#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/63/2016356.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016356_Fobs loop_ _publ_author_name 'Genther, Dane J.' 'Squattrito, Philip J.' 'Kirschbaum, Kristin' 'Yearley, Eric J.' 'Pinkerton, A. Alan' _publ_section_title ; 5-Aminonaphthalene-1-sulfonic acid and its manganese, nickel and cobalt salts ; _journal_coeditor_code SK3173 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m604 _journal_page_last m609 _journal_volume 63 _journal_year 2007 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1031 _cell_length_b 22.9375 _cell_length_c 7.4607 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.7497 _[local]_cod_data_source_file sk3173IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 51Nix in P2(1)2(1)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 145.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 521.02 568.70 20.00 o 4 0 0 7579.12 7963.07 125.23 o 6 0 0 519.18 498.15 23.59 o 8 0 0 1229.68 1220.27 50.71 o 10 0 0 860.15 857.15 32.87 o 1 1 0 327.88 253.49 5.60 o 2 1 0 5657.17 5813.22 51.12 o 3 1 0 1439.70 1284.38 21.68 o 4 1 0 2432.88 2428.39 35.39 o 5 1 0 3367.72 3353.31 46.18 o 6 1 0 330.55 352.32 12.14 o 7 1 0 65.57 76.48 5.59 o 8 1 0 176.91 189.17 6.78 o 9 1 0 2.57 8.63 6.02 o 10 1 0 200.48 196.29 9.58 o 0 2 0 1289.27 1317.48 22.81 o 1 2 0 1930.75 2121.79 20.57 o 2 2 0 17640.95 18715.60 116.09 o 3 2 0 60.79 60.43 2.60 o 4 2 0 10995.73 10997.25 90.79 o 5 2 0 30.77 38.17 3.20 o 6 2 0 467.64 467.03 15.97 o 7 2 0 2497.02 2361.16 54.41 o 8 2 0 946.36 882.72 27.69 o 9 2 0 19.15 7.84 5.97 o 10 2 0 66.46 75.51 7.49 o 1 3 0 13543.76 14039.16 94.77 o 2 3 0 2780.36 2685.23 26.65 o 3 3 0 366.10 390.57 9.23 o 4 3 0 1366.22 1359.00 25.17 o 5 3 0 809.87 767.78 18.05 o 6 3 0 30.61 39.82 4.02 o 7 3 0 235.60 232.22 7.45 o 8 3 0 118.91 115.52 6.61 o 9 3 0 513.99 484.56 13.54 o 10 3 0 14.68 5.29 6.44 o 0 4 0 4334.26 4198.11 52.05 o 1 4 0 67.78 85.90 3.69 o 2 4 0 530.67 628.47 11.10 o 3 4 0 880.75 961.10 16.16 o 4 4 0 3937.63 3768.66 40.35 o 5 4 0 71.36 69.46 4.33 o 6 4 0 1333.98 1357.77 35.41 o 7 4 0 768.50 744.70 21.34 o 8 4 0 143.93 143.98 6.60 o 9 4 0 53.10 56.07 5.50 o 10 4 0 65.47 57.45 7.47 o 1 5 0 9887.29 10329.26 78.38 o 2 5 0 1316.81 1328.00 18.01 o 3 5 0 713.90 829.22 14.93 o 4 5 0 10.74 10.54 1.97 o 5 5 0 109.42 120.31 3.80 o 6 5 0 1146.81 1158.26 23.70 o 7 5 0 882.99 837.72 23.20 o 8 5 0 0.09 5.85 4.45 o 9 5 0 495.23 495.57 13.49 o 10 5 0 28.47 22.68 8.78 o 0 6 0 457.76 581.21 16.58 o 1 6 0 1245.42 1256.43 20.44 o 2 6 0 1766.32 1878.85 22.85 o 3 6 0 2899.51 2985.63 33.42 o 4 6 0 1269.26 1153.94 20.04 o 5 6 0 76.05 75.85 3.57 o 6 6 0 1514.08 1518.51 28.95 o 7 6 0 0.56 4.15 3.76 o 8 6 0 152.71 157.27 6.32 o 9 6 0 11.85 22.68 6.09 o 10 6 0 72.54 84.81 10.56 o 1 7 0 106.37 98.49 3.70 o 2 7 0 46.33 43.30 2.25 o 3 7 0 1276.84 1276.97 19.98 o 4 7 0 1420.60 1497.38 23.85 o 5 7 0 339.92 370.10 8.91 o 6 7 0 614.30 573.09 13.95 o 7 7 0 447.84 430.10 12.53 o 8 7 0 742.39 738.64 20.28 o 9 7 0 320.12 279.67 9.82 o 10 7 0 62.33 61.49 9.13 o 0 8 0 119.56 102.80 4.85 o 1 8 0 958.02 995.64 16.27 o 2 8 0 2031.42 2157.26 29.86 o 3 8 0 1017.21 1032.57 17.47 o 4 8 0 37.64 33.67 2.36 o 5 8 0 47.51 51.04 3.79 o 6 8 0 85.53 79.39 4.59 o 7 8 0 3.31 9.62 3.91 o 8 8 0 1311.92 1256.08 37.42 o 9 8 0 380.14 399.32 14.43 o 10 8 0 556.96 580.53 17.41 o 1 9 0 6295.29 6715.41 55.86 o 2 9 0 917.68 978.17 18.71 o 3 9 0 164.02 142.21 4.31 o 4 9 0 195.19 192.41 5.06 o 5 9 0 832.35 817.81 16.82 o 6 9 0 133.05 123.87 4.26 o 7 9 0 775.68 776.77 25.07 o 8 9 0 301.83 312.07 11.53 o 9 9 0 2.30 -1.56 7.40 o 10 9 0 28.61 42.04 9.18 o 0 10 0 15073.50 15710.64 175.26 o 1 10 0 896.39 1158.01 19.30 o 2 10 0 2300.12 2257.32 39.47 o 3 10 0 3178.31 3375.17 43.75 o 4 10 0 668.87 703.61 14.31 o 5 10 0 203.17 197.35 5.36 o 6 10 0 220.09 233.50 5.75 o 7 10 0 23.75 24.61 4.52 o 8 10 0 1266.52 1231.41 46.14 o 9 10 0 0.20 -1.99 7.57 o 10 10 0 787.57 759.17 24.53 o 1 11 0 71.76 98.68 3.71 o 2 11 0 3770.74 3917.10 46.49 o 3 11 0 45.65 62.08 3.32 o 4 11 0 279.60 295.63 8.12 o 5 11 0 510.26 501.41 11.22 o 6 11 0 573.94 549.59 13.71 o 7 11 0 44.91 50.86 6.71 o 8 11 0 461.89 460.38 16.57 o 9 11 0 56.96 65.99 11.33 o 10 11 0 2.58 10.77 9.48 o 0 12 0 490.89 429.14 19.15 o 1 12 0 5424.77 5825.11 51.35 o 2 12 0 2502.28 2492.43 35.91 o 3 12 0 779.99 723.04 16.52 o 4 12 0 5259.15 5085.78 60.88 o 5 12 0 289.41 303.61 8.41 o 6 12 0 626.69 636.68 18.08 o 7 12 0 69.98 63.77 7.80 o 8 12 0 1078.12 1039.28 39.82 o 9 12 0 181.01 184.71 10.28 o 1 13 0 3358.87 3249.32 36.97 o 2 13 0 11.59 18.61 2.12 o 3 13 0 1651.26 1664.21 29.26 o 4 13 0 169.94 164.83 4.58 o 5 13 0 78.64 73.88 5.16 o 6 13 0 106.10 96.77 5.90 o 7 13 0 236.92 221.51 8.69 o 8 13 0 66.11 103.38 11.44 o 9 13 0 1182.27 1194.41 44.13 o 0 14 0 904.39 923.17 32.59 o 1 14 0 116.82 125.51 7.31 o 2 14 0 796.48 750.12 16.91 o 3 14 0 74.67 69.25 4.17 o 4 14 0 3714.12 3586.08 50.20 o 5 14 0 816.64 812.91 23.27 o 6 14 0 565.47 558.23 15.89 o 7 14 0 0.16 6.27 6.21 o 8 14 0 97.21 78.90 11.95 o 9 14 0 35.29 55.54 8.79 o 1 15 0 6961.18 6787.79 60.97 o 2 15 0 843.81 803.79 17.90 o 3 15 0 3241.53 3134.60 56.88 o 4 15 0 19.78 21.55 4.73 o 5 15 0 15.42 18.05 3.85 o 6 15 0 0.17 5.97 4.46 o 7 15 0 990.48 988.26 39.04 o 8 15 0 5.48 8.82 7.58 o 9 15 0 20.84 29.16 9.02 o 0 16 0 749.88 673.59 17.59 o 1 16 0 4.34 3.97 5.95 o 2 16 0 1976.28 1906.12 32.77 o 3 16 0 2398.37 2333.43 48.46 o 4 16 0 299.52 295.82 9.75 o 5 16 0 199.55 179.82 7.55 o 6 16 0 1032.33 1045.02 28.09 o 7 16 0 88.48 83.15 8.61 o 8 16 0 151.09 166.14 10.10 o 9 16 0 32.22 48.38 9.41 o 1 17 0 920.17 907.92 15.69 o 2 17 0 1110.30 1089.77 22.77 o 3 17 0 2959.73 2793.22 55.19 o 4 17 0 6.39 7.07 3.82 o 5 17 0 2751.32 2681.72 56.55 o 6 17 0 78.00 89.77 6.67 o 7 17 0 22.28 37.20 7.01 o 8 17 0 385.04 393.24 11.54 o 0 18 0 2309.55 2216.82 40.67 o 1 18 0 312.82 336.81 7.00 o 2 18 0 4787.97 4730.40 74.63 o 3 18 0 365.87 380.65 11.72 o 4 18 0 18.78 34.93 4.07 o 5 18 0 99.66 99.69 6.28 o 6 18 0 133.57 157.61 8.57 o 7 18 0 105.39 115.24 9.13 o 8 18 0 1188.26 1184.63 42.24 o 1 19 0 8.47 12.83 3.80 o 2 19 0 968.66 889.98 24.51 o 3 19 0 960.81 919.72 26.22 o 4 19 0 222.10 227.98 7.25 o 5 19 0 126.61 127.76 6.85 o 6 19 0 0.31 0.22 5.44 o 7 19 0 1152.32 1121.49 40.90 o 8 19 0 14.48 14.13 8.92 o 0 20 0 1720.46 1780.23 35.94 o 1 20 0 732.00 673.85 20.76 o 2 20 0 1456.81 1435.29 35.43 o 3 20 0 1.09 2.65 4.21 o 4 20 0 269.53 258.90 7.72 o 5 20 0 27.60 25.16 5.16 o 6 20 0 1620.06 1574.31 39.52 o 7 20 0 282.13 276.39 10.29 o 8 20 0 12.98 19.04 9.35 o 1 21 0 38.06 62.95 7.32 o 2 21 0 202.50 232.17 7.67 o 3 21 0 4.23 5.91 4.54 o 4 21 0 737.39 703.96 20.06 o 5 21 0 40.48 60.70 6.89 o 6 21 0 0.11 -0.86 6.25 o 7 21 0 3.34 5.05 8.41 o 0 22 0 1.74 2.57 10.86 o 1 22 0 25.49 29.19 4.06 o 2 22 0 423.33 391.45 11.05 o 3 22 0 240.05 224.21 7.67 o 4 22 0 858.25 832.56 23.55 o 5 22 0 158.63 161.63 7.65 o 6 22 0 574.02 572.74 20.13 o 7 22 0 51.56 54.38 9.02 o 1 23 0 493.18 504.82 14.63 o 2 23 0 11.81 12.46 4.87 o 3 23 0 28.65 44.78 5.96 o 4 23 0 14.68 26.26 5.62 o 5 23 0 86.59 73.80 7.61 o 6 23 0 9.64 23.21 7.58 o 7 23 0 97.08 116.48 11.47 o 0 24 0 39.40 71.75 17.46 o 1 24 0 0.66 -5.58 9.14 o 2 24 0 13.78 20.37 6.08 o 3 24 0 403.61 370.61 9.99 o 4 24 0 776.43 756.69 20.15 o 5 24 0 11.85 19.11 7.64 o 6 24 0 233.25 257.58 10.52 o 1 25 0 261.75 267.51 13.05 o 2 25 0 829.08 770.40 47.62 o 3 25 0 26.90 33.02 5.95 o 4 25 0 31.46 51.87 6.86 o 5 25 0 353.57 359.14 9.75 o 6 25 0 14.38 9.83 8.63 o 0 26 0 554.01 533.44 34.18 o 1 26 0 1.22 -0.57 10.58 o 2 26 0 22.03 32.06 10.78 o 3 26 0 405.90 436.48 11.88 o 4 26 0 33.95 33.33 6.91 o 5 26 0 129.29 137.85 9.41 o 1 27 0 1.40 -6.62 11.07 o 2 27 0 28.61 47.31 12.17 o 3 27 0 339.13 306.27 26.10 o 4 27 0 161.58 192.40 10.01 o 5 27 0 1322.31 1356.40 31.69 o 0 28 0 1061.83 1055.83 63.05 o 1 28 0 128.95 120.46 14.93 o 2 28 0 387.96 404.61 17.56 o 3 28 0 255.03 297.33 16.75 o 4 28 0 15.80 14.51 10.84 o 1 29 0 87.91 125.91 15.61 o 2 29 0 194.57 237.95 16.69 o 3 29 0 336.13 393.88 17.72 o 0 30 0 221.84 219.65 23.50 o 1 30 0 88.58 83.40 13.99 o 2 30 0 339.45 330.25 52.83 o 0 0 1 1052.40 1155.36 25.71 o 1 0 1 9144.21 9132.78 86.49 o 2 0 1 808.91 913.54 23.36 o 3 0 1 2607.76 2639.44 49.24 o 4 0 1 5137.85 5370.92 71.54 o 5 0 1 1676.77 1712.88 38.95 o 6 0 1 1482.34 1441.82 37.40 o 7 0 1 1530.40 1504.85 40.43 o 8 0 1 163.21 166.32 8.07 o 9 0 1 606.30 599.72 18.28 o 10 0 1 40.10 51.46 7.57 o -10 1 1 0.86 6.80 7.59 o -9 1 1 138.39 133.99 8.00 o -8 1 1 216.19 203.23 8.37 o -7 1 1 309.81 302.78 10.23 o -6 1 1 338.63 348.79 12.35 o -5 1 1 899.51 917.42 25.82 o -4 1 1 2268.91 2252.75 42.38 o -3 1 1 3427.88 3782.56 61.18 o -2 1 1 21041.58 22548.79 196.94 o -1 1 1 8225.83 8770.66 74.72 o 0 1 1 810.18 792.36 11.69 o 1 1 1 7884.30 8123.37 98.43 o 2 1 1 20082.78 21367.04 168.02 o 3 1 1 3611.25 4001.61 62.99 o 4 1 1 2495.53 2491.10 45.46 o 5 1 1 886.22 890.18 25.43 o 6 1 1 397.05 406.73 11.77 o 7 1 1 339.00 344.36 11.80 o 8 1 1 252.90 249.03 14.01 o 9 1 1 139.69 129.31 9.11 o 10 1 1 1.83 11.47 7.61 o -10 2 1 30.49 31.88 8.42 o -9 2 1 296.25 301.96 8.87 o -8 2 1 657.47 640.01 20.11 o -7 2 1 1695.41 1710.25 43.61 o -6 2 1 449.85 421.29 14.73 o -5 2 1 51.29 58.76 5.82 o -4 2 1 597.22 614.31 18.39 o -3 2 1 12671.45 13400.23 131.38 o -2 2 1 7156.81 7695.39 71.18 o -1 2 1 5865.71 6036.08 62.98 o 0 2 1 55.51 52.36 1.95 o 1 2 1 6241.09 6362.23 69.46 o 2 2 1 7176.89 7626.37 72.01 o 3 2 1 12893.81 13460.11 111.59 o 4 2 1 493.70 520.54 14.46 o 5 2 1 76.34 75.21 3.99 o 6 2 1 376.48 358.87 10.66 o 7 2 1 1630.86 1638.94 43.38 o 8 2 1 625.40 593.16 19.01 o 9 2 1 285.26 269.66 8.90 o 10 2 1 19.57 18.75 6.54 o -10 3 1 40.69 35.62 7.25 o -9 3 1 8.20 14.19 5.42 o -8 3 1 1413.27 1365.74 38.36 o -7 3 1 140.40 151.46 6.91 o -6 3 1 180.67 190.55 8.51 o -5 3 1 951.11 941.25 25.56 o -4 3 1 2296.98 2283.89 41.69 o -3 3 1 1272.69 1274.85 21.52 o -2 3 1 1285.88 1388.51 19.08 o -1 3 1 1023.74 1070.01 17.73 o 0 3 1 2586.57 2626.48 23.01 o 1 3 1 1128.94 1146.90 13.72 o 2 3 1 1462.74 1557.42 23.00 o 3 3 1 1132.16 1162.01 23.38 o 4 3 1 2176.39 2183.69 36.80 o 5 3 1 1026.06 1006.69 23.57 o 6 3 1 265.87 255.78 8.51 o 7 3 1 181.76 172.95 6.43 o 8 3 1 1428.80 1365.43 38.57 o 9 3 1 4.57 14.06 5.40 o 10 3 1 23.62 28.76 6.59 o -10 4 1 223.65 206.74 10.65 o -9 4 1 64.10 69.18 6.32 o -8 4 1 671.18 674.87 18.88 o -7 4 1 301.34 293.59 9.63 o -6 4 1 256.83 264.23 11.56 o -5 4 1 1873.07 1862.25 39.82 o -4 4 1 707.37 696.70 14.91 o -3 4 1 1266.41 1194.62 17.41 o -2 4 1 2543.37 2646.85 29.26 o -1 4 1 1765.78 1825.95 25.74 o 0 4 1 8808.65 9215.85 66.23 o 1 4 1 1943.53 2004.55 22.61 o 2 4 1 2488.43 2546.92 31.52 o 3 4 1 1338.16 1286.45 25.15 o 4 4 1 682.08 688.01 16.29 o 5 4 1 2003.11 2017.80 34.97 o 6 4 1 217.47 219.75 6.52 o 7 4 1 245.60 225.95 6.90 o 8 4 1 645.41 631.95 18.42 o 9 4 1 79.40 69.73 6.79 o 10 4 1 190.10 199.59 10.35 o -10 5 1 256.63 239.97 10.91 o -9 5 1 66.52 70.38 7.51 o -8 5 1 885.70 855.03 23.36 o -7 5 1 132.93 134.97 5.32 o -6 5 1 174.16 175.94 5.47 o -5 5 1 978.64 984.18 19.83 o -4 5 1 1776.04 1821.44 24.48 o -3 5 1 226.95 205.57 5.18 o -2 5 1 384.16 367.85 10.13 o -1 5 1 4035.29 4135.39 43.84 o 0 5 1 5309.16 5493.67 39.17 o 1 5 1 4170.57 4281.46 41.22 o 2 5 1 486.31 459.72 12.53 o 3 5 1 197.68 186.23 6.02 o 4 5 1 1792.56 1872.07 34.02 o 5 5 1 912.48 901.91 20.79 o 6 5 1 209.81 214.09 6.42 o 7 5 1 129.16 134.12 5.48 o 8 5 1 874.38 840.66 23.91 o 9 5 1 55.49 69.81 8.02 o 10 5 1 272.06 270.78 9.42 o -10 6 1 298.33 286.76 12.90 o -8 6 1 817.15 799.52 21.54 o -7 6 1 380.08 384.17 11.08 o -6 6 1 264.26 273.33 8.13 o -5 6 1 319.31 285.91 7.63 o -4 6 1 2327.82 2443.76 30.00 o -3 6 1 969.15 916.78 14.99 o -2 6 1 320.41 337.06 9.90 o -1 6 1 3856.44 3894.53 43.59 o 0 6 1 14097.92 14772.21 128.11 o 1 6 1 3469.36 3502.96 37.78 o 2 6 1 341.48 363.53 9.56 o 3 6 1 893.82 880.33 20.72 o 4 6 1 2291.13 2431.97 36.60 o 5 6 1 400.51 359.45 10.08 o 6 6 1 318.34 334.16 9.06 o 7 6 1 412.56 415.70 12.76 o 8 6 1 814.49 793.36 22.29 o 9 6 1 78.20 89.61 7.26 o 10 6 1 297.79 310.95 15.39 o -10 7 1 102.52 111.05 12.24 o -9 7 1 330.68 330.13 11.75 o -8 7 1 525.32 495.20 19.06 o -7 7 1 474.01 463.98 13.17 o -6 7 1 998.47 1011.10 21.36 o -5 7 1 65.33 66.92 3.72 o -4 7 1 3203.76 3384.33 37.40 o -3 7 1 667.29 663.02 13.84 o -2 7 1 550.61 521.22 14.13 o -1 7 1 467.43 470.18 12.34 o 0 7 1 2141.07 2315.30 25.71 o 1 7 1 570.12 567.64 12.73 o 2 7 1 707.15 643.05 26.07 o 3 7 1 568.31 596.22 14.19 o 4 7 1 3498.26 3631.81 46.87 o 5 7 1 63.83 68.95 3.95 o 6 7 1 864.41 866.56 20.92 o 7 7 1 411.80 409.29 13.42 o 8 7 1 490.49 481.00 13.56 o 9 7 1 310.41 332.69 11.15 o 10 7 1 114.98 121.61 13.90 o -10 8 1 13.15 11.10 9.18 o -9 8 1 472.66 482.06 15.04 o -8 8 1 157.25 155.64 8.38 o -7 8 1 645.88 665.70 21.41 o -6 8 1 1690.43 1752.09 31.55 o -5 8 1 720.45 750.83 14.76 o -4 8 1 1332.36 1320.90 20.57 o -3 8 1 849.40 851.52 20.52 o -2 8 1 229.09 273.77 9.91 o -1 8 1 4150.32 4244.46 49.48 o 0 8 1 990.77 1077.35 16.71 o 1 8 1 3731.64 3827.39 42.55 o 2 8 1 288.58 351.27 9.69 o 3 8 1 873.51 883.50 18.79 o 4 8 1 1341.77 1323.83 28.74 o 5 8 1 584.17 601.84 14.23 o 6 8 1 1750.91 1772.11 34.48 o 7 8 1 759.97 744.80 21.00 o 8 8 1 178.01 185.44 7.31 o 9 8 1 474.99 473.50 13.87 o 10 8 1 11.61 17.48 8.95 o -10 9 1 0.28 1.25 9.29 o -9 9 1 430.66 424.59 16.94 o -8 9 1 155.71 138.23 8.23 o -7 9 1 58.64 57.46 13.02 o -5 9 1 151.97 165.59 4.33 o -4 9 1 1664.32 1642.62 27.28 o -3 9 1 1262.15 1273.27 27.44 o -2 9 1 42.05 81.70 6.96 o -1 9 1 4895.72 5008.40 57.26 o 0 9 1 1567.76 1727.70 24.36 o 1 9 1 5176.25 5348.85 60.15 o 2 9 1 65.09 90.07 3.34 o 3 9 1 1153.77 1195.27 23.02 o 4 9 1 1700.88 1678.63 29.85 o 5 9 1 152.18 161.88 5.10 o 6 9 1 47.96 42.53 3.71 o 7 9 1 52.82 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