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Information card for entry 2020527
Preview
| Coordinates | 2020527.cif |
|---|---|
| Structure factors | 2020527.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis[μ~2~-<i>N</i>'-(2-oxidobenzylidene)benzohydrazidato-κ^4^<i>O</i>:<i>O</i>,<i>N</i>',<i>O</i>']dilead(II) |
|---|---|
| Formula | C28 H20 N4 O4 Pb2 |
| Calculated formula | C28 H20 N4 O4 Pb2 |
| SMILES | c12ccccc1C=[N]1N=C(O[Pb]31[O]2[Pb]12[N](=Cc4c(cccc4)[O]31)N=C(c1ccccc1)O2)c1ccccc1 |
| Title of publication | Intermolecular Pb···N interactions in lead(II) dimers producing a supramolecular two-dimensional metal‒organic compound: bis[μ~2~-<i>N</i>'-(2-oxidobenzylidene)benzohydrazidato-κ^4^<i>O</i>:<i>O</i>,<i>N</i>',<i>O</i>']dilead(II) |
| Authors of publication | Schwade, Vânia Denise; Faoro, Eliandro; Schulz Lang, Ernesto |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2016 |
| Journal volume | 72 |
| Journal issue | 7 |
| Pages of publication | 525 - 529 |
| a | 8.3754 ± 0.0007 Å |
| b | 12.6354 ± 0.001 Å |
| c | 13.6686 ± 0.0011 Å |
| α | 112.213 ± 0.003° |
| β | 101.395 ± 0.003° |
| γ | 95.781 ± 0.003° |
| Cell volume | 1287.99 ± 0.19 Å3 |
| Cell temperature | 300 ± 2 K |
| Ambient diffraction temperature | 300 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0251 |
| Residual factor for significantly intense reflections | 0.0177 |
| Weighted residual factors for significantly intense reflections | 0.0354 |
| Weighted residual factors for all reflections included in the refinement | 0.037 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.068 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 185014 (current) | 2016-08-05 | cif/ Updating files of 2020527 Original log message: Adding full bibliography for 2020527.cif. |
2020527.cif 2020527.hkl |
| 183499 | 2016-06-16 | cif/ hkl/ Adding structures of 2020527 via cif-deposit CGI script. |
2020527.cif 2020527.hkl |
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