#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015244.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015244_Fobs loop_ _publ_author_name 'Muniappan, Sankar' 'Liptsman, Sophia' 'Goldberg, Israel' _publ_section_title ; Clathrate solvates of tetrakis(4-methoxycarbonylphenyl)porphyrin and its zinc(II)--pyridine complex, in which the porphyrin host structures are stabilized by porphyrin--porphyrin stacking and C---H···O attractions ; _journal_coeditor_code GD3004 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m140 _journal_page_last m143 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.292 _cell_angle_gamma 90.000 _cell_length_a 32.6249 _cell_length_b 7.0657 _cell_length_c 23.5160 _exptl_crystal_F_000 2255.11 _reflns_d_resolution_high 0.7522 _[local]_cod_data_source_file gd3004Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound so13 symmetry C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 526.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 29286.37 30254.67 736.27 o 6 0 0 30676.26 26582.09 642.53 o 8 0 0 277200.38 263853.25 5948.08 o 10 0 0 12311.82 12397.71 341.30 o 12 0 0 6952.91 7113.58 213.41 o 14 0 0 3722.56 4093.47 136.94 o 16 0 0 2767.76 3474.44 134.81 o 18 0 0 84.64 59.83 43.26 o 20 0 0 1447.02 1634.69 98.36 o 22 0 0 388.30 361.89 62.97 o 24 0 0 1.22 63.26 60.78 o 26 0 0 55.42 20.71 51.55 o 28 0 0 1221.81 978.73 98.95 o 30 0 0 2.25 91.85 105.40 o 32 0 0 69.90 181.63 125.88 o 34 0 0 967.34 840.90 170.74 o 36 0 0 44.45 -76.28 98.60 o 38 0 0 166.64 421.54 176.83 o 40 0 0 1385.78 1964.62 299.75 o 42 0 0 35.88 -126.29 193.05 o 1 1 0 2039.03 1915.33 36.22 o 3 1 0 22256.95 19423.94 305.14 o 5 1 0 30412.76 28874.39 504.34 o 7 1 0 29185.24 26996.17 479.66 o 9 1 0 3597.81 3185.34 74.15 o 11 1 0 2638.47 2521.16 65.99 o 13 1 0 15820.95 15200.33 299.93 o 15 1 0 3876.80 3613.46 93.56 o 17 1 0 1450.44 1607.29 60.48 o 19 1 0 87.59 91.85 33.08 o 21 1 0 2045.87 1877.21 75.87 o 23 1 0 480.66 392.13 50.13 o 25 1 0 1280.41 1080.17 70.37 o 27 1 0 1238.03 1101.06 75.87 o 29 1 0 242.93 212.34 65.93 o 31 1 0 42.71 43.79 64.09 o 33 1 0 583.72 649.98 119.07 o 35 1 0 406.40 514.04 109.19 o 37 1 0 342.38 339.11 89.60 o 39 1 0 4.17 15.92 119.96 o 41 1 0 270.26 312.77 129.96 o 0 2 0 132237.89 131969.75 2987.09 o 2 2 0 59645.77 57080.99 976.42 o 4 2 0 7339.92 6833.24 112.62 o 6 2 0 12847.63 12064.11 208.43 o 8 2 0 355.00 374.02 18.82 o 10 2 0 2780.48 2580.10 66.76 o 12 2 0 3230.50 3514.74 83.62 o 14 2 0 7474.49 7158.80 156.41 o 16 2 0 2374.11 2369.60 73.44 o 18 2 0 1313.16 1342.22 58.83 o 20 2 0 60.31 74.57 35.75 o 22 2 0 428.57 353.60 43.02 o 24 2 0 5578.10 6193.38 179.97 o 26 2 0 2789.81 2812.50 123.87 o 28 2 0 123.73 144.99 52.73 o 30 2 0 1335.34 1503.66 105.64 o 32 2 0 5.08 17.10 68.00 o 34 2 0 252.48 84.57 98.00 o 36 2 0 3.06 15.92 97.47 o 38 2 0 13.20 -51.49 97.77 o 40 2 0 582.19 455.16 141.15 o 1 3 0 1431.30 1620.96 43.08 o 3 3 0 10286.00 10006.57 184.94 o 5 3 0 13670.00 13840.54 240.39 o 7 3 0 71.70 64.03 12.84 o 9 3 0 4403.30 4384.88 93.45 o 11 3 0 24287.94 25685.44 436.69 o 13 3 0 13.72 -2.96 19.00 o 15 3 0 8.62 30.77 23.20 o 17 3 0 3822.29 3994.46 110.73 o 19 3 0 2185.71 2436.35 86.46 o 21 3 0 273.15 295.79 45.21 o 23 3 0 418.89 384.44 45.81 o 25 3 0 206.59 191.63 50.48 o 27 3 0 5083.35 5192.16 182.28 o 29 3 0 91.40 78.00 65.75 o 31 3 0 10.24 -48.05 77.59 o 33 3 0 0.18 31.84 85.69 o 35 3 0 59.42 -65.22 81.73 o 37 3 0 53.58 108.42 100.78 o 39 3 0 0.53 158.19 137.65 o 0 4 0 27783.63 30534.59 1190.24 o 2 4 0 8837.20 8854.26 178.55 o 4 4 0 3068.36 3212.86 71.73 o 6 4 0 42.19 70.84 18.41 o 8 4 0 5962.20 6495.68 133.33 o 10 4 0 241.47 325.85 26.34 o 12 4 0 0.38 -18.94 16.51 o 14 4 0 3301.82 3587.18 84.51 o 16 4 0 0.60 17.10 25.33 o 18 4 0 3435.43 3645.71 99.90 o 20 4 0 2900.25 3004.01 93.33 o 22 4 0 889.37 839.48 52.14 o 24 4 0 446.34 340.05 46.63 o 26 4 0 335.96 289.99 62.97 o 28 4 0 88.84 37.28 61.49 o 30 4 0 1063.89 1115.62 102.38 o 32 4 0 4.46 75.87 94.10 o 34 4 0 1514.28 1943.08 175.89 o 36 4 0 66.68 119.31 88.24 o 38 4 0 303.73 293.30 87.47 o 1 5 0 379.13 371.24 45.92 o 3 5 0 182.97 151.50 16.16 o 5 5 0 458.81 442.79 25.57 o 7 5 0 684.20 737.10 35.69 o 9 5 0 198.61 203.94 27.10 o 11 5 0 89.66 85.93 13.08 o 13 5 0 1118.00 1261.50 43.20 o 15 5 0 8.11 19.59 20.65 o 17 5 0 3178.30 3196.35 88.00 o 19 5 0 560.47 552.27 41.19 o 21 5 0 0.39 7.69 31.31 o 23 5 0 284.50 255.42 44.33 o 25 5 0 1.94 62.91 63.26 o 27 5 0 357.55 480.43 68.24 o 29 5 0 148.51 41.90 51.96 o 31 5 0 821.36 722.60 99.42 o 33 5 0 67.71 200.45 83.33 o 35 5 0 17.20 156.95 87.17 o 0 6 0 8953.17 10055.34 541.56 o 2 6 0 388.47 397.93 55.33 o 4 6 0 4.96 -1.18 33.32 o 6 6 0 1258.92 1196.69 45.45 o 8 6 0 3947.84 4426.84 123.04 o 10 6 0 744.08 688.98 47.23 o 12 6 0 759.94 739.70 54.27 o 14 6 0 7.85 38.47 47.40 o 16 6 0 2159.73 1999.24 63.09 o 18 6 0 138.42 124.69 27.70 o 20 6 0 171.62 164.34 35.57 o 22 6 0 6.18 -67.55 45.04 o 24 6 0 17.05 94.69 51.61 o 26 6 0 173.46 166.89 69.77 o 28 6 0 336.51 230.45 141.09 o 30 6 0 7.37 245.42 181.39 o 32 6 0 15.34 234.89 167.78 o 1 7 0 21.59 60.25 59.30 o 3 7 0 1772.78 1799.98 125.94 o 5 7 0 26.56 17.10 60.78 o 7 7 0 2256.58 2197.56 59.30 o 9 7 0 2208.56 2560.40 123.10 o 11 7 0 0.94 -2.37 44.21 o 13 7 0 351.08 393.08 62.67 o 15 7 0 5.41 10.65 50.30 o 17 7 0 15.86 7.69 58.59 o 19 7 0 624.41 541.98 87.23 o 21 7 0 1034.90 927.66 158.55 o 23 7 0 133.09 50.78 129.01 o 25 7 0 549.23 576.54 165.88 o 0 8 0 1563.66 1545.50 197.01 o 2 8 0 43.70 11.78 70.78 o 4 8 0 104.44 113.04 78.59 o 6 8 0 4.42 0.59 63.50 o 8 8 0 541.57 625.42 141.15 o 10 8 0 91.02 129.61 119.66 o 12 8 0 0.06 11.24 120.85 o 14 8 0 210.31 218.02 126.47 o 16 8 0 93.01 -47.40 121.91 o 18 8 0 125.84 244.65 147.66 o 20 8 0 13.07 -11.24 148.13 o 22 8 0 656.13 1023.35 214.77 o 1 9 0 42.74 30.24 99.48 o 3 9 0 214.58 163.75 113.92 o 5 9 0 8.32 140.38 149.85 o 7 9 0 27.39 -39.71 137.95 o 9 9 0 1.24 180.32 122.86 o 11 9 0 496.58 794.97 174.23 o -41 1 1 151.99 123.57 134.70 o -39 1 1 47.60 30.24 116.11 o -37 1 1 6.51 4.68 80.66 o -35 1 1 1.18 45.10 90.49 o -33 1 1 171.73 203.94 94.51 o -31 1 1 1922.76 1640.61 130.08 o -29 1 1 217.42 192.28 57.35 o -27 1 1 725.18 743.66 59.71 o -25 1 1 1418.99 1430.99 79.12 o -23 1 1 2375.81 2572.70 98.71 o -21 1 1 262.36 293.30 41.66 o -19 1 1 8.38 36.69 31.84 o -17 1 1 2306.33 2238.81 71.37 o -15 1 1 43769.76 47638.59 860.19 o -13 1 1 2212.50 1994.92 60.84 o -11 1 1 380.21 263.30 24.50 o -9 1 1 4491.72 4177.92 94.33 o -7 1 1 1130.32 1020.28 32.61 o -5 1 1 1905.89 1860.35 46.16 o -3 1 1 1821.92 1349.38 30.36 o -1 1 1 56265.65 48192.40 715.61 o 1 1 1 13850.94 12300.42 178.07 o 3 1 1 2385.19 2243.42 41.49 o 5 1 1 1.71 32.67 13.61 o 7 1 1 21363.82 20649.69 384.56 o 9 1 1 44597.36 43587.02 741.53 o 11 1 1 897.09 885.17 36.16 o 13 1 1 2508.05 3025.38 80.31 o 15 1 1 1893.03 2062.86 66.28 o 17 1 1 1801.27 1562.73 63.50 o 19 1 1 5608.02 6693.22 167.19 o 21 1 1 280.04 338.22 45.63 o 23 1 1 1920.02 1760.98 79.60 o 25 1 1 3252.55 3111.60 119.43 o 27 1 1 41.15 -18.94 50.42 o 29 1 1 161.16 156.95 64.63 o 31 1 1 1132.51 892.45 110.49 o 33 1 1 35.52 218.02 83.33 o 35 1 1 11.08 41.54 93.80 o 37 1 1 8.66 49.77 95.40 o 39 1 1 1.26 -48.05 120.79 o 41 1 1 356.57 199.79 138.90 o -40 2 1 255.36 361.89 118.48 o -38 2 1 240.43 111.50 112.50 o -36 2 1 1047.05 895.35 135.41 o -34 2 1 2.72 108.89 94.93 o -32 2 1 42.43 111.97 85.46 o -30 2 1 601.48 549.97 76.46 o -28 2 1 39.38 82.79 42.49 o -26 2 1 7773.89 8224.94 238.26 o -24 2 1 836.34 818.47 57.05 o -22 2 1 193.29 252.35 42.49 o -20 2 1 1073.19 1183.26 58.59 o -18 2 1 578.29 601.34 42.97 o -16 2 1 3466.39 3332.53 95.52 o -14 2 1 3048.73 3095.39 83.92 o -12 2 1 2334.35 2784.22 71.90 o -10 2 1 1000.36 972.64 34.92 o -8 2 1 207.38 163.75 17.46 o -6 2 1 1830.70 1613.15 39.06 o -4 2 1 2342.13 2190.75 43.26 o -2 2 1 1512.38 1181.60 35.09 o 0 2 1 3112.58 3237.72 52.61 o 2 2 1 25342.90 23698.09 322.06 o 4 2 1 6210.84 5555.95 94.27 o 6 2 1 1990.81 1545.50 38.23 o 8 2 1 74.73 41.54 13.49 o 10 2 1 5341.56 5401.07 114.40 o 12 2 1 1.24 19.59 19.59 o 14 2 1 136.66 203.94 29.18 o 16 2 1 181.33 195.00 30.60 o 18 2 1 454.47 503.10 42.55 o 20 2 1 13.24 15.92 27.76 o 22 2 1 1.32 31.84 38.47 o 24 2 1 934.16 1173.26 74.98 o 26 2 1 7566.41 7618.75 225.06 o 28 2 1 312.15 234.89 55.93 o 30 2 1 421.57 291.64 74.80 o 32 2 1 555.99 524.05 90.19 o 34 2 1 765.02 893.87 117.83 o 36 2 1 24.27 0.59 104.22 o 38 2 1 1.05 2.37 84.87 o 40 2 1 0.91 21.36 134.46 o -39 3 1 2.44 173.87 84.04 o -37 3 1 1.00 -113.04 89.48 o -35 3 1 56.36 37.28 86.46 o -33 3 1 0.14 26.10 73.56 o -31 3 1 226.27 135.76 60.07 o -29 3 1 167.56 102.44 71.37 o -27 3 1 1289.22 1213.56 77.94 o -25 3 1 1665.73 1710.32 84.51 o -23 3 1 524.04 411.66 47.40 o -21 3 1 1339.27 1208.47 62.55 o -19 3 1 181.15 180.32 35.27 o -17 3 1 69.08 96.58 29.65 o -15 3 1 311.90 247.73 27.58 o -13 3 1 3376.17 3633.99 79.18 o -11 3 1 32.81 27.10 17.75 o -9 3 1 5384.56 6197.23 114.93 o -7 3 1 998.91 914.34 26.45 o -5 3 1 6140.20 6590.13 106.64 o -3 3 1 4404.92 4696.29 93.39 o -1 3 1 66.67 109.96 12.25 o 1 3 1 6957.45 7316.10 112.38 o 3 3 1 7807.09 7146.43 111.08 o 5 3 1 207.79 244.65 13.67 o 7 3 1 470.44 481.49 22.43 o 9 3 1 14277.72 14872.23 261.05 o 11 3 1 1361.73 1317.42 42.37 o 13 3 1 196.35 201.87 23.49 o 15 3 1 73.26 104.39 25.33 o 17 3 1 3005.02 3149.72 81.91 o 19 3 1 1047.43 980.27 53.32 o 21 3 1 46.84 24.15 39.00 o 23 3 1 2811.71 3106.22 113.86 o 25 3 1 3786.26 3924.04 146.29 o 27 3 1 1080.10 1009.39 77.29 o 29 3 1 279.42 242.40 81.08 o 31 3 1 358.39 198.37 76.05 o 33 3 1 38.79 116.11 92.80 o 35 3 1 147.51 166.89 89.90 o 37 3 1 10.54 102.92 119.43 o 39 3 1 35.16 168.13 145.70 o -38 4 1 391.87 317.98 116.23 o -36 4 1 1.90 139.78 88.00 o -34 4 1 221.56 117.71 67.58 o -32 4 1 618.24 428.59 83.62 o -30 4 1 1002.97 853.62 92.38 o -28 4 1 53.27 132.39 59.36 o -26 4 1 81.48 117.18 48.47 o -24 4 1 55.65 31.84 37.88 o -22 4 1 509.37 428.59 42.31 o -20 4 1 1132.61 1075.37 52.67 o -18 4 1 96.02 116.11 27.28 o -16 4 1 325.35 303.42 28.82 o -14 4 1 985.88 935.06 37.17 o -12 4 1 185.57 129.07 17.70 o -10 4 1 2414.39 2590.04 61.90 o -8 4 1 331.61 362.84 15.74 o -6 4 1 3452.00 3408.81 90.90 o -4 4 1 2857.25 2856.54 67.58 o -2 4 1 10826.65 11671.92 231.28 o 0 4 1 220.43 321.47 43.62 o 2 4 1 139.23 142.68 13.97 o 4 4 1 3891.14 3933.21 85.46 o 6 4 1 389.43 353.60 17.40 o 8 4 1 376.22 368.40 19.59 o 10 4 1 900.75 1031.16 35.92 o 12 4 1 784.40 859.30 34.21 o 14 4 1 517.53 571.86 31.42 o 16 4 1 280.57 260.16 30.60 o 18 4 1 9083.61 9914.31 218.02 o 20 4 1 342.30 252.35 34.03 o 22 4 1 123.74 86.82 34.92 o 24 4 1 1858.43 1694.28 74.09 o 26 4 1 270.39 197.01 60.13 o 28 4 1 120.93 16.51 62.67 o 30 4 1 11.34 58.71 70.07 o 32 4 1 257.61 186.89 85.81 o 34 4 1 74.83 179.67 112.15 o 36 4 1 14.94 -49.77 109.48 o -35 5 1 1105.08 1208.47 164.05 o -33 5 1 105.02 114.57 88.53 o -31 5 1 7.82 -79.72 65.57 o -29 5 1 132.13 147.36 60.25 o -27 5 1 509.47 467.71 68.41 o -25 5 1 1150.11 1249.42 87.71 o -23 5 1 4618.27 4956.50 150.73 o -21 5 1 1024.43 1093.01 59.54 o -19 5 1 581.89 608.50 39.59 o -17 5 1 788.77 745.03 39.83 o -15 5 1 5.40 30.77 21.31 o -13 5 1 998.92 1003.23 38.53 o -11 5 1 29.92 48.41 9.47 o -9 5 1 566.72 555.71 41.31 o -7 5 1 6462.11 7158.80 148.19 o -5 5 1 76.11 104.87 18.94 o -3 5 1 3.28 12.96 12.96 o -1 5 1 722.58 775.86 60.96 o 1 5 1 422.20 408.70 48.17 o 3 5 1 97.85 98.00 14.91 o 5 5 1 92.62 86.82 19.94 o 7 5 1 175.65 152.09 22.78 o 9 5 1 43.04 58.71 23.85 o 11 5 1 38.07 10.00 14.14 o 13 5 1 29.73 41.90 16.69 o 15 5 1 303.35 298.33 29.41 o 17 5 1 4339.57 4391.33 112.86 o 19 5 1 263.33 276.08 37.17 o 21 5 1 69.59 37.28 36.81 o 23 5 1 963.03 951.51 67.53 o 25 5 1 98.49 97.53 53.32 o 27 5 1 724.93 699.28 77.17 o 29 5 1 489.77 331.12 100.02 o 31 5 1 22.63 69.24 124.69 o 33 5 1 1742.46 2027.65 159.91 o 35 5 1 132.92 215.89 85.10 o -32 6 1 433.78 338.22 173.58 o -30 6 1 47.65 -90.96 141.97 o -28 6 1 0.00 45.10 147.66 o -26 6 1 205.21 174.46 78.41 o -24 6 1 323.46 426.57 68.35 o -22 6 1 326.68 264.89 51.49 o -20 6 1 838.72 835.22 50.60 o -18 6 1 698.18 811.49 44.33 o -16 6 1 46.04 48.05 16.51 o -14 6 1 194.91 68.83 49.24 o -12 6 1 13.18 2.96 34.44 o -10 6 1 564.11 495.46 39.00 o -8 6 1 2172.47 2177.08 72.67 o -6 6 1 1655.95 1583.97 54.21 o -4 6 1 1190.63 1225.46 91.97 o -2 6 1 330.32 418.59 62.73 o 0 6 1 200.55 153.34 46.99 o 2 6 1 19.83 -1.78 47.52 o 4 6 1 3.29 30.77 47.23 o 6 6 1 2.50 -16.51 19.00 o 8 6 1 2375.36 2218.15 82.50 o 10 6 1 12.78 15.92 26.57 o 12 6 1 11.76 11.78 34.86 o 14 6 1 468.80 444.86 51.31 o 16 6 1 39.50 31.84 26.10 o 18 6 1 814.18 872.21 48.88 o 20 6 1 42.18 45.39 31.78 o 22 6 1 860.02 719.99 69.18 o 24 6 1 77.07 118.24 59.24 o 26 6 1 124.47 171.27 64.33 o 28 6 1 209.23 27.10 122.86 o 30 6 1 323.11 459.36 180.38 o 32 6 1 23.31 113.04 155.17 o -25 7 1 88.30 120.37 147.36 o -23 7 1 1225.00 1117.27 191.92 o -21 7 1 164.55 175.77 117.41 o -19 7 1 317.69 175.77 109.01 o -17 7 1 389.92 319.69 69.60 o -15 7 1 2152.97 2218.15 137.48 o -13 7 1 387.75 501.97 71.96 o -11 7 1 409.23 336.44 58.88 o -9 7 1 1481.76 1672.33 91.55 o -7 7 1 23.83 8.82 17.04 o -5 7 1 241.48 334.67 77.41 o -3 7 1 1.37 81.02 62.20 o -1 7 1 705.15 682.65 78.83 o 1 7 1 245.02 124.69 62.49 o 3 7 1 233.25 170.68 66.76 o 5 7 1 2.47 -54.33 49.12 o 7 7 1 1560.04 1553.14 46.04 o 9 7 1 201.75 210.92 49.48 o 11 7 1 0.45 3.49 45.87 o 13 7 1 677.58 604.89 70.60 o 15 7 1 910.27 1065.84 98.48 o 17 7 1 7.77 -14.80 63.97 o 19 7 1 400.57 423.56 82.08 o 21 7 1 888.14 658.68 154.82 o 23 7 1 460.75 210.21 141.80 o -22 8 1 61.46 97.06 110.25 o -20 8 1 14.46 73.32 140.85 o -18 8 1 25.16 -85.93 91.08 o -16 8 1 90.69 -108.42 120.55 o -14 8 1 210.07 175.12 137.12 o -12 8 1 751.84 1076.97 166.06 o -10 8 1 14.29 66.82 86.29 o -8 8 1 688.30 647.50 152.27 o -6 8 1 156.51 105.87 119.13 o -4 8 1 85.25 84.10 78.53 o -2 8 1 141.00 231.16 72.50 o 0 8 1 828.69 1020.28 107.24 o 2 8 1 15.55 35.51 78.00 o 4 8 1 881.54 921.74 112.27 o 6 8 1 365.02 328.45 98.77 o 8 8 1 73.08 12.43 110.67 o 10 8 1 224.20 -21.84 120.43 o 12 8 1 60.46 -11.24 77.59 o 14 8 1 180.18 116.11 87.05 o 16 8 1 28.13 -94.22 133.63 o 18 8 1 9.48 -52.55 128.72 o 20 8 1 2.53 2.37 99.01 o 22 8 1 33.67 196.36 156.83 o -11 9 1 19.81 147.36 167.13 o -9 9 1 146.82 303.42 167.78 o -7 9 1 90.98 116.65 148.19 o -5 9 1 18.53 -94.22 94.93 o -3 9 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195.00 97.83 o -17 1 29 1547.08 1781.46 180.74 o -15 1 29 47.10 -70.43 79.24 o -13 1 29 74.26 18.35 90.01 o -11 1 29 26.57 106.41 93.33 o -9 1 29 29.23 65.22 92.32 o -7 1 29 44.03 -64.03 109.01 o -5 1 29 164.72 112.50 99.07 o -3 1 29 198.00 81.02 92.85 o -1 1 29 91.22 136.94 100.19 o 1 1 29 0.53 -15.92 85.58 o 3 1 29 38.06 -2.96 128.30 o 5 1 29 53.30 63.26 120.73 o -18 2 29 45.13 -17.10 108.66 o -16 2 29 1.26 -10.65 91.02 o -14 2 29 0.78 4.68 112.50 o -12 2 29 107.63 39.71 110.67 o -10 2 29 221.26 268.03 90.78 o -8 2 29 5.61 8.23 109.78 o -6 2 29 99.87 11.24 109.60 o -4 2 29 77.45 37.88 122.50 o -2 2 29 255.75 170.03 120.55 o 0 2 29 2.27 -1.78 121.79 o 2 2 29 105.09 101.91 127.24 o 4 2 29 13.63 46.75 130.02 o -13 3 29 367.31 590.62 124.16 o -11 3 29 654.99 705.73 147.36 o -9 3 29 580.04 433.62 119.55 o -7 3 29 10.71 -139.78 117.95 o -5 3 29 0.42 -17.10 92.74 o -3 3 29 176.29 110.43 105.82 o -1 3 29 129.93 74.15 106.82 o -16 0 30 326.69 52.20 164.17 o -14 0 30 277.86 -18.35 163.93 o -12 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