#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/53/2015347.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015347_Fobs loop_ _publ_author_name 'Wu, Xiao-Yuan' 'Zhai, Quan-Guo' 'Chen, Li-Juan' 'Lu, Can-Zhong' _publ_section_title ; An extended two-dimensional copper--molybdate compound with mixed dicarboxyl and organodiamine ligands ; _journal_coeditor_code DN3010 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m261 _journal_page_last m263 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.603 _cell_angle_beta 85.529 _cell_angle_gamma 83.151 _cell_length_a 7.4592 _cell_length_b 10.2514 _cell_length_c 11.6240 _exptl_crystal_F_000 602.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file dn3010Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 822.75 884.26 8.20 o 2 0 0 39.31 30.55 2.10 o 3 0 0 26.45 8.09 3.29 o 4 0 0 3802.78 3900.98 47.48 o 5 0 0 2161.39 2099.79 29.33 o 6 0 0 325.31 334.03 10.71 o 7 0 0 149.82 156.57 7.65 o 8 0 0 75.50 74.80 11.35 o 9 0 0 2378.00 2351.30 85.02 o -9 1 0 1097.95 1150.56 43.03 o -8 1 0 69.23 70.06 13.55 o -6 1 0 137.28 133.10 6.52 o -5 1 0 201.28 184.03 6.29 o -4 1 0 118.16 129.75 5.62 o -3 1 0 1347.02 1524.07 15.58 o -2 1 0 4632.46 4738.66 34.65 o -1 1 0 59.38 61.96 3.71 o 1 1 0 2229.57 2302.06 21.01 o 2 1 0 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