#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/80/2018056.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018056_Fobs loop_ _publ_author_name 'Frampton, Christopher S.' 'MacNicol, David D.' 'Wilson, Derek R.' _publ_section_title ; (R)-4-(4-Aminophenyl)-2,2,4-trimethylchroman and (S)-4-(4-aminophenyl)-2,2,4-trimethylthiachroman ; _journal_coeditor_code BM3104 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o188 _journal_page_last o191 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.6043 _cell_length_b 10.4104 _cell_length_c 13.4126 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.8001 _[local]_cod_data_source_file bm3104IVsup4.hkl _[local]_cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' p11025_11 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 11543.70 9707.62 30.92 o 6 0 0 446.77 646.01 18.81 o 8 0 0 643.49 610.66 22.41 o 10 0 0 2930.14 2739.69 27.56 o 12 0 0 159.92 146.67 4.79 o 2 1 0 4251.55 3558.02 18.93 o 3 1 0 7647.83 6334.56 148.47 o 4 1 0 239.03 231.51 7.43 o 5 1 0 1268.31 1229.47 14.50 o 6 1 0 222.12 191.86 5.34 o 7 1 0 189.69 183.36 7.92 o 8 1 0 705.83 632.11 16.01 o 9 1 0 15.41 20.74 2.23 o 10 1 0 319.25 300.21 6.48 o 11 1 0 564.87 548.22 8.00 o 12 1 0 48.24 49.01 2.88 o 13 1 0 355.02 340.93 4.66 o 1 2 0 152.73 125.24 3.71 o 2 2 0 1887.57 1683.86 16.42 o 3 2 0 1277.80 1202.02 14.98 o 4 2 0 26.46 23.61 2.28 o 5 2 0 1775.15 1673.88 87.00 o 6 2 0 354.21 332.49 9.57 o 7 2 0 190.74 183.70 5.91 o 8 2 0 701.53 695.32 14.68 o 9 2 0 5.75 8.67 3.65 o 10 2 0 1188.94 1135.81 12.62 o 11 2 0 51.46 46.92 2.37 o 12 2 0 62.73 58.48 3.00 o 13 2 0 187.59 173.42 2.88 o 1 3 0 281.99 250.78 2.66 o 2 3 0 3604.90 3114.20 13.71 o 3 3 0 0.13 2.43 0.71 o 4 3 0 363.47 326.96 7.41 o 5 3 0 97.85 123.16 4.05 o 6 3 0 580.81 581.04 10.16 o 7 3 0 3.96 3.92 1.32 o 8 3 0 2120.47 2065.04 14.48 o 9 3 0 43.76 47.87 2.71 o 10 3 0 167.14 170.70 4.94 o 11 3 0 12.99 12.71 1.80 o 12 3 0 72.24 64.07 4.19 o 0 4 0 1724.99 1736.59 22.53 o 1 4 0 347.65 333.79 7.02 o 2 4 0 1009.38 1056.37 8.27 o 3 4 0 312.40 291.72 5.21 o 4 4 0 1.16 0.81 0.80 o 5 4 0 4536.21 4896.67 33.10 o 6 4 0 116.44 118.64 4.46 o 7 4 0 1.06 0.64 1.47 o 8 4 0 959.95 943.78 11.91 o 9 4 0 911.13 945.11 11.91 o 10 4 0 644.96 669.82 9.38 o 11 4 0 51.80 49.99 2.29 o 12 4 0 3.32 2.85 0.51 o 1 5 0 3185.37 3300.82 71.96 o 2 5 0 2835.44 2969.29 36.31 o 3 5 0 267.10 223.36 10.43 o 4 5 0 37.55 46.97 5.03 o 5 5 0 257.67 243.02 11.50 o 6 5 0 989.47 1038.40 18.03 o 7 5 0 95.57 100.21 3.78 o 8 5 0 540.10 588.71 9.63 o 9 5 0 36.17 37.88 3.71 o 10 5 0 480.22 482.24 7.57 o 11 5 0 429.97 433.86 13.00 o 12 5 0 44.86 45.42 2.40 o 0 6 0 3267.02 3426.81 41.46 o 1 6 0 19.54 27.32 4.07 o 2 6 0 54.04 77.53 6.83 o 3 6 0 19.30 25.76 4.31 o 4 6 0 467.88 450.68 17.02 o 5 6 0 861.32 997.71 25.40 o 6 6 0 28.13 30.97 1.33 o 7 6 0 0.02 1.42 0.70 o 8 6 0 5.90 5.55 1.01 o 9 6 0 31.92 35.14 1.88 o 10 6 0 221.58 234.63 5.25 o 11 6 0 11.13 10.97 1.44 o 1 7 0 230.99 219.77 12.10 o 2 7 0 836.63 883.27 24.69 o 3 7 0 844.69 950.98 26.24 o 4 7 0 14.50 14.29 1.47 o 5 7 0 42.50 47.54 1.67 o 6 7 0 124.80 127.68 3.00 o 7 7 0 72.65 76.75 2.91 o 8 7 0 61.55 65.30 2.62 o 9 7 0 100.09 92.21 2.75 o 10 7 0 0.48 1.02 0.66 o 11 7 0 176.88 187.42 4.67 o 0 8 0 265.69 255.96 8.39 o 1 8 0 404.83 396.74 11.14 o 2 8 0 12.11 9.81 1.66 o 3 8 0 127.37 122.65 3.18 o 4 8 0 350.57 348.45 6.38 o 5 8 0 347.74 365.11 5.06 o 6 8 0 231.73 221.40 3.94 o 7 8 0 156.31 161.32 3.50 o 8 8 0 27.95 29.76 1.72 o 9 8 0 193.91 215.58 4.79 o 10 8 0 6.22 5.49 0.72 o 1 9 0 28.68 25.72 2.11 o 2 9 0 347.02 358.58 6.85 o 3 9 0 273.12 304.97 6.30 o 4 9 0 2.13 5.39 1.92 o 5 9 0 5.76 5.91 1.31 o 6 9 0 6.45 8.04 0.97 o 7 9 0 63.98 66.65 1.99 o 8 9 0 447.94 457.63 16.24 o 9 9 0 0.40 -0.12 0.60 o 0 10 0 486.14 514.31 12.82 o 1 10 0 64.98 67.16 2.96 o 2 10 0 3.96 8.63 2.04 o 3 10 0 120.17 116.24 6.35 o 4 10 0 43.90 44.98 2.70 o 5 10 0 647.85 705.79 9.07 o 6 10 0 83.84 80.55 3.07 o 7 10 0 55.30 52.77 1.71 o 8 10 0 13.46 15.58 1.56 o 1 11 0 186.10 204.24 5.27 o 2 11 0 337.11 328.68 13.30 o 3 11 0 151.47 139.91 9.29 o 4 11 0 106.86 96.79 3.30 o 5 11 0 12.49 13.39 1.03 o 6 11 0 23.68 24.30 0.91 o 7 11 0 95.34 94.55 3.00 o 0 12 0 248.55 233.19 6.23 o 1 12 0 0.39 -0.47 0.66 o 2 12 0 192.14 189.33 6.11 o 3 12 0 0.41 -0.09 1.08 o 4 12 0 354.12 354.73 14.08 o 5 12 0 182.02 163.02 24.15 o 2 0 1 3669.84 3195.68 8.09 o 3 0 1 130.56 118.29 1.94 o 4 0 1 885.74 830.45 17.12 o 5 0 1 2923.32 2861.25 15.00 o 6 0 1 1110.06 1112.63 25.40 o 7 0 1 326.55 357.46 15.94 o 8 0 1 547.18 503.33 17.68 o 9 0 1 43.24 36.37 2.00 o 10 0 1 10.82 11.22 1.35 o 11 0 1 14.12 9.11 1.80 o 12 0 1 75.32 68.66 3.59 o 13 0 1 176.12 153.50 4.55 o -13 1 1 299.73 289.46 7.13 o -12 1 1 32.36 29.00 2.28 o -11 1 1 60.48 62.67 3.95 o -10 1 1 401.52 408.59 7.49 o -9 1 1 46.95 50.78 2.71 o -8 1 1 289.68 280.12 10.72 o -7 1 1 42.92 48.17 5.99 o -6 1 1 993.78 944.83 25.70 o -5 1 1 928.54 895.69 9.28 o -4 1 1 57.64 64.18 2.09 o -3 1 1 2142.75 1961.19 36.61 o -2 1 1 2779.29 2394.37 95.09 o 2 1 1 2904.16 2665.64 27.26 o 3 1 1 2172.33 2046.67 11.91 o 4 1 1 76.85 79.92 3.22 o 5 1 1 990.10 1001.80 12.10 o 6 1 1 1033.96 1099.93 24.92 o 7 1 1 46.54 41.39 3.85 o 8 1 1 320.54 321.16 17.38 o 9 1 1 71.77 80.05 4.91 o 10 1 1 424.43 424.56 11.26 o 11 1 1 56.89 55.48 3.83 o 12 1 1 32.84 28.64 2.28 o 13 1 1 297.72 290.47 5.87 o -13 2 1 31.97 28.73 1.80 o -12 2 1 0.65 2.16 0.72 o -11 2 1 69.11 70.72 2.88 o -10 2 1 130.36 123.01 5.45 o -9 2 1 608.99 586.52 9.71 o -8 2 1 401.44 381.10 6.15 o -7 2 1 515.40 523.39 13.03 o -6 2 1 37.81 56.55 4.01 o -5 2 1 46.55 44.47 2.23 o -4 2 1 216.53 226.96 8.39 o -3 2 1 550.45 486.87 15.10 o -2 2 1 641.49 558.67 6.99 o -1 2 1 3788.33 3419.17 43.08 o 0 2 1 3653.58 3012.81 36.79 o 1 2 1 3792.12 3365.13 30.62 o 2 2 1 694.29 666.28 4.65 o 3 2 1 558.29 524.79 8.09 o 4 2 1 288.58 297.10 11.26 o 5 2 1 63.93 68.35 3.45 o 6 2 1 36.07 44.71 5.39 o 7 2 1 570.64 562.34 13.85 o 8 2 1 363.19 361.86 7.74 o 9 2 1 564.57 533.73 12.82 o 10 2 1 128.77 115.52 5.99 o 11 2 1 93.55 101.38 5.15 o 12 2 1 3.68 4.67 1.08 o 13 2 1 40.38 37.24 1.31 o -12 3 1 15.01 12.34 1.32 o -11 3 1 17.70 18.61 2.28 o -10 3 1 201.17 203.81 5.38 o -9 3 1 349.30 366.86 7.46 o -8 3 1 267.01 257.57 5.19 o -7 3 1 33.03 33.43 2.73 o -6 3 1 67.29 62.37 3.37 o -5 3 1 310.28 322.97 6.61 o -4 3 1 475.52 438.93 8.53 o -3 3 1 783.80 712.80 34.57 o -2 3 1 752.28 700.78 9.80 o -1 3 1 808.53 748.05 8.72 o 0 3 1 12181.15 9904.15 78.37 o 1 3 1 918.94 850.33 8.52 o 2 3 1 727.94 688.02 5.80 o 3 3 1 734.56 665.09 14.98 o 4 3 1 446.98 429.43 8.45 o 5 3 1 297.93 298.85 8.33 o 6 3 1 62.35 62.00 3.16 o 7 3 1 15.54 15.11 2.37 o 8 3 1 284.81 281.20 10.02 o 9 3 1 347.73 362.13 10.90 o 10 3 1 205.20 221.33 8.27 o 11 3 1 6.26 8.51 1.68 o 12 3 1 21.77 19.82 1.31 o -12 4 1 32.41 33.19 2.28 o -11 4 1 130.21 131.35 3.56 o -10 4 1 252.36 258.51 5.93 o -9 4 1 122.24 118.46 4.36 o -8 4 1 797.83 798.77 11.10 o -7 4 1 787.78 791.87 9.31 o -6 4 1 522.36 512.16 12.37 o -5 4 1 365.47 404.18 9.12 o -4 4 1 876.52 859.08 20.37 o -3 4 1 1971.67 2003.02 42.60 o -2 4 1 1427.41 1451.98 40.80 o -1 4 1 610.04 693.07 16.72 o 0 4 1 2394.40 2278.10 37.87 o 1 4 1 523.32 584.60 8.37 o 2 4 1 1433.94 1465.33 11.54 o 3 4 1 1905.94 2031.92 17.68 o 4 4 1 984.08 967.30 15.54 o 5 4 1 366.20 399.97 7.63 o 6 4 1 482.72 498.32 9.95 o 7 4 1 871.20 874.44 9.65 o 8 4 1 821.62 802.75 16.30 o 9 4 1 142.74 144.76 7.07 o 10 4 1 235.10 240.26 8.63 o 11 4 1 142.11 151.06 4.49 o 12 4 1 31.82 31.94 1.98 o -12 5 1 75.18 81.84 3.12 o -11 5 1 256.50 257.87 5.42 o -10 5 1 103.42 101.27 3.56 o -9 5 1 40.75 42.68 2.67 o -8 5 1 703.60 708.10 10.63 o -7 5 1 1121.38 1090.94 9.58 o -6 5 1 834.56 850.72 15.86 o -5 5 1 726.24 717.83 27.98 o -4 5 1 104.80 111.32 7.55 o -3 5 1 985.08 1033.18 22.17 o -2 5 1 993.44 1100.89 22.29 o -1 5 1 514.83 540.98 17.91 o 0 5 1 11.50 14.19 1.92 o 1 5 1 595.67 643.09 17.97 o 2 5 1 899.25 1013.77 20.97 o 3 5 1 1008.94 1055.35 22.29 o 4 5 1 89.25 98.62 7.19 o 5 5 1 763.84 794.24 20.85 o 6 5 1 797.55 839.54 21.69 o 7 5 1 1082.56 1058.96 12.35 o 8 5 1 781.13 803.11 16.78 o 9 5 1 22.06 23.73 3.00 o 10 5 1 90.60 96.82 5.15 o 11 5 1 263.91 276.96 8.63 o 12 5 1 100.36 97.44 7.79 o -11 6 1 40.36 39.68 3.18 o -10 6 1 124.61 127.01 3.06 o -9 6 1 430.62 462.42 6.67 o -8 6 1 462.94 491.42 7.19 o -7 6 1 522.95 489.17 7.00 o -6 6 1 322.46 291.70 4.20 o -5 6 1 781.51 842.76 17.30 o -4 6 1 485.09 526.53 13.44 o -3 6 1 189.66 199.66 8.04 o -2 6 1 1057.84 1072.20 27.14 o -1 6 1 1108.58 1194.19 14.13 o 0 6 1 23.89 19.72 2.18 o 1 6 1 1189.54 1302.92 26.12 o 2 6 1 1116.20 1171.35 25.52 o 3 6 1 187.84 187.89 10.66 o 4 6 1 518.01 550.98 18.93 o 5 6 1 757.86 819.04 23.49 o 6 6 1 391.87 367.64 5.48 o 7 6 1 521.85 493.13 6.98 o 8 6 1 428.32 447.00 8.37 o 9 6 1 398.79 424.07 7.79 o 10 6 1 151.12 160.40 4.28 o 11 6 1 43.65 46.05 3.30 o -11 7 1 38.29 40.62 2.28 o -10 7 1 184.13 185.42 4.37 o -9 7 1 229.78 228.92 5.41 o -8 7 1 218.11 254.31 5.14 o -7 7 1 71.76 82.24 2.98 o -6 7 1 375.45 379.48 4.68 o -5 7 1 688.28 682.01 7.36 o -4 7 1 258.87 264.27 5.83 o -3 7 1 38.83 41.10 5.99 o -2 7 1 21.22 15.82 3.71 o -1 7 1 314.11 309.28 13.66 o 0 7 1 412.68 410.53 10.53 o 1 7 1 365.10 362.37 15.34 o 2 7 1 23.60 25.88 4.43 o 3 7 1 25.82 26.72 4.67 o 4 7 1 235.56 238.86 5.92 o 5 7 1 709.70 699.13 8.35 o 6 7 1 438.94 453.93 6.82 o 7 7 1 56.40 61.93 2.19 o 8 7 1 225.93 254.64 6.26 o 9 7 1 252.41 257.17 5.80 o 10 7 1 198.20 211.56 4.49 o 11 7 1 37.89 35.64 1.36 o -10 8 1 28.13 26.03 1.50 o -9 8 1 73.58 73.21 3.84 o -8 8 1 22.04 19.20 1.44 o -7 8 1 281.05 303.92 5.81 o -6 8 1 62.21 62.66 1.98 o -5 8 1 196.42 193.25 3.77 o -4 8 1 178.56 178.84 4.23 o -3 8 1 599.86 577.99 7.03 o -2 8 1 9.22 6.29 1.49 o -1 8 1 528.77 525.26 9.77 o 0 8 1 5.67 5.69 1.06 o 1 8 1 531.98 544.58 8.25 o 2 8 1 10.05 7.87 1.60 o 3 8 1 588.34 573.07 13.01 o 4 8 1 213.67 210.06 6.01 o 5 8 1 183.01 181.16 4.36 o 6 8 1 63.31 62.44 2.62 o 7 8 1 276.49 296.43 5.42 o 8 8 1 30.47 30.01 3.77 o 9 8 1 67.34 71.87 2.79 o 10 8 1 16.79 17.02 1.56 o -9 9 1 72.79 80.17 3.12 o -8 9 1 378.11 380.99 6.01 o -7 9 1 254.11 264.56 3.61 o -6 9 1 144.39 149.45 2.81 o -5 9 1 45.24 50.76 1.95 o -4 9 1 784.79 792.30 10.39 o -3 9 1 603.42 627.16 9.36 o -2 9 1 432.73 441.33 13.36 o -1 9 1 156.74 153.62 7.73 o 0 9 1 231.88 225.01 6.65 o 1 9 1 122.92 117.43 6.11 o 2 9 1 417.81 418.21 11.74 o 3 9 1 684.67 689.63 15.34 o 4 9 1 735.89 772.31 16.54 o 5 9 1 51.14 57.87 3.10 o 6 9 1 151.18 160.29 5.53 o 7 9 1 241.51 260.46 6.79 o 8 9 1 387.24 424.08 9.59 o 9 9 1 70.65 76.21 3.24 o -8 10 1 217.00 232.23 5.15 o -7 10 1 207.13 226.26 7.43 o -6 10 1 149.99 155.84 3.37 o -5 10 1 14.47 12.90 0.98 o -4 10 1 180.50 198.59 4.05 o -3 10 1 434.42 438.53 7.54 o -2 10 1 110.94 130.94 4.91 o -1 10 1 317.82 317.00 24.15 o 0 10 1 6.96 8.51 1.50 o 1 10 1 367.26 349.83 21.57 o 2 10 1 110.08 129.06 6.47 o 3 10 1 382.98 398.80 11.38 o 4 10 1 196.02 214.65 8.15 o 5 10 1 8.33 5.45 1.14 o 6 10 1 158.00 162.99 3.68 o 7 10 1 202.06 211.44 17.85 o 8 10 1 212.95 243.02 5.63 o -7 11 1 226.70 244.81 4.67 o -6 11 1 183.98 184.10 5.40 o -5 11 1 124.41 124.00 3.39 o -4 11 1 27.71 26.91 1.54 o -3 11 1 197.38 203.17 4.40 o -2 11 1 96.76 105.92 4.24 o -1 11 1 83.68 83.48 2.58 o 0 11 1 1.32 2.83 0.70 o 1 11 1 85.65 84.86 3.42 o 2 11 1 101.26 108.56 11.38 o 3 11 1 200.74 222.86 21.39 o 4 11 1 20.22 22.58 1.43 o 5 11 1 128.53 135.89 3.51 o 6 11 1 193.70 208.88 3.80 o 7 11 1 232.60 241.22 4.79 o -5 12 1 32.26 32.95 1.23 o -4 12 1 15.34 16.47 4.25 o -3 12 1 67.53 65.29 2.32 o -2 12 1 199.42 190.89 5.99 o -1 12 1 26.70 24.41 1.92 o 0 12 1 145.92 140.96 4.55 o 1 12 1 17.16 17.03 1.24 o 2 12 1 199.44 195.40 3.05 o 3 12 1 60.09 57.37 2.40 o 4 12 1 19.58 18.95 4.49 o 5 12 1 20.24 20.83 0.97 o 2 0 2 120.69 116.27 3.17 o 3 0 2 274.70 240.09 5.12 o 4 0 2 1523.52 1489.76 12.37 o 5 0 2 678.30 669.63 9.77 o 6 0 2 22.83 20.97 3.95 o 7 0 2 3.59 4.67 2.28 o 8 0 2 395.21 408.16 8.21 o 9 0 2 19.01 17.73 2.52 o 10 0 2 0.01 0.12 1.20 o 11 0 2 259.05 268.42 8.39 o 12 0 2 44.63 45.54 3.00 o 13 0 2 83.99 94.07 3.36 o -13 1 2 21.28 19.17 1.56 o -12 1 2 173.42 159.61 5.39 o -11 1 2 17.52 16.06 2.28 o -10 1 2 651.76 618.93 13.78 o -9 1 2 407.41 385.62 10.90 o -8 1 2 636.75 619.20 19.58 o -7 1 2 67.53 65.07 7.07 o -6 1 2 382.33 431.69 9.75 o -5 1 2 224.37 214.34 5.33 o -4 1 2 149.23 158.56 5.01 o -3 1 2 345.69 321.09 9.77 o -2 1 2 4558.09 3978.34 26.12 o -1 1 2 5479.25 4714.38 24.51 o 1 1 2 5247.65 4398.02 16.60 o 2 1 2 4644.23 4141.84 14.48 o 3 1 2 346.23 335.61 5.77 o 4 1 2 232.84 251.40 7.01 o 5 1 2 185.13 184.28 11.74 o 6 1 2 441.72 487.23 9.77 o 7 1 2 62.43 54.28 6.35 o 8 1 2 706.54 661.33 10.43 o 9 1 2 469.64 439.06 11.62 o 10 1 2 655.80 608.26 13.66 o 11 1 2 15.65 16.06 2.28 o 12 1 2 164.28 152.95 4.01 o 13 1 2 30.27 30.80 1.92 o -13 2 2 58.52 64.47 2.40 o -12 2 2 16.06 16.78 1.80 o -11 2 2 118.98 108.69 5.27 o -10 2 2 272.31 264.95 8.99 o -9 2 2 228.13 224.68 8.39 o -8 2 2 504.30 489.98 9.10 o -7 2 2 53.41 42.04 4.49 o -6 2 2 154.59 123.65 5.56 o -5 2 2 639.09 679.95 26.24 o -4 2 2 473.96 524.18 7.00 o -3 2 2 223.61 208.64 4.16 o -2 2 2 852.24 786.21 5.89 o -1 2 2 3214.32 2829.47 26.24 o 0 2 2 5138.86 4576.42 27.50 o 1 2 2 3085.30 2895.33 62.79 o 2 2 2 728.53 708.63 6.06 o 3 2 2 203.76 188.52 5.03 o 4 2 2 429.46 541.07 53.38 o 5 2 2 613.33 634.94 11.98 o 6 2 2 153.88 128.17 8.57 o 7 2 2 32.29 24.09 4.19 o 8 2 2 476.26 457.28 8.81 o 9 2 2 230.73 235.23 8.63 o 10 2 2 297.72 281.84 9.35 o 11 2 2 120.77 117.07 5.63 o 12 2 2 7.05 7.55 0.97 o 13 2 2 52.62 56.68 2.28 o -12 3 2 39.86 40.30 1.74 o -11 3 2 21.24 20.85 2.40 o -10 3 2 44.69 42.54 3.71 o 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