#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015667.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015667_Fobs loop_ _publ_author_name 'Youngme, Sujittra' 'Phatchimkun, Jaturong' 'Chaichit, Narongsak' _publ_section_title ; Aqua(2,2'-bipyridyl)chloronitratocopper(II) ; _journal_coeditor_code AV3035 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m574 _journal_page_last m576 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.863 _cell_angle_gamma 90.000 _cell_length_a 10.8944 _cell_length_b 10.6760 _cell_length_c 11.0496 _exptl_crystal_F_000 676.00 _reflns_d_resolution_high 0.7800 _[local]_cod_data_source_file av3035Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' l61n1 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 156.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8542.73 8179.70 198.72 o 4 0 0 48.29 64.37 5.42 o 6 0 0 7738.61 7435.94 128.18 o 8 0 0 2904.04 2841.37 50.98 o 10 0 0 219.43 217.13 6.97 o 12 0 0 18.60 20.01 5.49 o 1 1 0 1069.99 1034.81 35.40 o 2 1 0 10070.42 9235.23 189.25 o 3 1 0 4189.54 4294.02 61.28 o 4 1 0 1611.77 1547.35 23.55 o 5 1 0 49.68 56.54 3.11 o 6 1 0 2496.42 2288.19 33.85 o 7 1 0 121.50 141.65 3.85 o 8 1 0 478.43 446.97 7.54 o 9 1 0 65.56 63.73 3.05 o 10 1 0 528.32 520.93 8.56 o 11 1 0 10.08 13.84 2.97 o 12 1 0 1169.61 1147.35 23.06 o 13 1 0 23.78 22.08 4.26 o 0 2 0 18947.76 16792.65 298.32 o 1 2 0 299.40 387.02 8.36 o 2 2 0 13834.38 13049.12 181.66 o 3 2 0 75.17 93.72 3.54 o 4 2 0 10923.14 10073.98 140.87 o 5 2 0 3136.60 3221.49 49.14 o 6 2 0 1803.37 1940.79 29.12 o 7 2 0 103.11 103.14 3.39 o 8 2 0 956.75 976.03 13.84 o 9 2 0 413.27 391.15 10.02 o 10 2 0 1243.02 1210.21 23.56 o 11 2 0 35.82 37.96 3.98 o 12 2 0 96.92 100.16 5.46 o 13 2 0 81.33 78.35 5.18 o 1 3 0 3850.70 3913.52 44.87 o 2 3 0 9718.05 9019.28 126.27 o 3 3 0 4868.21 4699.52 66.90 o 4 3 0 4898.70 4914.56 90.99 o 5 3 0 2292.24 2506.00 36.86 o 6 3 0 726.35 716.63 12.28 o 7 3 0 1.61 3.73 2.21 o 8 3 0 916.78 890.37 19.37 o 9 3 0 561.88 571.30 9.12 o 10 3 0 622.79 605.36 11.14 o 11 3 0 21.86 26.53 3.28 o 12 3 0 857.70 775.14 13.65 o 13 3 0 1.56 5.21 3.71 o 0 4 0 132.71 121.91 4.94 o 1 4 0 69.56 85.81 2.70 o 2 4 0 1187.99 1133.78 14.28 o 3 4 0 1587.43 1577.77 24.00 o 4 4 0 14078.70 13367.97 186.25 o 5 4 0 154.98 150.32 5.42 o 6 4 0 297.56 304.22 6.66 o 7 4 0 985.66 987.19 13.96 o 8 4 0 16.24 17.66 2.49 o 9 4 0 191.10 176.70 4.44 o 10 4 0 1389.48 1370.07 21.67 o 11 4 0 70.80 74.53 3.99 o 12 4 0 179.59 178.60 6.72 o 1 5 0 235.64 216.28 4.17 o 2 5 0 6925.28 6799.47 76.82 o 3 5 0 793.31 818.56 14.07 o 4 5 0 286.90 283.39 6.30 o 5 5 0 1409.97 1454.89 26.00 o 6 5 0 1060.68 1027.90 16.63 o 7 5 0 4.20 11.17 3.29 o 8 5 0 938.87 965.42 18.52 o 9 5 0 36.38 38.43 3.30 o 10 5 0 304.94 290.27 6.86 o 11 5 0 13.98 14.07 3.15 o 12 5 0 108.67 97.81 4.38 o 0 6 0 5341.57 5320.89 96.70 o 1 6 0 3876.69 3805.69 49.49 o 2 6 0 730.67 774.52 10.40 o 3 6 0 10.03 8.77 2.20 o 4 6 0 1593.20 1671.65 22.45 o 5 6 0 73.45 82.98 3.65 o 6 6 0 1758.99 1714.53 26.09 o 7 6 0 2714.15 2644.04 44.28 o 8 6 0 1595.21 1592.67 21.29 o 9 6 0 7.04 5.88 2.80 o 10 6 0 273.41 263.29 8.02 o 11 6 0 17.13 13.28 3.79 o 12 6 0 0.34 3.51 3.69 o 1 7 0 3058.69 3163.15 54.04 o 2 7 0 2835.82 2810.97 37.20 o 3 7 0 60.16 64.85 3.45 o 4 7 0 359.40 356.04 9.48 o 5 7 0 1692.37 1608.18 25.37 o 6 7 0 860.42 866.57 18.95 o 7 7 0 119.93 129.79 5.93 o 8 7 0 423.29 418.46 10.67 o 9 7 0 382.94 356.30 9.56 o 10 7 0 8.39 10.79 4.65 o 11 7 0 33.20 34.72 4.28 o 0 8 0 2602.87 2487.84 46.97 o 1 8 0 657.49 677.46 10.67 o 2 8 0 1.94 3.11 2.60 o 3 8 0 1658.86 1641.00 25.85 o 4 8 0 35.14 35.17 3.13 o 5 8 0 182.16 186.05 5.31 o 6 8 0 354.72 357.95 7.77 o 7 8 0 445.98 452.26 9.15 o 8 8 0 96.35 101.18 4.30 o 9 8 0 140.90 128.27 5.75 o 10 8 0 101.16 96.29 5.28 o 1 9 0 1532.46 1559.18 21.72 o 2 9 0 1065.36 1081.20 15.80 o 3 9 0 204.59 211.02 5.68 o 4 9 0 694.62 689.63 12.47 o 5 9 0 328.61 340.89 7.56 o 6 9 0 436.19 424.48 8.80 o 7 9 0 13.68 13.29 3.71 o 8 9 0 103.47 103.08 5.92 o 9 9 0 434.02 436.31 23.05 o 10 9 0 2.51 -1.07 4.88 o 0 10 0 1.98 12.53 9.74 o 1 10 0 27.22 30.07 2.79 o 2 10 0 337.61 339.29 6.64 o 3 10 0 2694.99 2573.16 48.64 o 4 10 0 282.02 270.49 7.66 o 5 10 0 257.92 255.83 6.45 o 6 10 0 17.65 15.97 3.06 o 7 10 0 201.02 187.88 9.10 o 8 10 0 0.12 1.67 5.02 o 1 11 0 5.29 5.39 2.50 o 2 11 0 501.94 480.57 12.13 o 3 11 0 208.24 205.53 5.78 o 4 11 0 157.51 156.46 5.11 o 5 11 0 385.27 409.23 11.40 o 6 11 0 1.56 2.27 5.02 o 7 11 0 13.05 8.50 5.29 o 0 12 0 293.72 275.41 8.44 o 1 12 0 772.18 772.12 16.56 o 2 12 0 65.16 60.41 3.38 o 3 12 0 412.53 405.80 8.71 o 4 12 0 90.21 91.47 5.25 o 5 12 0 52.17 46.44 6.09 o 6 12 0 6.51 -3.14 4.95 o 1 13 0 126.69 133.96 4.98 o 2 13 0 14.43 13.24 3.83 o 3 13 0 161.94 151.79 6.39 o 4 13 0 26.70 30.46 4.28 o -13 0 1 865.96 924.10 27.50 o -11 0 1 7.89 8.30 5.15 o -9 0 1 5.67 5.65 3.26 o -7 0 1 10781.89 9791.20 167.90 o -5 0 1 2456.09 2343.65 42.32 o -3 0 1 2367.34 2190.03 39.58 o -1 0 1 937.32 1098.74 29.78 o 1 0 1 16333.07 13814.79 333.08 o 3 0 1 365.07 444.49 14.45 o 5 0 1 3697.88 3742.99 93.27 o 7 0 1 13985.30 13271.94 320.77 o 9 0 1 92.93 93.32 4.87 o 11 0 1 523.00 523.64 12.31 o 13 0 1 154.51 131.48 8.63 o -13 1 1 240.10 251.96 8.11 o -12 1 1 3.58 -2.32 3.45 o -11 1 1 121.50 124.77 5.79 o -10 1 1 39.73 42.13 3.31 o -9 1 1 1228.67 1174.97 16.25 o -8 1 1 1.01 1.72 2.16 o -7 1 1 389.60 353.77 6.35 o -6 1 1 627.72 612.61 9.37 o -5 1 1 2978.79 2788.58 36.58 o -4 1 1 111.03 139.49 3.63 o -3 1 1 1315.70 1384.00 19.57 o -2 1 1 3678.56 3800.50 47.11 o -1 1 1 15298.71 13442.87 313.19 o 0 1 1 615.69 627.59 8.43 o 1 1 1 5115.19 4944.05 72.20 o 2 1 1 365.23 376.48 9.04 o 3 1 1 246.71 322.67 8.18 o 4 1 1 107.43 120.86 4.85 o 5 1 1 10448.34 9945.56 224.72 o 6 1 1 73.12 89.00 4.47 o 7 1 1 432.05 391.74 14.22 o 8 1 1 115.76 117.21 4.18 o 9 1 1 706.71 674.58 10.35 o 10 1 1 75.39 76.80 3.33 o 11 1 1 169.49 161.92 4.40 o 12 1 1 27.65 26.34 3.32 o 13 1 1 669.87 651.82 16.63 o -13 2 1 224.85 221.50 7.61 o -12 2 1 29.12 23.28 5.89 o -11 2 1 1508.72 1514.79 29.10 o -10 2 1 784.76 794.59 13.71 o -9 2 1 417.96 408.32 15.79 o -8 2 1 0.77 2.61 2.19 o -7 2 1 1380.79 1277.54 17.34 o -6 2 1 31.00 23.95 2.38 o -5 2 1 264.01 315.23 16.32 o -4 2 1 2294.38 2363.92 30.13 o -3 2 1 19970.10 16536.56 198.79 o -2 2 1 1142.63 1206.14 16.25 o -1 2 1 2785.26 2833.95 32.37 o 0 2 1 177.62 173.73 3.60 o 1 2 1 21522.72 18977.07 271.01 o 2 2 1 14382.95 13239.27 225.93 o 3 2 1 13827.42 13428.15 229.18 o 4 2 1 29.26 13.42 3.15 o 5 2 1 3193.32 3255.71 57.78 o 6 2 1 2.42 6.28 3.12 o 7 2 1 2147.18 2074.43 32.20 o 8 2 1 5.91 3.39 2.64 o 9 2 1 73.81 78.54 3.29 o 10 2 1 51.26 46.08 2.95 o 11 2 1 780.93 780.86 13.66 o 12 2 1 9.76 11.23 3.09 o -13 3 1 73.64 75.88 5.15 o -12 3 1 206.62 194.31 9.67 o -11 3 1 524.05 491.02 9.64 o -10 3 1 86.91 79.62 3.89 o -9 3 1 900.11 891.00 14.97 o -8 3 1 108.51 110.51 3.54 o -7 3 1 38.86 63.23 7.08 o -6 3 1 190.24 158.90 9.12 o -5 3 1 6604.10 6207.15 75.97 o -4 3 1 224.24 253.02 5.02 o -3 3 1 284.93 335.98 10.37 o -2 3 1 355.53 386.68 5.91 o -1 3 1 805.94 721.92 8.78 o 0 3 1 1156.51 1182.76 14.76 o 1 3 1 8698.47 8200.57 104.04 o 2 3 1 14236.88 13526.90 193.93 o 3 3 1 12320.34 11671.97 199.64 o 4 3 1 9.72 11.63 3.14 o 5 3 1 298.57 310.17 6.68 o 6 3 1 171.30 167.58 4.76 o 7 3 1 27.55 26.48 2.91 o 8 3 1 118.21 111.20 4.14 o 9 3 1 2572.71 2467.99 31.73 o 10 3 1 42.95 47.56 2.98 o 11 3 1 118.60 117.09 4.53 o 12 3 1 41.66 36.22 3.49 o -13 4 1 215.27 210.58 7.45 o -12 4 1 69.94 67.04 4.90 o -11 4 1 1467.69 1463.71 23.05 o -10 4 1 551.00 547.88 10.35 o -9 4 1 527.22 558.81 10.42 o -8 4 1 88.28 81.49 3.21 o -7 4 1 701.75 826.01 53.67 o -6 4 1 232.36 242.53 5.01 o -5 4 1 470.43 461.00 7.56 o -4 4 1 2318.22 2414.86 30.78 o -3 4 1 17457.10 16226.01 195.17 o -2 4 1 57.68 87.06 2.70 o -1 4 1 6.53 7.19 1.67 o 0 4 1 779.95 833.78 10.96 o 1 4 1 4749.64 4669.81 53.27 o 2 4 1 165.09 169.74 3.66 o 3 4 1 12965.44 12632.61 176.08 o 4 4 1 1239.09 1202.14 18.91 o 5 4 1 248.37 245.20 5.82 o 6 4 1 51.89 43.67 3.09 o 7 4 1 930.85 920.37 17.32 o 8 4 1 106.09 97.54 3.99 o 9 4 1 4.95 3.53 2.37 o 10 4 1 11.28 11.23 2.56 o 11 4 1 769.24 694.10 12.50 o 12 4 1 100.68 95.40 4.36 o -12 5 1 188.16 169.64 5.36 o -11 5 1 416.88 391.86 8.34 o -10 5 1 329.38 292.26 6.89 o -9 5 1 1614.86 1593.50 24.66 o -8 5 1 1014.37 1052.06 17.15 o -7 5 1 4.51 4.64 2.26 o -6 5 1 879.06 901.66 12.89 o -5 5 1 1947.59 1878.59 26.22 o -4 5 1 5.13 28.01 10.95 o -3 5 1 18.68 11.14 1.95 o -2 5 1 2824.77 2941.38 31.08 o -1 5 1 4559.28 4523.74 46.88 o 0 5 1 2345.62 2411.40 28.40 o 1 5 1 2806.95 2892.89 38.08 o 2 5 1 955.62 957.11 13.80 o 3 5 1 916.30 908.14 21.16 o 4 5 1 186.73 201.66 5.21 o 5 5 1 2281.99 2354.19 39.60 o 6 5 1 993.41 998.86 16.26 o 7 5 1 3.19 4.59 2.67 o 8 5 1 5.05 4.10 2.71 o 9 5 1 738.93 729.74 11.07 o 10 5 1 66.48 62.27 3.75 o 11 5 1 0.39 0.60 2.79 o 12 5 1 91.25 86.14 4.27 o -12 6 1 95.79 91.06 6.09 o -11 6 1 5.76 5.34 3.64 o -10 6 1 2.64 6.01 2.84 o -9 6 1 178.09 183.69 5.31 o -8 6 1 396.10 421.36 8.51 o -7 6 1 1590.61 1604.17 25.21 o -6 6 1 1979.84 1932.23 25.19 o -5 6 1 158.35 167.29 4.13 o -4 6 1 1.90 2.97 1.92 o -3 6 1 101.76 99.49 2.92 o -2 6 1 42.64 44.56 2.13 o -1 6 1 292.91 306.56 4.72 o 0 6 1 4491.09 4335.36 56.09 o 1 6 1 6094.33 5853.78 75.01 o 2 6 1 1039.07 996.60 12.84 o 3 6 1 3199.65 3156.86 40.51 o 4 6 1 1008.52 999.00 14.27 o 5 6 1 102.52 117.21 12.66 o 6 6 1 1463.77 1395.60 21.75 o 7 6 1 1052.77 1095.11 22.01 o 8 6 1 228.64 242.76 14.65 o 9 6 1 20.42 21.89 3.11 o 10 6 1 45.62 48.72 4.52 o 11 6 1 27.65 42.61 4.49 o -11 7 1 180.52 188.66 9.00 o -10 7 1 7.24 2.57 3.41 o -9 7 1 1206.24 1197.66 23.70 o -8 7 1 543.94 574.96 13.11 o -7 7 1 3.44 14.62 5.06 o -6 7 1 194.02 221.32 4.96 o -5 7 1 293.75 290.21 5.78 o -4 7 1 91.68 91.16 3.29 o -3 7 1 27.79 24.15 2.44 o -2 7 1 787.39 745.02 11.46 o -1 7 1 4494.36 4426.13 57.28 o 0 7 1 357.29 373.46 6.83 o 1 7 1 156.32 162.12 4.19 o 2 7 1 168.33 169.86 4.31 o 3 7 1 276.44 288.89 5.83 o 4 7 1 9.03 8.26 2.69 o 5 7 1 3295.05 3218.19 48.21 o 6 7 1 2016.78 1970.29 36.48 o 7 7 1 107.58 106.59 7.16 o 8 7 1 0.76 -0.01 2.68 o 9 7 1 24.31 27.80 4.04 o 10 7 1 2.39 5.47 3.66 o 11 7 1 60.83 60.10 4.75 o -11 8 1 4.02 5.35 5.02 o -10 8 1 201.03 207.82 10.24 o -9 8 1 19.86 17.60 5.35 o -8 8 1 1.99 2.07 4.88 o -7 8 1 1746.49 1643.29 37.67 o -6 8 1 521.08 555.51 10.55 o -5 8 1 63.42 60.84 3.52 o -4 8 1 885.62 892.85 15.27 o -3 8 1 118.76 123.07 4.36 o -2 8 1 813.22 800.47 12.20 o -1 8 1 220.54 225.20 5.05 o 0 8 1 1196.64 1177.73 16.91 o 1 8 1 1401.84 1371.72 19.32 o 2 8 1 142.17 152.68 4.18 o 3 8 1 558.33 570.37 9.39 o 4 8 1 1940.97 1856.95 28.94 o 5 8 1 1.84 1.09 2.66 o 6 8 1 86.56 82.30 4.64 o 7 8 1 635.67 641.28 11.86 o 8 8 1 292.33 321.18 7.29 o 9 8 1 0.74 4.01 3.59 o 10 8 1 436.49 439.65 11.19 o -10 9 1 2.94 2.80 3.66 o -9 9 1 69.16 65.67 5.92 o -8 9 1 156.29 154.34 6.36 o -7 9 1 2.27 6.33 3.55 o -6 9 1 1002.43 996.62 16.87 o -5 9 1 134.77 127.01 4.54 o -4 9 1 1070.54 1043.07 17.47 o -3 9 1 154.64 160.67 5.04 o -2 9 1 418.16 422.83 8.85 o -1 9 1 1121.68 1105.98 17.58 o 0 9 1 180.99 179.76 4.86 o 1 9 1 4.84 5.73 2.37 o 2 9 1 681.31 725.14 11.37 o 3 9 1 1793.73 1778.91 24.50 o 4 9 1 364.12 350.44 7.68 o 5 9 1 1024.52 1007.31 17.04 o 6 9 1 347.50 345.29 7.69 o 7 9 1 18.41 15.26 3.72 o 8 9 1 369.94 374.03 14.25 o 9 9 1 29.49 23.75 5.69 o -9 10 1 68.43 60.79 4.85 o -8 10 1 51.68 54.55 4.66 o -7 10 1 6.56 8.44 3.64 o -6 10 1 132.42 128.56 5.87 o -5 10 1 24.82 20.13 3.71 o -4 10 1 1046.04 1078.22 18.07 o -3 10 1 160.01 157.79 6.47 o -2 10 1 1255.68 1251.30 17.97 o -1 10 1 56.42 52.76 3.04 o 0 10 1 580.31 604.21 9.91 o 1 10 1 145.17 148.01 4.25 o 2 10 1 0.24 3.30 2.41 o 3 10 1 597.10 597.03 9.87 o 4 10 1 1152.07 1149.58 19.64 o 5 10 1 47.36 50.07 4.35 o 6 10 1 16.56 17.73 3.78 o 7 10 1 9.26 10.30 5.35 o 8 10 1 359.15 366.14 14.19 o -8 11 1 315.86 322.95 9.51 o -7 11 1 3.32 -0.07 3.55 o -6 11 1 7.63 11.50 3.81 o -5 11 1 124.32 119.49 4.60 o -4 11 1 335.78 330.99 8.05 o -3 11 1 35.92 35.45 3.35 o -2 11 1 1696.17 1693.22 25.14 o -1 11 1 12.01 10.25 2.61 o 0 11 1 108.51 106.91 3.80 o 1 11 1 58.15 55.67 3.63 o 2 11 1 799.86 791.58 17.04 o 3 11 1 434.90 425.27 10.74 o 4 11 1 0.33 0.50 3.36 o 5 11 1 109.92 95.48 7.16 o 6 11 1 33.55 32.06 4.13 o 7 11 1 27.08 19.34 5.62 o -6 12 1 565.25 573.17 14.08 o -5 12 1 7.64 7.48 3.76 o -4 12 1 151.34 147.07 5.57 o -3 12 1 56.88 48.86 3.67 o -2 12 1 1.25 0.72 2.82 o -1 12 1 149.23 148.31 4.42 o 0 12 1 656.89 676.12 12.55 o 1 12 1 13.72 12.94 3.13 o 2 12 1 150.58 148.16 5.13 o 3 12 1 27.70 27.03 4.02 o 4 12 1 147.55 156.97 6.36 o 5 12 1 11.64 15.67 3.88 o 6 12 1 23.09 28.84 5.96 o -4 13 1 97.82 91.73 5.39 o -3 13 1 8.64 9.63 3.10 o -2 13 1 538.71 544.21 10.77 o -1 13 1 113.59 93.80 4.41 o 0 13 1 27.59 32.78 3.54 o 1 13 1 126.10 122.61 4.88 o 2 13 1 7.95 7.90 3.09 o 3 13 1 22.71 21.96 4.02 o -12 0 2 75.17 81.16 7.23 o -10 0 2 1225.06 1185.12 33.12 o -8 0 2 432.99 427.85 10.28 o -6 0 2 6763.09 6139.39 106.30 o -4 0 2 2.84 17.46 3.07 o -2 0 2 80.37 80.72 3.99 o 0 0 2 4283.86 4030.29 59.18 o 2 0 2 10038.21 9894.62 239.74 o 4 0 2 7610.15 7462.69 182.00 o 6 0 2 22.53 47.71 5.42 o 8 0 2 665.71 680.15 20.68 o 10 0 2 342.91 324.53 10.47 o 12 0 2 79.43 97.02 5.32 o -13 1 2 129.35 117.35 5.87 o -12 1 2 34.39 32.66 4.16 o -11 1 2 7.05 1.57 3.45 o -10 1 2 9.97 4.32 3.57 o -9 1 2 68.48 78.20 3.75 o -8 1 2 6572.66 6239.10 76.47 o -7 1 2 3.09 4.31 2.16 o -6 1 2 389.12 428.61 7.16 o -5 1 2 67.14 68.58 2.82 o -4 1 2 62.74 106.70 3.21 o -3 1 2 1001.37 1037.03 14.25 o -2 1 2 16977.05 14880.27 206.68 o -1 1 2 1544.41 1484.20 17.74 o 0 1 2 3148.52 3173.85 36.07 o 1 1 2 5805.41 6251.73 69.43 o 2 1 2 23.42 26.70 3.22 o 3 1 2 54.62 41.98 3.50 o 4 1 2 102.69 106.63 4.68 o 5 1 2 943.58 982.81 19.51 o 6 1 2 7900.51 7437.13 128.36 o 7 1 2 26.31 28.60 3.57 o 8 1 2 106.97 112.81 10.50 o 9 1 2 5.40 9.46 3.35 o 10 1 2 75.01 77.27 3.37 o 11 1 2 10.86 11.72 2.61 o 12 1 2 118.51 117.21 4.65 o -13 2 2 79.63 77.69 5.18 o -12 2 2 679.59 650.19 14.69 o -11 2 2 41.52 38.99 4.28 o -10 2 2 1214.22 1217.06 19.48 o -9 2 2 162.42 157.62 4.82 o -8 2 2 43.74 42.69 2.70 o -7 2 2 20.63 25.62 2.43 o -6 2 2 3685.43 3586.96 44.77 o -5 2 2 165.61 192.48 4.31 o -4 2 2 4140.49 3783.29 47.01 o -3 2 2 203.72 200.15 4.29 o -2 2 2 1827.73 1756.43 22.81 o -1 2 2 1701.32 1814.03 21.34 o 0 2 2 662.22 800.95 9.56 o 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