#------------------------------------------------------------------------------
#$Date: 2019-02-02 05:33:04 +0200 (Sat, 02 Feb 2019) $
#$Revision: 213441 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/14/2021469.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2021469
_cell_angle_alpha                90.000
_cell_angle_beta                 94.402
_cell_angle_gamma                90.000
_cell_length_a                   9.5383
_cell_length_b                   17.9660
_cell_length_c                   11.3703
_exptl_crystal_F_000             856.00
_reflns_d_resolution_high        0.8403
_cod_data_source_file            lf3085150910g_sqsup4.hkl
_cod_data_source_block           150910g_sq
_shelx_title                     ' 150910g in P2(1)/n'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            258.55
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 63587.29 63349.34 547.39 o
4 0 0 23407.07 23963.49 1610.06 o
6 0 0 12192.35 10839.01 366.01 o
8 0 0 937.07 970.80 152.44 o
10 0 0 539.90 451.04 198.29 o
3 1 0 5918.77 6859.17 750.99 o
4 1 0 2034.79 1842.19 92.67 o
5 1 0 11455.68 11256.06 170.58 o
7 1 0 1598.62 1924.40 138.15 o
8 1 0 851.26 814.93 105.46 o
9 1 0 551.14 575.75 119.49 o
10 1 0 528.73 629.11 191.73 o
11 1 0 192.32 268.87 193.87 o
0 2 0 11388.58 9915.32 1422.25 o
4 2 0 710.96 561.43 60.61 o
5 2 0 6880.35 5883.04 213.85 o
7 2 0 3349.19 3693.28 233.74 o
8 2 0 203.54 95.49 114.98 o
9 2 0 2397.61 2691.40 273.39 o
10 2 0 84.40 11.61 93.21 o
11 2 0 442.43 613.86 186.29 o
1 3 0 692.36 715.08 64.94 o
2 3 0 573.84 753.14 60.88 o
3 3 0 1266.88 1687.35 109.24 o
4 3 0 3325.67 3151.88 115.55 o
5 3 0 1765.32 1622.68 102.73 o
6 3 0 2742.56 2505.39 170.58 o
7 3 0 609.86 575.07 103.14 o
8 3 0 1805.85 1758.07 167.73 o
9 3 0 109.47 108.69 110.87 o
10 3 0 1128.74 1097.78 242.29 o
11 3 0 28.87 94.78 137.09 o
0 4 0 23908.86 27970.62 2149.78 o
2 4 0 14480.87 13084.46 995.68 o
3 4 0 963.70 978.16 64.70 o
4 4 0 19226.08 18768.69 1449.40 o
6 4 0 8638.07 8417.33 482.25 o
7 4 0 1211.41 1018.35 121.87 o
8 4 0 1410.87 1197.78 135.07 o
9 4 0 556.42 381.61 108.66 o
10 4 0 191.47 228.61 112.77 o
11 4 0 266.15 270.95 153.94 o
1 5 0 39251.68 43680.63 5803.17 o
2 5 0 310.71 350.80 39.43 o
3 5 0 24626.21 27095.02 1323.41 o
4 5 0 64.39 24.27 75.18 o
5 5 0 13357.27 13372.20 1143.39 o
6 5 0 3.13 47.59 63.09 o
7 5 0 3635.65 3272.94 303.85 o
8 5 0 24.77 153.47 95.16 o
9 5 0 557.35 461.35 108.12 o
10 5 0 7.28 -18.84 105.65 o
11 5 0 45.05 112.03 108.50 o
0 6 0 28875.88 27182.59 536.22 o
1 6 0 2793.71 3069.94 263.84 o
2 6 0 26107.01 26453.52 2651.86 o
4 6 0 15595.27 16562.16 956.54 o
5 6 0 626.90 580.39 87.06 o
6 6 0 5110.86 4593.15 609.81 o
7 6 0 620.01 630.41 123.40 o
8 6 0 527.72 545.86 110.22 o
9 6 0 484.16 501.89 123.78 o
10 6 0 144.81 79.68 103.78 o
3 7 0 1901.69 1835.91 623.10 o
4 7 0 5072.05 4794.82 192.00 o
5 7 0 12.61 46.48 121.87 o
6 7 0 3482.50 3699.86 455.05 o
7 7 0 116.43 95.68 74.15 o
8 7 0 2374.47 1863.62 165.09 o
9 7 0 4.38 6.48 108.84 o
10 7 0 693.74 861.27 225.53 o
0 8 0 10362.60 9867.98 580.21 o
2 8 0 9583.47 10417.81 798.36 o
3 8 0 1529.15 1755.92 87.34 o
5 8 0 950.65 830.12 94.02 o
6 8 0 881.11 707.96 95.29 o
7 8 0 2968.22 2172.02 167.33 o
8 8 0 655.90 717.76 125.71 o
9 8 0 1115.99 1323.65 166.18 o
10 8 0 57.50 77.32 92.95 o
1 9 0 21826.07 24377.82 515.97 o
2 9 0 2963.73 3416.61 414.29 o
3 9 0 10404.54 11645.59 629.19 o
4 9 0 346.68 245.33 63.10 o
5 9 0 4161.49 3708.76 169.34 o
6 9 0 553.44 379.15 89.04 o
7 9 0 1163.46 1211.08 141.77 o
8 9 0 1111.93 914.66 122.23 o
9 9 0 345.34 272.31 93.27 o
10 9 0 302.03 331.11 185.02 o
0 10 0 17519.29 15948.44 544.60 o
1 10 0 107.70 126.76 64.40 o
2 10 0 23092.31 24387.51 1523.38 o
3 10 0 289.56 151.58 56.45 o
4 10 0 9176.79 8504.16 255.08 o
5 10 0 305.46 284.75 80.34 o
6 10 0 3544.65 3790.41 233.56 o
7 10 0 60.18 164.51 101.31 o
8 10 0 2353.62 1993.77 168.14 o
9 10 0 70.92 101.34 128.09 o
10 10 0 259.46 172.72 124.45 o
1 11 0 9890.46 9404.74 571.13 o
2 11 0 57.22 53.52 46.85 o
3 11 0 7454.14 7244.97 513.54 o
4 11 0 369.48 255.45 63.61 o
5 11 0 3671.09 3908.07 188.37 o
6 11 0 1630.45 1498.51 182.28 o
7 11 0 1779.54 1934.58 218.67 o
8 11 0 553.34 510.69 144.12 o
9 11 0 126.32 188.72 155.00 o
0 12 0 35.41 180.14 124.28 o
1 12 0 52.50 29.52 68.75 o
2 12 0 1573.47 1414.87 150.82 o
3 12 0 790.54 669.61 112.98 o
4 12 0 62.64 -15.51 88.85 o
5 12 0 1786.49 1538.81 171.12 o
6 12 0 16.63 17.82 95.28 o
7 12 0 1541.18 1590.92 210.33 o
8 12 0 29.43 47.48 99.73 o
9 12 0 899.28 783.43 180.30 o
1 13 0 2922.90 3198.42 214.47 o
2 13 0 1085.68 1279.39 233.20 o
3 13 0 1507.51 1541.51 285.57 o
4 13 0 684.30 751.39 136.85 o
5 13 0 1466.31 1223.76 229.71 o
6 13 0 1547.27 1414.33 183.80 o
7 13 0 327.68 188.38 132.67 o
8 13 0 1042.46 888.40 171.81 o
0 14 0 10567.43 12220.02 587.89 o
1 14 0 84.60 62.41 84.90 o
2 14 0 11565.62 13261.79 2024.80 o
3 14 0 706.92 571.87 122.25 o
4 14 0 7855.73 8653.41 379.47 o
5 14 0 890.01 782.35 155.33 o
6 14 0 2571.34 2348.75 518.07 o
7 14 0 605.03 422.37 130.03 o
8 14 0 865.19 635.35 159.03 o
1 15 0 10242.14 11517.70 1846.06 o
2 15 0 307.80 376.90 132.21 o
3 15 0 3985.52 3872.14 408.45 o
4 15 0 272.09 409.59 231.80 o
5 15 0 3033.11 2796.81 694.02 o
6 15 0 4.32 -52.99 105.97 o
7 15 0 1154.51 1321.89 214.35 o
8 15 0 7.09 -107.52 215.05 o
0 16 0 6321.75 5796.51 451.04 o
1 16 0 115.75 178.61 112.67 o
2 16 0 4484.94 4992.54 704.49 o
3 16 0 589.85 512.84 142.93 o
4 16 0 2202.82 1866.21 260.43 o
5 16 0 952.12 757.31 161.42 o
6 16 0 702.41 644.48 176.34 o
7 16 0 579.49 454.58 391.69 o
1 17 0 327.55 348.62 113.92 o
2 17 0 612.87 589.90 335.14 o
3 17 0 220.42 241.28 107.57 o
4 17 0 420.01 237.26 112.80 o
5 17 0 62.49 -78.20 156.40 o
6 17 0 863.36 652.70 167.64 o
0 18 0 740.76 1355.92 276.49 o
1 18 0 48.39 95.86 96.09 o
2 18 0 2357.14 2093.93 222.91 o
3 18 0 196.03 213.90 127.84 o
4 18 0 1203.00 948.51 181.52 o
5 18 0 789.03 619.92 157.39 o
6 18 0 352.74 241.45 136.79 o
1 19 0 3883.74 3857.07 309.48 o
2 19 0 270.68 184.98 113.52 o
3 19 0 5132.21 6300.91 396.98 o
4 19 0 159.21 154.61 118.08 o
5 19 0 1483.82 1841.57 245.01 o
0 20 0 3783.08 4306.54 474.78 o
1 20 0 0.60 8.23 135.31 o
2 20 0 4784.46 5871.17 1257.47 o
3 20 0 54.00 101.46 117.19 o
4 20 0 2471.72 2358.61 423.81 o
1 21 0 1317.32 1389.91 266.02 o
2 21 0 44.04 114.69 125.92 o
-11 0 1 2.97 76.80 184.33 o
-9 0 1 18.66 -33.51 199.69 o
-7 0 1 1336.47 1083.62 215.05 o
-5 0 1 4804.51 4407.42 146.35 o
1 0 1 66849.78 78817.77 798.75 o
3 0 1 10917.82 9744.17 986.10 o
5 0 1 30818.00 32169.39 1295.87 o
7 0 1 4236.28 4660.95 275.48 o
9 0 1 2353.55 2625.02 263.39 o
11 0 1 499.90 488.74 244.37 o
-11 1 1 227.39 260.54 143.15 o
-10 1 1 2.27 138.08 132.78 o
-9 1 1 862.61 966.72 179.13 o
-8 1 1 20.62 -17.43 111.31 o
-7 1 1 1576.11 1854.67 152.13 o
-6 1 1 2091.54 1813.58 104.56 o
-5 1 1 4910.65 4499.81 281.17 o
-4 1 1 1181.08 1385.11 81.23 o
-3 1 1 5035.46 5188.11 312.81 o
-1 1 1 7147.30 7707.40 608.77 o
1 1 1 5195.24 4693.34 261.69 o
3 1 1 17.12 72.41 34.47 o
4 1 1 14958.13 13572.85 744.54 o
5 1 1 105.22 132.62 55.37 o
6 1 1 7631.92 5915.48 196.23 o
7 1 1 201.82 256.30 70.85 o
8 1 1 2152.34 2344.16 161.47 o
9 1 1 240.89 228.87 85.77 o
10 1 1 1163.97 998.03 138.64 o
11 1 1 150.72 172.35 118.09 o
-11 2 1 1.43 29.14 133.01 o
-10 2 1 1423.90 1716.20 236.92 o
-9 2 1 31.47 42.40 130.56 o
-8 2 1 4484.20 4069.15 228.42 o
-7 2 1 475.99 282.00 101.06 o
-6 2 1 4605.43 4760.05 277.21 o
-5 2 1 37.31 45.63 40.50 o
-4 2 1 18426.78 18597.86 886.96 o
-2 2 1 24972.46 25666.59 680.25 o
-1 2 1 7790.83 10146.42 1289.21 o
3 2 1 1507.36 1658.01 87.00 o
4 2 1 419.33 294.65 51.40 o
5 2 1 3518.48 3110.62 129.34 o
6 2 1 1811.93 1617.86 110.40 o
7 2 1 699.71 576.81 87.34 o
8 2 1 727.75 727.35 129.95 o
9 2 1 391.33 301.30 91.58 o
10 2 1 507.68 525.67 130.50 o
11 2 1 61.30 16.70 99.37 o
-11 3 1 699.66 719.49 174.74 o
-10 3 1 11.66 113.37 156.66 o
-9 3 1 2022.13 1946.86 284.87 o
-8 3 1 0.64 -40.34 80.68 o
-7 3 1 4212.34 4632.89 309.62 o
-6 3 1 16.24 -2.08 66.31 o
-5 3 1 13293.28 13487.19 371.67 o
-4 3 1 6779.49 6518.10 408.35 o
-3 3 1 10491.56 12259.92 170.39 o
-1 3 1 9970.10 11331.20 1356.21 o
0 3 1 6704.47 8775.49 403.09 o
1 3 1 11680.10 11282.32 660.90 o
2 3 1 7420.47 7204.91 319.14 o
3 3 1 1389.26 1153.84 146.80 o
5 3 1 38.97 70.20 54.69 o
7 3 1 284.30 380.55 77.57 o
8 3 1 838.72 585.76 99.44 o
9 3 1 978.22 897.02 123.57 o
10 3 1 51.07 116.29 111.80 o
11 3 1 367.07 608.26 151.27 o
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-8 4 1 1237.35 1569.11 269.45 o
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-6 4 1 2712.70 2783.94 160.97 o
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6 4 1 23.64 64.03 64.97 o
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10 4 1 331.81 344.31 120.15 o
11 4 1 505.73 598.85 144.94 o
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-5 5 1 0.63 -17.17 34.35 o
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-3 5 1 1.41 -1.54 29.07 o
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-1 5 1 13.91 71.78 34.43 o
0 5 1 43401.21 45853.25 3278.40 o
1 5 1 445.63 411.59 58.19 o
2 5 1 27119.71 23918.93 1969.59 o
3 5 1 41.54 91.23 35.83 o
4 5 1 21420.40 19339.27 514.19 o
5 5 1 29.65 -1.17 66.87 o
6 5 1 15811.29 14995.18 898.73 o
7 5 1 3.35 12.32 60.69 o
8 5 1 2884.39 2839.53 306.28 o
9 5 1 2.36 44.47 84.33 o
10 5 1 701.53 685.67 140.21 o
-10 6 1 590.77 766.93 281.38 o
-9 6 1 29.65 -44.89 89.79 o
-8 6 1 1295.08 1146.21 132.47 o
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-6 6 1 1405.93 1644.03 129.95 o
-5 6 1 3108.54 3479.18 235.21 o
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-3 6 1 8871.28 8714.73 595.11 o
-2 6 1 2454.42 2618.54 184.22 o
-1 6 1 17321.63 19675.29 2858.85 o
0 6 1 1425.51 1502.57 159.30 o
1 6 1 23859.16 23881.20 1209.31 o
2 6 1 91.54 189.78 41.77 o
3 6 1 15661.92 17723.58 511.55 o
4 6 1 497.76 440.70 73.59 o
5 6 1 11772.50 11404.75 906.50 o
6 6 1 8.16 -4.99 57.40 o
7 6 1 3761.39 3079.49 190.66 o
8 6 1 36.14 99.40 79.22 o
9 6 1 1014.61 1171.76 143.72 o
10 6 1 108.52 46.53 110.87 o
-10 7 1 1.16 -69.60 139.21 o
-9 7 1 2420.42 2219.26 345.18 o
-8 7 1 21.46 -41.35 82.70 o
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-6 7 1 82.09 31.09 60.56 o
-5 7 1 6316.93 7200.46 312.21 o
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-3 7 1 21051.43 22083.09 906.65 o
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-1 7 1 13882.50 14355.65 303.92 o
0 7 1 1817.32 1887.52 113.78 o
1 7 1 1958.69 2040.05 102.05 o
2 7 1 37.33 79.15 42.68 o
3 7 1 357.77 219.92 63.29 o
5 7 1 532.94 550.66 80.33 o
6 7 1 641.12 571.63 95.69 o
7 7 1 720.01 500.87 97.33 o
8 7 1 87.48 20.87 76.50 o
9 7 1 328.24 361.56 112.28 o
10 7 1 24.45 34.89 95.77 o
-10 8 1 671.15 868.66 177.06 o
-9 8 1 68.36 84.73 89.96 o
-8 8 1 2608.04 2215.33 310.56 o
-7 8 1 168.20 299.83 84.57 o
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-4 8 1 4491.02 4124.67 197.52 o
-3 8 1 3557.06 3805.25 116.86 o
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0 8 1 11809.59 11453.10 587.91 o
1 8 1 13015.41 15318.59 1932.05 o
2 8 1 2029.28 2062.75 109.72 o
3 8 1 1477.37 1707.93 141.32 o
4 8 1 254.59 144.38 60.58 o
5 8 1 2176.21 1785.50 126.11 o
6 8 1 710.23 513.75 96.81 o
7 8 1 1095.11 1080.77 148.78 o
8 8 1 646.31 536.77 114.59 o
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10 8 1 231.55 263.61 122.12 o
-10 9 1 12.10 4.86 116.89 o
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1 9 1 83.52 152.62 49.70 o
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6 9 1 4260.56 3582.50 238.46 o
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8 9 1 2096.86 1777.59 163.85 o
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-10 10 1 121.17 144.97 153.18 o
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-5 10 1 1607.20 1636.63 130.02 o
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9 12 1 0.30 -19.29 106.86 o
-9 13 1 721.26 779.82 195.98 o
-8 13 1 92.13 31.15 110.94 o
-7 13 1 2529.64 2270.57 242.07 o
-6 13 1 635.43 686.43 254.85 o
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-4 13 1 581.20 673.43 106.73 o
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-1 13 1 3600.06 3613.68 304.51 o
0 13 1 2175.14 1913.58 134.87 o
1 13 1 398.86 489.91 89.33 o
2 13 1 1422.75 1791.16 170.79 o
3 13 1 1015.29 841.04 133.36 o
4 13 1 2235.10 2111.68 444.76 o
5 13 1 7.64 137.81 105.34 o
6 13 1 603.35 352.65 132.27 o
7 13 1 376.33 311.86 121.47 o
8 13 1 394.28 238.96 127.05 o
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