5 1 6084.66 6363.75 43.42 o 9 5 1 11301.89 11620.42 96.74 o 11 5 1 2104.00 2359.55 21.16 o 13 5 1 2907.42 2896.60 36.33 o 15 5 1 1629.06 1560.50 20.08 o 17 5 1 1180.33 1235.28 20.56 o 19 5 1 1668.45 1648.71 42.19 o 21 5 1 34.15 50.75 6.34 o 23 5 1 955.66 882.44 19.72 o 25 5 1 95.97 95.55 8.79 o 27 5 1 125.02 119.63 10.18 o 1 7 1 44229.40 43382.67 338.46 o 3 7 1 22060.66 22108.66 178.94 o 5 7 1 5171.96 5441.33 34.17 o 7 7 1 3816.40 3958.72 24.58 o 9 7 1 324.55 393.87 12.07 o 11 7 1 3373.24 3346.53 50.65 o 13 7 1 719.38 769.52 14.41 o 15 7 1 258.47 268.76 9.17 o 17 7 1 217.50 235.92 11.77 o 19 7 1 1484.30 1420.17 24.25 o 21 7 1 857.23 824.86 24.31 o 23 7 1 97.38 73.81 7.76 o 25 7 1 45.56 48.35 10.93 o 1 9 1 4800.93 4939.47 26.05 o 3 9 1 3588.99 3632.17 22.82 o 5 9 1 1479.36 1537.84 53.89 o 7 9 1 2450.91 2326.60 23.83 o 9 9 1 322.51 331.24 10.65 o 11 9 1 764.72 742.38 13.09 o 13 9 1 29.33 29.20 4.45 o 15 9 1 865.11 834.92 15.74 o 17 9 1 122.08 114.91 8.11 o 19 9 1 687.52 677.74 16.15 o 21 9 1 246.73 277.54 11.54 o 23 9 1 13.80 13.17 5.66 o 25 9 1 93.00 82.86 8.50 o 1 11 1 1203.66 1153.13 13.85 o 3 11 1 3709.72 3840.61 27.23 o 5 11 1 2877.80 2804.87 33.17 o 7 11 1 4621.31 4694.74 30.50 o 9 11 1 1364.41 1298.83 19.66 o 11 11 1 5691.24 5500.45 36.64 o 13 11 1 1039.51 1068.43 17.26 o 15 11 1 635.62 606.94 13.96 o 17 11 1 378.13 340.66 11.54 o 19 11 1 1631.33 1675.07 39.92 o 21 11 1 604.26 636.97 33.65 o 23 11 1 34.78 36.28 8.89 o 25 11 1 59.87 78.57 8.55 o 1 13 1 3809.18 4001.02 27.74 o 3 13 1 1572.87 1757.80 18.67 o 5 13 1 1542.47 1491.80 17.78 o 7 13 1 5327.75 5278.04 35.26 o 9 13 1 662.66 641.23 29.70 o 11 13 1 1610.97 1661.20 21.18 o 13 13 1 248.01 256.21 9.59 o 15 13 1 988.24 1026.25 25.86 o 17 13 1 282.37 263.91 10.73 o 19 13 1 249.33 253.33 11.91 o 21 13 1 611.74 640.29 22.00 o 23 13 1 226.65 237.66 19.20 o 1 15 1 1769.44 1798.85 27.63 o 3 15 1 5329.50 5331.44 46.97 o 5 15 1 985.73 983.15 15.60 o 7 15 1 1017.25 1041.73 16.46 o 9 15 1 1722.40 1662.54 24.68 o 11 15 1 1660.72 1699.96 22.56 o 13 15 1 1755.17 1654.51 23.42 o 15 15 1 503.72 444.36 13.28 o 17 15 1 730.32 738.16 17.24 o 19 15 1 274.48 288.07 19.32 o 21 15 1 360.80 348.41 17.28 o 23 15 1 117.09 106.32 9.20 o 1 17 1 3463.33 3411.35 77.58 o 3 17 1 1075.89 1066.68 16.90 o 5 17 1 908.93 890.49 15.95 o 7 17 1 18.16 18.92 4.40 o 9 17 1 1217.28 1189.78 19.33 o 11 17 1 1254.23 1226.41 20.36 o 13 17 1 2160.47 2160.07 32.43 o 15 17 1 378.17 379.02 12.81 o 17 17 1 79.17 90.88 10.72 o 19 17 1 243.28 240.54 13.44 o 21 17 1 554.33 534.14 17.29 o 1 19 1 70.10 72.33 6.22 o 3 19 1 378.58 359.77 11.01 o 5 19 1 168.79 143.75 10.87 o 7 19 1 295.90 271.14 10.21 o 9 19 1 952.49 928.23 18.14 o 11 19 1 138.45 137.73 9.97 o 13 19 1 434.04 447.62 22.87 o 15 19 1 61.60 68.95 7.22 o 17 19 1 69.68 73.63 7.64 o 19 19 1 223.78 273.30 13.82 o 21 19 1 73.40 88.15 8.91 o 1 21 1 344.48 324.47 11.24 o 3 21 1 16.10 12.53 4.69 o 5 21 1 14.75 8.56 4.89 o 7 21 1 117.12 109.36 7.70 o 9 21 1 28.96 14.77 8.93 o 11 21 1 413.75 422.53 13.78 o 13 21 1 29.96 20.92 7.47 o 15 21 1 93.91 81.18 7.94 o 17 21 1 106.09 118.51 9.44 o 19 21 1 257.10 255.89 16.45 o 1 23 1 92.35 103.42 7.61 o 3 23 1 162.28 168.15 9.40 o 5 23 1 16.94 15.96 5.25 o 7 23 1 634.31 638.76 16.56 o 9 23 1 635.98 647.48 17.09 o 11 23 1 167.15 170.69 16.61 o 13 23 1 62.51 66.79 16.98 o 15 23 1 5.07 2.96 5.66 o 17 23 1 123.57 141.36 10.44 o 1 25 1 324.72 320.29 12.51 o 3 25 1 48.73 45.74 9.30 o 5 25 1 443.90 473.86 25.63 o 7 25 1 1.50 4.58 5.31 o 9 25 1 759.20 792.78 19.66 o 11 25 1 143.44 147.93 14.40 o 13 25 1 99.25 84.71 8.67 o 1 27 1 213.62 219.69 13.90 o 3 27 1 169.60 150.39 10.22 o 5 27 1 353.13 362.24 14.13 o 7 27 1 58.24 59.66 7.91 o 9 27 1 704.00 704.02 19.75 o 11 27 1 210.58 214.83 16.33 o 1 29 1 49.00 47.51 14.94 o 3 29 1 65.82 73.39 8.32 o 5 29 1 119.26 124.18 10.00 o 2 0 2 1097.50 1154.01 11.72 o 6 0 2 36859.21 38750.29 523.11 o 10 0 2 7454.27 8212.05 63.69 o 14 0 2 12878.54 13034.21 164.73 o 18 0 2 5024.43 5008.48 150.96 o 22 0 2 1119.04 1124.07 21.97 o 26 0 2 286.43 285.64 14.39 o 0 2 2 9206.24 9374.88 47.01 o 2 2 2 8955.90 9386.48 294.98 o 4 2 2 10548.16 10754.06 124.59 o 6 2 2 1022.18 930.47 11.86 o 8 2 2 669.75 740.92 11.35 o 10 2 2 344.76 364.77 8.86 o 12 2 2 1152.94 1169.56 16.26 o 14 2 2 593.17 568.68 12.46 o 16 2 2 173.22 173.17 8.77 o 18 2 2 5511.27 5550.21 110.82 o 20 2 2 293.26 316.41 11.83 o 22 2 2 46.46 38.93 6.34 o 24 2 2 84.15 84.70 8.26 o 26 2 2 158.03 166.14 14.19 o 2 4 2 16329.68 18323.69 270.92 o 4 4 2 3094.47 3082.07 21.46 o 6 4 2 206.77 222.29 6.40 o 8 4 2 4071.55 3884.59 31.28 o 10 4 2 3092.02 3092.69 24.85 o 12 4 2 169.78 156.36 6.67 o 14 4 2 1465.46 1433.91 41.23 o 16 4 2 2786.51 2720.68 59.91 o 18 4 2 94.21 90.24 7.05 o 20 4 2 116.82 121.96 8.26 o 22 4 2 136.11 149.67 10.47 o 24 4 2 381.97 391.57 14.60 o 26 4 2 5.54 -6.39 6.39 o 0 6 2 1924.20 2230.98 25.08 o 2 6 2 4041.04 4199.52 83.42 o 4 6 2 586.26 692.60 12.87 o 6 6 2 6691.25 6993.55 78.52 o 8 6 2 1523.48 1615.25 17.49 o 10 6 2 3793.37 3664.33 35.34 o 12 6 2 198.73 217.16 11.56 o 14 6 2 1651.82 1587.61 43.21 o 16 6 2 219.02 222.18 9.23 o 18 6 2 1564.75 1553.26 24.12 o 20 6 2 65.16 70.71 6.78 o 22 6 2 104.84 107.45 8.52 o 24 6 2 304.85 302.97 14.30 o 26 6 2 68.05 91.18 9.06 o 2 8 2 3745.47 3760.84 56.20 o 4 8 2 9303.28 9581.04 108.33 o 6 8 2 7566.01 7674.91 63.94 o 8 8 2 2456.10 2547.09 22.83 o 10 8 2 158.75 213.16 7.55 o 12 8 2 350.87 367.36 10.18 o 14 8 2 1400.69 1359.27 31.78 o 16 8 2 2174.97 2119.96 59.30 o 18 8 2 39.05 35.56 8.59 o 20 8 2 7.55 5.56 8.47 o 22 8 2 32.66 23.87 6.17 o 24 8 2 32.49 24.13 6.70 o 0 10 2 23612.15 25072.83 98.57 o 2 10 2 6290.28 6055.02 57.72 o 4 10 2 12866.82 13272.12 197.85 o 6 10 2 1667.44 1664.35 18.65 o 8 10 2 242.13 237.45 7.82 o 10 10 2 214.93 254.56 17.90 o 12 10 2 3976.46 3990.78 50.09 o 14 10 2 1095.09 1013.52 42.20 o 16 10 2 453.25 440.92 12.93 o 18 10 2 555.41 503.48 14.20 o 20 10 2 792.01 756.36 20.25 o 22 10 2 151.06 145.06 10.05 o 24 10 2 12.49 18.54 6.66 o 2 12 2 3581.58 3554.07 27.24 o 4 12 2 5362.18 5228.27 33.73 o 6 12 2 2735.64 2718.82 53.62 o 8 12 2 489.20 522.07 19.67 o 10 12 2 1711.60 1682.73 21.39 o 12 12 2 3930.89 3923.33 33.98 o 14 12 2 1923.09 1838.30 27.99 o 16 12 2 2437.40 2347.99 41.35 o 18 12 2 16.37 17.52 5.63 o 20 12 2 656.47 646.36 17.39 o 22 12 2 238.78 238.00 14.91 o 24 12 2 80.16 96.20 9.06 o 0 14 2 507.79 471.69 15.45 o 2 14 2 1063.62 1037.55 15.93 o 4 14 2 1053.64 1049.94 16.22 o 6 14 2 709.05 752.67 19.05 o 8 14 2 745.93 736.94 14.50 o 10 14 2 240.69 234.25 9.18 o 12 14 2 522.38 513.77 13.34 o 14 14 2 93.57 108.09 7.64 o 16 14 2 253.86 242.10 11.39 o 18 14 2 141.76 160.18 14.77 o 20 14 2 64.86 66.01 7.67 o 22 14 2 4.62 5.58 11.43 o 2 16 2 375.23 409.09 11.01 o 4 16 2 285.51 321.98 15.36 o 6 16 2 370.46 335.76 15.32 o 8 16 2 638.67 612.11 14.08 o 10 16 2 31.37 37.74 6.26 o 12 16 2 714.91 710.85 16.06 o 14 16 2 24.39 30.18 5.54 o 16 16 2 204.49 205.27 24.24 o 18 16 2 121.26 106.62 8.97 o 20 16 2 332.76 368.75 14.43 o 22 16 2 64.15 69.38 8.37 o 0 18 2 2817.79 2860.98 41.39 o 2 18 2 3.93 5.01 4.21 o 4 18 2 1531.15 1574.33 22.23 o 6 18 2 1700.12 1670.89 23.30 o 8 18 2 1672.08 1692.98 24.01 o 10 18 2 133.91 130.96 9.68 o 12 18 2 172.98 157.82 12.33 o 14 18 2 98.23 95.06 7.99 o 16 18 2 94.12 89.03 8.02 o 18 18 2 87.14 84.21 8.32 o 20 18 2 331.60 355.65 14.69 o 2 20 2 1353.11 1331.56 21.52 o 4 20 2 84.93 89.83 9.51 o 6 20 2 686.13 683.90 16.12 o 8 20 2 1171.46 1144.68 21.06 o 10 20 2 480.75 475.37 29.76 o 12 20 2 36.49 22.63 6.02 o 14 20 2 311.57 360.29 19.45 o 16 20 2 276.50 272.96 13.55 o 18 20 2 2.78 6.44 6.55 o 0 22 2 1065.29 1055.35 28.91 o 2 22 2 89.63 84.30 7.20 o 4 22 2 1302.28 1308.92 22.72 o 6 22 2 526.03 502.25 14.79 o 8 22 2 333.98 354.15 12.98 o 10 22 2 115.36 111.51 8.35 o 12 22 2 165.67 160.65 11.31 o 14 22 2 197.87 195.66 13.27 o 16 22 2 298.65 325.84 13.69 o 2 24 2 71.80 79.30 7.34 o 4 24 2 65.11 62.79 7.08 o 6 24 2 68.50 65.20 7.38 o 8 24 2 202.37 201.68 14.58 o 10 24 2 105.67 97.56 8.67 o 12 24 2 43.70 54.09 7.34 o 14 24 2 71.01 85.15 16.56 o 0 26 2 23.96 34.21 9.18 o 2 26 2 294.29 317.66 13.10 o 4 26 2 164.77 161.80 10.70 o 6 26 2 73.58 75.79 8.01 o 8 26 2 22.56 10.12 6.24 o 10 26 2 34.20 22.95 10.26 o 2 28 2 35.86 27.91 7.31 o 4 28 2 49.84 41.61 7.55 o 6 28 2 176.56 158.45 11.09 o 1 1 3 1671.28 1712.31 17.35 o 3 1 3 4421.58 4656.24 62.98 o 5 1 3 10780.51 11105.62 46.42 o 7 1 3 1752.06 1782.96 21.81 o 9 1 3 721.46 800.54 24.61 o 11 1 3 222.05 214.67 10.27 o 13 1 3 1893.38 1828.51 22.87 o 15 1 3 216.31 225.15 9.12 o 17 1 3 169.71 166.63 18.94 o 19 1 3 278.50 267.15 11.11 o 21 1 3 237.64 249.91 13.58 o 23 1 3 74.92 75.26 8.80 o 25 1 3 75.83 75.23 8.57 o 1 3 3 529.24 599.40 10.63 o 3 3 3 3183.50 3355.92 134.42 o 5 3 3 1574.34 1823.33 30.05 o 7 3 3 7365.68 7692.69 42.86 o 9 3 3 2121.16 2330.53 37.23 o 11 3 3 212.17 216.49 8.23 o 13 3 3 1578.30 1606.39 73.15 o 15 3 3 1272.42 1231.59 22.95 o 17 3 3 452.92 445.63 13.19 o 19 3 3 694.83 698.64 32.28 o 21 3 3 96.93 114.17 8.49 o 23 3 3 19.42 8.51 15.19 o 25 3 3 12.04 4.67 7.26 o 1 5 3 1356.21 1487.86 16.80 o 3 5 3 2535.38 2801.54 57.29 o 5 5 3 2034.13 2237.19 37.87 o 7 5 3 899.17 806.87 32.01 o 9 5 3 339.04 330.20 9.42 o 11 5 3 144.90 132.89 9.54 o 13 5 3 153.89 145.04 20.61 o 15 5 3 2554.47 2548.98 65.27 o 17 5 3 4769.58 4728.59 121.28 o 19 5 3 816.22 760.23 18.06 o 21 5 3 16.71 10.90 11.43 o 23 5 3 92.94 111.88 9.32 o 1 7 3 80.22 58.23 4.57 o 3 7 3 388.24 348.87 16.83 o 5 7 3 5497.27 5679.23 120.01 o 7 7 3 2764.30 2766.16 57.56 o 9 7 3 206.19 188.83 7.67 o 11 7 3 735.23 763.63 15.70 o 13 7 3 7096.88 7210.33 46.77 o 15 7 3 4560.06 4397.25 92.44 o 17 7 3 10.10 17.71 5.43 o 19 7 3 761.74 742.94 43.47 o 21 7 3 37.14 44.06 8.72 o 23 7 3 100.20 113.39 22.36 o 1 9 3 1251.10 1258.68 16.74 o 3 9 3 1160.30 1173.48 16.41 o 5 9 3 6.62 5.96 3.73 o 7 9 3 842.27 760.44 30.29 o 9 9 3 433.20 441.88 17.62 o 11 9 3 793.75 805.41 15.74 o 13 9 3 236.18 209.86 9.81 o 15 9 3 547.77 579.70 14.85 o 17 9 3 611.60 571.35 18.41 o 19 9 3 52.78 53.11 9.97 o 21 9 3 77.56 90.23 8.44 o 23 9 3 184.08 238.82 35.76 o 1 11 3 67.54 56.21 5.07 o 3 11 3 330.32 322.12 9.44 o 5 11 3 180.48 195.39 12.44 o 7 11 3 387.59 344.50 10.27 o 9 11 3 4.85 9.64 4.07 o 11 11 3 329.76 332.30 11.07 o 13 11 3 344.83 355.68 11.71 o 15 11 3 150.48 130.15 8.73 o 17 11 3 291.86 247.16 23.37 o 19 11 3 187.68 180.18 14.31 o 21 11 3 107.96 120.13 9.23 o 23 11 3 16.34 27.82 6.99 o 1 13 3 1854.20 1796.34 22.01 o 3 13 3 719.98 722.26 14.38 o 5 13 3 592.32 582.85 13.29 o 7 13 3 2094.09 2084.19 55.16 o 9 13 3 259.14 276.23 15.57 o 11 13 3 321.37 339.17 11.39 o 13 13 3 146.44 145.11 10.60 o 15 13 3 756.10 686.97 24.55 o 17 13 3 427.02 474.02 23.92 o 19 13 3 211.57 203.13 14.95 o 21 13 3 48.79 51.89 7.58 o 1 15 3 291.87 290.38 10.39 o 3 15 3 4611.58 4577.11 59.61 o 5 15 3 5960.19 6015.20 43.00 o 7 15 3 1461.26 1396.53 33.95 o 9 15 3 145.93 141.50 9.81 o 11 15 3 382.85 417.28 12.93 o 13 15 3 334.52 320.26 11.98 o 15 15 3 1012.80 994.99 20.72 o 17 15 3 84.20 95.02 8.29 o 19 15 3 76.94 65.32 9.30 o 21 15 3 31.93 26.56 18.94 o 1 17 3 380.62 362.68 11.63 o 3 17 3 1218.08 1093.05 19.81 o 5 17 3 794.66 797.29 16.77 o 7 17 3 772.31 725.32 16.42 o 9 17 3 1332.62 1372.15 22.84 o 11 17 3 78.03 77.35 7.97 o 13 17 3 154.14 169.66 11.74 o 15 17 3 130.94 129.26 9.26 o 17 17 3 108.73 100.67 8.91 o 19 17 3 147.72 154.75 11.01 o 1 19 3 166.31 153.92 10.18 o 3 19 3 668.51 613.01 28.19 o 5 19 3 476.81 493.74 30.22 o 7 19 3 55.57 61.29 7.59 o 9 19 3 4.82 1.11 11.18 o 11 19 3 34.45 38.32 6.28 o 13 19 3 47.11 39.02 7.02 o 15 19 3 284.19 278.40 12.78 o 17 19 3 457.59 490.01 23.71 o 1 21 3 483.47 469.66 20.66 o 3 21 3 98.45 106.48 8.05 o 5 21 3 245.69 234.12 12.94 o 7 21 3 207.74 191.95 14.75 o 9 21 3 137.58 127.54 9.44 o 11 21 3 51.63 54.46 7.37 o 13 21 3 128.87 124.08 9.73 o 15 21 3 225.05 227.92 32.34 o 1 23 3 441.90 432.79 14.70 o 3 23 3 503.30 522.52 16.99 o 5 23 3 794.86 788.89 24.64 o 7 23 3 239.25 234.67 15.86 o 9 23 3 12.58 9.01 6.02 o 11 23 3 6.15 19.49 6.30 o 13 23 3 25.60 25.01 7.26 o 1 25 3 90.27 91.67 8.44 o 3 25 3 296.31 349.20 18.28 o 5 25 3 244.47 211.66 16.78 o 7 25 3 277.07 258.28 18.74 o 9 25 3 89.99 94.90 8.85 o 1 27 3 69.02 53.70 8.14 o 3 27 3 68.70 66.06 10.14 o 0 0 4 1298.83 1227.82 24.67 o 4 0 4 916.11 905.81 15.45 o 8 0 4 1508.53 1566.33 21.11 o 12 0 4 1674.19 1617.34 56.24 o 16 0 4 1569.18 1581.30 25.03 o 20 0 4 773.09 786.13 31.44 o 2 2 4 920.95 922.90 19.14 o 4 2 4 3193.78 3313.60 94.29 o 6 2 4 112.99 98.57 7.07 o 8 2 4 271.34 270.77 18.95 o 10 2 4 41.88 30.56 5.04 o 12 2 4 1197.68 1152.86 19.65 o 14 2 4 1014.05 963.23 40.27 o 16 2 4 2245.88 2141.54 79.53 o 18 2 4 104.89 90.30 10.47 o 20 2 4 99.58 87.81 8.37 o 22 2 4 57.68 63.02 8.26 o 0 4 4 1181.87 1182.11 24.50 o 2 4 4 816.84 777.34 14.36 o 4 4 4 2178.21 2313.96 63.22 o 6 4 4 471.64 480.15 15.28 o 8 4 4 719.86 722.66 14.82 o 10 4 4 8.70 6.84 4.72 o 12 4 4 408.08 433.19 12.66 o 14 4 4 1187.81 1270.61 21.77 o 16 4 4 126.44 120.33 8.37 o 18 4 4 324.72 300.90 12.58 o 20 4 4 26.92 33.93 9.89 o 22 4 4 160.81 192.73 17.07 o 2 6 4 597.25 631.34 13.32 o 4 6 4 1196.37 1226.44 20.77 o 6 6 4 1719.22 1672.86 42.67 o 8 6 4 46.60 50.28 5.60 o 10 6 4 152.18 168.91 15.15 o 12 6 4 46.92 52.76 6.04 o 14 6 4 434.62 395.04 12.90 o 16 6 4 73.09 67.37 7.05 o 18 6 4 164.49 160.80 12.28 o 20 6 4 4.94 -6.80 6.80 o 22 6 4 38.17 31.67 7.43 o 0 8 4 1856.18 1851.01 31.97 o 2 8 4 1901.95 1840.56 22.66 o 4 8 4 2078.65 2093.33 52.99 o 6 8 4 1461.66 1548.57 30.31 o 8 8 4 1077.73 1096.96 18.82 o 10 8 4 915.45 837.56 31.12 o 12 8 4 144.79 146.12 9.41 o 14 8 4 7.42 4.25 5.55 o 16 8 4 260.05 291.01 15.65 o 18 8 4 95.63 79.63 14.35 o 20 8 4 301.96 296.55 16.94 o 2 10 4 2965.97 3118.32 30.28 o 4 10 4 880.97 894.42 16.81 o 6 10 4 2520.00 2636.11 65.19 o 8 10 4 965.94 892.08 34.21 o 10 10 4 431.93 498.89 17.20 o 12 10 4 372.16 338.90 11.98 o 14 10 4 1886.37 1771.91 27.00 o 16 10 4 821.66 804.72 48.57 o 18 10 4 113.35 127.48 9.81 o 20 10 4 108.33 116.29 9.68 o 0 12 4 737.42 672.31 21.13 o 2 12 4 646.94 630.27 14.56 o 4 12 4 2256.15 2198.59 67.26 o 6 12 4 1736.58 1671.33 29.90 o 8 12 4 6.84 13.09 7.01 o 10 12 4 757.01 733.23 26.85 o 12 12 4 371.35 423.95 29.47 o 14 12 4 1078.23 1078.78 21.65 o 16 12 4 240.51 257.65 14.44 o 18 12 4 756.52 756.34 19.90 o 20 12 4 133.28 148.01 10.98 o 2 14 4 341.65 313.58 11.15 o 4 14 4 46.95 23.39 6.43 o 6 14 4 124.65 120.81 8.17 o 8 14 4 19.89 21.52 5.43 o 10 14 4 163.33 178.59 13.30 o 12 14 4 225.98 253.49 11.33 o 14 14 4 624.45 643.43 17.53 o 16 14 4 275.81 314.37 13.40 o 18 14 4 149.59 176.01 11.85 o 0 16 4 749.57 830.86 25.22 o 2 16 4 539.00 516.09 14.41 o 4 16 4 36.26 50.78 6.05 o 6 16 4 305.79 301.13 11.92 o 8 16 4 62.38 65.07 7.02 o 10 16 4 86.09 78.66 10.14 o 12 16 4 109.45 115.61 8.84 o 14 16 4 330.30 363.66 14.22 o 16 16 4 97.86 97.87 10.64 o 2 18 4 246.22 270.65 14.36 o 4 18 4 86.48 69.79 7.37 o 6 18 4 1378.34 1257.12 26.83 o 8 18 4 175.70 153.82 11.54 o 10 18 4 83.32 108.46 8.82 o 12 18 4 4.39 0.42 5.52 o 14 18 4 271.10 282.13 13.28 o 16 18 4 198.60 197.79 24.04 o 0 20 4 483.56 429.03 20.45 o 2 20 4 197.34 170.44 11.57 o 4 20 4 155.74 106.40 22.16 o 6 20 4 292.46 273.59 12.10 o 8 20 4 203.83 215.64 22.03 o 10 20 4 63.68 67.19 8.02 o 12 20 4 124.63 146.35 10.32 o 2 22 4 142.31 132.49 9.53 o 4 22 4 395.39 380.21 14.58 o 6 22 4 188.24 193.16 13.69 o 8 22 4 87.21 81.01 8.16 o 10 22 4 68.71 69.96 8.67 o 0 24 4 192.30 230.42 24.62 o 2 24 4 161.06 151.35 10.81 o 4 24 4 181.84 196.93 13.59 o 6 24 4 145.94 151.41 10.86 o 1 1 5 1353.17 1359.35 29.80 o 3 1 5 193.08 176.03 9.91 o 5 1 5 1398.49 1412.79 25.54 o 7 1 5 175.41 170.28 12.10 o 9 1 5 40.88 43.10 6.05 o 11 1 5 107.11 101.09 8.18 o 13 1 5 248.39 224.72 11.52 o 15 1 5 150.01 143.38 10.30 o 17 1 5 65.98 64.39 7.59 o 19 1 5 153.74 154.92 10.90 o 1 3 5 2435.38 2447.08 50.61 o 3 3 5 1481.23 1432.05 22.45 o 5 3 5 194.53 223.72 14.90 o 7 3 5 8.21 -4.09 4.90 o 9 3 5 130.86 125.36 8.78 o 11 3 5 1002.98 947.93 19.91 o 13 3 5 317.60 292.26 11.89 o 15 3 5 976.62 910.11 21.05 o 17 3 5 328.40 342.42 32.59 o 19 3 5 56.69 61.03 8.26 o 1 5 5 260.80 276.97 10.51 o 3 5 5 2967.19 2882.89 31.16 o 5 5 5 821.13 844.70 19.50 o 7 5 5 505.89 494.92 20.92 o 9 5 5 47.41 46.38 6.08 o 11 5 5 910.59 894.05 19.67 o 13 5 5 49.90 26.86 14.27 o 15 5 5 71.88 75.84 7.79 o 17 5 5 196.54 216.15 14.88 o 19 5 5 44.54 29.36 7.41 o 1 7 5 1525.17 1514.22 23.06 o 3 7 5 610.83 591.30 14.97 o 5 7 5 1391.21 1323.62 36.82 o 7 7 5 256.71 250.40 10.68 o 9 7 5 506.37 517.76 21.29 o 11 7 5 61.92 64.33 7.05 o 13 7 5 40.37 38.84 6.40 o 15 7 5 98.40 95.05 8.55 o 17 7 5 100.39 111.19 9.20 o 1 9 5 126.86 139.29 9.97 o 3 9 5 94.19 112.54 7.87 o 5 9 5 38.54 27.83 5.93 o 7 9 5 152.51 135.94 9.73 o 9 9 5 35.92 47.78 6.58 o 11 9 5 10.82 1.79 5.55 o 13 9 5 98.23 97.18 8.17 o 15 9 5 17.10 17.56 6.42 o 17 9 5 329.04 362.53 15.08 o 1 11 5 281.30 277.91 11.07 o 3 11 5 269.72 270.92 16.61 o 5 11 5 359.39 352.10 17.03 o 7 11 5 50.68 57.17 6.78 o 9 11 5 296.74 282.91 20.53 o 11 11 5 43.28 40.51 13.77 o 13 11 5 198.76 239.07 12.45 o 15 11 5 128.35 138.63 9.97 o 17 11 5 168.80 182.08 11.92 o 1 13 5 190.19 168.38 12.41 o 3 13 5 62.17 56.03 6.81 o 5 13 5 159.28 143.15 13.10 o 7 13 5 5.08 -2.57 10.18 o 9 13 5 391.31 347.06 13.28 o 11 13 5 90.86 91.62 9.14 o 13 13 5 109.98 120.58 9.43 o 15 13 5 2.47 -0.97 6.59 o 1 15 5 422.78 412.42 14.14 o 3 15 5 46.94 67.20 7.29 o 5 15 5 281.82 250.01 19.82 o 7 15 5 79.61 49.61 16.02 o 9 15 5 379.22 344.78 14.36 o 11 15 5 152.27 174.17 11.33 o 13 15 5 23.93 24.89 7.17 o 1 17 5 151.74 164.64 11.93 o 3 17 5 125.13 141.38 9.85 o 5 17 5 149.24 146.30 10.24 o 7 17 5 20.36 13.68 6.32 o 9 17 5 42.86 35.48 6.96 o 11 17 5 213.02 249.84 19.06 o 1 19 5 453.00 480.70 31.51 o 3 19 5 54.16 60.83 14.69 o 5 19 5 124.07 147.90 13.89 o 7 19 5 74.54 86.34 24.24 o 9 19 5 154.93 182.25 12.07 o 1 21 5 36.51 51.19 7.91 o 3 21 5 126.14 126.61 10.15 o 2 0 6 3955.67 3978.35 123.16 o 6 0 6 303.16 289.80 12.25 o 10 0 6 284.50 266.71 12.38 o 14 0 6 33.40 19.72 8.05 o 0 2 6 64.97 94.13 11.35 o 2 2 6 1668.78 1649.29 26.39 o 4 2 6 253.66 257.51 11.63 o 6 2 6 80.62 66.50 7.41 o 8 2 6 4.52 8.30 10.56 o 10 2 6 392.92 370.07 14.01 o 12 2 6 23.10 25.05 6.66 o 14 2 6 15.60 15.34 6.13 o 2 4 6 1.21 2.30 5.44 o 4 4 6 13.34 15.24 12.06 o 6 4 6 117.08 117.59 8.88 o 8 4 6 98.15 99.13 8.50 o 10 4 6 9.47 10.09 5.63 o 12 4 6 9.29 6.82 12.35 o 14 4 6 17.92 29.73 6.87 o 0 6 6 629.91 641.37 24.30 o 2 6 6 305.92 324.41 12.83 o 4 6 6 500.39 528.41 15.79 o 6 6 6 55.95 64.48 7.40 o 8 6 6 132.54 132.79 9.56 o 10 6 6 62.93 74.27 8.08 o 12 6 6 53.96 49.17 7.72 o 14 6 6 183.87 164.90 12.60 o 2 8 6 629.85 667.97 17.77 o 4 8 6 78.88 74.65 7.76 o 6 8 6 29.45 16.11 6.31 o 8 8 6 159.73 154.39 11.25 o 10 8 6 449.75 444.48 15.85 o 12 8 6 33.04 30.80 8.22 o 0 10 6 721.52 696.20 26.05 o 2 10 6 1.04 9.61 5.28 o 4 10 6 26.72 28.20 10.43 o 6 10 6 178.52 187.71 13.68 o 8 10 6 30.15 33.76 6.90 o 10 10 6 150.54 216.24 30.13 o 12 10 6 78.10 70.38 8.20 o 2 12 6 82.63 99.86 8.79 o 4 12 6 345.65 355.03 14.16 o 6 12 6 14.45 15.13 11.81 o 8 12 6 135.64 114.02 9.70 o 10 12 6 207.68 219.72 22.58 o 0 14 6 838.76 967.77 31.90 o 2 14 6 194.32 192.65 13.42 o 4 14 6 1.01 5.94 8.30 o 6 14 6 38.93 52.77 7.55 o 8 14 6 36.55 63.18 10.39 o 2 16 6 176.65 163.88 11.54 o 4 16 6 96.33 99.47 13.02 o 1 1 7 24.69 27.99 7.17 o 3 1 7 95.54 98.84 10.26 o 5 1 7 44.37 47.50 7.96 o 1 3 7 266.42 249.38 18.92 o 3 3 7 87.54 80.30 8.85 o 5 3 7 4.76 2.21 6.31 o 1 5 7 50.62 43.28 7.60 o 3 5 7 570.97 580.44 18.48 o