#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016825.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016825_Fobs loop_ _publ_author_name 'Cadoni, Marcella' 'Ferraris, Giovanni' _publ_section_title ; Penkvilksite-2O: Na~2~TiSi~4~O~11~·2H~2~O ; _journal_coeditor_code FA3162 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i87 _journal_page_last i90 _journal_volume 64 _journal_year 2008 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2a 2n' _symmetry_space_group_name_H-M 'P n c a' _audit_update_record ; 2008-07-28 # Formatted by publCIF ; _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.3204 _cell_length_b 8.7378 _cell_length_c 7.3854 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.7500 _[local]_cod_data_source_file fa3162Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sdt90_3 in Pnca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 193.07 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22955.74 21459.44 482.04 o 4 0 0 12938.66 12922.29 339.25 o 6 0 0 840.25 779.78 75.54 o 8 0 0 3269.03 2736.58 72.27 o 10 0 0 4912.63 4402.39 117.14 o 12 0 0 24138.85 21300.67 376.65 o 14 0 0 1508.09 1554.44 103.76 o 16 0 0 123.22 170.64 76.37 o 18 0 0 1536.01 1464.42 109.24 o 20 0 0 3132.21 3161.55 129.39 o 2 1 0 5591.95 4859.63 66.16 o 4 1 0 977.59 1166.52 39.20 o 6 1 0 8.57 10.89 24.22 o 8 1 0 7853.76 8018.85 115.63 o 10 1 0 1048.72 1075.15 56.05 o 12 1 0 4409.83 4012.51 88.67 o 14 1 0 3755.95 3204.93 85.59 o 16 1 0 1502.35 1453.82 86.35 o 18 1 0 97.73 106.55 82.16 o 20 1 0 436.88 381.42 104.04 o 0 2 0 4943.26 5978.23 132.18 o 2 2 0 1401.78 983.35 33.55 o 4 2 0 462.89 509.73 30.59 o 6 2 0 521.59 202.71 26.00 o 8 2 0 8151.72 7645.43 125.70 o 10 2 0 1568.36 1403.44 66.27 o 12 2 0 129.57 177.94 59.31 o 14 2 0 32.33 -11.70 55.38 o 16 2 0 739.74 811.29 80.47 o 18 2 0 3938.89 3468.71 111.74 o 20 2 0 2489.54 2231.85 97.17 o 2 3 0 7995.85 7024.35 94.07 o 4 3 0 117.95 388.16 28.09 o 6 3 0 145.42 279.82 29.72 o 8 3 0 21.23 68.26 25.91 o 10 3 0 892.02 857.16 59.41 o 12 3 0 778.88 995.70 58.63 o 14 3 0 0.89 73.54 46.77 o 16 3 0 204.73 219.96 66.82 o 18 3 0 562.78 529.58 77.27 o 20 3 0 6.34 23.82 61.02 o 0 4 0 27910.01 30359.39 778.51 o 2 4 0 3037.91 3165.11 56.34 o 4 4 0 4153.60 3635.80 66.81 o 6 4 0 11147.35 10247.38 134.39 o 8 4 0 9879.10 9652.49 133.89 o 10 4 0 165.52 231.70 34.97 o 12 4 0 1340.50 1306.75 51.92 o 14 4 0 8.88 27.82 51.81 o 16 4 0 973.75 958.13 86.42 o 18 4 0 3684.46 3355.06 115.04 o 20 4 0 2998.21 2835.64 108.93 o 2 5 0 5279.12 5508.96 83.09 o 4 5 0 8908.65 8147.37 110.72 o 6 5 0 129.55 161.80 35.14 o 8 5 0 14994.79 14851.93 177.66 o 10 5 0 691.15 838.06 55.67 o 12 5 0 716.61 835.29 66.23 o 14 5 0 22.98 107.74 52.60 o 16 5 0 1468.54 1601.15 70.48 o 18 5 0 1382.59 1683.12 160.28 o 0 6 0 6548.26 6352.79 152.56 o 2 6 0 5752.27 5629.98 90.56 o 4 6 0 2646.64 2402.45 61.71 o 6 6 0 8191.07 7995.88 118.45 o 8 6 0 2.10 24.50 51.31 o 10 6 0 7934.10 7480.34 130.33 o 12 6 0 1948.73 2302.74 90.44 o 14 6 0 717.80 889.46 83.17 o 16 6 0 2204.38 2231.91 117.91 o 18 6 0 708.78 824.98 103.12 o 2 7 0 64.09 125.84 47.11 o 4 7 0 1046.50 1055.30 54.36 o 6 7 0 552.82 652.01 46.33 o 8 7 0 458.69 455.32 64.35 o 10 7 0 695.16 812.59 67.50 o 12 7 0 2280.73 2063.44 91.88 o 14 7 0 0.82 -8.38 62.22 o 16 7 0 206.26 441.39 87.18 o 0 8 0 4153.13 3928.83 132.26 o 2 8 0 514.24 627.37 60.27 o 4 8 0 11783.91 9835.80 201.22 o 6 8 0 1626.38 1619.02 72.38 o 8 8 0 1469.00 1611.31 94.31 o 10 8 0 222.39 294.45 112.69 o 12 8 0 161.43 123.66 65.76 o 14 8 0 809.78 927.04 86.99 o 2 9 0 1837.01 1711.73 71.97 o 4 9 0 744.92 629.49 73.97 o 6 9 0 45.13 27.99 60.66 o 8 9 0 255.48 191.17 71.59 o 10 9 0 553.47 553.53 106.16 o 12 9 0 10.09 -15.71 73.03 o 0 10 0 1973.84 1668.38 201.85 o 2 10 0 400.53 316.26 70.01 o 4 10 0 6526.69 5400.71 138.12 o 6 10 0 337.96 258.10 72.18 o 8 10 0 1733.53 1604.51 104.79 o 10 10 0 2358.37 2214.73 132.38 o 2 11 0 5534.13 4675.96 141.14 o 4 11 0 80.88 55.01 62.14 o 6 11 0 614.41 530.15 79.69 o 0 1 1 1297.17 1691.02 31.27 o 1 1 1 5847.00 5466.89 46.29 o 2 1 1 4087.24 4056.04 37.08 o 3 1 1 2950.03 2531.05 29.30 o 4 1 1 14886.20 14103.49 116.54 o 5 1 1 14951.65 15218.53 127.40 o 6 1 1 11162.38 10637.69 88.01 o 7 1 1 727.82 901.36 24.73 o 8 1 1 2296.65 1781.82 31.41 o 9 1 1 5988.44 5766.79 60.67 o 10 1 1 1907.26 1668.02 37.60 o 11 1 1 872.96 877.15 37.03 o 12 1 1 655.16 730.70 31.90 o 13 1 1 1463.61 1325.29 45.62 o 14 1 1 701.25 702.75 46.30 o 15 1 1 287.81 328.36 42.18 o 16 1 1 1069.34 1242.94 54.00 o 17 1 1 1246.39 1454.10 70.78 o 18 1 1 1296.81 1353.02 69.77 o 19 1 1 0.16 -48.96 48.96 o 20 1 1 1384.61 1300.48 78.43 o 21 1 1 1671.59 1719.30 64.17 o 1 2 1 11.70 21.37 15.29 o 2 2 1 5564.68 6354.11 55.55 o 3 2 1 9978.96 11093.01 87.51 o 4 2 1 265.38 199.44 21.95 o 5 2 1 3616.63 3750.93 44.32 o 6 2 1 65.76 96.92 17.12 o 7 2 1 5697.15 5332.85 55.93 o 8 2 1 1352.09 1269.61 30.18 o 9 2 1 55.80 72.44 23.26 o 10 2 1 798.72 798.45 33.90 o 11 2 1 0.05 0.20 23.97 o 12 2 1 7.47 11.89 27.95 o 13 2 1 5.51 36.19 34.42 o 14 2 1 0.67 -15.23 37.69 o 15 2 1 716.39 672.96 52.55 o 16 2 1 247.56 225.47 45.54 o 17 2 1 32.00 -41.17 41.17 o 18 2 1 82.78 85.17 43.63 o 19 2 1 1270.95 1241.80 64.18 o 20 2 1 57.83 112.30 44.22 o 21 2 1 4.06 41.57 43.80 o 0 3 1 12417.26 12612.68 151.42 o 1 3 1 16764.11 18669.72 133.93 o 2 3 1 13448.95 13056.15 121.50 o 3 3 1 3306.15 2709.27 37.04 o 4 3 1 110.97 215.74 20.99 o 5 3 1 199.43 189.14 21.65 o 6 3 1 2505.63 2783.40 39.55 o 7 3 1 5006.56 4858.60 52.08 o 8 3 1 396.50 469.42 26.04 o 9 3 1 3459.61 3203.55 48.01 o 10 3 1 4064.06 3904.47 54.61 o 11 3 1 562.64 654.61 34.72 o 12 3 1 5492.66 5124.85 73.22 o 13 3 1 2363.69 2392.55 52.21 o 14 3 1 1901.84 1753.07 53.75 o 15 3 1 1095.02 1172.04 52.44 o 16 3 1 28.27 57.09 36.05 o 17 3 1 137.58 116.89 45.23 o 18 3 1 48.01 65.77 45.64 o 19 3 1 312.30 383.45 52.36 o 20 3 1 134.00 205.97 46.98 o 1 4 1 636.02 924.40 31.07 o 2 4 1 3277.43 3451.78 42.47 o 3 4 1 2103.17 2196.57 35.77 o 4 4 1 419.15 482.25 26.08 o 5 4 1 10.43 -5.65 21.27 o 6 4 1 4954.35 4818.68 56.50 o 7 4 1 2288.41 1944.07 38.07 o 8 4 1 138.55 172.48 26.98 o 9 4 1 3009.99 2626.51 44.72 o 10 4 1 3307.88 3027.06 48.38 o 11 4 1 115.10 144.63 31.61 o 12 4 1 1882.21 1802.43 48.67 o 13 4 1 5903.01 5540.99 78.19 o 14 4 1 22.99 69.89 31.05 o 15 4 1 56.50 14.73 42.76 o 16 4 1 1128.25 1203.11 62.32 o 17 4 1 937.63 958.03 61.21 o 18 4 1 81.45 157.89 46.29 o 19 4 1 0.41 24.40 41.48 o 20 4 1 814.42 839.77 67.51 o 0 5 1 2760.19 2658.79 73.70 o 1 5 1 1093.80 1043.21 35.32 o 2 5 1 2093.74 2263.71 42.70 o 3 5 1 3551.16 3161.49 42.95 o 4 5 1 8107.19 7218.03 75.22 o 5 5 1 22.53 19.05 25.06 o 6 5 1 11310.71 10727.10 106.55 o 7 5 1 31.34 -2.07 29.65 o 8 5 1 2787.39 2590.88 47.01 o 9 5 1 1763.39 1610.56 39.86 o 10 5 1 1168.60 1399.64 39.00 o 11 5 1 24.68 1.79 31.65 o 12 5 1 530.47 690.93 38.89 o 13 5 1 0.03 30.82 35.64 o 14 5 1 961.30 1099.27 50.55 o 15 5 1 193.75 192.65 38.39 o 16 5 1 1645.12 1978.68 67.33 o 17 5 1 87.96 232.89 45.38 o 18 5 1 1140.62 1182.73 71.96 o 19 5 1 62.80 165.71 49.78 o 1 6 1 1532.20 1390.84 35.17 o 2 6 1 111.21 131.08 26.35 o 3 6 1 4254.87 4105.85 55.85 o 4 6 1 541.49 689.75 29.01 o 5 6 1 48.89 16.18 29.35 o 6 6 1 716.08 800.67 37.79 o 7 6 1 1560.31 1680.31 44.82 o 8 6 1 28.23 41.22 30.75 o 9 6 1 291.24 516.01 49.56 o 10 6 1 234.30 223.23 46.04 o 11 6 1 911.02 1102.72 64.86 o 12 6 1 65.44 70.99 39.96 o 13 6 1 2489.34 2349.51 63.19 o 14 6 1 593.73 745.47 55.84 o 15 6 1 338.54 332.45 47.57 o 16 6 1 570.90 619.86 61.35 o 17 6 1 573.52 712.42 56.98 o 18 6 1 11.38 64.90 54.58 o 0 7 1 167.33 211.93 47.84 o 1 7 1 1738.78 1539.99 40.43 o 2 7 1 261.72 372.38 33.51 o 3 7 1 1218.66 1426.60 43.45 o 4 7 1 173.03 184.02 30.72 o 5 7 1 2014.52 2014.18 47.01 o 6 7 1 1126.87 1180.25 44.59 o 7 7 1 985.47 1074.08 45.65 o 8 7 1 2111.80 2035.07 53.10 o 9 7 1 16.55 26.91 37.80 o 10 7 1 569.98 732.07 45.86 o 11 7 1 1506.15 1707.43 59.44 o 12 7 1 6.82 -32.70 40.90 o 13 7 1 64.77 22.04 43.52 o 14 7 1 19.72 34.92 45.06 o 15 7 1 2019.22 2006.62 68.19 o 16 7 1 381.11 432.50 51.96 o 17 7 1 266.08 326.82 53.88 o 1 8 1 3683.74 3365.82 60.95 o 2 8 1 3028.53 2600.85 54.35 o 3 8 1 182.39 194.27 37.96 o 4 8 1 1514.07 1675.32 57.23 o 5 8 1 1068.19 1038.29 45.52 o 6 8 1 74.39 151.94 34.83 o 7 8 1 1117.17 1265.57 49.10 o 8 8 1 855.24 899.38 57.41 o 9 8 1 49.86 34.28 37.86 o 10 8 1 127.26 98.09 48.34 o 11 8 1 374.69 431.47 61.02 o 12 8 1 214.06 212.26 51.45 o 13 8 1 319.73 380.83 52.80 o 14 8 1 608.66 634.57 55.51 o 15 8 1 2.64 140.71 40.71 o 0 9 1 7157.94 6891.36 131.57 o 1 9 1 34.46 362.93 42.85 o 2 9 1 3444.22 3185.54 63.45 o 3 9 1 189.82 329.79 44.11 o 4 9 1 294.56 421.69 45.68 o 5 9 1 3775.01 3491.50 70.67 o 6 9 1 336.22 348.52 48.58 o 7 9 1 246.16 344.60 52.04 o 8 9 1 942.01 919.45 61.60 o 9 9 1 978.27 1039.46 61.11 o 10 9 1 1684.44 1730.49 65.73 o 11 9 1 2.24 -0.28 60.37 o 12 9 1 2367.42 2099.57 85.07 o 13 9 1 0.66 36.04 51.09 o 1 10 1 48.58 51.81 40.15 o 2 10 1 61.33 101.99 42.12 o 3 10 1 367.94 453.33 48.64 o 4 10 1 48.44 40.28 43.23 o 5 10 1 0.35 -42.69 42.69 o 6 10 1 209.71 160.25 47.15 o 7 10 1 128.66 68.68 46.69 o 8 10 1 25.88 103.05 48.16 o 9 10 1 36.44 -17.06 55.14 o 10 10 1 149.02 162.55 51.85 o 0 11 1 14.04 201.63 69.17 o 1 11 1 849.68 1037.69 54.70 o 2 11 1 103.46 217.11 43.56 o 3 11 1 424.79 475.68 54.46 o 4 11 1 533.32 574.44 56.38 o 5 11 1 1310.52 1278.85 68.93 o 6 11 1 766.26 759.78 60.94 o 0 0 2 2833.70 4311.68 106.19 o 1 0 2 3588.10 3412.12 57.82 o 2 0 2 23447.21 31026.94 487.99 o 3 0 2 37275.89 45100.74 544.58 o 4 0 2 10232.98 8309.03 100.09 o 5 0 2 1346.27 967.52 31.90 o 6 0 2 8.10 34.49 22.98 o 7 0 2 9697.07 9012.70 111.68 o 8 0 2 16176.34 14460.48 192.00 o 9 0 2 4299.71 3900.68 71.24 o 10 0 2 31687.49 30047.70 324.05 o 11 0 2 330.67 436.40 46.14 o 12 0 2 118.71 94.74 42.20 o 13 0 2 3417.48 2967.08 76.15 o 14 0 2 437.16 551.18 43.99 o 15 0 2 4423.74 3844.65 103.27 o 16 0 2 5993.29 5389.73 125.60 o 17 0 2 52.62 -42.38 68.53 o 18 0 2 335.43 321.75 88.06 o 19 0 2 1.03 -20.03 66.81 o 20 0 2 217.98 185.38 75.64 o 21 0 2 161.78 224.46 89.79 o 1 1 2 3174.32 3743.32 41.40 o 2 1 2 1963.55 2148.18 31.28 o 3 1 2 0.65 -6.98 15.62 o 4 1 2 1741.06 1736.81 27.54 o 5 1 2 7296.82 7786.66 69.13 o 6 1 2 480.96 611.38 24.58 o 7 1 2 137.76 152.56 23.63 o 8 1 2 2507.92 2266.41 36.55 o 9 1 2 1956.26 1722.57 34.42 o 10 1 2 840.56 920.54 31.95 o 11 1 2 1010.16 968.75 38.76 o 12 1 2 1629.39 1423.11 41.13 o 13 1 2 2664.72 2270.26 47.52 o 14 1 2 322.28 526.85 39.30 o 15 1 2 1379.31 1527.53 73.87 o 16 1 2 233.94 208.81 48.04 o 17 1 2 153.84 100.41 49.52 o 18 1 2 795.76 853.35 75.17 o 19 1 2 873.37 871.46 81.60 o 20 1 2 80.12 70.82 58.95 o 21 1 2 100.71 65.48 52.70 o 0 2 2 42.74 34.60 21.74 o 1 2 2 2058.71 2183.59 30.77 o 2 2 2 1606.80 1015.20 26.19 o 3 2 2 6746.90 6740.75 61.46 o 4 2 2 168.74 388.42 21.11 o 5 2 2 521.96 590.73 24.73 o 6 2 2 1086.83 984.51 25.49 o 7 2 2 233.18 187.79 23.17 o 8 2 2 2683.09 2693.34 42.23 o 9 2 2 0.06 -18.76 23.73 o 10 2 2 9819.80 8787.34 87.63 o 11 2 2 1301.08 1236.37 38.68 o 12 2 2 45.07 71.08 30.41 o 13 2 2 500.91 563.85 35.51 o 14 2 2 381.62 374.31 38.90 o 15 2 2 1494.28 1560.14 60.45 o 16 2 2 1184.46 1259.16 64.26 o 17 2 2 18.69 80.18 39.26 o 18 2 2 338.67 471.52 52.95 o 19 2 2 9.79 97.17 39.49 o 20 2 2 9.95 -2.73 42.63 o 1 3 2 3424.21 3995.82 41.95 o 2 3 2 645.77 749.71 26.58 o 3 3 2 823.72 856.82 29.77 o 4 3 2 3.46 -9.68 18.17 o 5 3 2 797.37 797.72 29.07 o 6 3 2 1086.07 1126.80 28.83 o 7 3 2 2186.28 2156.19 40.68 o 8 3 2 2896.52 3096.12 47.52 o 9 3 2 9.01 3.47 26.03 o 10 3 2 385.56 526.66 34.64 o 11 3 2 1.27 -20.92 27.02 o 12 3 2 776.80 930.83 41.75 o 13 3 2 12.15 87.42 35.95 o 14 3 2 958.59 1010.08 47.20 o 15 3 2 31.98 46.43 33.69 o 16 3 2 46.43 18.02 38.00 o 17 3 2 236.52 295.28 42.63 o 18 3 2 345.26 370.24 44.01 o 19 3 2 486.52 616.87 47.44 o 20 3 2 212.93 258.93 47.11 o 0 4 2 384.68 389.51 37.19 o 1 4 2 11.80 72.44 19.35 o 2 4 2 6901.53 7079.77 65.08 o 3 4 2 408.06 470.96 26.82 o 4 4 2 3834.88 3762.20 50.24 o 5 4 2 1735.00 1770.14 39.71 o 6 4 2 2916.16 2726.78 46.97 o 7 4 2 200.69 237.83 29.67 o 8 4 2 3720.59 3268.87 49.14 o 9 4 2 1062.47 1225.22 36.39 o 10 4 2 8492.58 7508.19 82.63 o 11 4 2 743.66 936.33 40.74 o 12 4 2 489.27 499.34 35.74 o 13 4 2 37.64 71.91 31.68 o 14 4 2 1321.94 1400.60 50.59 o 15 4 2 88.76 127.11 39.15 o 16 4 2 1300.83 1348.99 57.32 o 17 4 2 451.02 510.89 52.87 o 18 4 2 580.10 676.39 56.46 o 19 4 2 45.02 80.61 43.03 o 1 5 2 4508.89 4240.03 55.22 o 2 5 2 4776.33 4593.49 52.64 o 3 5 2 288.73 397.67 30.42 o 4 5 2 1840.79 1726.16 39.77 o 5 5 2 5437.25 5109.49 67.57 o 6 5 2 160.26 151.24 32.04 o 7 5 2 4268.64 3695.47 59.11 o 8 5 2 5770.73 5381.21 67.40 o 9 5 2 21.36 44.50 29.48 o 10 5 2 2050.20 1869.72 43.46 o 11 5 2 703.00 787.28 37.50 o 12 5 2 2874.09 2712.48 77.87 o 13 5 2 103.66 110.57 37.96 o 14 5 2 1207.09 1388.90 64.76 o 15 5 2 27.01 76.78 35.92 o 16 5 2 45.27 43.71 47.64 o 17 5 2 172.64 119.33 49.06 o 18 5 2 1717.99 1564.14 75.40 o 19 5 2 313.96 352.00 54.18 o 0 6 2 3980.07 3733.47 79.27 o 1 6 2 529.60 765.69 39.99 o 2 6 2 706.42 873.86 40.75 o 3 6 2 7354.88 6985.77 85.53 o 4 6 2 37.28 -7.87 27.90 o 5 6 2 1112.99 1209.79 43.96 o 6 6 2 7230.55 7007.56 86.50 o 7 6 2 2500.56 2341.91 52.44 o 8 6 2 483.70 495.38 40.10 o 9 6 2 2697.69 2911.83 57.10 o 10 6 2 3.45 15.82 35.06 o 11 6 2 348.65 437.31 40.71 o 12 6 2 2566.57 2492.21 81.73 o 13 6 2 176.66 206.26 38.05 o 14 6 2 1787.24 1775.22 60.48 o 15 6 2 773.42 850.31 76.49 o 16 6 2 164.85 248.75 48.24 o 17 6 2 162.07 172.30 54.40 o 18 6 2 1167.76 1127.01 75.75 o 1 7 2 669.17 758.95 38.28 o 2 7 2 71.08 173.85 31.27 o 3 7 2 428.40 501.31 43.43 o 4 7 2 74.46 30.82 34.67 o 5 7 2 607.91 720.38 35.61 o 6 7 2 283.11 384.59 37.22 o 7 7 2 1339.16 1357.15 53.35 o 8 7 2 648.28 753.00 45.64 o 9 7 2 841.05 942.29 46.24 o 10 7 2 47.52 59.98 38.85 o 11 7 2 35.68 68.58 44.32 o 12 7 2 321.42 392.02 47.61 o 13 7 2 579.88 470.29 55.62 o 14 7 2 14.42 9.34 45.99 o 15 7 2 992.64 946.87 75.76 o 16 7 2 17.45 84.29 50.40 o 0 8 2 3048.64 2675.24 116.01 o 1 8 2 11.29 135.02 35.63 o 2 8 2 1024.78 1268.21 43.44 o 3 8 2 1226.78 1231.25 51.44 o 4 8 2 346.90 382.62 42.19 o 5 8 2 623.21 704.11 47.72 o 6 8 2 4853.83 4373.84 79.24 o 7 8 2 1544.57 1507.38 55.70 o 8 8 2 71.90 94.05 37.92 o 9 8 2 510.95 694.19 61.94 o 10 8 2 6.27 28.62 50.42 o 11 8 2 65.88 150.28 48.62 o 12 8 2 2035.74 1914.10 72.82 o 13 8 2 247.83 278.32 54.60 o 14 8 2 1839.55 1682.08 62.34 o 15 8 2 35.17 222.46 44.59 o 1 9 2 468.35 505.90 46.72 o 2 9 2 72.88 82.13 39.21 o 3 9 2 35.29 6.73 38.04 o 4 9 2 114.98 70.93 40.05 o 5 9 2 574.38 661.05 49.93 o 6 9 2 145.59 162.47 42.95 o 7 9 2 135.68 103.07 45.59 o 8 9 2 55.56 64.52 43.51 o 9 9 2 8.59 93.08 41.06 o 10 9 2 10.11 10.50 48.46 o 11 9 2 232.37 292.68 47.55 o 12 9 2 23.40 78.22 47.83 o 13 9 2 618.65 741.35 56.07 o 0 10 2 3300.58 2867.41 103.09 o 1 10 2 116.07 334.98 50.14 o 2 10 2 553.76 721.15 53.85 o 3 10 2 143.21 86.68 42.39 o 4 10 2 154.02 115.77 41.97 o 5 10 2 83.43 168.16 41.46 o 6 10 2 4502.58 3647.45 79.02 o 7 10 2 7.99 55.72 44.87 o 8 10 2 51.75 117.51 46.89 o 9 10 2 392.82 585.25 66.03 o 10 10 2 127.82 238.81 72.34 o 1 11 2 1344.31 1245.19 67.06 o 2 11 2 479.44 653.66 58.38 o 3 11 2 19.74 99.94 43.92 o 4 11 2 611.60 858.86 53.06 o 5 11 2 1532.93 1469.53 65.82 o 0 1 3 2095.55 1589.30 45.43 o 1 1 3 2782.59 2868.28 39.02 o 2 1 3 3743.69 4015.09 49.85 o 3 1 3 2296.71 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63.18 o 2 2 4 2822.59 2748.82 41.69 o 3 2 4 0.46 -17.48 24.70 o 4 2 4 294.96 489.80 26.53 o 5 2 4 183.34 223.63 25.81 o 6 2 4 963.51 1003.05 31.83 o 7 2 4 436.09 503.21 29.77 o 8 2 4 106.92 151.80 25.67 o 9 2 4 68.00 32.60 28.60 o 10 2 4 82.44 101.06 31.50 o 11 2 4 3317.13 2859.35 52.75 o 12 2 4 5601.62 5040.34 99.79 o 13 2 4 10.68 12.52 31.84 o 14 2 4 1627.53 1576.11 49.70 o 15 2 4 35.78 109.49 32.97 o 16 2 4 203.42 304.03 40.35 o 17 2 4 606.55 604.73 56.98 o 18 2 4 263.75 238.07 45.77 o 19 2 4 252.92 299.51 46.36 o 1 3 4 161.65 241.35 27.02 o 2 3 4 2627.10 2957.70 50.03 o 3 3 4 1977.48 2040.07 36.38 o 4 3 4 340.14 395.86 28.51 o 5 3 4 116.85 116.14 25.48 o 6 3 4 562.40 625.28 33.38 o 7 3 4 8.28 -13.64 22.63 o 8 3 4 2294.02 2209.26 42.19 o 9 3 4 4003.02 3665.40 53.21 o 10 3 4 11.91 0.53 29.25 o 11 3 4 460.20 417.36 36.92 o 12 3 4 649.30 667.21 38.24 o 13 3 4 393.91 401.92 40.47 o 14 3 4 122.41 198.28 36.24 o 15 3 4 234.74 273.41 38.90 o 16 3 4 441.42 533.73 47.43 o 17 3 4 207.64 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59.78 o 5 1 5 2625.91 2582.93 44.02 o 6 1 5 187.60 268.43 31.13 o 7 1 5 75.10 64.20 26.20 o 8 1 5 19.79 32.46 23.06 o 9 1 5 36.37 155.18 23.77 o 10 1 5 1404.43 1569.31 42.75 o 11 1 5 1490.34 1612.32 56.54 o 12 1 5 1106.85 1270.76 49.52 o 13 1 5 885.22 948.68 58.02 o 14 1 5 2209.32 2335.65 89.86 o 15 1 5 1250.00 1363.58 53.82 o 16 1 5 918.08 1071.38 74.80 o 17 1 5 11.15 141.52 45.39 o 18 1 5 94.39 154.25 49.46 o 1 2 5 2342.92 2494.19 46.38 o 2 2 5 397.49 589.79 33.81 o 3 2 5 678.86 963.35 39.73 o 4 2 5 1924.12 1842.77 36.19 o 5 2 5 655.17 802.63 33.61 o 6 2 5 334.23 479.35 30.66 o 7 2 5 674.56 865.00 34.42 o 8 2 5 778.92 859.52 39.42 o 9 2 5 170.76 246.16 35.15 o 10 2 5 954.02 1123.46 38.34 o 11 2 5 102.59 161.48 29.26 o 12 2 5 73.05 65.30 33.47 o 13 2 5 2316.45 2283.06 69.37 o 14 2 5 35.27 79.41 33.28 o 15 2 5 71.31 186.62 59.12 o 16 2 5 266.44 392.85 61.72 o 17 2 5 161.04 237.25 47.92 o 18 2 5 95.28 241.35 58.14 o 0 3 5 1642.58 1733.34 53.68 o 1 3 5 348.14 572.60 32.25 o 2 3 5 1387.38 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192.69 194.79 67.72 o 2 5 8 461.94 528.22 56.00 o 3 5 8 10.40 54.73 42.81 o 4 5 8 2160.16 1898.27 64.74 o 5 5 8 4.70 86.16 41.75 o 6 5 8 0.62 33.98 40.04 o 7 5 8 0.81 98.59 48.06 o 8 5 8 2575.85 2066.89 71.43 o 0 6 8 4777.83 3828.37 164.91 o 1 6 8 14.28 79.24 64.08 o 2 6 8 2871.11 2356.59 90.72 o 3 6 8 6.46 118.72 57.22 o 4 6 8 364.22 436.69 56.15 o 5 6 8 71.48 114.62 45.86 o 0 1 9 193.25 353.55 73.78 o 1 1 9 537.50 641.12 60.03 o 2 1 9 2034.92 1809.51 63.82 o 3 1 9 35.43 25.92 39.83 o 4 1 9 794.83 811.00 59.94 o 5 1 9 1664.40 1578.00 62.12 o 6 1 9 171.58 239.75 43.58 o 7 1 9 32.93 70.38 37.78 o 8 1 9 1005.41 793.69 70.18 o 1 2 9 6.78 83.56 43.46 o 2 2 9 679.17 696.30 51.41 o 3 2 9 823.70 741.75 62.30 o 4 2 9 108.45 111.28 44.35 o 5 2 9 217.21 228.39 43.89 o 6 2 9 11.09 101.76 40.98 o 7 2 9 941.48 1026.35 56.61 o 8 2 9 8.30 147.87 48.78 o 0 3 9 5598.27 5125.04 149.13 o 1 3 9 1426.65 1436.73 89.97 o 2 3 9 4126.84 3557.41 92.95 o 3 3 9 1012.72 1171.66 80.20 o 4 3 9 88.13 195.09 45.13 o 5 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