#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/84/2018413.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018413_Fobs loop_ _publ_author_name 'Pereira, Carla F.' 'Fernandes, Jos\'e A.' 'Rodrigues, Jo\~ao M. M.' 'Vilela, S\'ergio M. F.' 'Tom\'e, Jo\~ao P. C.' 'Almeida Paz, Filipe A.' _publ_section_title ; 5-[4-(Diethoxyphosphoryl)-2,3,5,6-tetrafluorophenyl]-10,15,20-tris(pentafluorophenyl)porphyrin ; _journal_coeditor_code GG3269 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o104 _journal_page_last o107 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.024 _cell_angle_gamma 90.000 _cell_length_a 15.5300 _cell_length_b 11.2539 _cell_length_c 26.3749 _exptl_crystal_F_000 2184.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file gg3269Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'I in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 284.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 4051.97 5704.20 278.36 o 4 0 0 53862.26 62725.25 3193.96 o 5 0 0 60200.27 62669.10 2938.87 o 6 0 0 32817.29 33353.75 1447.00 o 7 0 0 22266.22 23141.43 1004.13 o 8 0 0 389.04 459.25 39.00 o 9 0 0 4557.05 3691.98 170.97 o 10 0 0 55.46 71.82 33.48 o 11 0 0 7877.53 8280.20 458.16 o 12 0 0 6.86 -0.49 57.27 o 13 0 0 31.32 3.14 60.65 o 14 0 0 30.55 33.30 66.08 o 15 0 0 773.83 850.06 142.84 o 16 0 0 0.51 -17.01 76.94 o 17 0 0 243.60 455.61 103.67 o 18 0 0 43.67 172.78 118.78 o 3 1 0 1902.54 2814.92 105.49 o 4 1 0 25694.52 31382.11 1020.29 o 5 1 0 4650.47 4241.28 134.10 o 6 1 0 5449.79 5141.23 155.18 o 7 1 0 1990.99 2057.89 72.58 o 8 1 0 3229.13 3433.37 112.33 o 9 1 0 309.37 353.15 26.59 o 10 1 0 3085.77 3483.80 143.84 o 11 1 0 8.87 -31.97 31.97 o 12 1 0 196.93 273.67 45.37 o 13 1 0 1495.49 1540.99 91.78 o 14 1 0 301.28 390.32 79.87 o 15 1 0 37.48 12.20 51.13 o 16 1 0 209.30 254.63 68.65 o 17 1 0 7.98 26.86 98.79 o 18 1 0 18.51 67.89 66.54 o 0 2 0 18643.29 25829.26 1992.93 o 1 2 0 872.24 1521.43 67.80 o 2 2 0 7845.62 13811.31 787.66 o 3 2 0 5433.92 5457.37 444.47 o 4 2 0 5097.26 4684.71 195.71 o 5 2 0 64.51 11.22 15.35 o 6 2 0 97.77 52.68 20.37 o 7 2 0 4128.58 4358.46 164.26 o 8 2 0 333.31 409.42 29.39 o 9 2 0 603.61 648.19 40.79 o 10 2 0 83.37 113.62 33.80 o 11 2 0 82.87 75.96 36.52 o 12 2 0 618.29 674.10 69.57 o 13 2 0 236.75 308.00 54.59 o 14 2 0 320.35 390.45 63.67 o 15 2 0 11.29 -48.35 48.35 o 16 2 0 98.68 84.86 64.03 o 17 2 0 3.24 59.84 64.88 o 18 2 0 0.01 81.51 86.92 o 1 3 0 4778.66 7122.16 301.57 o 2 3 0 3465.00 7244.96 417.32 o 3 3 0 346.94 448.77 35.34 o 4 3 0 1128.66 897.43 46.48 o 5 3 0 136.76 160.70 18.55 o 6 3 0 6864.87 7343.06 234.48 o 7 3 0 26.89 -11.20 20.42 o 8 3 0 29.07 -19.56 19.56 o 9 3 0 721.85 661.45 42.10 o 10 3 0 254.27 195.29 36.01 o 11 3 0 139.42 134.21 49.02 o 12 3 0 8.41 30.64 40.44 o 13 3 0 316.09 285.79 55.54 o 14 3 0 429.44 455.37 64.48 o 15 3 0 74.08 58.18 53.66 o 16 3 0 0.03 103.00 62.91 o 17 3 0 53.19 209.51 67.68 o 0 4 0 351.79 542.59 140.92 o 1 4 0 868.97 1273.79 73.52 o 2 4 0 38.17 52.17 18.32 o 3 4 0 3338.25 3691.26 239.57 o 4 4 0 82.01 68.53 23.56 o 5 4 0 416.44 383.71 41.56 o 6 4 0 7998.14 6931.52 233.14 o 7 4 0 27.42 21.83 15.96 o 8 4 0 3.55 -19.45 19.45 o 9 4 0 243.13 232.09 25.87 o 10 4 0 355.43 394.78 34.15 o 11 4 0 29.07 13.25 35.93 o 12 4 0 460.13 444.78 56.49 o 13 4 0 0.50 20.40 48.19 o 14 4 0 17.53 -29.94 48.53 o 15 4 0 2.91 -37.81 68.60 o 16 4 0 67.39 127.73 90.56 o 17 4 0 0.01 144.04 92.09 o 1 5 0 1619.67 2124.32 116.73 o 2 5 0 8842.90 11629.50 654.62 o 3 5 0 717.24 921.72 81.10 o 4 5 0 4252.16 4813.13 321.28 o 5 5 0 1899.23 1587.35 77.83 o 6 5 0 998.32 986.99 45.56 o 7 5 0 297.00 253.09 23.25 o 8 5 0 6.68 -19.71 19.71 o 9 5 0 1310.69 1255.13 58.30 o 10 5 0 1176.65 1053.07 75.45 o 11 5 0 885.34 861.81 63.73 o 12 5 0 21.85 -60.48 60.48 o 13 5 0 391.23 263.04 65.76 o 14 5 0 12.55 -59.24 59.24 o 15 5 0 56.89 23.78 71.12 o 16 5 0 18.38 29.37 85.36 o 17 5 0 7.79 -35.15 89.09 o 0 6 0 1946.49 2252.45 160.06 o 1 6 0 174.48 80.95 41.57 o 2 6 0 459.40 684.90 68.33 o 3 6 0 2847.79 3502.92 352.55 o 4 6 0 172.49 162.24 36.16 o 5 6 0 122.38 57.98 26.91 o 6 6 0 117.77 109.35 28.17 o 7 6 0 895.23 795.05 50.80 o 8 6 0 203.32 128.08 34.45 o 9 6 0 229.57 263.54 48.16 o 10 6 0 14.10 36.82 54.20 o 11 6 0 46.82 19.35 54.35 o 12 6 0 357.19 293.09 63.22 o 13 6 0 91.20 53.57 71.97 o 14 6 0 14.32 35.02 75.00 o 15 6 0 166.39 275.59 98.59 o 16 6 0 8.12 -12.07 106.37 o 1 7 0 169.72 187.35 50.01 o 2 7 0 585.35 588.65 63.68 o 3 7 0 81.09 67.17 42.92 o 4 7 0 143.12 132.88 51.59 o 5 7 0 182.39 202.81 78.86 o 6 7 0 85.21 48.11 58.90 o 7 7 0 24.18 53.18 37.62 o 8 7 0 158.01 138.00 73.10 o 9 7 0 24.32 -10.10 56.12 o 10 7 0 0.06 -25.73 63.23 o 11 7 0 206.97 147.26 64.52 o 12 7 0 76.35 75.34 74.28 o 13 7 0 63.11 76.95 74.58 o 14 7 0 85.74 174.54 98.33 o 15 7 0 18.18 32.28 92.84 o 0 8 0 0.07 82.07 91.79 o 1 8 0 72.33 122.16 53.22 o 2 8 0 460.12 503.25 64.85 o 3 8 0 137.62 71.99 51.50 o 4 8 0 122.35 41.12 103.67 o 5 8 0 13.95 -33.43 73.55 o 6 8 0 71.89 64.58 81.53 o 7 8 0 1243.92 1332.45 119.51 o 8 8 0 1.93 137.85 57.29 o 9 8 0 4.18 49.92 60.41 o 10 8 0 171.80 118.75 64.84 o 11 8 0 112.94 73.61 62.35 o 12 8 0 118.03 120.36 78.12 o 13 8 0 18.91 68.11 77.96 o 14 8 0 0.03 134.31 99.62 o 1 9 0 16.33 -29.23 78.55 o 2 9 0 67.68 -77.94 77.94 o 3 9 0 0.04 52.04 140.38 o 4 9 0 70.16 102.54 95.57 o 5 9 0 147.12 177.10 137.14 o 6 9 0 1042.01 1008.97 249.45 o 7 9 0 1714.43 1530.89 353.11 o 8 9 0 506.16 255.87 74.45 o 9 9 0 7.69 -16.67 65.88 o 10 9 0 38.22 -65.66 65.66 o 11 9 0 43.94 114.60 130.12 o 12 9 0 79.88 136.13 94.70 o 13 9 0 13.00 135.11 100.29 o 0 10 0 296.52 278.60 127.42 o 1 10 0 23.09 -79.42 82.97 o 2 10 0 10.12 -75.49 75.49 o 3 10 0 100.62 4.49 81.95 o 4 10 0 229.40 246.21 145.78 o 5 10 0 219.37 103.67 152.26 o 6 10 0 526.17 449.22 176.02 o 7 10 0 13.76 -28.58 85.05 o 8 10 0 0.01 -63.44 88.64 o 9 10 0 41.69 -12.77 118.24 o 10 10 0 83.90 99.02 117.70 o 11 10 0 4.77 -43.07 86.70 o 12 10 0 0.93 -64.57 91.73 o 1 11 0 18.03 -82.85 82.85 o 2 11 0 0.98 -42.47 81.32 o 3 11 0 0.12 -138.22 138.22 o 4 11 0 20.66 -128.50 137.14 o 5 11 0 6.05 186.82 160.90 o 6 11 0 36.24 322.88 164.14 o 7 11 0 215.46 173.86 169.54 o 8 11 0 22.19 79.91 165.22 o 9 11 0 10.19 79.91 163.06 o 10 11 0 0.14 -137.14 163.06 o 0 12 0 29.92 18.36 126.34 o 1 12 0 26.57 62.63 88.99 o 2 12 0 138.23 249.45 142.54 o 3 12 0 198.46 -132.82 132.82 o 4 12 0 93.55 -132.82 132.82 o 5 12 0 63.67 -23.76 158.74 o 6 12 0 0.26 -86.39 157.66 o 7 12 0 201.60 306.68 171.70 o 8 12 0 73.10 150.10 180.34 o 1 13 0 31.98 38.87 143.62 o 2 13 0 13.72 145.78 150.10 o 3 13 0 6.94 -134.98 142.54 o 4 13 0 28.76 134.98 160.90 o 5 13 0 7.54 77.75 165.22 o -18 1 1 2.77 70.22 99.27 o -17 1 1 26.07 93.47 66.41 o -16 1 1 33.15 4.76 63.25 o -15 1 1 3.53 55.84 52.33 o -14 1 1 370.05 399.81 60.30 o -13 1 1 300.32 338.03 51.11 o -12 1 1 79.31 85.08 42.53 o -11 1 1 93.56 104.97 32.35 o -10 1 1 147.81 242.72 29.98 o -9 1 1 76.21 49.62 21.82 o -8 1 1 373.14 351.04 24.38 o -7 1 1 4036.45 3571.77 112.26 o -6 1 1 283.94 340.74 31.52 o -5 1 1 11565.59 12540.49 410.97 o -4 1 1 39241.56 50262.39 1674.98 o -3 1 1 1670.64 2082.49 82.32 o 3 1 1 486.27 628.32 24.03 o 4 1 1 10835.71 12301.03 431.71 o 5 1 1 1881.66 1951.61 72.74 o 6 1 1 14829.92 14544.97 469.77 o 7 1 1 5767.80 6405.82 211.41 o 8 1 1 5183.45 5430.56 181.07 o 9 1 1 30.31 -20.33 20.33 o 10 1 1 111.22 130.99 29.19 o 11 1 1 9.09 -31.65 31.65 o 12 1 1 46.28 89.98 41.43 o 13 1 1 5.24 -46.56 46.56 o 14 1 1 38.66 -48.54 48.54 o 15 1 1 77.93 104.94 54.34 o 16 1 1 2.74 -0.53 60.45 o 17 1 1 2.15 28.55 63.28 o 18 1 1 2.04 86.88 66.29 o -18 2 1 5.17 -1.55 74.69 o -17 2 1 5.57 71.39 66.51 o -16 2 1 61.15 68.00 78.66 o -15 2 1 49.05 59.56 50.79 o -14 2 1 2.55 34.32 50.59 o -13 2 1 1.76 -15.29 49.11 o -12 2 1 163.86 130.71 41.67 o -11 2 1 430.04 408.21 44.58 o -10 2 1 698.56 684.42 50.63 o -9 2 1 5.73 -5.46 22.24 o -8 2 1 827.27 835.18 40.46 o -7 2 1 112.17 106.55 21.89 o -6 2 1 922.36 995.55 42.06 o -5 2 1 780.20 694.48 31.08 o -4 2 1 11402.39 13898.15 526.36 o -3 2 1 5736.86 6610.92 366.93 o -2 2 1 4268.54 5048.45 351.73 o -1 2 1 3977.16 6535.64 364.65 o 0 2 1 6381.89 9475.73 515.47 o 1 2 1 32.14 16.68 12.00 o 2 2 1 24544.40 41935.97 2118.51 o 3 2 1 9.32 7.69 16.98 o 4 2 1 8493.64 8578.61 322.69 o 5 2 1 0.94 -3.11 12.92 o 6 2 1 498.21 660.57 34.09 o 7 2 1 1553.74 2040.21 85.45 o 8 2 1 476.73 447.61 32.58 o 9 2 1 97.82 129.28 25.65 o 10 2 1 1497.24 1703.94 95.04 o 11 2 1 789.21 883.20 60.73 o 12 2 1 6.56 -25.03 45.03 o 13 2 1 2442.55 2830.94 167.59 o 14 2 1 474.04 458.52 61.92 o 15 2 1 18.01 -2.02 49.13 o 16 2 1 132.93 102.84 67.90 o 17 2 1 27.39 58.88 86.66 o 18 2 1 3.09 -11.49 61.83 o -18 3 1 21.90 2.92 92.16 o -17 3 1 42.64 107.89 155.50 o -16 3 1 1.48 84.55 62.61 o -15 3 1 292.16 362.08 59.19 o -14 3 1 834.37 923.97 87.08 o -13 3 1 107.15 62.89 49.53 o -12 3 1 43.93 23.41 39.86 o -11 3 1 328.94 224.98 40.73 o -10 3 1 48.20 25.20 25.97 o -9 3 1 4711.70 5084.27 219.06 o -8 3 1 2956.06 2997.53 102.83 o -7 3 1 624.21 724.10 32.50 o -6 3 1 4097.54 4029.79 133.05 o -5 3 1 80.21 45.53 17.12 o -4 3 1 8.70 6.62 14.46 o -3 3 1 13406.42 10888.14 1167.87 o -2 3 1 9660.65 12954.42 1516.66 o -1 3 1 7353.77 9416.25 429.54 o 0 3 1 4783.83 6448.03 288.23 o 1 3 1 551.46 853.66 42.62 o 2 3 1 7684.96 10081.43 510.41 o 3 3 1 10508.90 10644.70 630.47 o 4 3 1 6266.46 5860.75 257.43 o 5 3 1 2601.83 2354.72 112.87 o 6 3 1 2011.81 1964.61 78.30 o 7 3 1 103.59 41.46 27.55 o 8 3 1 1008.10 1038.40 46.15 o 9 3 1 89.01 85.83 31.44 o 10 3 1 30.33 16.08 32.75 o 11 3 1 413.46 413.99 45.55 o 12 3 1 1405.90 1343.88 93.48 o 13 3 1 540.95 714.94 89.96 o 14 3 1 944.42 749.31 71.65 o 15 3 1 3.92 -24.97 49.15 o 16 3 1 3.29 -52.78 58.73 o 17 3 1 2.08 70.37 77.93 o -17 4 1 44.24 20.16 91.85 o -16 4 1 23.56 -41.37 85.02 o -15 4 1 319.07 321.44 70.26 o -14 4 1 2.17 -25.07 78.71 o -13 4 1 79.81 -2.65 48.43 o -12 4 1 7.21 -43.74 43.74 o -11 4 1 468.58 409.23 41.59 o -10 4 1 1961.01 2192.41 101.63 o -9 4 1 798.17 737.34 40.15 o -8 4 1 2448.82 2218.78 79.62 o -7 4 1 2.47 -11.05 16.63 o -6 4 1 274.44 305.27 24.73 o -5 4 1 1426.08 1090.06 52.18 o -4 4 1 2944.04 2760.78 143.98 o -3 4 1 183.14 177.07 26.78 o -2 4 1 6107.01 7858.07 438.34 o -1 4 1 827.67 1162.57 85.26 o 0 4 1 6403.09 8994.06 445.80 o 1 4 1 198.84 252.72 23.46 o 2 4 1 3609.50 4335.87 199.39 o 3 4 1 770.90 783.04 40.54 o 4 4 1 5531.73 5276.88 289.70 o 5 4 1 7400.26 6187.23 241.42 o 6 4 1 3791.33 3403.88 126.65 o 7 4 1 2186.58 1944.90 69.56 o 8 4 1 840.72 766.46 38.25 o 9 4 1 288.72 301.91 27.65 o 10 4 1 94.08 101.61 35.37 o 11 4 1 80.47 33.75 37.62 o 12 4 1 105.33 34.34 46.79 o 13 4 1 114.85 172.80 50.89 o 14 4 1 215.28 323.74 60.67 o 15 4 1 236.29 223.34 103.64 o 16 4 1 0.01 51.44 85.88 o 17 4 1 103.27 194.61 91.58 o -17 5 1 13.75 -84.67 87.00 o -16 5 1 46.51 46.87 91.80 o -15 5 1 56.23 -44.86 69.60 o -14 5 1 20.32 35.60 61.52 o -13 5 1 259.97 171.02 64.22 o -12 5 1 18.19 -56.57 56.57 o -11 5 1 11.39 -15.88 56.11 o -10 5 1 269.25 194.28 61.57 o -9 5 1 348.94 261.71 39.03 o -8 5 1 799.21 795.22 41.74 o -7 5 1 1842.50 1738.99 71.95 o -6 5 1 844.79 946.86 43.79 o -5 5 1 47.26 55.97 23.87 o -4 5 1 24.85 -32.26 32.26 o -3 5 1 2885.19 2869.10 233.17 o -2 5 1 675.60 667.71 56.77 o -1 5 1 1208.71 1734.81 111.38 o 0 5 1 4.61 15.67 21.66 o 1 5 1 6442.80 8934.34 487.68 o 2 5 1 4403.92 5397.03 309.55 o 3 5 1 3736.19 3529.06 343.21 o 4 5 1 0.09 22.82 19.64 o 5 5 1 836.95 761.27 38.85 o 6 5 1 347.03 278.77 25.78 o 7 5 1 740.31 732.66 42.53 o 8 5 1 66.04 43.32 22.69 o 9 5 1 487.18 498.45 36.54 o 10 5 1 279.92 244.51 42.48 o 11 5 1 50.91 -44.01 44.01 o 12 5 1 29.28 17.69 54.15 o 13 5 1 2.84 -11.67 57.24 o 14 5 1 5.00 -49.96 58.21 o 15 5 1 45.15 -7.87 67.54 o 16 5 1 73.28 132.46 89.09 o 17 5 1 9.60 35.15 89.70 o -16 6 1 15.23 -9.19 90.94 o -15 6 1 137.97 141.31 187.90 o -14 6 1 6.65 -20.09 74.80 o -13 6 1 16.59 -50.08 58.25 o -12 6 1 15.54 -53.79 53.79 o -11 6 1 34.03 21.27 54.71 o -10 6 1 259.07 281.59 52.43 o -9 6 1 0.02 -3.15 42.09 o -8 6 1 1042.65 973.61 59.41 o -7 6 1 177.43 152.30 31.95 o -6 6 1 18.93 7.21 22.30 o -5 6 1 6.61 -19.85 28.28 o -4 6 1 304.75 237.44 54.98 o -3 6 1 585.08 757.47 60.75 o -2 6 1 2392.52 2784.67 214.75 o -1 6 1 10.42 -33.53 42.88 o 0 6 1 7.18 4.06 29.52 o 1 6 1 15.14 66.99 52.38 o 2 6 1 210.61 187.60 41.39 o 3 6 1 869.71 1191.61 76.19 o 4 6 1 2859.30 3064.43 181.58 o 5 6 1 743.69 667.16 39.49 o 6 6 1 3.56 -22.30 22.30 o 7 6 1 52.90 36.44 29.43 o 8 6 1 12.24 -40.39 40.39 o 9 6 1 670.17 559.06 47.92 o 10 6 1 587.29 639.33 62.64 o 11 6 1 45.73 -41.90 49.55 o 12 6 1 134.34 134.98 72.05 o 13 6 1 12.41 -32.72 66.80 o 14 6 1 82.24 65.72 129.58 o 15 6 1 5.80 38.49 90.55 o 16 6 1 1.30 29.80 93.06 o -15 7 1 5.26 94.45 99.11 o -14 7 1 0.16 -80.08 132.82 o -13 7 1 144.89 78.21 75.69 o -12 7 1 0.25 -27.77 72.04 o -11 7 1 161.69 123.85 62.43 o -10 7 1 8.76 -56.47 56.47 o -9 7 1 8.49 -30.68 66.84 o -8 7 1 1878.74 1624.71 135.57 o -7 7 1 669.68 550.98 53.41 o -6 7 1 1811.65 1842.01 118.27 o -5 7 1 49.39 40.76 36.26 o -4 7 1 75.19 -26.55 34.34 o -3 7 1 1885.46 2165.55 154.66 o -2 7 1 1181.88 1062.00 92.45 o -1 7 1 2844.83 3486.70 286.89 o 0 7 1 479.55 591.53 97.17 o 1 7 1 3.66 18.92 46.34 o 2 7 1 568.24 560.74 65.25 o 3 7 1 4242.97 5102.79 332.27 o 4 7 1 441.60 336.51 38.97 o 5 7 1 1361.94 1321.37 110.55 o 6 7 1 81.78 20.37 56.33 o 7 7 1 277.45 257.76 55.80 o 8 7 1 1.49 -63.12 63.12 o 9 7 1 213.41 201.44 60.08 o 10 7 1 8.42 60.98 58.47 o 11 7 1 36.49 -51.28 60.39 o 12 7 1 61.67 32.65 70.49 o 13 7 1 0.41 -10.33 84.90 o 14 7 1 11.99 5.02 92.99 o 15 7 1 55.62 98.62 94.69 o -14 8 1 0.02 -73.21 125.26 o -13 8 1 0.28 -10.02 76.17 o -12 8 1 65.82 76.83 104.57 o -11 8 1 10.11 -20.04 73.26 o -10 8 1 428.47 465.41 119.86 o -9 8 1 1.70 -57.28 57.28 o -8 8 1 1.92 -5.87 60.30 o -7 8 1 29.94 74.71 70.55 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