#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015208.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2015208_Fobs
loop_
_publ_author_name
'Nichol, Gary S.'
'Clegg, William'
_publ_section_title
;
 Hydrogen-bonding and carbonyl--carbonyl interactions in violuric acid
 methanol solvate
;
_journal_coeditor_code           SK1883
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              o718
_journal_page_last               o721
_journal_volume                  61
_journal_year                    2005
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                100.474
_cell_angle_beta                 102.939
_cell_angle_gamma                99.823
_cell_length_a                   4.9650
_cell_length_b                   8.6210
_cell_length_c                   10.2610
_exptl_crystal_F_000             196.00
_reflns_d_resolution_high        0.8302
_[local]_cod_data_source_file    sk1883Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '   gsn108 in P -1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            34.45
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
3 0 0 203.14 196.73 1.86 o
4 0 0 3.73 3.96 0.50 o
5 0 0 34.20 36.11 1.14 o
-5 1 0 13.17 12.51 0.91 o
-4 1 0 3.21 5.32 0.51 o
-3 1 0 589.74 623.44 5.84 o
-2 1 0 398.42 410.35 3.15 o
-1 1 0 1.30 2.73 0.18 o
2 1 0 12.39 8.53 0.51 o
3 1 0 1.49 2.26 0.36 o
4 1 0 156.26 153.11 2.36 o
5 1 0 17.37 18.29 0.91 o
-5 2 0 5.01 6.59 0.63 o
-4 2 0 115.53 113.46 1.92 o
-3 2 0 113.97 131.58 1.70 o
-1 2 0 147.28 156.27 1.82 o
0 2 0 265.87 218.21 4.50 o
2 2 0 55.43 51.17 0.76 o
3 2 0 47.21 43.79 1.05 o
4 2 0 0.01 -0.06 0.30 o
5 2 0 8.00 8.29 0.70 o
-5 3 0 84.47 81.52 1.74 o
-4 3 0 7.38 7.02 0.56 o
-3 3 0 17.03 19.10 0.52 o
-2 3 0 14.53 23.45 0.50 o
-1 3 0 262.96 265.59 2.15 o
0 3 0 1.98 4.09 0.30 o
1 3 0 90.06 94.44 1.07 o
2 3 0 4.18 6.57 0.36 o
3 3 0 28.59 29.86 1.36 o
4 3 0 3.76 3.72 1.00 o
5 3 0 0.71 1.79 0.50 o
-5 4 0 1.35 1.31 0.43 o
-4 4 0 119.71 121.75 2.01 o
-3 4 0 4.29 4.53 0.36 o
-2 4 0 3.05 3.92 0.28 o
-1 4 0 105.77 107.88 2.27 o
0 4 0 11.13 11.95 0.37 o
1 4 0 30.17 29.31 0.60 o
2 4 0 0.07 0.47 0.28 o
3 4 0 1.82 1.78 0.61 o
4 4 0 0.87 1.39 0.41 o
-5 5 0 8.34 6.34 1.10 o
-4 5 0 3.99 3.65 0.47 o
-3 5 0 26.08 31.92 0.73 o
-2 5 0 19.80 18.78 0.50 o
-1 5 0 49.86 50.17 0.80 o
0 5 0 210.55 197.03 1.89 o
1 5 0 27.67 29.63 0.67 o
2 5 0 8.94 10.48 0.49 o
3 5 0 23.46 24.64 0.96 o
4 5 0 0.09 0.11 0.33 o
-5 6 0 0.24 0.21 0.71 o
-4 6 0 4.20 4.55 0.87 o
-3 6 0 15.14 18.61 0.81 o
-2 6 0 5.82 5.62 0.43 o
-1 6 0 49.95 49.53 0.86 o
0 6 0 1.57 1.36 0.25 o
1 6 0 9.25 10.53 0.46 o
2 6 0 9.16 9.73 0.55 o
3 6 0 20.17 19.28 0.88 o
-5 7 0 7.70 7.71 1.12 o
-4 7 0 0.67 0.38 0.44 o
-3 7 0 0.20 1.27 0.44 o
-2 7 0 25.17 23.73 1.26 o
-1 7 0 0.91 1.65 0.77 o
0 7 0 0.89 1.54 0.29 o
1 7 0 20.64 20.67 0.62 o
2 7 0 0.29 0.29 0.30 o
-4 8 0 10.23 6.18 1.01 o
-3 8 0 19.16 20.79 1.04 o
-2 8 0 38.10 38.37 1.17 o
-1 8 0 1.89 2.78 0.49 o
0 8 0 16.35 15.83 1.16 o
1 8 0 18.49 18.69 0.80 o
2 8 0 52.90 54.33 1.97 o
-3 9 0 13.23 14.56 0.87 o
-2 9 0 105.78 105.32 2.04 o
-1 9 0 311.68 355.50 4.39 o
0 9 0 7.94 9.37 1.06 o
1 9 0 12.25 12.63 1.02 o
-2 10 0 4.26 2.97 0.58 o
-1 10 0 154.85 171.16 3.97 o
0 -10 1 1.74 1.38 0.70 o
1 -10 1 12.12 14.61 1.22 o
2 -10 1 4.80 5.68 1.00 o
-1 -9 1 0.65 0.35 0.59 o
0 -9 1 0.91 1.00 0.65 o
1 -9 1 15.14 16.01 1.40 o
2 -9 1 0.64 0.46 0.43 o
3 -9 1 0.80 0.49 0.49 o
-2 -8 1 2.85 3.36 1.10 o
-1 -8 1 0.34 0.36 0.39 o
0 -8 1 23.28 21.81 0.82 o
1 -8 1 3.96 4.01 0.54 o
2 -8 1 6.20 5.58 0.56 o
3 -8 1 9.79 8.91 0.73 o
4 -8 1 0.99 0.75 0.70 o
-3 -7 1 5.55 7.65 0.96 o
-2 -7 1 3.36 2.35 0.65 o
-1 -7 1 35.47 34.86 0.81 o
0 -7 1 3.48 4.50 0.37 o
1 -7 1 0.07 -0.30 0.23 o
2 -7 1 20.99 21.96 0.85 o
3 -7 1 9.43 7.51 0.65 o
4 -7 1 3.41 3.24 0.85 o
-3 -6 1 2.15 0.86 0.56 o
-2 -6 1 16.25 15.77 0.56 o
-1 -6 1 0.10 -0.12 0.20 o
0 -6 1 24.11 21.05 0.57 o
1 -6 1 42.73 43.94 0.79 o
2 -6 1 26.87 25.40 0.64 o
3 -6 1 170.68 160.43 1.86 o
4 -6 1 0.00 -0.45 0.51 o
5 -6 1 0.26 -0.31 0.66 o
-3 -5 1 13.20 12.99 0.76 o
-2 -5 1 39.07 36.65 0.76 o
-1 -5 1 9.87 8.22 0.43 o
0 -5 1 77.24 73.97 1.00 o
1 -5 1 43.23 40.95 0.71 o
2 -5 1 5.21 3.97 0.30 o
3 -5 1 7.17 7.59 0.44 o
4 -5 1 185.08 158.63 2.42 o
5 -5 1 68.81 63.96 1.60 o
-4 -4 1 10.71 15.00 1.24 o
-3 -4 1 3.14 4.04 0.38 o
-2 -4 1 334.01 321.91 2.83 o
-1 -4 1 1.73 1.55 0.26 o
0 -4 1 100.77 101.81 1.11 o
2 -4 1 227.41 259.50 2.76 o
3 -4 1 257.19 276.09 2.60 o
4 -4 1 10.30 9.22 0.61 o
5 -4 1 129.30 122.57 2.24 o
-5 -3 1 43.72 50.56 1.41 o
-4 -3 1 0.00 -0.14 0.94 o
-3 -3 1 0.81 0.91 0.26 o
-2 -3 1 762.50 740.35 6.89 o
-1 -3 1 465.84 443.04 4.19 o
0 -3 1 136.13 139.45 1.29 o
1 -3 1 501.21 492.86 4.57 o
2 -3 1 577.97 705.25 5.23 o
3 -3 1 10.51 13.76 0.45 o
4 -3 1 16.99 17.35 0.77 o
5 -3 1 14.07 14.96 0.81 o
-5 -2 1 0.01 0.10 0.52 o
-4 -2 1 23.24 24.30 0.89 o
-3 -2 1 286.87 273.57 2.57 o
-2 -2 1 217.22 218.49 1.98 o
2 -2 1 445.60 502.86 4.34 o
3 -2 1 41.20 39.82 0.73 o
4 -2 1 85.29 87.08 2.82 o
5 -2 1 26.30 24.42 0.99 o
-5 -1 1 1.42 2.44 0.50 o
-4 -1 1 231.74 235.22 3.08 o
-3 -1 1 215.52 215.46 2.10 o
-2 -1 1 62.81 62.50 0.83 o
1 -1 1 79.96 79.24 1.06 o
2 -1 1 6.83 8.90 0.43 o
3 -1 1 410.63 428.78 4.51 o
4 -1 1 51.81 47.63 1.22 o
5 -1 1 0.90 0.28 0.34 o
-5 0 1 21.41 22.57 1.04 o
-4 0 1 56.76 55.97 1.28 o
-3 0 1 345.42 340.78 2.89 o
-2 0 1 25.24 25.00 0.52 o
2 0 1 105.56 104.38 1.51 o
3 0 1 4.23 4.95 0.44 o
4 0 1 23.05 23.09 0.87 o
5 0 1 13.13 11.55 0.72 o
-5 1 1 4.21 2.52 0.45 o
-4 1 1 27.69 27.40 0.91 o
-3 1 1 24.86 25.30 0.57 o
-1 1 1 88.71 89.25 1.09 o
1 1 1 29.82 26.21 0.42 o
2 1 1 130.96 137.23 1.30 o
3 1 1 22.08 22.40 0.95 o
4 1 1 21.73 20.15 0.81 o
5 1 1 2.87 1.79 0.45 o
-5 2 1 65.45 56.88 1.41 o
-4 2 1 0.05 -0.01 0.27 o
-3 2 1 3.55 4.59 0.40 o
-2 2 1 343.33 492.47 8.15 o
-1 2 1 190.72 195.43 2.09 o
0 2 1 83.08 97.04 0.93 o
1 2 1 76.96 69.57 0.84 o
2 2 1 13.27 13.38 0.56 o
3 2 1 0.36 0.50 0.32 o
4 2 1 0.28 0.34 0.36 o
5 2 1 10.79 10.12 0.76 o
-5 3 1 6.10 3.99 0.52 o
-4 3 1 20.24 19.81 0.76 o
-3 3 1 18.43 23.94 0.59 o
-2 3 1 32.14 34.86 0.60 o
0 3 1 102.00 103.47 1.06 o
1 3 1 30.91 32.90 0.62 o
2 3 1 190.42 185.72 1.84 o
3 3 1 0.33 0.46 0.31 o
4 3 1 7.72 7.40 0.63 o
-5 4 1 5.94 6.38 0.61 o
-4 4 1 29.60 30.80 0.76 o
-3 4 1 9.37 11.65 0.52 o
-2 4 1 180.13 196.40 2.46 o
-1 4 1 1.57 1.94 0.24 o
0 4 1 67.53 64.88 0.86 o
1 4 1 68.97 59.22 0.90 o
2 4 1 81.63 87.25 1.50 o
3 4 1 38.08 38.45 1.08 o
4 4 1 11.80 13.21 0.77 o
-5 5 1 6.00 5.17 1.01 o
-4 5 1 1.24 1.55 0.45 o
-3 5 1 39.74 43.33 1.14 o
-2 5 1 13.65 17.93 0.46 o
-1 5 1 1.99 3.36 0.26 o
0 5 1 109.17 107.56 1.26 o
1 5 1 10.37 8.78 0.42 o
2 5 1 0.08 -0.15 0.23 o
3 5 1 70.18 70.67 1.49 o
4 5 1 16.84 17.58 0.88 o
-5 6 1 9.37 9.50 1.25 o
-4 6 1 75.10 81.54 1.75 o
-3 6 1 50.79 52.15 1.30 o
-2 6 1 2.13 2.54 0.44 o
-1 6 1 67.18 64.04 1.29 o
0 6 1 60.75 64.46 1.01 o
1 6 1 219.20 202.75 2.61 o
2 6 1 27.14 29.68 1.45 o
3 6 1 5.47 5.81 0.55 o
-5 7 1 0.27 0.00 0.74 o
-4 7 1 24.97 27.91 1.08 o
-3 7 1 292.11 299.15 3.77 o
-2 7 1 703.50 751.97 7.46 o
-1 7 1 0.00 -0.38 0.33 o
0 7 1 33.31 35.42 1.93 o
1 7 1 4.71 6.08 0.54 o
2 7 1 4.09 3.72 0.54 o
3 7 1 0.33 1.14 0.42 o
-4 8 1 87.09 93.00 1.99 o
-3 8 1 4.93 3.79 0.56 o
-2 8 1 371.06 378.15 4.52 o
-1 8 1 48.90 50.18 1.26 o
0 8 1 29.85 31.07 1.01 o
1 8 1 20.87 21.08 0.84 o
2 8 1 34.37 39.22 1.73 o
-3 9 1 0.00 -0.03 0.65 o
-2 9 1 0.01 -0.35 0.40 o
-1 9 1 17.36 18.56 0.87 o
0 9 1 16.84 17.46 0.83 o
1 9 1 8.63 7.97 0.99 o
-1 10 1 111.34 121.71 2.28 o
0 -10 2 0.03 0.39 0.57 o
1 -10 2 4.81 6.00 0.92 o
2 -10 2 6.14 5.23 0.86 o
-1 -9 2 0.03 0.65 0.64 o
0 -9 2 0.99 0.67 0.62 o
1 -9 2 26.10 27.29 1.43 o
2 -9 2 11.08 11.92 0.80 o
3 -9 2 4.44 3.68 0.61 o
-2 -8 2 0.14 -0.16 0.34 o
-1 -8 2 1.64 2.13 0.45 o
0 -8 2 26.50 25.23 2.45 o
1 -8 2 8.71 8.35 0.60 o
2 -8 2 153.65 151.48 2.88 o
3 -8 2 0.00 -0.39 0.43 o
4 -8 2 0.76 0.46 0.82 o
-3 -7 2 20.50 19.00 1.32 o
-2 -7 2 2.69 2.97 0.47 o
-1 -7 2 32.74 32.84 1.01 o
0 -7 2 12.91 12.48 0.50 o
1 -7 2 2.48 3.02 0.53 o
2 -7 2 13.39 11.12 0.52 o
3 -7 2 204.91 188.57 2.18 o
4 -7 2 74.22 61.25 2.40 o
-4 -6 2 1.80 1.47 0.69 o
-3 -6 2 70.40 68.89 1.47 o
-2 -6 2 1.34 0.93 0.37 o
-1 -6 2 7.75 9.48 0.43 o
0 -6 2 225.51 230.44 2.25 o
1 -6 2 85.67 94.78 1.27 o
2 -6 2 122.96 129.37 1.58 o
3 -6 2 10.91 8.24 0.81 o
4 -6 2 145.12 140.00 2.35 o
5 -6 2 5.08 5.40 0.63 o
-4 -5 2 1.09 1.21 0.65 o
-3 -5 2 146.20 154.37 2.11 o
-2 -5 2 126.58 116.51 1.42 o
-1 -5 2 22.73 22.03 0.52 o
0 -5 2 306.93 304.91 2.60 o
1 -5 2 271.16 287.35 2.84 o
2 -5 2 0.06 0.24 0.20 o
3 -5 2 2.08 3.79 0.33 o
4 -5 2 34.09 36.71 1.15 o
5 -5 2 0.00 0.53 0.38 o
-4 -4 2 47.46 47.66 1.34 o
-3 -4 2 112.30 111.99 1.49 o
-1 -4 2 91.47 86.50 1.02 o
0 -4 2 622.62 624.48 8.16 o
1 -4 2 339.70 346.72 2.82 o
2 -4 2 34.85 39.66 1.10 o
3 -4 2 77.28 83.98 1.18 o
4 -4 2 37.11 31.93 1.05 o
5 -4 2 4.93 4.69 1.18 o
-5 -3 2 72.88 76.78 1.74 o
-4 -3 2 69.33 70.44 1.60 o
-3 -3 2 20.99 21.02 0.59 o
-2 -3 2 288.10 277.09 5.01 o
-1 -3 2 209.95 221.50 1.89 o
0 -3 2 24.31 29.19 0.48 o
1 -3 2 147.42 160.28 1.49 o
2 -3 2 720.39 804.76 5.91 o
3 -3 2 56.22 64.04 1.30 o
4 -3 2 0.40 0.76 0.39 o
5 -3 2 22.46 22.86 1.13 o
-5 -2 2 26.24 23.84 0.97 o
-4 -2 2 58.08 52.23 1.32 o
-3 -2 2 24.57 23.03 0.60 o
-2 -2 2 7.11 4.63 0.34 o
0 -2 2 317.65 280.96 2.66 o
1 -2 2 20.25 15.23 0.36 o
2 -2 2 34.91 37.35 0.59 o
3 -2 2 77.49 84.56 1.53 o
4 -2 2 17.50 17.27 0.80 o
5 -2 2 2.02 2.01 0.45 o
-5 -1 2 10.12 11.81 0.72 o
-4 -1 2 3.68 3.78 0.79 o
-3 -1 2 234.48 226.94 2.18 o
-2 -1 2 0.50 0.44 0.19 o
0 -1 2 0.83 1.29 0.37 o
1 -1 2 102.14 105.49 1.82 o
2 -1 2 46.44 49.04 1.01 o
3 -1 2 97.72 96.54 1.66 o
4 -1 2 6.18 5.71 0.54 o
5 -1 2 12.97 13.15 0.78 o
-5 0 2 0.66 0.49 0.51 o
-4 0 2 5.36 6.84 0.89 o
-3 0 2 98.44 99.76 1.29 o
-2 0 2 11.39 11.74 0.39 o
-1 0 2 257.32 247.21 3.38 o
0 0 2 253.28 199.26 1.89 o
1 0 2 1.04 1.35 0.23 o
2 0 2 0.28 1.04 0.27 o
3 0 2 12.25 11.04 0.61 o
4 0 2 41.68 38.22 1.45 o
5 0 2 0.55 0.29 0.65 o
-5 1 2 1.60 2.40 0.51 o
-4 1 2 1.81 3.79 0.79 o
-3 1 2 22.17 19.27 0.52 o
-2 1 2 228.65 243.65 2.10 o
-1 1 2 1.74 4.05 0.21 o
0 1 2 27.71 27.44 0.41 o
1 1 2 573.00 522.39 4.80 o
2 1 2 0.97 2.08 0.32 o
3 1 2 23.20 18.95 0.72 o
4 1 2 22.93 21.61 0.88 o
5 1 2 90.41 86.04 1.85 o
-5 2 2 7.87 9.07 0.66 o
-4 2 2 20.23 16.91 0.56 o
-3 2 2 193.01 207.13 2.02 o
-2 2 2 1.71 3.93 0.24 o
0 2 2 362.29 325.81 3.18 o
1 2 2 533.44 525.63 6.28 o
2 2 2 96.51 93.72 1.11 o
3 2 2 25.35 27.73 0.91 o
4 2 2 5.11 5.01 0.53 o
-5 3 2 1.80 2.49 0.45 o
-4 3 2 92.72 96.98 1.38 o
-3 3 2 47.80 59.97 1.59 o
-2 3 2 0.70 2.34 0.20 o
-1 3 2 577.51 561.01 7.51 o
0 3 2 167.84 145.68 1.46 o
1 3 2 8.61 8.70 0.34 o
2 3 2 390.92 396.31 3.32 o
3 3 2 41.93 42.77 1.15 o
4 3 2 5.33 6.14 0.60 o
-5 4 2 88.07 93.09 2.91 o
-4 4 2 72.17 98.72 1.69 o
-3 4 2 48.55 47.57 0.82 o
-2 4 2 135.24 138.75 1.38 o
-1 4 2 76.44 85.97 1.39 o
0 4 2 912.64 923.05 11.79 o
1 4 2 138.82 132.65 1.48 o
2 4 2 27.09 25.89 0.64 o
3 4 2 75.87 78.66 1.60 o
4 4 2 8.56 9.13 0.69 o
-5 5 2 23.30 34.85 1.88 o
-4 5 2 342.66 355.58 4.65 o
-3 5 2 1186.41 1247.42 11.38 o
-2 5 2 23.52 20.50 0.77 o
-1 5 2 114.99 113.93 1.77 o
0 5 2 117.34 98.07 1.20 o
1 5 2 11.92 10.82 0.42 o
2 5 2 13.81 12.01 0.48 o
3 5 2 43.12 44.39 1.21 o
-5 6 2 70.30 82.08 2.83 o
-4 6 2 13.06 13.84 0.99 o
-3 6 2 464.39 436.86 4.84 o
-2 6 2 84.61 90.78 1.68 o
-1 6 2 75.22 80.12 1.57 o
0 6 2 77.08 79.04 1.48 o
1 6 2 152.88 155.98 2.71 o
2 6 2 10.61 11.51 0.54 o
3 6 2 0.42 0.41 0.34 o
-5 7 2 26.26 31.47 1.77 o
-4 7 2 0.95 1.09 0.49 o
-3 7 2 2.23 2.65 0.52 o
-2 7 2 76.98 80.41 1.65 o
-1 7 2 57.56 56.19 1.34 o
0 7 2 53.92 54.26 1.28 o
1 7 2 61.27 62.08 1.38 o
2 7 2 1.05 1.76 0.70 o
-4 8 2 126.75 136.78 2.49 o
-3 8 2 0.97 0.86 0.45 o
-2 8 2 217.17 211.03 3.03 o
-1 8 2 27.61 30.38 1.04 o
0 8 2 0.50 0.35 0.36 o
1 8 2 0.08 0.20 0.38 o
-3 9 2 29.11 30.20 1.15 o
-2 9 2 8.38 9.66 0.76 o
-1 9 2 15.84 16.58 0.84 o
0 9 2 0.03 -0.05 0.42 o
0 -10 3 3.10 3.22 0.80 o
1 -10 3 53.64 59.54 2.10 o
2 -10 3 1.54 1.75 0.69 o
-2 -9 3 10.66 10.23 0.72 o
-1 -9 3 0.14 0.76 0.40 o
0 -9 3 0.09 -0.31 0.59 o
1 -9 3 1.20 0.74 0.60 o
2 -9 3 85.06 80.40 2.30 o
3 -9 3 49.19 42.19 1.75 o
-2 -8 3 0.41 1.02 0.60 o
-1 -8 3 64.97 68.24 1.51 o
0 -8 3 14.01 13.82 0.73 o
1 -8 3 36.03 36.33 1.06 o
2 -8 3 26.55 21.52 0.70 o
3 -8 3 71.61 63.44 1.64 o
4 -8 3 10.93 10.53 1.29 o
-3 -7 3 32.25 32.71 1.06 o
-2 -7 3 2.91 3.11 0.74 o
-1 -7 3 79.70 82.27 1.58 o
0 -7 3 114.88 112.00 1.84 o
1 -7 3 1.80 0.85 0.29 o
2 -7 3 2.21 1.77 0.39 o
3 -7 3 54.82 54.23 1.11 o
4 -7 3 0.37 0.20 0.38 o
-4 -6 3 48.30 47.66 2.02 o
-3 -6 3 509.08 507.18 5.43 o
-2 -6 3 10.50 10.88 0.62 o
-1 -6 3 125.70 118.57 1.81 o
0 -6 3 190.85 182.83 4.19 o
1 -6 3 4.99 4.66 0.34 o
2 -6 3 56.07 53.90 0.98 o
3 -6 3 63.31 50.76 1.43 o
4 -6 3 2.40 0.90 0.43 o
-4 -5 3 7.87 8.42 1.01 o
-3 -5 3 61.83 63.06 1.41 o
-2 -5 3 26.43 26.64 0.85 o
-1 -5 3 9.06 9.26 0.36 o
0 -5 3 38.97 38.47 0.69 o
1 -5 3 620.24 637.69 4.89 o
2 -5 3 43.02 44.65 1.03 o
3 -5 3 2.86 2.90 0.59 o
4 -5 3 42.09 37.66 1.19 o
5 -5 3 8.20 7.81 0.70 o
-5 -4 3 10.12 10.44 1.11 o
-4 -4 3 11.99 10.89 1.07 o
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