#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016503.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016503_Fobs loop_ _publ_author_name 'Dahlenburg, Lutz' 'Heinemann, Frank W.' 'Kramer, Dagmar' 'Menzel, Ralf' _publ_section_title ; syn-Tri-\m-chlorido-bis{[(R,R)/(S,S)-2,2'-bis(diphenylphosphino)-1,1'-biphenyl]hydridoiridium(III)} tetrafluoridoborate dichloromethane disolvate ; _journal_coeditor_code JZ3123 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m144 _journal_page_last m146 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.701 _cell_angle_beta 86.357 _cell_angle_gamma 86.228 _cell_length_a 13.6578 _cell_length_b 14.7640 _cell_length_c 18.5300 _exptl_crystal_F_000 1760.00 _reflns_d_resolution_high 0.7600 _[local]_cod_data_source_file jz3123Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LD0704 in P-1, MENZEL/DAHLENBURG, RM 128' _shelx_refln_list_code 4 _shelx_F_calc_maximum 378.00 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 3185.60 3389.20 56.57 o 4 0 0 1368.65 1610.28 50.72 o 5 0 0 346.18 437.12 40.79 o 6 0 0 8610.54 9092.84 139.61 o 7 0 0 43254.71 43374.12 480.64 o 8 0 0 15474.24 15455.64 218.89 o 9 0 0 178.58 342.07 75.13 o 10 0 0 3192.96 3130.21 102.67 o 11 0 0 667.02 673.17 81.40 o 12 0 0 509.07 569.23 93.55 o 13 0 0 1806.12 1731.60 120.30 o 14 0 0 935.88 1363.82 209.11 o 15 0 0 8216.25 8793.03 259.63 o 16 0 0 1267.47 1861.58 223.33 o 17 0 0 3057.78 3917.85 266.22 o -17 1 0 110.04 -13.73 194.86 o -16 1 0 2213.07 2557.55 253.82 o -15 1 0 43.93 273.82 150.23 o -14 1 0 10978.02 10970.38 241.62 o -13 1 0 6040.88 6801.10 315.43 o -12 1 0 229.11 145.24 94.32 o -11 1 0 406.09 510.33 92.31 o -10 1 0 378.39 237.66 75.64 o -9 1 0 5070.56 5481.82 125.06 o -8 1 0 2992.44 2773.22 90.48 o -7 1 0 17478.67 17274.55 228.07 o -6 1 0 67100.02 66704.77 694.85 o -5 1 0 7659.31 7729.13 118.40 o -4 1 0 5439.58 5779.14 113.28 o -3 1 0 1806.10 2091.49 70.62 o -2 1 0 162.33 245.78 40.53 o 3 1 0 842.34 1001.13 54.63 o 4 1 0 8998.24 8987.85 110.40 o 5 1 0 6840.96 6834.74 99.59 o 6 1 0 1308.83 1275.24 52.58 o 7 1 0 17809.29 18505.11 220.82 o 8 1 0 3072.50 2966.62 118.59 o 9 1 0 18035.25 18301.33 235.45 o 10 1 0 1087.79 1117.25 80.06 o 11 1 0 6714.12 6472.45 143.03 o 12 1 0 3917.87 4027.94 129.84 o 13 1 0 77.80 57.04 99.90 o 14 1 0 1753.40 1553.43 133.07 o 15 1 0 175.75 469.42 150.50 o 16 1 0 5826.26 6038.53 237.76 o 17 1 0 2918.24 3050.38 294.85 o -17 2 0 255.19 3.55 316.38 o -16 2 0 47.60 237.45 169.28 o -15 2 0 921.59 551.77 172.91 o -14 2 0 879.43 1345.17 158.40 o -13 2 0 11963.19 12070.43 307.64 o -12 2 0 28197.16 27846.38 388.27 o -11 2 0 1898.88 2097.75 117.86 o -10 2 0 1895.46 1615.71 91.40 o -9 2 0 180.01 187.56 68.06 o -8 2 0 65.74 183.46 53.60 o -7 2 0 9027.67 8515.75 144.05 o -6 2 0 3143.42 3708.78 98.69 o -5 2 0 117779.27 121098.10 1363.06 o -4 2 0 4811.26 4887.13 102.38 o -3 2 0 12258.28 12056.82 166.74 o -2 2 0 369.52 446.56 42.13 o -1 2 0 9582.67 6477.56 187.63 o 2 2 0 6148.34 6073.88 71.46 o 3 2 0 4125.08 4072.44 61.00 o 4 2 0 5095.61 5006.25 75.59 o 5 2 0 22162.45 21975.17 234.82 o 6 2 0 538.16 771.01 47.43 o 7 2 0 5020.19 5167.30 99.25 o 8 2 0 2470.27 2064.48 77.52 o 9 2 0 6.03 57.65 69.44 o 10 2 0 30856.88 29938.79 351.48 o 11 2 0 9109.59 8897.38 170.60 o 12 2 0 6932.92 7252.90 164.20 o 13 2 0 19772.39 19658.95 330.96 o 14 2 0 113.26 220.43 144.90 o 15 2 0 151.33 70.75 141.29 o 16 2 0 38.34 -107.56 148.00 o 17 2 0 385.42 511.56 158.59 o -17 3 0 1639.01 1570.95 215.99 o -16 3 0 85.61 105.41 193.31 o -15 3 0 190.70 315.05 187.97 o -14 3 0 792.38 692.67 189.87 o -13 3 0 2857.25 3092.50 247.00 o -12 3 0 5359.49 5233.33 297.02 o -11 3 0 72020.05 70489.46 789.68 o -10 3 0 315.89 350.90 97.77 o -9 3 0 9540.57 8833.56 164.47 o -8 3 0 6482.89 6264.53 127.94 o -7 3 0 550.87 369.17 46.95 o -6 3 0 26634.29 27066.80 373.73 o -5 3 0 137.52 -14.41 70.56 o -4 3 0 97231.73 100209.50 1100.78 o -3 3 0 5895.76 5388.09 93.78 o -2 3 0 711.94 860.32 25.73 o -1 3 0 85095.68 83274.98 799.43 o 0 3 0 20686.41 21290.46 183.70 o 1 3 0 2795.00 3736.34 78.53 o 2 3 0 10322.85 10917.40 118.53 o 3 3 0 7011.48 7409.89 94.12 o 4 3 0 6364.67 6289.07 89.15 o 5 3 0 1724.98 1833.60 54.91 o 6 3 0 29060.69 28482.45 300.86 o 7 3 0 5287.77 5056.20 96.88 o 8 3 0 197.03 188.30 63.29 o 9 3 0 4745.72 4714.86 107.50 o 10 3 0 614.97 557.13 87.90 o 11 3 0 13502.79 13583.55 213.72 o 12 3 0 18859.19 18924.04 276.58 o 13 3 0 5423.22 6490.23 226.62 o 14 3 0 21801.33 21706.69 307.44 o 15 3 0 1519.89 1337.61 146.37 o 16 3 0 815.98 658.47 134.64 o 17 3 0 5.99 98.26 156.28 o -17 4 0 5717.17 5887.34 287.52 o -16 4 0 323.70 561.66 203.14 o -15 4 0 653.67 548.96 162.97 o -14 4 0 27.54 -92.03 164.12 o -13 4 0 1595.70 1511.55 119.77 o -12 4 0 12638.01 12652.86 293.80 o -11 4 0 612.11 577.50 100.93 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226.17 169.30 o -12 5 0 371.18 209.53 207.80 o -11 5 0 8347.50 7944.24 164.74 o -10 5 0 4435.46 4308.55 108.48 o -9 5 0 14433.73 14241.43 185.98 o -8 5 0 6798.01 6642.28 113.00 o -7 5 0 7989.97 8216.40 155.57 o -6 5 0 25495.16 25885.69 277.25 o -5 5 0 326.82 170.80 36.93 o -4 5 0 3025.59 3270.40 64.62 o -3 5 0 231.85 145.83 36.98 o -2 5 0 637.37 728.42 25.29 o -1 5 0 41675.94 43407.04 340.12 o 0 5 0 7284.32 7759.94 93.64 o 1 5 0 18661.68 20093.80 223.20 o 2 5 0 46811.21 49213.54 565.70 o 3 5 0 1113.03 1177.76 43.05 o 4 5 0 2667.38 2700.49 69.40 o 5 5 0 170.39 143.97 44.24 o 6 5 0 15042.02 15031.71 186.99 o 7 5 0 21525.28 20847.00 246.62 o 8 5 0 1220.82 1329.87 82.64 o 9 5 0 36266.88 35947.76 398.32 o 10 5 0 10011.11 9672.71 146.34 o 11 5 0 1571.93 1643.65 78.95 o 12 5 0 791.95 851.56 77.81 o 13 5 0 1365.74 1370.04 98.32 o 14 5 0 1058.14 1187.34 146.73 o 15 5 0 1707.18 1917.26 125.84 o 16 5 0 3055.37 3641.46 185.18 o 17 5 0 3555.42 3749.92 237.31 o -16 6 0 56.09 348.50 205.98 o -15 6 0 8467.24 8034.29 268.06 o -14 6 0 2003.64 2304.94 203.53 o -13 6 0 3627.36 3494.99 190.76 o -12 6 0 7086.03 7065.34 215.72 o -11 6 0 47.82 13.48 109.15 o -10 6 0 4086.02 3888.90 139.87 o -9 6 0 282.89 180.40 69.45 o -8 6 0 3611.72 3530.64 88.54 o -7 6 0 10308.02 10583.31 143.96 o -6 6 0 108.35 72.91 55.91 o -5 6 0 26344.11 25819.46 292.15 o -4 6 0 3150.49 3134.81 71.17 o -3 6 0 5708.96 6522.76 82.92 o -2 6 0 274.68 282.65 26.84 o -1 6 0 1142.81 1185.28 37.92 o 0 6 0 17391.50 17303.04 184.74 o 1 6 0 66007.42 66844.81 770.80 o 2 6 0 16725.36 16193.42 181.42 o 3 6 0 70220.66 71940.20 817.47 o 4 6 0 3028.23 3188.73 77.78 o 5 6 0 8197.54 8374.14 137.37 o 6 6 0 1737.34 1593.10 67.85 o 7 6 0 254.36 261.85 67.38 o 8 6 0 17657.94 17375.04 227.34 o 9 6 0 19.52 20.10 72.54 o 10 6 0 12257.76 11923.40 192.88 o 11 6 0 6494.32 6661.38 152.91 o 12 6 0 1774.39 1800.32 117.23 o 13 6 0 1580.35 1809.29 127.43 o 14 6 0 663.31 754.92 129.30 o 15 6 0 3013.67 2960.69 173.04 o 16 6 0 698.46 1120.18 188.94 o 17 6 0 681.15 1386.61 261.42 o -16 7 0 295.90 181.39 239.33 o -15 7 0 1081.40 1166.95 223.09 o -14 7 0 1477.22 1620.07 257.73 o -13 7 0 9017.35 9162.93 266.75 o -12 7 0 1501.54 1628.71 142.84 o -11 7 0 5613.77 5682.02 152.59 o -10 7 0 3267.89 3113.89 102.84 o -9 7 0 1219.99 1201.23 81.79 o -8 7 0 458.49 457.50 61.93 o -7 7 0 531.39 404.12 62.57 o -6 7 0 30038.03 29214.07 344.46 o -5 7 0 2352.29 2222.79 101.69 o -4 7 0 17319.77 17063.41 190.24 o -3 7 0 26222.57 26039.64 240.16 o -2 7 0 2168.91 2012.93 43.24 o -1 7 0 1210.09 1021.74 41.03 o 0 7 0 6632.81 6404.69 97.73 o 1 7 0 13910.89 13258.00 171.89 o 2 7 0 68856.66 69690.84 641.46 o 3 7 0 59.94 -58.05 58.05 o 4 7 0 71295.96 70042.14 819.51 o 5 7 0 7868.71 7878.80 139.75 o 6 7 0 20726.54 20570.25 315.31 o 7 7 0 2460.13 2561.02 93.31 o 8 7 0 326.28 222.82 80.31 o 9 7 0 3258.28 3412.83 123.70 o 10 7 0 2198.74 2096.31 104.43 o 11 7 0 1841.75 2045.72 110.62 o 12 7 0 11983.76 11744.95 277.17 o 13 7 0 76.09 252.72 116.87 o 14 7 0 1970.41 1891.94 143.42 o 15 7 0 145.24 223.11 143.39 o 16 7 0 3067.20 3477.38 226.24 o -15 8 0 35.22 -66.96 290.30 o -14 8 0 363.47 450.83 155.43 o -13 8 0 159.11 95.26 163.20 o -12 8 0 13018.14 12498.78 248.93 o -11 8 0 487.12 363.87 103.81 o -10 8 0 5968.84 5862.88 142.80 o -9 8 0 12428.05 12071.94 178.20 o -8 8 0 48.04 60.15 58.33 o -7 8 0 19.99 70.21 53.65 o -6 8 0 2610.23 2645.39 92.53 o -5 8 0 27799.86 27763.49 278.10 o -4 8 0 17734.71 16946.55 183.90 o -3 8 0 6849.96 7089.80 91.50 o -2 8 0 13911.08 13313.49 140.65 o -1 8 0 3100.72 3050.98 60.88 o 0 8 0 1994.12 2124.15 59.31 o 1 8 0 6999.06 7410.13 108.34 o 2 8 0 51.69 90.30 50.68 o 3 8 0 45165.09 45630.66 449.49 o 4 8 0 6102.84 6080.98 115.74 o 5 8 0 9116.75 8523.72 168.74 o 6 8 0 11006.26 11355.39 186.57 o 7 8 0 10902.00 10905.61 187.91 o 8 8 0 5445.64 5579.66 170.43 o 9 8 0 100.44 157.54 89.36 o 10 8 0 5274.83 5153.34 157.76 o 11 8 0 10340.97 10096.75 249.32 o 12 8 0 73.19 292.15 132.22 o 13 8 0 14388.50 14434.22 315.96 o 14 8 0 599.72 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6587.09 351.91 o -13 11 0 4741.36 4869.42 357.04 o -12 11 0 93.14 58.46 154.07 o -11 11 0 802.19 498.21 161.14 o -10 11 0 641.90 736.34 134.93 o -9 11 0 2095.80 2019.23 144.63 o -8 11 0 22389.18 22432.22 391.19 o -7 11 0 720.49 551.08 103.78 o -6 11 0 20734.29 20865.09 409.28 o -5 11 0 5167.22 4955.47 138.77 o -4 11 0 11902.51 11768.81 193.67 o -3 11 0 1311.72 1397.88 70.44 o -2 11 0 136.51 227.51 68.93 o -1 11 0 3680.91 3749.64 92.12 o 0 11 0 20885.38 21396.62 241.80 o 1 11 0 443.97 442.69 64.17 o 2 11 0 31688.51 32494.98 332.85 o 3 11 0 4018.50 4121.14 107.29 o 4 11 0 1146.90 1102.35 81.13 o 5 11 0 2856.98 2829.69 100.02 o 6 11 0 3864.26 3912.40 120.08 o 7 11 0 2854.87 2703.07 108.67 o 8 11 0 44.44 -86.38 105.15 o 9 11 0 17084.63 17007.27 284.74 o 10 11 0 9176.78 8779.12 230.38 o 11 11 0 496.45 735.87 155.08 o 12 11 0 4739.81 4095.07 250.82 o 13 11 0 49.61 215.99 240.54 o 14 11 0 44.98 72.98 262.64 o -12 12 0 8265.90 8263.46 341.77 o -11 12 0 131.44 195.79 171.14 o -10 12 0 5757.84 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3924.92 172.93 o -3 13 0 26128.13 25460.75 332.06 o -2 13 0 3169.13 2936.36 107.57 o -1 13 0 3549.93 3556.27 103.21 o 0 13 0 975.26 1014.34 79.40 o 1 13 0 212.09 151.13 75.05 o 2 13 0 3177.46 3108.07 117.23 o 3 13 0 373.84 386.78 91.27 o 4 13 0 13547.04 13483.83 262.36 o 5 13 0 12721.26 12559.57 273.39 o 6 13 0 360.91 339.12 108.48 o 7 13 0 9308.99 9188.72 204.23 o 8 13 0 497.01 498.76 150.45 o 9 13 0 650.05 438.96 153.38 o 10 13 0 388.93 259.10 178.34 o 11 13 0 7.60 14.99 224.61 o 12 13 0 5411.42 5114.47 297.48 o 13 13 0 2519.00 3085.50 430.55 o -10 14 0 2428.75 2547.43 265.52 o -9 14 0 10619.76 11021.95 521.21 o -8 14 0 604.05 301.95 191.97 o -7 14 0 239.35 171.80 132.78 o -6 14 0 423.78 448.87 149.30 o -5 14 0 1859.49 1910.64 196.09 o -4 14 0 3698.12 4194.18 277.47 o -3 14 0 663.27 522.76 100.65 o -2 14 0 19731.93 19568.06 264.19 o -1 14 0 6125.47 6126.76 154.48 o 0 14 0 619.19 640.58 85.07 o 1 14 0 2691.31 2782.75 106.66 o 2 14 0 1121.57 1143.39 101.34 o 3 14 0 142.67 -86.86 86.86 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