#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/84/2018421.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018421_Fobs loop_ _publ_author_name 'Medvedev, Alexander G.' 'Mikhaylov, Alexey A.' 'Churakov, Andrei V.' 'Prikhodchenko, Petr V.' 'Lev, Ovadia' _publ_section_title ; Ammonium and caesium carbonate peroxosolvates: supramolecular networks formed by hydrogen bonds ; _journal_coeditor_code LG3077 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i20 _journal_page_last i24 _journal_volume 68 _journal_year 2012 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.8202 _cell_length_b 5.9357 _cell_length_c 16.8881 _exptl_crystal_F_000 1552.00 _reflns_d_resolution_high 0.7569 _[local]_cod_data_source_file lg3077IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' z in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 833.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5033.25 4306.60 158.20 o 4 0 0 58258.36 60156.30 1905.21 o 6 0 0 694844.13 684263.94 27287.32 o 8 0 0 2336.61 2565.82 70.25 o 10 0 0 155795.56 159783.69 3299.46 o 12 0 0 112033.91 111016.66 2305.80 o 14 0 0 155.01 248.26 27.17 o 16 0 0 92928.72 90526.52 1898.71 o 18 0 0 16688.99 16150.26 464.29 o 20 0 0 3578.94 3550.77 217.87 o 22 0 0 57631.52 60988.68 2087.76 o 1 1 0 22911.04 24002.71 352.82 o 3 1 0 350487.19 359656.69 5742.75 o 5 1 0 9.86 409.53 54.94 o 7 1 0 248695.75 247745.83 5968.04 o 9 1 0 199083.91 195310.80 2623.70 o 11 1 0 653.14 847.87 44.29 o 13 1 0 186370.89 184086.13 2474.30 o 15 1 0 79977.03 79593.48 1181.94 o 17 1 0 6874.26 6744.23 158.33 o 19 1 0 92506.80 95048.45 1782.58 o 21 1 0 11159.32 10940.41 286.10 o 23 1 0 4894.31 4953.02 206.13 o 2 2 0 10446.85 10878.09 166.66 o 4 2 0 38062.99 36631.10 774.87 o 6 2 0 417985.78 420596.22 6125.63 o 8 2 0 18.81 142.64 22.80 o 10 2 0 104428.17 102612.98 1504.36 o 12 2 0 126437.77 124288.02 1824.75 o 14 2 0 7.35 74.40 15.67 o 16 2 0 78780.77 78593.24 1428.57 o 18 2 0 21689.46 21654.29 433.55 o 20 2 0 3047.15 3238.14 101.87 o 22 2 0 55600.38 57511.50 1237.79 o 1 3 0 25450.57 25166.80 378.19 o 3 3 0 264210.13 257643.28 4612.08 o 5 3 0 8343.50 8707.36 144.06 o 7 3 0 95851.01 95952.75 1408.84 o 9 3 0 149992.61 151696.25 2372.91 o 11 3 0 1079.87 1211.68 81.05 o 13 3 0 107342.33 103567.60 1859.32 o 15 3 0 57503.14 56787.55 1274.41 o 17 3 0 45.10 129.33 38.18 o 19 3 0 77382.04 77030.48 1412.11 o 21 3 0 7232.79 7067.40 179.51 o 2 4 0 7742.74 7537.14 127.75 o 4 4 0 16446.71 16170.99 253.97 o 6 4 0 172298.36 169264.39 2472.53 o 8 4 0 652.34 859.87 83.63 o 10 4 0 47845.68 46989.14 773.70 o 12 4 0 108655.91 107709.45 1935.56 o 14 4 0 146.81 179.34 26.22 o 16 4 0 50056.68 49513.66 1561.61 o 18 4 0 23375.23 23144.57 578.87 o 20 4 0 2237.96 2419.91 162.08 o 1 5 0 14979.18 15123.13 242.94 o 3 5 0 152802.23 152114.31 2227.33 o 5 5 0 5128.59 5195.05 98.62 o 7 5 0 38519.88 39180.61 652.59 o 9 5 0 79482.69 80024.12 1401.17 o 11 5 0 1247.65 1424.16 57.83 o 13 5 0 52270.81 53574.65 1460.73 o 15 5 0 28246.08 27055.47 621.34 o 17 5 0 793.23 900.40 68.69 o 0 6 0 96126.90 99333.06 2074.46 o 2 6 0 1433.34 1612.17 97.37 o 4 6 0 8033.94 8076.04 189.84 o 6 6 0 77428.61 78997.24 1451.56 o 8 6 0 24.60 167.16 73.72 o 10 6 0 25585.64 25752.90 590.64 o 12 6 0 51460.15 51551.21 1127.86 o 14 6 0 130.58 245.14 62.84 o 1 7 0 4748.46 5199.56 203.96 o 3 7 0 67328.45 68142.07 1488.91 o 5 7 0 327.92 546.72 128.86 o 7 7 0 18322.35 19962.39 739.21 o 9 7 0 32376.05 32279.36 925.63 o 1 1 1 486.98 530.50 9.47 o 2 1 1 562.26 573.14 10.06 o 3 1 1 3.05 18.15 3.09 o 4 1 1 169.42 175.78 5.59 o 5 1 1 1059.67 951.79 15.24 o 6 1 1 508.29 516.08 11.13 o 7 1 1 1572.66 1563.56 23.98 o 8 1 1 156.91 155.73 7.96 o 9 1 1 3.23 3.65 4.13 o 10 1 1 4.05 7.47 4.63 o 11 1 1 25.30 18.33 5.63 o 12 1 1 228.78 220.74 11.54 o 13 1 1 626.72 641.84 19.08 o 14 1 1 28.09 31.05 8.04 o 15 1 1 0.53 2.94 7.24 o 16 1 1 0.07 -4.25 8.51 o 17 1 1 19.62 15.27 10.03 o 18 1 1 15.32 2.89 11.35 o 19 1 1 8.95 19.85 14.37 o 20 1 1 49.71 25.00 17.12 o 21 1 1 9.33 18.89 16.68 o 22 1 1 0.01 -5.63 17.84 o 23 1 1 17.66 13.94 22.82 o 1 2 1 1124.04 1211.72 18.06 o 2 2 1 32.56 47.24 3.87 o 3 2 1 52.52 60.76 4.34 o 4 2 1 9534.15 9548.14 109.80 o 5 2 1 72.02 72.76 5.12 o 6 2 1 2933.33 3067.29 40.23 o 7 2 1 1847.36 1965.54 33.80 o 8 2 1 972.70 941.33 18.30 o 9 2 1 115.82 129.63 7.71 o 10 2 1 4841.30 4781.01 61.89 o 11 2 1 379.00 340.41 12.92 o 12 2 1 582.68 637.17 18.36 o 13 2 1 144.58 160.30 12.30 o 14 2 1 0.91 -3.63 7.27 o 15 2 1 145.62 161.89 15.27 o 16 2 1 30.71 27.74 11.73 o 17 2 1 146.76 144.50 16.81 o 18 2 1 22.80 19.91 12.99 o 19 2 1 19.96 21.83 13.40 o 20 2 1 2.35 7.84 14.48 o 21 2 1 30.09 25.76 18.17 o 22 2 1 187.04 158.44 26.66 o 1 3 1 462.83 512.60 12.03 o 2 3 1 1149.87 1130.81 22.96 o 3 3 1 0.93 6.08 4.13 o 4 3 1 780.88 795.73 16.20 o 5 3 1 1759.71 1726.86 27.14 o 6 3 1 1213.09 1234.55 22.08 o 7 3 1 1769.29 1758.69 42.00 o 8 3 1 238.38 262.33 11.09 o 9 3 1 94.88 91.98 7.94 o 10 3 1 96.28 96.39 9.40 o 11 3 1 0.05 10.96 7.34 o 12 3 1 735.23 715.69 23.68 o 13 3 1 562.21 529.61 23.52 o 14 3 1 163.42 145.08 16.18 o 15 3 1 64.46 50.45 13.15 o 16 3 1 8.02 4.18 11.24 o 17 3 1 59.49 58.85 15.11 o 18 3 1 94.96 70.06 14.69 o 19 3 1 74.41 52.16 16.98 o 20 3 1 217.89 186.18 21.42 o 21 3 1 3.91 -8.23 16.45 o 1 4 1 1310.97 1304.65 24.24 o 2 4 1 201.97 206.60 10.71 o 3 4 1 140.01 141.06 10.79 o 4 4 1 3023.85 3072.05 44.30 o 5 4 1 26.16 30.46 6.05 o 6 4 1 446.82 479.16 15.22 o 7 4 1 1698.22 1698.61 31.96 o 8 4 1 30.34 31.01 7.24 o 9 4 1 338.74 362.17 23.02 o 10 4 1 2709.19 2557.88 47.79 o 11 4 1 183.28 187.67 15.70 o 12 4 1 483.38 492.97 23.55 o 13 4 1 202.57 236.59 19.58 o 14 4 1 18.27 10.53 11.14 o 15 4 1 327.58 370.87 25.36 o 16 4 1 158.77 128.77 18.54 o 17 4 1 186.34 184.15 20.94 o 18 4 1 269.66 225.30 24.34 o 19 4 1 0.80 3.15 15.60 o 20 4 1 9.79 -0.32 15.96 o 1 5 1 402.08 403.22 15.30 o 2 5 1 559.56 536.06 17.78 o 3 5 1 6.72 6.03 7.57 o 4 5 1 942.15 894.26 22.26 o 5 5 1 742.40 731.69 21.63 o 6 5 1 462.64 470.30 19.64 o 7 5 1 97.44 94.34 11.74 o 8 5 1 61.09 67.66 11.36 o 9 5 1 278.18 274.79 19.18 o 10 5 1 368.33 346.66 22.74 o 11 5 1 148.63 161.07 17.57 o 12 5 1 441.88 479.75 29.77 o 13 5 1 218.62 244.13 23.39 o 14 5 1 147.87 127.38 19.55 o 15 5 1 386.76 401.58 33.66 o 16 5 1 81.81 50.42 18.46 o 17 5 1 26.72 32.46 18.98 o 18 5 1 185.20 225.64 29.13 o 1 6 1 639.19 668.00 25.18 o 2 6 1 349.63 395.04 19.87 o 3 6 1 101.66 98.55 13.92 o 4 6 1 274.27 297.98 19.79 o 5 6 1 151.84 126.90 15.06 o 6 6 1 2.07 -5.51 11.03 o 7 6 1 733.99 751.93 31.86 o 8 6 1 144.51 172.21 20.20 o 9 6 1 307.81 334.49 26.02 o 10 6 1 349.47 329.07 29.30 o 11 6 1 6.22 -7.54 15.09 o 12 6 1 275.52 256.80 28.58 o 13 6 1 189.41 227.77 27.03 o 14 6 1 14.66 10.44 17.29 o 15 6 1 355.82 296.75 31.13 o 1 7 1 670.42 691.34 45.04 o 2 7 1 283.90 302.55 27.48 o 3 7 1 60.03 66.88 21.02 o 4 7 1 662.24 647.37 40.33 o 5 7 1 276.44 316.06 30.41 o 6 7 1 113.68 73.47 18.56 o 7 7 1 1234.29 1301.20 54.08 o 8 7 1 43.68 39.38 21.62 o 9 7 1 504.43 515.27 43.25 o 10 7 1 469.96 575.87 45.18 o 1 0 2 9687.87 10057.73 149.82 o 2 0 2 83.05 171.47 9.34 o 3 0 2 72209.05 74764.67 2118.72 o 4 0 2 180.28 200.59 7.54 o 5 0 2 79608.63 81283.52 1187.97 o 6 0 2 2058.20 2126.94 41.80 o 7 0 2 1386.14 2623.63 105.29 o 8 0 2 198.44 208.92 12.38 o 9 0 2 51245.82 51835.65 1173.37 o 10 0 2 2252.19 2175.62 47.21 o 11 0 2 48173.60 47633.89 774.83 o 12 0 2 1695.33 1755.58 43.73 o 13 0 2 16023.94 15531.58 249.02 o 14 0 2 269.31 243.00 18.74 o 15 0 2 2704.88 2798.39 90.83 o 16 0 2 1551.07 1488.65 49.92 o 17 0 2 36125.27 36100.48 610.48 o 18 0 2 6.51 94.11 41.17 o 19 0 2 23803.60 24311.69 478.48 o 20 0 2 579.99 778.07 61.37 o 21 0 2 1348.87 1625.19 258.90 o 22 0 2 208.75 329.50 58.23 o 23 0 2 4161.30 4294.63 426.94 o 0 1 2 47209.96 48624.23 711.65 o 1 1 2 68.04 94.47 3.69 o 2 1 2 29731.79 30957.59 322.88 o 3 1 2 48.86 240.06 28.34 o 4 1 2 185.35 287.18 25.54 o 5 1 2 355.92 504.15 10.46 o 6 1 2 75845.88 77814.03 883.84 o 7 1 2 1395.59 1409.51 22.34 o 8 1 2 53633.54 53480.51 558.97 o 9 1 2 938.35 906.01 18.26 o 10 1 2 2164.67 2091.42 48.57 o 11 1 2 1122.77 1159.39 22.89 o 12 1 2 7571.48 7642.20 98.82 o 13 1 2 3551.68 3381.83 49.82 o 14 1 2 44174.59 42797.75 456.77 o 15 1 2 407.37 408.66 18.27 o 16 1 2 27442.04 26789.08 324.38 o 17 1 2 1292.11 1272.26 33.77 o 18 1 2 331.04 387.28 30.85 o 19 1 2 1390.20 1389.91 47.14 o 20 1 2 16256.55 16398.03 257.56 o 21 1 2 8.62 61.03 19.41 o 22 1 2 15661.28 15804.82 302.27 o 23 1 2 253.06 291.69 33.95 o 0 2 2 3560.03 3699.59 62.62 o 1 2 2 10265.12 10463.17 118.73 o 2 2 2 992.91 994.77 17.74 o 3 2 2 82144.23 80867.54 874.86 o 4 2 2 1448.71 1399.75 21.55 o 5 2 2 82199.88 81957.65 884.01 o 6 2 2 2808.36 2763.79 41.44 o 7 2 2 63.19 179.23 23.03 o 8 2 2 111.91 152.19 7.17 o 9 2 2 36202.53 36108.69 399.16 o 10 2 2 1144.70 1150.51 24.99 o 11 2 2 44163.35 43011.77 475.19 o 12 2 2 568.67 586.04 19.24 o 13 2 2 16998.14 17044.37 212.21 o 14 2 2 117.20 106.25 13.72 o 15 2 2 794.79 961.31 51.17 o 16 2 2 469.25 471.34 25.04 o 17 2 2 26299.28 25845.32 354.90 o 18 2 2 0.18 -5.86 11.73 o 19 2 2 18348.02 17960.38 279.31 o 20 2 2 201.00 216.74 23.81 o 21 2 2 1340.70 1431.09 54.29 o 22 2 2 71.14 68.42 22.72 o 0 3 2 63291.46 64206.80 976.89 o 1 3 2 994.86 938.04 17.70 o 2 3 2 39046.19 38758.01 407.23 o 3 3 2 1902.72 1852.12 28.02 o 4 3 2 19.19 189.73 29.71 o 5 3 2 79.60 99.70 7.05 o 6 3 2 52323.65 52083.80 568.37 o 7 3 2 1832.13 1829.92 29.29 o 8 3 2 52636.23 51629.89 566.33 o 9 3 2 504.95 482.43 16.39 o 10 3 2 7768.71 7551.93 97.78 o 11 3 2 365.22 365.67 15.94 o 12 3 2 2514.93 2549.50 68.16 o 13 3 2 542.18 532.66 23.87 o 14 3 2 27247.74 27014.80 345.51 o 15 3 2 34.69 29.57 12.21 o 16 3 2 22784.39 22441.92 313.46 o 17 3 2 177.81 129.24 17.28 o 18 3 2 709.63 787.29 55.52 o 19 3 2 94.53 61.86 16.22 o 20 3 2 8723.65 8928.83 161.51 o 21 3 2 0.04 19.60 17.93 o 0 4 2 6027.96 5796.26 102.27 o 1 4 2 7116.39 7288.21 116.28 o 2 4 2 1238.74 1180.00 22.90 o 3 4 2 61327.34 59859.59 626.67 o 4 4 2 1927.17 1863.39 31.29 o 5 4 2 55326.28 54557.06 597.83 o 6 4 2 2069.95 1961.79 32.75 o 7 4 2 1811.06 2199.53 107.96 o 8 4 2 43.50 57.63 7.99 o 9 4 2 18068.72 17741.26 209.10 o 10 4 2 242.91 233.44 16.47 o 11 4 2 31362.70 30516.35 385.19 o 12 4 2 33.51 43.28 11.44 o 13 4 2 14005.10 13998.13 193.11 o 14 4 2 0.58 -2.00 10.23 o 15 4 2 12.19 99.63 35.35 o 16 4 2 4.05 4.37 13.43 o 17 4 2 13799.91 13253.39 217.75 o 18 4 2 0.68 0.03 15.05 o 19 4 2 10642.60 10500.32 184.16 o 20 4 2 6.53 27.12 17.36 o 0 5 2 40191.89 39523.46 598.08 o 1 5 2 831.62 803.76 20.85 o 2 5 2 22443.44 22207.19 245.18 o 3 5 2 1922.22 1864.39 32.34 o 4 5 2 81.01 250.89 32.80 o 5 5 2 0.75 4.37 8.03 o 6 5 2 28019.87 27935.81 336.32 o 7 5 2 675.34 676.19 32.08 o 8 5 2 31055.04 30224.32 470.11 o 9 5 2 138.24 91.26 14.43 o 10 5 2 6187.83 6266.94 107.68 o 11 5 2 61.73 104.47 15.97 o 12 5 2 1495.69 1552.18 49.34 o 13 5 2 3.54 1.65 12.56 o 14 5 2 14740.19 14266.81 230.23 o 15 5 2 15.51 27.04 16.67 o 16 5 2 14403.83 14177.58 232.99 o 17 5 2 4.32 13.46 18.46 o 18 5 2 501.37 607.98 58.44 o 0 6 2 1807.70 1987.50 60.02 o 1 6 2 3131.87 3334.00 70.47 o 2 6 2 282.22 221.67 17.17 o 3 6 2 27367.76 27790.88 358.71 o 4 6 2 751.85 760.74 34.36 o 5 6 2 21363.38 21770.87 305.44 o 6 6 2 729.30 709.60 28.82 o 7 6 2 705.07 910.08 40.52 o 8 6 2 3.52 2.01 11.54 o 9 6 2 9483.06 9802.24 156.03 o 10 6 2 154.72 177.20 21.46 o 11 6 2 16301.72 16676.03 287.10 o 12 6 2 29.85 28.72 17.50 o 13 6 2 6926.05 6980.44 145.97 o 14 6 2 18.86 0.07 16.46 o 15 6 2 48.74 141.06 53.05 o 0 7 2 15138.89 14822.60 371.65 o 1 7 2 134.80 82.78 23.07 o 2 7 2 7197.08 7611.13 224.23 o 3 7 2 433.59 508.78 32.01 o 4 7 2 125.47 273.46 63.97 o 5 7 2 1.73 -7.60 15.21 o 6 7 2 11996.39 12521.22 229.46 o 7 7 2 103.98 131.02 23.69 o 8 7 2 12020.57 12495.02 236.63 o 9 7 2 18.44 6.74 19.50 o 10 7 2 2032.29 2114.59 78.07 o 1 1 3 187.41 214.53 6.35 o 2 1 3 1024.92 1036.30 19.11 o 3 1 3 14.28 29.31 2.60 o 4 1 3 360.12 400.13 15.40 o 5 1 3 543.59 483.67 12.21 o 6 1 3 2202.86 2251.52 33.90 o 7 1 3 2051.70 2036.23 40.55 o 8 1 3 16.85 24.17 4.34 o 9 1 3 0.15 6.93 4.23 o 10 1 3 303.64 321.74 14.60 o 11 1 3 150.59 149.54 10.32 o 12 1 3 128.11 134.16 9.76 o 13 1 3 1357.99 1299.20 28.59 o 14 1 3 30.74 36.76 8.78 o 15 1 3 62.00 60.89 10.74 o 16 1 3 247.95 273.11 17.23 o 17 1 3 60.17 53.22 12.60 o 18 1 3 208.50 205.08 17.70 o 19 1 3 10.74 8.92 13.97 o 20 1 3 8.42 16.50 13.84 o 21 1 3 195.96 203.34 27.12 o 22 1 3 0.28 -8.11 16.22 o 23 1 3 45.28 7.39 22.36 o 1 2 3 1721.21 1963.89 26.37 o 2 2 3 441.94 346.99 9.16 o 3 2 3 54.78 87.35 4.94 o 4 2 3 5941.44 6277.52 76.02 o 5 2 3 1264.61 1251.08 21.82 o 6 2 3 2052.00 2199.31 33.69 o 7 2 3 493.82 539.12 19.56 o 8 2 3 2252.14 2183.89 34.74 o 9 2 3 2.30 8.13 4.81 o 10 2 3 2319.57 2215.45 36.51 o 11 2 3 1979.18 1914.32 34.41 o 12 2 3 40.56 43.30 8.72 o 13 2 3 399.22 419.87 19.12 o 14 2 3 171.02 133.22 12.50 o 15 2 3 298.18 305.63 18.08 o 16 2 3 103.55 89.54 13.99 o 17 2 3 0.12 -2.52 10.84 o 18 2 3 190.07 176.51 19.20 o 19 2 3 373.10 369.43 29.43 o 20 2 3 40.15 30.09 16.95 o 21 2 3 153.05 186.27 23.59 o 22 2 3 415.83 434.05 33.94 o 1 3 3 98.43 103.21 8.30 o 2 3 3 322.07 351.93 10.57 o 3 3 3 12.11 16.06 4.58 o 4 3 3 15.83 17.53 5.18 o 5 3 3 201.78 186.93 8.35 o 6 3 3 1778.51 1762.09 30.52 o 7 3 3 5064.57 4963.53 67.01 o 8 3 3 14.70 13.02 6.01 o 9 3 3 39.78 48.26 7.65 o 10 3 3 917.24 923.08 22.94 o 11 3 3 321.02 310.11 16.15 o 12 3 3 62.67 53.78 9.55 o 13 3 3 3239.59 3035.80 58.22 o 14 3 3 4.83 4.99 10.00 o 15 3 3 291.60 302.49 20.81 o 16 3 3 458.63 483.45 27.70 o 17 3 3 127.79 101.86 16.81 o 18 3 3 537.14 565.32 31.41 o 19 3 3 22.14 40.04 16.46 o 20 3 3 31.29 29.02 17.56 o 21 3 3 676.14 617.76 41.73 o 1 4 3 42.43 41.77 6.23 o 2 4 3 735.07 758.58 25.72 o 3 4 3 124.68 121.76 8.82 o 4 4 3 326.95 332.08 12.69 o 5 4 3 558.43 592.79 16.60 o 6 4 3 11.81 17.44 6.78 o 7 4 3 45.89 41.14 7.69 o 8 4 3 778.17 793.67 24.00 o 9 4 3 318.32 344.36 15.72 o 10 4 3 196.94 189.55 14.46 o 11 4 3 203.01 204.66 19.57 o 12 4 3 193.91 217.50 18.64 o 13 4 3 180.82 167.12 18.25 o 14 4 3 18.98 18.61 11.20 o 15 4 3 335.68 366.75 26.82 o 16 4 3 100.76 90.91 18.15 o 17 4 3 84.93 73.21 17.73 o 18 4 3 283.15 304.28 28.14 o 19 4 3 181.10 149.23 22.70 o 20 4 3 111.84 105.88 21.54 o 1 5 3 1075.19 1099.36 26.00 o 2 5 3 269.41 288.95 15.10 o 3 5 3 18.58 29.97 8.74 o 4 5 3 1237.82 1181.87 29.74 o 5 5 3 116.25 123.25 11.92 o 6 5 3 166.25 148.05 13.49 o 7 5 3 1620.88 1579.01 35.99 o 8 5 3 5.72 -4.76 9.52 o 9 5 3 329.78 324.52 22.30 o 10 5 3 514.80 499.75 26.86 o 11 5 3 16.15 3.04 10.85 o 12 5 3 217.75 219.84 19.70 o 13 5 3 698.87 620.39 34.06 o 14 5 3 118.13 117.71 20.27 o 15 5 3 383.54 400.99 30.65 o 16 5 3 37.52 29.73 17.55 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