#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:22:23 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180856 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/87/2018707.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018707_Fobs loop_ _publ_author_name 'Dal Bo, Fabrice' 'Hatert, Fr\'ed\'eric' _publ_section_title ; Fe~6.67~(PO~4~)~5.35~(HPO~4~)~0.65~ and Fe~6.23~(PO~4~)~4.45~(HPO~4~)~1.55~: two new mixed-valence iron phosphates ; _journal_coeditor_code FN3113 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i83 _journal_page_last i85 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 105.278 _cell_angle_beta 108.055 _cell_angle_gamma 101.993 _cell_length_a 6.3609 _cell_length_b 7.9750 _cell_length_c 9.3220 _exptl_crystal_F_000 465.00 _reflns_d_resolution_high 0.7006 _cod_data_source_file fn3113H339sup2.hkl _cod_data_source_block H339 #BEGIN Tags that were not found in dictionaries: _shelx_title ' H339-a in P-1 #2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1530.96 1576.31 9.96 o 2 0 0 28.23 25.21 2.92 o 3 0 0 4608.62 4532.53 35.81 o 4 0 0 204.82 199.62 8.09 o 5 0 0 432.02 429.35 13.81 o 6 0 0 1144.88 1131.15 25.95 o 7 0 0 4.89 0.13 6.30 o 8 0 0 237.69 191.67 27.74 o -8 1 0 105.24 79.59 18.97 o -7 1 0 15.54 20.87 7.69 o -6 1 0 698.76 692.56 18.33 o -5 1 0 186.46 177.47 9.13 o -4 1 0 2.76 8.24 3.11 o -3 1 0 385.06 434.48 8.63 o -2 1 0 10909.60 10999.77 50.47 o -1 1 0 702.45 709.84 6.93 o 0 1 0 1156.34 1181.18 9.18 o 1 1 0 1141.18 1175.40 9.03 o 2 1 0 214.07 204.87 6.71 o 3 1 0 169.34 163.33 8.13 o 4 1 0 17889.27 17198.39 94.95 o 5 1 0 248.78 236.44 10.67 o 6 1 0 3.80 9.47 5.61 o 7 1 0 947.90 923.55 29.91 o -8 2 0 7.63 6.20 8.25 o -7 2 0 19.22 29.14 7.88 o -6 2 0 952.35 959.02 20.82 o -5 2 0 434.13 437.84 13.86 o -4 2 0 249.60 224.53 8.74 o -3 2 0 119.20 114.73 5.79 o -2 2 0 4398.64 4489.20 30.50 o -1 2 0 67.57 79.85 2.57 o 0 2 0 2003.16 2059.17 13.68 o 1 2 0 6.88 8.46 2.13 o 2 2 0 3027.27 3124.24 28.29 o 3 2 0 62.02 63.96 5.80 o 4 2 0 1839.66 1774.53 26.03 o 5 2 0 213.97 212.92 10.37 o 6 2 0 7.07 11.72 6.11 o 7 2 0 1.29 -6.93 7.12 o -8 3 0 19.82 18.11 7.56 o -7 3 0 219.23 234.13 12.60 o -6 3 0 1702.10 1706.03 32.80 o -5 3 0 15.22 9.03 5.87 o -4 3 0 2139.27 2093.36 26.66 o -3 3 0 2.19 8.35 3.14 o -2 3 0 1376.27 1374.88 14.11 o -1 3 0 1873.02 1613.50 15.56 o 0 3 0 3081.14 3194.78 26.55 o 1 3 0 606.64 566.98 11.52 o 2 3 0 6440.56 6548.68 43.48 o 3 3 0 25.71 25.97 5.14 o 4 3 0 0.12 9.47 4.78 o 5 3 0 3.74 11.76 5.61 o 6 3 0 16.80 17.64 6.65 o 7 3 0 49.28 24.42 22.49 o -8 4 0 12.68 7.46 6.51 o -7 4 0 89.20 101.53 9.22 o -6 4 0 3592.66 3534.57 43.70 o -5 4 0 789.23 751.42 18.35 o -4 4 0 871.16 852.53 18.24 o -3 4 0 493.96 493.07 11.51 o -2 4 0 3215.69 3184.73 30.38 o -1 4 0 467.58 510.93 11.23 o 0 4 0 7122.90 7556.86 52.32 o 1 4 0 1.47 8.72 4.56 o 2 4 0 155.43 163.14 8.82 o 3 4 0 3623.95 3621.35 51.85 o 4 4 0 632.84 631.36 16.09 o 5 4 0 446.46 454.62 17.95 o 6 4 0 2391.13 2426.38 53.64 o -8 5 0 968.56 945.47 31.05 o -7 5 0 23.94 14.84 7.06 o -6 5 0 150.69 152.27 10.43 o -5 5 0 874.97 861.09 20.44 o -4 5 0 163.24 166.43 8.50 o -3 5 0 334.49 320.53 13.87 o -2 5 0 6512.69 6529.48 45.68 o -1 5 0 19.23 15.17 4.39 o 0 5 0 1972.60 1953.12 23.69 o 1 5 0 32.13 29.90 3.68 o 2 5 0 1578.13 1562.74 28.11 o 3 5 0 15.56 31.32 7.32 o 4 5 0 231.81 234.93 12.94 o 5 5 0 135.47 143.96 13.72 o 6 5 0 0.25 -5.75 18.99 o -8 6 0 301.29 291.66 17.82 o -7 6 0 2107.10 2142.12 39.18 o -6 6 0 456.22 431.73 16.26 o -5 6 0 569.71 532.74 19.21 o -4 6 0 4041.83 3977.89 44.20 o -3 6 0 671.18 658.08 15.16 o -2 6 0 17.89 18.97 3.82 o -1 6 0 249.48 258.33 10.46 o 0 6 0 24.04 26.46 6.19 o 1 6 0 787.56 789.50 21.46 o 2 6 0 1656.14 1660.35 30.42 o 3 6 0 124.49 127.99 10.03 o 4 6 0 247.31 251.29 17.67 o 5 6 0 105.38 107.97 16.25 o -7 7 0 683.25 656.69 22.33 o -6 7 0 740.45 745.53 20.55 o -5 7 0 23.96 29.72 5.83 o -4 7 0 525.29 522.35 16.14 o -3 7 0 1812.71 1755.97 31.66 o -2 7 0 813.89 828.96 17.75 o -1 7 0 1169.58 1136.79 25.82 o 0 7 0 859.16 844.62 21.24 o 1 7 0 850.47 834.91 24.42 o 2 7 0 230.90 236.99 12.27 o 3 7 0 9.97 9.73 8.18 o 4 7 0 51.59 34.32 10.21 o -7 8 0 1.42 -2.07 7.92 o -6 8 0 361.59 377.82 15.11 o -5 8 0 124.64 110.73 8.61 o -4 8 0 104.69 97.32 8.59 o -3 8 0 2606.63 2630.37 41.42 o -2 8 0 1053.86 1075.24 23.08 o -1 8 0 7.63 8.35 5.29 o 0 8 0 120.29 123.98 9.15 o 1 8 0 58.04 53.74 7.90 o 2 8 0 318.17 314.21 19.41 o 3 8 0 648.40 656.08 23.36 o -6 9 0 10.69 20.53 14.37 o -5 9 0 933.73 937.05 24.56 o -4 9 0 763.97 777.19 22.01 o -3 9 0 227.72 261.48 13.89 o -2 9 0 6.17 9.21 5.23 o -1 9 0 6.98 8.27 5.40 o 0 9 0 21.93 12.49 7.87 o 1 9 0 1473.76 1475.38 38.01 o 2 9 0 150.55 128.14 31.59 o -5 10 0 72.62 55.22 16.95 o -4 10 0 913.03 958.94 37.75 o -3 10 0 26.38 16.68 9.31 o -2 10 0 110.11 126.42 13.71 o -1 10 0 1168.47 1223.15 35.00 o 0 10 0 17.17 -2.74 20.23 o 2 -11 1 42.34 41.54 23.20 o -1 -10 1 356.55 435.71 58.63 o 0 -10 1 213.20 228.21 17.53 o 1 -10 1 1.15 -1.29 7.36 o 2 -10 1 14.67 13.33 9.11 o 3 -10 1 60.64 69.25 12.08 o 4 -10 1 3.85 -3.21 8.86 o 5 -10 1 751.56 768.98 65.22 o -2 -9 1 1.96 -0.05 9.83 o -1 -9 1 128.84 125.90 14.39 o 0 -9 1 1381.90 1386.65 39.69 o 1 -9 1 84.42 81.57 12.07 o 2 -9 1 193.53 210.21 14.49 o 3 -9 1 1176.38 1213.30 44.38 o 4 -9 1 942.58 967.57 39.59 o 5 -9 1 63.27 76.50 12.65 o 6 -9 1 2.54 8.96 8.69 o -3 -8 1 10.91 13.31 6.94 o -2 -8 1 59.44 70.61 8.54 o -1 -8 1 655.98 679.69 27.80 o 0 -8 1 272.66 258.52 12.33 o 1 -8 1 3547.02 3473.27 43.83 o 2 -8 1 116.72 117.18 7.99 o 3 -8 1 39.73 32.99 5.74 o 4 -8 1 2037.60 2009.07 31.67 o 5 -8 1 148.43 147.81 9.45 o 6 -8 1 47.97 45.12 6.65 o 7 -8 1 647.24 628.73 26.42 o -4 -7 1 45.73 42.92 8.26 o -3 -7 1 1.19 1.40 5.88 o -2 -7 1 215.12 235.97 12.11 o -1 -7 1 4128.47 4136.59 51.24 o 0 -7 1 207.74 208.01 11.16 o 1 -7 1 1.80 0.17 3.64 o 2 -7 1 43.27 34.33 4.44 o 3 -7 1 273.65 261.43 11.47 o 4 -7 1 729.00 723.09 18.42 o 5 -7 1 2251.71 2349.22 34.98 o 6 -7 1 290.34 298.06 13.61 o 7 -7 1 572.47 589.64 21.55 o -5 -6 1 417.50 443.80 21.33 o -4 -6 1 862.22 896.54 26.21 o -3 -6 1 1085.28 1071.72 27.16 o -2 -6 1 597.37 581.13 17.49 o -1 -6 1 806.61 816.30 23.75 o 0 -6 1 607.46 577.16 17.88 o 1 -6 1 4.62 3.11 3.68 o 2 -6 1 64.96 67.68 5.54 o 3 -6 1 5860.01 5795.14 50.60 o 4 -6 1 392.88 374.49 13.19 o 5 -6 1 137.92 138.75 9.30 o 6 -6 1 15.93 29.33 5.81 o 7 -6 1 34.65 28.12 7.04 o 8 -6 1 75.44 89.84 25.83 o -6 -5 1 1306.75 1261.27 43.96 o -5 -5 1 487.59 531.46 24.48 o -4 -5 1 48.34 45.36 6.96 o -3 -5 1 169.23 176.49 9.59 o -2 -5 1 748.16 739.35 17.71 o -1 -5 1 2380.96 2316.38 28.36 o 0 -5 1 10475.78 10341.72 66.66 o 1 -5 1 2233.29 2241.44 25.28 o 2 -5 1 377.88 382.93 10.64 o 3 -5 1 7838.50 7578.87 65.38 o 4 -5 1 986.80 963.83 21.06 o 5 -5 1 182.27 181.72 10.29 o 6 -5 1 286.19 264.96 12.47 o 7 -5 1 255.57 242.56 13.96 o 8 -5 1 6.16 7.05 8.09 o -6 -4 1 648.49 649.58 25.48 o -5 -4 1 226.92 244.58 12.79 o -4 -4 1 1123.80 1108.63 22.96 o -3 -4 1 254.78 249.18 9.56 o -2 -4 1 6478.62 6333.66 51.71 o -1 -4 1 2103.55 2093.50 21.68 o 0 -4 1 26.06 39.60 3.54 o 1 -4 1 971.04 959.58 12.51 o 2 -4 1 261.91 290.57 8.99 o 3 -4 1 342.85 331.57 9.90 o 4 -4 1 6519.89 6404.17 57.95 o 5 -4 1 73.69 72.15 7.51 o 6 -4 1 26.49 27.23 5.55 o 7 -4 1 4744.29 4764.52 57.26 o 8 -4 1 121.07 123.97 12.48 o -7 -3 1 1054.11 1118.91 47.26 o -6 -3 1 83.31 79.23 9.13 o -5 -3 1 143.41 146.00 9.39 o -4 -3 1 1027.64 995.47 17.31 o -3 -3 1 23.02 29.30 5.29 o -2 -3 1 4621.45 4645.68 36.20 o -1 -3 1 179.04 207.34 6.38 o 0 -3 1 946.26 1073.08 10.24 o 1 -3 1 424.30 365.32 5.88 o 2 -3 1 1396.23 1140.77 13.09 o 3 -3 1 817.10 813.44 17.79 o 4 -3 1 13.27 18.13 5.57 o 5 -3 1 2182.41 2148.91 31.33 o 6 -3 1 3.54 2.31 5.43 o 7 -3 1 285.07 280.18 14.87 o 8 -3 1 312.05 346.83 28.45 o -7 -2 1 141.03 165.61 13.87 o -6 -2 1 1679.03 1700.48 36.12 o -5 -2 1 482.81 464.83 14.80 o -4 -2 1 472.36 472.26 11.94 o -3 -2 1 10344.21 10350.72 57.47 o -2 -2 1 2046.80 2122.85 18.54 o -1 -2 1 41.62 75.94 2.99 o 0 -2 1 1827.80 2005.67 10.89 o 1 -2 1 710.33 724.05 6.32 o 2 -2 1 4138.17 3981.15 24.25 o 3 -2 1 37.29 34.47 4.55 o 4 -2 1 10.69 13.99 4.88 o 5 -2 1 1670.31 1623.26 28.90 o 6 -2 1 184.69 191.46 9.66 o 7 -2 1 0.60 8.39 7.61 o 8 -2 1 0.38 9.76 10.88 o -8 -1 1 34.94 58.97 26.42 o -7 -1 1 110.15 100.75 11.38 o -6 -1 1 1653.22 1589.08 29.70 o -5 -1 1 37.56 24.48 5.44 o -4 -1 1 38.07 44.91 4.62 o -3 -1 1 410.13 438.10 10.35 o -2 -1 1 7234.63 7298.91 35.03 o -1 -1 1 675.99 677.93 5.59 o 0 -1 1 1001.12 1016.93 7.02 o 1 -1 1 5786.15 5818.96 21.37 o 2 -1 1 3021.90 3118.53 21.45 o 3 -1 1 191.49 167.09 7.64 o 4 -1 1 258.68 279.25 10.70 o 5 -1 1 582.77 583.17 16.74 o 6 -1 1 2577.53 2507.09 36.86 o 7 -1 1 113.68 114.18 10.89 o 8 -1 1 21.96 5.38 11.33 o -8 0 1 2256.49 2232.99 89.24 o -7 0 1 75.55 95.43 11.64 o -6 0 1 7.38 6.66 5.58 o -5 0 1 287.25 289.66 11.44 o -4 0 1 631.88 604.56 13.49 o -3 0 1 300.60 369.44 8.37 o -2 0 1 14094.53 13779.42 53.19 o -1 0 1 18.28 21.56 1.97 o 0 0 1 1.49 3.29 1.41 o 1 0 1 1065.41 1155.59 9.93 o 2 0 1 4426.97 4575.71 34.31 o 3 0 1 214.37 243.97 8.72 o 4 0 1 535.44 513.61 13.05 o 5 0 1 290.25 297.72 11.72 o 6 0 1 434.31 432.60 16.99 o 7 0 1 245.59 214.79 14.05 o -8 1 1 18.34 7.88 11.06 o -7 1 1 1509.44 1509.29 32.45 o -6 1 1 243.32 256.33 11.36 o -5 1 1 638.68 638.25 18.20 o -4 1 1 28124.89 26879.28 120.81 o -3 1 1 9.14 9.12 3.39 o -2 1 1 2.20 7.11 2.64 o -1 1 1 3347.52 3427.55 20.93 o 0 1 1 266.38 254.65 4.47 o 1 1 1 2093.62 2099.93 14.75 o 2 1 1 1099.20 937.40 14.34 o 3 1 1 0.50 2.56 3.94 o 4 1 1 496.81 503.61 13.29 o 5 1 1 769.22 751.96 20.14 o 6 1 1 173.75 174.09 10.70 o 7 1 1 57.59 47.01 7.77 o -8 2 1 4.20 14.47 7.82 o -7 2 1 26.14 24.39 6.13 o -6 2 1 820.29 801.61 19.04 o -5 2 1 354.77 334.97 16.16 o -4 2 1 32.53 28.10 3.87 o -3 2 1 7731.87 7795.02 48.37 o -2 2 1 2291.88 2361.40 24.85 o -1 2 1 727.23 753.11 10.49 o 0 2 1 43773.23 39263.33 156.71 o 1 2 1 185.57 147.18 5.17 o 2 2 1 394.76 408.39 9.76 o 3 2 1 6105.20 5919.35 45.43 o 4 2 1 259.31 258.73 9.21 o 5 2 1 327.68 308.79 12.81 o 6 2 1 118.81 132.98 10.37 o 7 2 1 2.59 -12.83 13.17 o -8 3 1 55.81 61.93 8.50 o -7 3 1 5.53 14.80 5.84 o -6 3 1 859.90 848.15 20.72 o -5 3 1 143.66 133.34 8.72 o -4 3 1 1064.31 1045.43 17.60 o -3 3 1 279.25 292.76 10.76 o -2 3 1 141.88 220.75 7.31 o -1 3 1 63.12 78.35 5.37 o 0 3 1 7027.03 7458.47 51.35 o 1 3 1 875.38 808.52 13.14 o 2 3 1 850.79 863.17 16.63 o 3 3 1 259.86 247.71 10.24 o 4 3 1 2228.20 2216.52 32.78 o 5 3 1 343.33 371.84 15.03 o 6 3 1 12.12 4.99 7.98 o -8 4 1 214.12 215.83 13.76 o -7 4 1 84.04 81.38 7.78 o -6 4 1 622.78 612.87 20.05 o -5 4 1 360.53 376.95 12.82 o -4 4 1 1219.20 1219.15 18.80 o -3 4 1 268.33 270.42 8.44 o -2 4 1 7286.11 7509.51 50.03 o -1 4 1 51.96 45.88 4.83 o 0 4 1 1092.16 1129.95 20.74 o 1 4 1 1269.51 1221.97 22.94 o 2 4 1 11.52 14.53 4.49 o 3 4 1 372.85 355.42 12.77 o 4 4 1 2045.48 1986.03 33.98 o 5 4 1 7.79 9.16 6.71 o 6 4 1 43.92 28.33 21.85 o -8 5 1 136.95 139.50 11.51 o -7 5 1 439.02 432.24 16.14 o -6 5 1 1558.24 1560.21 28.45 o -5 5 1 2.88 5.74 5.16 o -4 5 1 1185.04 1158.89 21.19 o -3 5 1 61.02 62.38 6.17 o -2 5 1 194.83 192.53 7.19 o -1 5 1 5279.47 4901.27 39.97 o 0 5 1 740.96 727.61 19.03 o 1 5 1 882.04 879.48 20.91 o 2 5 1 4751.42 4593.95 51.41 o 3 5 1 182.30 157.83 11.78 o 4 5 1 14.31 17.11 6.43 o 5 5 1 449.18 443.29 19.62 o -8 6 1 70.65 66.14 10.22 o -7 6 1 70.58 71.96 8.99 o -6 6 1 1682.93 1720.22 30.92 o -5 6 1 352.32 368.53 14.15 o -4 6 1 537.12 523.50 16.83 o -3 6 1 100.41 113.61 8.55 o -2 6 1 786.26 777.18 16.83 o -1 6 1 53.43 48.18 7.11 o 0 6 1 798.36 883.04 22.23 o 1 6 1 141.09 135.63 9.66 o 2 6 1 1.31 9.54 6.53 o 3 6 1 3689.10 3730.98 55.51 o 4 6 1 1.05 3.39 6.78 o -7 7 1 11.11 10.81 6.62 o -6 7 1 33.63 13.57 5.80 o -5 7 1 509.61 502.39 16.63 o -4 7 1 163.14 155.63 9.95 o -3 7 1 204.21 198.98 11.76 o -2 7 1 419.09 483.10 15.27 o -1 7 1 131.08 144.99 10.42 o 0 7 1 285.21 292.70 13.15 o 1 7 1 0.57 7.99 6.24 o 2 7 1 68.86 79.22 8.85 o 3 7 1 3.56 13.26 7.83 o -7 8 1 940.56 932.22 28.46 o -6 8 1 398.76 421.24 16.04 o -5 8 1 761.57 750.90 21.97 o -4 8 1 439.86 437.07 17.72 o -3 8 1 705.37 709.10 22.04 o -2 8 1 587.31 585.79 18.91 o -1 8 1 283.27 274.78 13.15 o 0 8 1 9.21 22.86 5.74 o 1 8 1 62.68 60.57 9.21 o 2 8 1 195.54 188.18 14.72 o 3 8 1 94.73 88.54 13.01 o -6 9 1 769.30 680.52 27.60 o -5 9 1 20.46 15.97 5.96 o -4 9 1 6.57 15.51 6.33 o -3 9 1 632.67 627.84 21.42 o -2 9 1 226.42 235.81 12.71 o -1 9 1 1655.44 1722.65 33.42 o 0 9 1 170.03 204.03 13.84 o 1 9 1 219.09 199.12 17.71 o -5 10 1 48.43 36.18 24.67 o -4 10 1 17.05 10.67 22.89 o -3 10 1 2014.77 2211.17 59.48 o -2 10 1 138.26 158.84 18.42 o 1 -11 2 355.61 350.69 36.36 o 2 -11 2 87.26 72.91 26.20 o -1 -10 2 115.92 96.99 15.01 o 0 -10 2 34.53 40.46 9.53 o 1 -10 2 1170.98 1209.06 32.04 o 2 -10 2 287.00 307.85 19.68 o 3 -10 2 219.23 213.39 18.43 o 4 -10 2 872.41 901.67 36.21 o 5 -10 2 206.64 196.85 26.45 o -3 -9 2 31.22 36.47 26.20 o -2 -9 2 460.72 441.03 30.48 o -1 -9 2 83.77 106.36 14.67 o 0 -9 2 0.03 -0.36 7.90 o 1 -9 2 2461.06 2466.80 47.54 o 2 -9 2 37.93 32.30 7.79 o 3 -9 2 121.21 99.99 13.27 o 4 -9 2 11.42 21.00 9.86 o 5 -9 2 11.06 13.29 7.77 o 6 -9 2 275.14 334.28 27.96 o -3 -8 2 103.06 105.78 13.67 o -2 -8 2 353.37 378.33 20.82 o -1 -8 2 603.31 618.28 20.25 o 0 -8 2 177.50 186.10 16.09 o 1 -8 2 251.53 239.38 10.38 o 2 -8 2 258.02 275.61 10.40 o 3 -8 2 1324.55 1290.77 23.63 o 4 -8 2 50.26 45.06 5.62 o 5 -8 2 1355.64 1387.67 28.15 o 6 -8 2 6.61 12.52 8.59 o 7 -8 2 6.06 43.13 24.67 o -5 -7 2 171.45 158.43 30.11 o -4 -7 2 5.22 0.47 6.51 o -3 -7 2 3265.90 3171.91 45.29 o -2 -7 2 304.81 312.67 13.07 o -1 -7 2 134.99 142.82 9.71 o 0 -7 2 2576.06 2593.15 36.66 o 1 -7 2 88.78 80.55 5.85 o 2 -7 2 1027.16 1012.64 17.80 o 3 -7 2 1984.27 1950.21 26.46 o 4 -7 2 213.64 220.89 10.35 o 5 -7 2 1006.24 1014.44 23.60 o 6 -7 2 0.98 5.52 5.67 o 7 -7 2 744.72 762.33 22.96 o -6 -6 2 5.04 42.32 24.44 o -5 -6 2 1701.57 1702.90 40.31 o -4 -6 2 25.01 28.54 6.45 o -3 -6 2 141.39 126.02 8.78 o -2 -6 2 436.92 443.41 14.01 o -1 -6 2 1029.34 999.53 21.99 o 0 -6 2 548.81 564.47 16.49 o 1 -6 2 6450.20 6189.47 45.13 o 2 -6 2 1907.57 1916.67 22.67 o 3 -6 2 2311.91 2380.53 29.45 o 4 -6 2 1319.15 1366.77 25.58 o 5 -6 2 1.87 4.63 5.15 o 6 -6 2 601.21 606.10 19.53 o 7 -6 2 995.94 1017.97 26.36 o -6 -5 2 176.50 217.94 15.32 o -5 -5 2 364.25 383.67 17.48 o -4 -5 2 5.99 5.02 5.06 o -3 -5 2 105.51 124.80 8.55 o -2 -5 2 262.37 254.88 9.93 o -1 -5 2 4253.30 4263.35 37.36 o 0 -5 2 1082.73 1077.68 16.17 o 1 -5 2 0.91 1.78 2.56 o 2 -5 2 523.90 547.93 11.00 o 3 -5 2 0.45 6.65 4.18 o 4 -5 2 2115.57 1950.06 30.09 o 5 -5 2 872.29 895.43 21.66 o 6 -5 2 620.41 603.98 19.39 o 7 -5 2 1043.75 1080.92 27.11 o -7 -4 2 15.78 37.92 23.98 o -6 -4 2 40.18 37.32 8.03 o -5 -4 2 964.10 996.08 33.82 o -4 -4 2 4259.87 4227.89 50.13 o -3 -4 2 659.53 647.44 14.17 o -2 -4 2 1334.57 1371.07 20.05 o -1 -4 2 5739.44 5574.47 38.73 o 0 -4 2 102.27 113.20 4.27 o 1 -4 2 173.25 154.51 4.98 o 2 -4 2 11.66 16.72 3.20 o 3 -4 2 882.49 921.17 16.82 o 4 -4 2 272.82 263.99 11.00 o 5 -4 2 29.41 49.18 7.09 o 6 -4 2 7.00 8.62 5.92 o 7 -4 2 140.60 151.94 12.23 o -7 -3 2 16.25 15.24 8.32 o -6 -3 2 1751.50 1735.96 36.87 o -5 -3 2 817.33 818.14 19.00 o -4 -3 2 9.42 18.60 4.59 o -3 -3 2 1237.07 1299.10 17.64 o -2 -3 2 9.12 22.29 3.63 o -1 -3 2 889.64 924.38 10.61 o 0 -3 2 12184.80 11691.95 47.03 o 1 -3 2 45.59 34.56 2.17 o 2 -3 2 1089.32 1171.63 13.31 o 3 -3 2 24515.17 23948.16 109.63 o 4 -3 2 314.31 326.12 11.54 o 5 -3 2 260.61 250.01 10.57 o 6 -3 2 81.05 93.00 8.96 o 7 -3 2 0.77 -6.65 6.81 o -8 -2 2 32.82 30.68 20.45 o 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393.23 389.89 15.53 o -4 0 2 18.12 19.02 4.10 o -3 0 2 7717.32 8040.24 43.55 o -2 0 2 4219.59 4218.34 23.73 o -1 0 2 1044.12 1056.31 8.21 o 0 0 2 278.22 309.58 4.08 o 1 0 2 5626.31 5810.13 30.22 o 2 0 2 4013.38 3806.06 31.69 o 3 0 2 188.95 168.48 6.67 o 4 0 2 180.32 169.40 7.36 o 5 0 2 1111.30 1087.08 24.13 o 6 0 2 69.50 71.41 8.24 o 7 0 2 151.50 158.83 13.48 o -8 1 2 78.84 78.54 10.70 o -7 1 2 40.18 36.70 6.69 o -6 1 2 2823.65 2857.08 39.95 o -5 1 2 439.01 416.97 13.49 o -4 1 2 5.18 8.74 4.31 o -3 1 2 10704.23 11305.62 64.83 o -2 1 2 9816.15 9884.81 56.28 o -1 1 2 208.43 240.36 5.47 o 0 1 2 38.28 43.80 2.71 o 1 1 2 831.71 778.86 9.44 o 2 1 2 1924.08 1996.55 24.04 o 3 1 2 2695.11 2644.17 27.52 o 4 1 2 155.54 153.04 7.47 o 5 1 2 647.74 632.78 17.88 o 6 1 2 1380.13 1464.38 34.21 o 7 1 2 14.08 48.44 12.87 o -8 2 2 1484.39 1519.01 34.47 o -7 2 2 15.13 26.37 6.52 o -6 2 2 12.30 25.71 5.76 o -5 2 2 219.32 221.37 12.92 o -4 2 2 893.46 934.12 17.03 o -3 2 2 943.98 990.41 14.43 o -2 2 2 4386.37 4142.48 38.98 o -1 2 2 5.13 9.61 4.45 o 0 2 2 50.17 106.56 4.19 o 1 2 2 9593.66 9874.37 55.99 o 2 2 2 1363.67 1347.56 20.95 o 3 2 2 141.08 125.79 8.91 o 4 2 2 8.49 13.38 5.01 o 5 2 2 119.19 129.86 9.13 o 6 2 2 3.61 8.09 7.06 o -8 3 2 1.12 3.56 6.80 o -7 3 2 1300.18 1323.81 29.01 o -6 3 2 881.97 886.12 25.24 o -5 3 2 13.88 10.30 5.10 o -4 3 2 9438.83 9119.05 63.74 o -3 3 2 1330.06 1375.07 21.14 o -2 3 2 537.71 608.94 17.20 o -1 3 2 7362.58 7771.47 61.04 o 0 3 2 9.35 14.69 5.15 o 1 3 2 2811.90 2828.04 28.70 o 2 3 2 1129.09 1097.27 17.69 o 3 3 2 117.25 106.80 8.78 o 4 3 2 1288.88 1286.69 26.50 o 5 3 2 305.87 323.94 16.40 o 6 3 2 6.70 16.09 9.73 o -8 4 2 110.14 121.37 9.34 o -7 4 2 181.82 187.92 11.57 o -6 4 2 177.28 182.95 10.98 o -5 4 2 0.43 0.17 5.83 o -4 4 2 140.87 142.35 8.21 o -3 4 2 3509.16 3504.64 33.95 o -2 4 2 1672.42 1680.07 21.79 o -1 4 2 331.65 320.28 12.55 o 0 4 2 11521.60 11478.38 87.83 o 1 4 2 1442.59 1434.30 26.58 o 2 4 2 3.64 1.94 3.63 o 3 4 2 1136.07 1126.58 27.07 o 4 4 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6.12 o -1 7 2 4562.00 4395.67 51.61 o 0 7 2 8.60 9.15 5.30 o 1 7 2 432.86 447.43 20.73 o 2 7 2 1173.68 1194.53 34.37 o 3 7 2 91.30 91.62 12.88 o -7 8 2 47.74 56.94 9.61 o -6 8 2 328.67 334.41 17.74 o -5 8 2 88.60 71.98 8.79 o -4 8 2 532.27 500.49 19.22 o -3 8 2 117.94 127.20 10.46 o -2 8 2 1.19 4.61 5.71 o -1 8 2 72.09 81.58 8.66 o 0 8 2 383.85 415.49 19.08 o 1 8 2 278.91 330.61 17.56 o 2 8 2 71.73 73.08 11.46 o -6 9 2 11.02 15.09 8.25 o -5 9 2 495.72 518.10 20.23 o -4 9 2 12.08 8.90 6.75 o -3 9 2 76.36 84.34 10.06 o -2 9 2 45.76 40.20 7.71 o -1 9 2 147.61 149.69 12.23 o 0 9 2 485.01 505.27 21.65 o 1 9 2 170.49 141.76 18.95 o -4 10 2 98.20 96.63 12.71 o -3 10 2 75.58 50.35 9.78 o -2 10 2 25.13 28.32 10.10 o 0 -11 3 1.16 2.56 23.52 o 1 -11 3 493.77 492.00 41.27 o 2 -11 3 260.97 356.43 51.69 o 3 -11 3 2.95 7.78 17.02 o -2 -10 3 307.84 314.80 48.74 o -1 -10 3 1263.23 1269.59 38.78 o 0 -10 3 11.27 12.06 7.53 o 1 -10 3 337.03 375.40 24.91 o 2 -10 3 562.25 519.13 22.22 o 3 -10 3 0.95 -0.52 9.35 o 4 -10 3 231.49 267.34 20.20 o 5 -10 3 209.50 210.40 30.18 o -3 -9 3 737.26 713.02 72.51 o -2 -9 3 288.30 324.48 21.76 o -1 -9 3 535.75 560.35 27.62 o 0 -9 3 995.98 1057.20 31.24 o 1 -9 3 381.67 348.48 17.95 o 2 -9 3 941.29 948.63 28.72 o 3 -9 3 267.47 269.59 17.23 o 4 -9 3 15.99 12.29 7.85 o 5 -9 3 358.12 376.39 26.39 o 6 -9 3 755.23 710.49 40.39 o -4 -8 3 3.74 -5.52 19.19 o -3 -8 3 1473.63 1491.79 50.02 o -2 -8 3 21.02 22.39 7.85 o -1 -8 3 474.72 434.96 23.67 o 0 -8 3 42.39 31.94 8.34 o 1 -8 3 6.33 10.49 5.47 o 2 -8 3 1003.08 980.18 23.42 o 3 -8 3 1196.10 1178.07 29.92 o 4 -8 3 1300.73 1240.29 35.31 o 5 -8 3 177.17 206.22 17.28 o 6 -8 3 528.44 537.29 25.39 o -4 -7 3 25.14 27.44 10.13 o -3 -7 3 80.69 80.26 8.83 o -2 -7 3 746.80 741.93 17.97 o -1 -7 3 1723.69 1651.11 28.40 o 0 -7 3 446.53 405.80 13.34 o 1 -7 3 4705.69 4611.42 38.19 o 2 -7 3 36.38 37.09 4.18 o 3 -7 3 130.60 125.96 6.71 o 4 -7 3 32.99 29.76 5.03 o 5 -7 3 160.17 157.35 9.88 o 6 -7 3 258.08 258.26 14.64 o 7 -7 3 914.32 940.77 46.36 o -6 -6 3 121.97 103.36 29.69 o -5 -6 3 105.72 90.97 16.09 o -4 -6 3 564.52 571.17 20.49 o -3 -6 3 61.76 62.48 6.49 o -2 -6 3 3098.67 3080.60 33.82 o -1 -6 3 420.88 394.01 11.58 o 0 -6 3 6.73 5.54 3.46 o 1 -6 3 2768.01 2634.20 23.17 o 2 -6 3 771.84 747.08 13.10 o 3 -6 3 1232.99 1194.90 20.44 o 4 -6 3 155.97 148.70 9.05 o 5 -6 3 1392.22 1439.31 28.47 o 6 -6 3 28.47 39.21 6.73 o 7 -6 3 4.02 -0.09 6.20 o -6 -5 3 303.13 290.84 16.06 o -5 -5 3 341.03 365.62 15.78 o -4 -5 3 92.99 90.85 7.13 o -3 -5 3 3989.19 3986.27 37.98 o -2 -5 3 2166.19 2182.59 26.24 o -1 -5 3 1438.05 1457.96 16.42 o 0 -5 3 8708.36 8790.80 41.06 o 1 -5 3 768.15 729.36 9.58 o 2 -5 3 3972.48 3945.73 35.62 o 3 -5 3 1560.71 1531.38 25.11 o 4 -5 3 96.87 98.27 7.23 o 5 -5 3 1665.71 1697.24 30.89 o 6 -5 3 59.86 59.27 7.38 o 7 -5 3 65.85 50.56 9.70 o -7 -4 3 121.04 104.22 12.61 o -6 -4 3 60.22 53.63 7.65 o -5 -4 3 215.85 230.72 13.32 o -4 -4 3 454.95 440.77 13.09 o -3 -4 3 6.87 15.15 3.94 o -2 -4 3 441.46 452.58 11.08 o -1 -4 3 715.80 733.15 9.56 o 0 -4 3 4796.76 4723.70 60.77 o 1 -4 3 4073.18 4052.92 22.85 o 2 -4 3 2523.13 2629.83 22.66 o 3 -4 3 1730.65 1779.38 20.99 o 4 -4 3 2725.69 2720.11 33.80 o 5 -4 3 550.03 540.77 18.69 o 6 -4 3 359.13 361.32 15.80 o 7 -4 3 256.64 272.87 16.07 o -7 -3 3 3.42 -3.89 7.57 o -6 -3 3 954.89 926.11 26.88 o -5 -3 3 1131.49 1160.52 26.21 o -4 -3 3 123.11 123.91 6.87 o -3 -3 3 10.08 12.97 3.35 o -2 -3 3 219.82 229.53 6.61 o -1 -3 3 19.11 11.93 1.69 o 0 -3 3 1913.65 2081.41 21.57 o 1 -3 3 2136.94 2317.25 14.87 o 2 -3 3 72.35 74.74 3.67 o 3 -3 3 24.35 29.46 3.57 o 4 -3 3 1947.49 1886.03 24.08 o 5 -3 3 578.75 602.39 18.97 o 6 -3 3 0.95 4.12 6.40 o 7 -3 3 620.35 657.83 24.16 o -8 -2 3 67.51 36.84 21.41 o -7 -2 3 38.23 52.13 8.84 o -6 -2 3 86.75 101.81 9.53 o -5 -2 3 150.66 155.46 8.49 o -4 -2 3 7511.83 7325.82 56.47 o -3 -2 3 157.29 147.86 5.05 o -2 -2 3 3629.22 3869.13 22.78 o -1 -2 3 10875.87 10401.34 46.18 o 0 -2 3 118.49 136.54 3.09 o 1 -2 3 90.64 68.83 2.89 o 2 -2 3 255.12 274.88 6.94 o 3 -2 3 145.88 160.63 6.32 o 4 -2 3 632.48 670.08 15.12 o 5 -2 3 75.98 75.25 6.96 o 6 -2 3 43.85 39.34 7.51 o 7 -2 3 8.34 5.54 8.13 o -8 -1 3 6.23 8.42 9.44 o -7 -1 3 219.22 209.02 16.19 o -6 -1 3 2029.42 2003.12 40.69 o -5 -1 3 310.99 307.38 11.50 o -4 -1 3 507.51 552.12 11.57 o -3 -1 3 1459.66 1578.66 15.96 o -2 -1 3 485.74 462.33 6.95 o -1 -1 3 191.75 214.99 3.93 o 0 -1 3 32120.95 30900.02 103.81 o 1 -1 3 1661.30 1714.02 13.72 o 2 -1 3 41.27 43.20 2.68 o 3 -1 3 11125.22 10833.73 51.87 o 4 -1 3 145.93 151.35 6.53 o 5 -1 3 47.13 43.74 7.12 o 6 -1 3 68.38 70.92 8.61 o 7 -1 3 0.63 -1.25 10.29 o -8 0 3 243.97 275.38 15.43 o -7 0 3 5.21 5.25 6.98 o -6 0 3 2576.35 2536.77 36.66 o -5 0 3 8.88 20.86 4.54 o -4 0 3 159.09 183.45 9.08 o -3 0 3 1049.02 1101.36 13.64 o -2 0 3 2330.70 2220.87 18.37 o -1 0 3 344.74 400.46 5.54 o 0 0 3 491.25 460.50 5.51 o 1 0 3 21.91 10.55 2.00 o 2 0 3 536.48 554.71 12.18 o 3 0 3 154.10 161.08 6.72 o 4 0 3 4902.28 4733.39 45.02 o 5 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5298.66 5138.86 60.40 o -5 3 3 32.12 26.90 4.88 o -4 3 3 288.58 281.36 11.10 o -3 3 3 5485.78 5574.39 50.12 o -2 3 3 3221.62 3207.58 36.32 o -1 3 3 157.24 159.89 7.62 o 0 3 3 206.10 236.13 9.89 o 1 3 3 162.45 157.12 7.93 o 2 3 3 163.31 163.31 9.26 o 3 3 3 618.48 638.01 18.29 o 4 3 3 31.12 35.09 6.10 o 5 3 3 182.00 189.80 13.50 o -8 4 3 1403.99 1440.90 33.46 o -7 4 3 233.13 261.49 15.17 o -6 4 3 40.37 53.48 7.92 o -5 4 3 80.00 87.29 7.39 o -4 4 3 123.38 118.46 8.04 o -3 4 3 1731.36 1703.08 24.85 o -2 4 3 6558.01 6502.70 51.78 o -1 4 3 184.92 189.89 10.62 o 0 4 3 2219.95 2243.69 33.42 o 1 4 3 285.61 329.19 13.59 o 2 4 3 54.63 66.01 9.86 o 3 4 3 62.37 75.28 8.79 o 4 4 3 33.50 30.72 6.55 o 5 4 3 29.68 19.17 17.80 o -8 5 3 84.29 87.46 9.94 o -7 5 3 731.08 755.65 21.44 o -6 5 3 737.54 698.88 20.75 o -5 5 3 124.56 129.10 8.22 o -4 5 3 7144.06 6906.69 63.75 o -3 5 3 1313.14 1323.79 23.37 o -2 5 3 79.06 73.49 5.73 o -1 5 3 331.36 362.34 14.67 o 0 5 3 431.57 407.81 13.95 o 1 5 3 1433.13 1440.71 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