#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016414.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016414_Fobs loop_ _publ_author_name 'Diab, Lisa' 'Daran, Jean-Claude' 'Gouygou, Maryse' 'Manoury, Eric' 'Urrutigo\"ity, Martine' _publ_section_title ; New enantiopure palladium(II) complexes from a stereodynamic 2,2'-biphosphole ligand ; _journal_coeditor_code SQ3103 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m43 _journal_page_last m45 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.868 _cell_angle_gamma 90.000 _cell_length_a 8.9627 _cell_length_b 12.1395 _cell_length_c 13.9887 _exptl_crystal_F_000 700.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file sq31034bsup3.hkl _[local]_cod_data_source_block 4b #BEGIN Tags that were not found in dictionaries: _shelx_title ' LD260706' _shelx_refln_list_code 4 _shelx_f_calc_maximum 227.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 -10 0 224.62 514.48 397.34 o 5 -9 0 320.18 313.47 358.75 o 5 -8 0 273.07 442.37 317.23 o 5 -7 0 712.11 556.24 272.99 o 5 -6 0 1712.05 1410.86 231.41 o 4 -5 0 59.06 115.72 180.88 o 5 -5 0 842.82 840.14 200.88 o 4 -4 0 8473.06 9174.04 188.41 o 5 -4 0 2932.80 3305.35 150.02 o 3 -3 0 13041.35 12745.15 182.12 o 4 -3 0 592.60 561.61 111.00 o 5 -3 0 463.92 531.07 96.27 o 3 -2 0 6586.77 6556.68 107.89 o 4 -2 0 14183.04 15486.36 138.40 o 5 -2 0 2848.06 2203.92 65.25 o 3 -1 0 13011.29 12934.09 105.75 o 4 -1 0 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