#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015641.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015641_Fobs loop_ _publ_author_name 'G\"ok\,ce, Ayta\,c G\"urhan' 'G\"ulcemal, S\"uleyman' 'Ayg\"un, Muhittin' '\,Cetinkaya, Bekir' 'B\"uy\"ukg\"ung\"or, Orhan' _publ_section_title ; trans-Bis[1-benzyl-3-(2,3,4,5,6-pentafluorobenzyl)benzimidazol-2-ylidene]dibromopalladium(II) ; _journal_coeditor_code GD3050 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m535 _journal_page_last m537 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.589 _cell_angle_beta 95.610 _cell_angle_gamma 92.520 _cell_length_a 11.6122 _cell_length_b 12.1401 _cell_length_c 13.6590 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file gd3050IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' TEST STRUCTURE D:\DATA\NEW\ORHMUHIT5' _shelx_refln_list_code 4 _shelx_f_calc_maximum 288.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2673.83 2750.05 138.88 o 3 0 0 5492.97 6011.55 125.83 o 4 0 0 7891.21 8089.63 188.48 o 5 0 0 80.27 67.29 72.10 o 6 0 0 13061.45 12247.68 267.98 o 7 0 0 947.36 967.43 68.62 o 8 0 0 397.37 476.61 80.31 o 9 0 0 44.95 139.34 77.19 o 10 0 0 517.02 578.71 58.25 o 11 0 0 270.22 283.39 56.82 o 12 0 0 1155.35 1163.67 63.92 o 13 0 0 95.63 100.15 61.18 o 14 0 0 189.20 195.93 62.59 o -14 1 0 0.96 -99.71 63.98 o -13 1 0 101.81 127.93 53.96 o -12 1 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