#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015674.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2015674_Fobs
loop_
_publ_author_name
'Ogorodnyk, Ivan V.'
'Zatovsky, Igor V.'
'Baumer, Vyacheslav N.'
'Slobodyanik, Nikolay S.'
'Shishkin, Oleg V.'
_publ_section_title
;
 A disordered cerium(IV) phosphate with a tunnel structure,
 K~4~CeZr(PO~4~)~4~
;
_journal_coeditor_code           BC3019
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              i100
_journal_page_last               i102
_journal_volume                  62
_journal_year                    2006
_space_group_IT_number           141
_symmetry_space_group_name_Hall  '-I 4bd 2'
_symmetry_space_group_name_H-M   'I 41/a m d :2'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   6.7039
_cell_length_b                   6.7039
_cell_length_c                   17.0652
_exptl_crystal_F_000             724.00
_reflns_d_resolution_high        0.7110
_[local]_cod_data_source_file    bc3019Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' z28 in I4(1)/amd'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            287.70
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y+1/2, z'
'x, -y, -z'
'-x, y+1/2, -z'
'-y+1/4, -x+1/4, -z+3/4'
'y+1/4, x+3/4, -z+1/4'
'y+1/4, -x+1/4, z+3/4'
'-y+1/4, x+3/4, z+1/4'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1, z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x+1/2, y+1, -z+1/2'
'-y+3/4, -x+3/4, -z+5/4'
'y+3/4, x+5/4, -z+3/4'
'y+3/4, -x+3/4, z+5/4'
'-y+3/4, x+5/4, z+3/4'
'-x, -y, -z'
'x, y-1/2, -z'
'-x, y, z'
'x, -y-1/2, z'
'y-1/4, x-1/4, z-3/4'
'-y-1/4, -x-3/4, z-1/4'
'-y-1/4, x-1/4, -z-3/4'
'y-1/4, -x-3/4, -z-1/4'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y, -z+1/2'
'-x+1/2, y+1/2, z+1/2'
'x+1/2, -y, z+1/2'
'y+1/4, x+1/4, z-1/4'
'-y+1/4, -x-1/4, z+1/4'
'-y+1/4, x+1/4, -z-1/4'
'y+1/4, -x-1/4, -z+1/4'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 2 0 82769.99 79036.42 1494.05 o
2 2 0 1600.78 2102.42 49.23 o
0 4 0 73972.27 70013.49 887.71 o
2 4 0 16265.99 16962.96 100.61 o
4 4 0 20744.29 20741.86 255.24 o
0 6 0 21342.59 20573.16 369.91 o
2 6 0 6573.06 6435.02 102.26 o
4 6 0 7783.85 7720.07 157.09 o
6 6 0 3511.73 3064.92 163.46 o
0 8 0 7460.06 7556.03 214.13 o
2 8 0 3277.07 3100.36 114.64 o
4 8 0 3149.49 3401.88 142.11 o
0 1 1 15849.83 15869.68 116.11 o
1 2 1 29418.62 28723.53 157.83 o
0 3 1 10545.93 11131.80 76.23 o
2 3 1 18523.32 18161.36 65.85 o
1 4 1 4577.94 5154.39 35.08 o
3 4 1 3968.29 4167.23 47.86 o
0 5 1 2673.58 2791.10 44.48 o
2 5 1 5453.98 5359.36 48.37 o
4 5 1 1645.12 1546.29 50.32 o
1 6 1 10556.02 10703.46 107.18 o
3 6 1 7274.90 7187.06 87.15 o
5 6 1 3154.44 3119.08 92.05 o
0 7 1 1783.49 1735.55 97.47 o
2 7 1 2718.79 2978.58 60.73 o
4 7 1 1222.95 1143.48 66.17 o
6 7 1 1543.88 1522.42 95.79 o
1 8 1 1255.09 1084.18 54.76 o
3 8 1 976.19 800.03 64.82 o
0 9 1 871.27 757.61 94.10 o
2 9 1 1103.19 1224.53 70.86 o
1 1 2 3604.56 3376.04 54.23 o
0 2 2 4041.25 3198.47 34.94 o
1 3 2 11604.14 12386.77 53.01 o
3 3 2 14247.93 13860.75 85.48 o
0 4 2 885.70 994.55 32.20 o
2 4 2 2811.79 2593.50 29.24 o
1 5 2 2917.63 2889.96 36.54 o
3 5 2 4642.29 4861.37 68.34 o
5 5 2 2467.09 2565.22 90.49 o
0 6 2 435.76 412.31 60.72 o
2 6 2 35.09 48.17 29.96 o
4 6 2 461.61 497.15 45.12 o
1 7 2 2569.01 2502.82 62.04 o
3 7 2 3014.26 3172.48 73.39 o
5 7 2 1884.41 1768.78 101.20 o
0 8 2 315.20 230.89 73.78 o
2 8 2 386.34 440.17 53.54 o
4 8 2 36.70 42.92 75.48 o
1 9 2 1479.23 1489.00 71.57 o
0 1 3 8160.62 6673.62 31.85 o
1 2 3 952.28 997.45 21.44 o
0 3 3 18397.69 19141.65 136.99 o
2 3 3 2074.86 2296.04 28.67 o
1 4 3 4450.81 4029.44 40.17 o
3 4 3 7538.23 7329.49 67.48 o
0 5 3 1230.46 1083.35 36.49 o
2 5 3 8.09 12.40 23.29 o
4 5 3 1414.41 1450.32 58.26 o
1 6 3 673.89 773.54 37.57 o
3 6 3 1641.50 1628.97 46.02 o
5 6 3 468.10 441.32 58.23 o
0 7 3 1310.53 1453.72 78.64 o
2 7 3 449.36 368.85 41.04 o
4 7 3 1238.07 1414.35 71.84 o
6 7 3 563.71 518.45 90.05 o
1 8 3 1148.59 1140.05 59.07 o
3 8 3 1391.67 1428.91 70.04 o
0 9 3 732.78 909.56 98.44 o
2 9 3 485.98 417.04 79.77 o
0 0 4 7357.68 8255.29 169.22 o
0 2 4 18613.11 17042.76 163.25 o
2 2 4 28685.71 25820.14 200.67 o
1 3 4 26.70 44.41 12.67 o
0 4 4 2751.20 3102.86 46.78 o
2 4 4 6511.09 6796.35 47.20 o
4 4 4 1667.94 1870.47 73.86 o
1 5 4 306.37 312.37 22.62 o
3 5 4 200.84 216.05 35.19 o
0 6 4 7749.03 7652.10 92.67 o
2 6 4 9169.47 8929.93 86.58 o
4 6 4 3724.08 3569.02 94.36 o
6 6 4 3292.60 3653.33 175.02 o
1 7 4 100.35 120.80 46.25 o
3 7 4 52.76 67.79 50.56 o
5 7 4 0.48 -5.35 71.79 o
0 8 4 1165.78 1203.51 85.27 o
2 8 4 1548.77 1642.75 63.64 o
4 8 4 819.09 748.10 86.50 o
1 9 4 27.27 60.47 63.45 o
0 1 5 50165.29 53588.78 500.10 o
1 2 5 1469.50 1560.97 17.91 o
0 3 5 43397.22 41519.05 151.38 o
2 3 5 6525.60 6786.42 46.35 o
1 4 5 11610.20 11239.55 55.15 o
3 4 5 12198.57 12272.78 77.87 o
0 5 5 8806.62 8720.69 99.65 o
2 5 5 1180.95 1187.79 32.27 o
4 5 5 3296.58 3161.28 86.32 o
1 6 5 3026.09 2925.63 59.43 o
3 6 5 3395.78 3180.98 69.01 o
5 6 5 1090.19 835.63 64.62 o
0 7 5 4822.51 4866.36 103.76 o
2 7 5 1644.18 1629.85 53.06 o
4 7 5 2076.71 2283.85 71.51 o
6 7 5 840.85 722.43 101.45 o
1 8 5 2004.35 2045.22 62.86 o
3 8 5 1869.99 1872.44 77.65 o
0 9 5 2331.78 2604.12 140.50 o
2 9 5 1242.84 1214.70 84.47 o
1 1 6 19419.62 17142.18 101.17 o
0 2 6 2629.97 2041.62 20.34 o
1 3 6 23306.07 24327.09 75.01 o
3 3 6 22312.90 22274.08 248.72 o
0 4 6 37.75 58.47 22.32 o
2 4 6 984.36 912.76 24.38 o
1 5 6 7172.41 7332.18 53.21 o
3 5 6 7757.54 7694.80 88.63 o
5 5 6 3488.30 3415.81 152.26 o
0 6 6 1924.44 2023.51 63.92 o
2 6 6 594.94 496.68 35.90 o
4 6 6 705.94 666.00 58.55 o
1 7 6 5202.62 5374.33 81.60 o
3 7 6 4782.46 4961.10 85.82 o
5 7 6 2441.22 2565.81 127.48 o
0 8 6 5.49 17.46 78.02 o
2 8 6 75.67 159.72 64.61 o
4 8 6 9.53 -7.70 81.50 o
1 9 6 2585.52 2657.26 126.27 o
0 1 7 1565.07 1629.34 20.34 o
1 2 7 8249.89 8244.88 39.90 o
0 3 7 2735.39 3163.76 34.78 o
2 3 7 7322.86 6811.41 58.83 o
1 4 7 729.86 729.26 18.07 o
3 4 7 1259.98 1253.52 39.23 o
0 5 7 1827.37 1999.32 53.18 o
2 5 7 3860.48 3820.66 47.67 o
4 5 7 1230.49 1196.02 67.60 o
1 6 7 3185.26 2947.62 57.76 o
3 6 7 2859.23 3037.25 70.18 o
5 6 7 1995.35 2074.20 88.74 o
0 7 7 1300.86 1213.97 73.34 o
2 7 7 1980.55 2056.39 67.90 o
4 7 7 908.42 862.63 76.19 o
1 8 7 268.57 209.44 60.66 o
3 8 7 365.45 313.44 75.48 o
0 9 7 708.64 668.04 111.86 o
0 0 8 56556.01 56531.06 323.94 o
0 2 8 6692.27 6525.86 38.89 o
2 2 8 525.81 475.28 25.37 o
1 3 8 227.75 243.02 14.35 o
0 4 8 12904.29 12471.70 87.89 o
2 4 8 2039.02 2011.23 33.24 o
4 4 8 5042.74 4910.11 149.94 o
1 5 8 215.15 228.47 26.24 o
3 5 8 277.05 238.37 42.97 o
0 6 8 4168.29 4112.51 90.42 o
2 6 8 1079.61 992.98 50.26 o
4 6 8 2326.71 2336.49 88.07 o
6 6 8 1388.75 1281.97 138.04 o
1 7 8 13.71 46.95 54.48 o
3 7 8 24.54 24.70 51.45 o
5 7 8 7.14 11.31 82.41 o
0 8 8 1443.07 1677.48 100.14 o
2 8 8 619.35 587.76 63.69 o
0 1 9 7120.98 7953.50 42.34 o
1 2 9 6654.33 6430.19 33.00 o
0 3 9 4113.68 4094.64 42.60 o
2 3 9 4051.67 4102.86 39.20 o
1 4 9 790.56 802.57 23.31 o
3 4 9 599.44 686.34 34.72 o
0 5 9 3218.99 3401.74 100.70 o
2 5 9 3059.55 3060.96 61.19 o
4 5 9 816.94 744.64 62.99 o
1 6 9 2557.76 2566.74 62.66 o
3 6 9 1745.58 1774.82 74.27 o
5 6 9 1254.96 1158.04 92.15 o
0 7 9 1605.54 1584.26 88.72 o
2 7 9 1439.34 1467.54 57.42 o
4 7 9 522.70 469.39 78.60 o
1 8 9 91.31 67.66 65.63 o
3 8 9 94.52 95.36 69.25 o
1 1 10 15314.06 17704.31 134.11 o
0 2 10 2011.38 2104.45 30.67 o
1 3 10 16092.82 16665.70 56.99 o
3 3 10 14537.94 14739.29 109.45 o
0 4 10 48.45 85.56 33.22 o
2 4 10 856.19 727.58 31.58 o
1 5 10 4814.07 4762.95 80.45 o
3 5 10 4696.46 4700.69 93.85 o
5 5 10 1688.12 1442.91 127.01 o
0 6 10 263.64 295.15 65.02 o
2 6 10 9.93 29.89 42.14 o
4 6 10 164.03 221.88 77.26 o
1 7 10 3246.86 3335.82 81.72 o
3 7 10 2800.74 3102.57 79.17 o
0 8 10 19.38 96.29 106.37 o
2 8 10 65.92 79.33 67.02 o
0 1 11 10161.11 9641.71 75.90 o
1 2 11 1968.53 2032.79 22.86 o
0 3 11 15071.06 16170.12 154.44 o
2 3 11 5701.13 5732.90 55.96 o
1 4 11 4296.37 4658.14 61.03 o
3 4 11 6171.91 6124.59 77.80 o
0 5 11 4077.92 4310.61 79.87 o
2 5 11 1515.44 1536.98 46.47 o
4 5 11 2041.97 2082.30 84.58 o
1 6 11 799.34 818.40 47.45 o
3 6 11 1514.91 1442.59 67.73 o
5 6 11 621.16 570.25 132.87 o
0 7 11 3067.48 3088.61 112.97 o
2 7 11 1690.33 1452.63 60.91 o
4 7 11 1515.72 1445.57 83.56 o
1 8 11 1000.65 1185.70 76.46 o
0 0 12 388.42 382.25 33.14 o
0 2 12 3693.54 3989.74 43.07 o
2 2 12 8399.72 8464.43 63.55 o
1 3 12 124.17 108.04 19.98 o
0 4 12 1049.21 1188.61 53.34 o
2 4 12 3192.77 3222.37 49.87 o
4 4 12 1514.28 1472.67 76.56 o
1 5 12 15.15 7.11 41.31 o
3 5 12 3.03 43.62 48.14 o
0 6 12 2541.53 2694.07 117.29 o
2 6 12 3820.67 4073.65 79.79 o
4 6 12 2163.05 2315.13 98.70 o
1 7 12 28.63 19.54 57.39 o
3 7 12 2.57 73.31 65.02 o
0 8 12 637.31 584.59 113.80 o
0 1 13 2635.37 2694.63 36.49 o
1 2 13 75.99 84.58 19.65 o
0 3 13 3124.37 3036.22 65.80 o
2 3 13 108.65 101.40 22.33 o
1 4 13 622.65 630.08 33.17 o
3 4 13 1016.96 1131.34 45.29 o
0 5 13 1552.93 1600.62 68.62 o
2 5 13 168.36 121.58 40.02 o
4 5 13 661.30 627.74 78.66 o
1 6 13 207.03 116.59 49.00 o
3 6 13 411.63 427.47 56.80 o
5 6 13 339.15 222.71 151.24 o
0 7 13 772.84 900.99 102.32 o
2 7 13 213.65 185.86 54.14 o
1 1 14 1504.01 1497.20 43.31 o
0 2 14 63.63 83.22 31.06 o
1 3 14 1921.42 1907.59 37.04 o
3 3 14 1984.11 2095.79 69.79 o
0 4 14 547.21 501.72 48.49 o
2 4 14 244.33 251.86 30.66 o
1 5 14 626.88 580.81 48.41 o
3 5 14 702.99 699.91 44.15 o
5 5 14 288.68 458.86 196.50 o
0 6 14 3.40 62.02 93.01 o
2 6 14 28.38 27.28 53.84 o
4 6 14 100.54 163.70 94.71 o
1 7 14 581.56 550.73 65.06 o
3 7 14 538.55 547.32 70.45 o
0 1 15 2150.10 2210.47 49.29 o
1 2 15 3315.41 3495.17 41.35 o
0 3 15 1898.29 1882.91 57.32 o
2 3 15 2579.27 2530.47 41.05 o
1 4 15 860.26 853.66 38.02 o
3 4 15 722.11 665.65 43.41 o
0 5 15 837.56 839.62 63.73 o
2 5 15 1076.59 1069.09 49.29 o
4 5 15 337.18 333.50 87.27 o
1 6 15 1115.91 1133.53 60.29 o
3 6 15 808.31 884.48 63.10 o
0 7 15 555.97 532.05 114.10 o
2 7 15 579.99 529.52 62.37 o
0 0 16 15771.89 14682.22 348.18 o
0 2 16 6292.91 6236.14 89.63 o
2 2 16 1852.83 1656.99 56.21 o
1 3 16 214.30 197.57 29.84 o
0 4 16 6542.60 7235.94 115.77 o
2 4 16 2867.81 2982.90 48.19 o
4 4 16 3038.79 3361.83 103.85 o
1 5 16 21.97 47.99 51.21 o
3 5 16 12.98 46.96 52.91 o
0 6 16 3057.97 3589.65 170.71 o
2 6 16 1576.48 1522.85 64.09 o
0 1 17 1377.11 1329.37 49.54 o
1 2 17 1915.29 1980.86 44.23 o
0 3 17 641.16 626.36 52.65 o
2 3 17 1008.50 1020.75 37.41 o
1 4 17 945.50 882.58 40.68 o
3 4 17 552.45 478.36 44.66 o
0 5 17 894.75 902.76 72.09 o
2 5 17 1125.31 1117.89 50.77 o
4 5 17 710.90 783.69 82.03 o
1 6 17 1383.31 1336.67 63.31 o
1 1 18 581.11 615.10 47.25 o
0 2 18 293.29 310.23 49.34 o
1 3 18 907.66 765.94 40.43 o
3 3 18 1134.91 1191.87 72.63 o
0 4 18 23.26 11.94 57.70 o
2 4 18 36.55 58.85 40.73 o
1 5 18 484.44 413.96 56.38 o
3 5 18 632.36 706.16 59.21 o
0 6 18 105.83 100.46 106.29 o
0 1 19 241.68 343.40 49.23 o
1 2 19 133.91 119.36 35.79 o
0 3 19 581.90 612.68 63.99 o
2 3 19 397.04 314.77 39.77 o
1 4 19 311.52 317.30 47.72 o
3 4 19 476.26 437.56 52.09 o
0 5 19 6.26 11.02 76.72 o
2 5 19 2.69 51.80 63.95 o
0 0 20 636.04 596.84 106.22 o
0 2 20 1037.53 1110.48 64.93 o
2 2 20 1393.38 1513.32 62.08 o
1 3 20 13.82 55.47 49.25 o
0 4 20 344.81 264.10 75.51 o
2 4 20 511.50 433.91 50.35 o
1 5 20 0.03 -4.27 72.91 o
0 1 21 988.18 962.67 80.22 o
1 2 21 300.80 263.22 43.15 o
0 3 21 749.96 674.89 72.47 o
2 3 21 263.09 209.13 52.38 o
1 4 21 591.69 524.35 56.07 o
1 1 22 560.46 579.09 76.47 o
0 2 22 24.30 51.19 69.44 o
1 3 22 577.63 567.08 53.99 o
0 1 23 51.26 45.35 86.33 o
1 2 23 184.33 214.96 57.25 o
0 0 24 603.34 667.77 229.99 o