#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/56/2015657.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015657_Fobs loop_ _publ_author_name 'Lipstman, Sophia' 'Muniappan, Sankar' 'Goldberg, Israel' _publ_section_title ; Hydrogen-bonded supramolecular arrays of aqua[20-(4-carboxyphenyl)-5,10,15-triphenylporphyrinato]zinc(II) in crystals of its nitrobenzene disolvate ; _journal_coeditor_code SF3019 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m538 _journal_page_last m540 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.109 _cell_angle_beta 69.598 _cell_angle_gamma 68.086 _cell_length_a 12.3796 _cell_length_b 13.4467 _cell_length_c 15.5757 _exptl_crystal_F_000 1020.00 _reflns_d_resolution_high 0.7512 _[local]_cod_data_source_file sf3019Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound so36 (symmerty P-1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 228.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4209.58 4177.16 158.70 o 2 0 0 1312.33 1357.57 44.76 o 3 0 0 2823.55 2826.81 89.32 o 4 0 0 10928.38 10726.70 232.89 o 5 0 0 331.28 432.40 19.34 o 6 0 0 1563.22 1751.13 56.25 o 7 0 0 6423.97 6235.19 175.52 o 8 0 0 842.01 722.59 34.74 o 9 0 0 28.48 -8.53 12.68 o 10 0 0 511.10 555.06 37.76 o 11 0 0 1090.07 1169.35 63.63 o 12 0 0 87.56 94.20 19.83 o 13 0 0 32.96 19.76 17.35 o 14 0 0 338.36 384.36 46.62 o -14 1 0 5.70 -18.52 26.59 o -13 1 0 229.31 325.02 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913.95 626.66 14.23 o 2 3 0 645.87 481.55 14.75 o 3 3 0 3155.09 2623.11 67.51 o 4 3 0 528.49 220.50 13.04 o 5 3 0 0.10 13.38 10.87 o 6 3 0 426.79 375.79 22.05 o 7 3 0 381.55 285.30 22.70 o 8 3 0 340.09 344.90 26.87 o 9 3 0 255.36 321.76 26.89 o 10 3 0 1237.16 1236.58 68.16 o 11 3 0 33.67 30.03 18.12 o 12 3 0 0.01 -9.85 19.24 o 13 3 0 108.08 98.26 30.48 o 14 3 0 169.98 142.60 49.39 o 15 3 0 49.88 36.43 40.55 o -13 4 0 8.63 -62.35 46.13 o -12 4 0 1049.97 979.75 73.62 o -11 4 0 432.35 428.64 33.17 o -10 4 0 505.56 487.81 33.10 o -9 4 0 3.64 8.15 12.84 o -8 4 0 124.84 128.45 12.89 o -7 4 0 1851.68 2036.65 57.15 o -6 4 0 663.90 740.06 26.02 o -5 4 0 1239.16 1203.19 34.97 o -4 4 0 1080.49 1036.37 29.96 o -3 4 0 55.20 107.96 6.45 o -2 4 0 69.42 65.04 3.96 o -1 4 0 17896.31 18120.47 382.73 o 0 4 0 907.56 771.33 18.66 o 1 4 0 658.03 534.55 13.75 o 2 4 0 8565.46 7832.40 146.39 o 3 4 0 4.19 35.34 8.15 o 4 4 0 25.62 10.52 8.22 o 5 4 0 1016.06 1116.06 43.17 o 6 4 0 115.62 157.15 15.88 o 7 4 0 376.57 447.03 23.50 o 8 4 0 967.22 1062.33 48.87 o 9 4 0 1817.50 1825.46 78.42 o 10 4 0 1488.88 1461.39 75.09 o 11 4 0 4.01 -11.72 13.55 o 12 4 0 325.45 262.64 37.28 o 13 4 0 45.91 105.56 41.15 o 14 4 0 232.95 273.64 55.58 o 15 4 0 32.75 34.27 39.80 o -12 5 0 17.85 -9.85 40.42 o -11 5 0 25.63 25.54 18.67 o -10 5 0 531.02 507.99 35.54 o -9 5 0 383.70 360.91 24.55 o -8 5 0 50.54 50.89 11.06 o -7 5 0 119.80 127.00 13.11 o -6 5 0 993.93 1033.05 30.73 o -5 5 0 207.20 209.88 10.86 o -4 5 0 129.56 129.04 7.63 o -3 5 0 489.50 339.63 10.00 o -2 5 0 1916.18 2179.02 59.12 o -1 5 0 634.57 719.82 23.58 o 0 5 0 216.89 162.38 5.28 o 1 5 0 11332.58 10195.38 159.20 o 2 5 0 618.57 654.12 17.85 o 3 5 0 3499.49 3249.68 86.93 o 4 5 0 1270.31 1491.17 51.91 o 5 5 0 4413.59 3941.70 113.59 o 6 5 0 3.76 -18.41 16.42 o 7 5 0 106.46 141.67 16.92 o 8 5 0 1414.84 1312.24 57.12 o 9 5 0 45.94 35.04 15.15 o 10 5 0 2.49 -19.54 20.23 o 11 5 0 690.45 684.21 51.38 o 12 5 0 402.05 382.34 41.44 o 13 5 0 287.69 265.58 51.81 o 14 5 0 18.08 -11.99 31.07 o 15 5 0 85.00 122.09 58.56 o -11 6 0 130.55 113.67 47.95 o -10 6 0 98.39 92.95 17.19 o -9 6 0 735.77 703.27 34.27 o -8 6 0 1836.61 2075.32 68.29 o -7 6 0 1442.28 1470.29 45.60 o -6 6 0 30.95 33.37 8.07 o -5 6 0 337.63 318.54 12.91 o -4 6 0 1995.09 2125.07 42.89 o -3 6 0 1313.30 1388.22 26.96 o -2 6 0 773.99 898.20 31.77 o -1 6 0 33.51 45.51 9.94 o 0 6 0 49.59 15.33 3.04 o 1 6 0 978.69 931.02 20.51 o 2 6 0 6218.51 5612.73 104.57 o 3 6 0 1461.13 1681.54 42.39 o 4 6 0 1308.86 1053.91 31.88 o 5 6 0 7.04 16.37 9.30 o 6 6 0 4054.71 4256.04 123.09 o 7 6 0 1484.13 1568.00 52.19 o 8 6 0 0.61 -5.85 12.18 o 9 6 0 192.06 183.44 22.05 o 10 6 0 3299.32 3591.22 159.54 o 11 6 0 867.18 937.35 68.06 o 12 6 0 20.49 40.27 23.78 o 13 6 0 175.27 227.08 47.52 o 14 6 0 78.64 24.50 46.06 o 15 6 0 41.60 28.91 54.62 o -11 7 0 5.71 43.27 38.26 o -10 7 0 202.50 147.90 52.81 o -9 7 0 914.57 919.23 39.18 o -8 7 0 193.47 211.38 16.90 o -7 7 0 281.25 294.10 15.95 o -6 7 0 231.91 236.12 11.91 o -5 7 0 815.34 887.38 23.10 o -4 7 0 156.43 190.50 19.26 o -3 7 0 1072.23 1222.98 38.87 o -2 7 0 9364.97 10529.52 238.70 o -1 7 0 2036.10 1960.39 54.93 o 0 7 0 2.47 16.05 10.04 o 1 7 0 2119.41 1860.97 34.57 o 2 7 0 2226.43 2514.38 51.84 o 3 7 0 4283.76 3925.48 80.97 o 4 7 0 1893.08 1752.22 45.45 o 5 7 0 608.42 513.84 21.09 o 6 7 0 2546.62 2662.96 72.02 o 7 7 0 163.86 161.73 17.75 o 8 7 0 1060.46 1171.12 55.72 o 9 7 0 393.71 394.05 31.30 o 10 7 0 600.50 650.83 38.90 o 11 7 0 332.18 292.33 31.82 o 12 7 0 1117.87 1278.75 74.87 o 13 7 0 1404.07 1657.25 125.21 o 14 7 0 23.12 -8.38 42.81 o 15 7 0 312.03 397.14 69.53 o -10 8 0 10.75 29.18 47.20 o -9 8 0 150.85 177.54 40.99 o -8 8 0 6.16 0.50 9.72 o -7 8 0 480.58 525.63 19.56 o -6 8 0 270.53 319.46 11.09 o -5 8 0 623.05 517.94 31.18 o -4 8 0 435.58 331.58 24.95 o -3 8 0 905.89 1041.37 36.69 o -2 8 0 3985.99 4272.93 108.13 o -1 8 0 270.44 216.67 18.26 o 0 8 0 2746.14 2549.49 66.56 o 1 8 0 1028.38 1047.21 21.75 o 2 8 0 1447.46 1582.36 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138.91 63.97 o -1 15 0 827.81 944.48 114.39 o 0 15 0 134.02 101.61 39.35 o 1 15 0 74.01 70.78 32.18 o 2 15 0 299.82 290.58 50.22 o 3 15 0 95.91 105.82 5.85 o 4 15 0 12.52 21.16 9.04 o 5 15 0 84.16 73.64 12.86 o 6 15 0 61.49 49.79 14.05 o 7 15 0 64.44 72.32 19.78 o 8 15 0 26.39 18.74 16.23 o 9 15 0 152.07 172.75 25.82 o 10 15 0 405.85 381.82 32.84 o 11 15 0 24.62 37.21 30.11 o -1 16 0 5.53 37.21 39.57 o 0 16 0 4.16 -42.09 50.14 o 1 16 0 331.15 461.91 73.32 o 2 16 0 282.98 271.09 66.39 o 3 16 0 0.26 -6.16 23.67 o 4 16 0 34.12 43.11 35.81 o 5 16 0 277.39 285.30 26.19 o 6 16 0 37.15 23.87 17.80 o 7 16 0 14.95 -2.02 23.48 o 8 16 0 3.05 30.03 18.69 o 9 16 0 407.88 468.59 47.00 o 10 16 0 19.30 -38.00 31.38 o 2 17 0 31.49 61.75 58.69 o 3 17 0 293.47 234.53 58.97 o 4 17 0 354.37 338.68 70.40 o 5 17 0 153.75 120.96 43.21 o 6 17 0 132.24 209.14 100.55 o 7 17 0 22.41 8.84 36.34 o 8 17 0 1.38 37.04 36.19 o -7 -17 1 69.20 89.49 43.78 o -6 -17 1 140.99 107.16 50.84 o -5 -17 1 343.84 367.33 66.37 o -4 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