#------------------------------------------------------------------------------ #$Date: 2019-02-03 22:01:58 +0200 (Sun, 03 Feb 2019) $ #$Revision: 213452 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/14/2021471.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021471 loop_ _publ_author_name 'Sabbaghi, Fahimeh' 'Pourayoubi, Mehrdad' 'Ne\R-(+)-\a-methylbenzylamido]phosphate ; _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 113.623(3) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 11.3449(2) _cell_length_b 7.35270(10) _cell_length_c 11.8641(3) _cell_measurement_reflns_used 13845 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 29.6790 _cell_measurement_theta_min 3.4120 _cell_volume 906.72(4) _computing_cell_refinement ; CrysAlis PRO (Rigaku OD, 2015) ; _computing_data_collection ; Rigaku CrystalClear-SM Expert 2.1 b32 (Rigaku, 2014) MSCServDetCCD = {5.7.3.4} ; _computing_data_reduction ; CrysAlis PRO (Rigaku OD, 2015) ; _computing_molecular_graphics ; Mercury (Macrae et al., 2008) ; _computing_publication_material ; enCIFer (Allen, et al., 2004 ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 120(2) _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'AFC11 (Right): Eulerian 3 circle CCD' _diffrn_measurement_method 'Profile data from \w-scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0295 _diffrn_reflns_av_unetI/netI 0.0181 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 16344 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.349 _diffrn_reflns_theta_min 3.209 _diffrn_source 'Rotating Anode MicroMax-007HF DW 1.2 kW' _exptl_absorpt_coefficient_mu 0.170 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.83842 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis PRO; Rigaku OD, 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.294 _exptl_crystal_description block _exptl_crystal_F_000 372 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.050 _exptl_crystal_size_min 0.050 _refine_diff_density_max 0.161 _refine_diff_density_min -0.230 _refine_ls_abs_structure_details ; Flack x determined using 1454 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons et al., 2013) ; _refine_ls_abs_structure_Flack -0.01(3) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.068 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 230 _refine_ls_number_reflns 3322 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.068 _refine_ls_R_factor_all 0.0244 _refine_ls_R_factor_gt 0.0235 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0363P)^2^+0.1116P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0605 _refine_ls_wR_factor_ref 0.0612 _reflns_number_gt 3245 _reflns_number_total 3322 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ky3152sup1.cif _cod_data_source_block I _cod_database_code 2021471 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.975 _shelx_estimated_absorpt_t_max 0.992 _shelx_hkl_file ; 0 -10 -1 8.74 1.23 0 -10 -2 6.00 1.08 0 -10 -3 7.37 1.14 0 -9 0 -0.19 0.44 0 -9 1 1.33 0.69 0 -9 -1 0.03 0.52 0 -9 -1 0.52 0.65 0 -9 2 11.27 1.30 0 -9 -2 10.28 1.38 0 -9 -2 10.51 1.21 0 -9 -3 3.86 0.77 0 -9 3 2.99 0.79 0 -9 -3 2.95 0.88 0 -9 -4 1.62 0.59 0 -9 -4 1.09 0.62 0 -9 -5 2.49 0.71 0 -9 -5 2.43 0.83 0 -8 0 7.22 0.90 0 -8 0 6.92 1.13 0 -8 1 12.71 1.23 0 -8 -1 12.10 1.14 0 -8 -1 12.41 1.39 0 -8 1 13.33 1.52 0 -8 -2 16.46 1.27 0 -8 -2 16.59 1.55 0 -8 2 16.23 1.68 0 -8 2 14.60 1.28 0 -8 -3 12.95 1.16 0 -8 3 13.43 1.26 0 -8 3 13.80 1.69 0 -8 -3 13.50 1.36 0 -8 -4 5.43 0.90 0 -8 4 4.47 0.78 0 -8 -4 5.59 0.82 0 -8 -5 8.97 1.01 0 -8 -5 10.27 1.14 0 -8 5 9.92 1.16 0 -8 -6 1.14 0.52 0 -8 6 0.51 0.48 0 -8 -6 1.56 0.65 0 -8 -7 1.70 0.54 0 -7 0 0.28 0.45 0 -7 0 0.63 0.36 0 -7 1 3.01 0.61 0 -7 1 2.81 0.77 0 -7 -1 3.36 0.55 0 -7 -1 2.97 0.74 0 -7 2 17.81 1.29 0 -7 2 22.41 1.80 0 -7 -2 18.38 1.45 0 -7 -2 18.61 1.24 0 -7 -3 43.68 2.15 0 -7 3 43.13 2.04 0 -7 3 46.75 2.67 0 -7 -3 43.23 1.85 0 -7 4 7.12 1.15 0 -7 -4 8.85 1.04 0 -7 -4 5.48 0.71 0 -7 4 8.88 1.01 0 -7 5 25.96 2.14 0 -7 -5 27.40 1.49 0 -7 5 25.23 1.67 0 -7 -5 27.89 1.67 0 -7 6 17.47 1.90 0 -7 6 19.91 1.54 0 -7 -6 23.27 1.47 0 -7 -6 21.52 1.33 0 -7 -7 39.93 1.81 0 -7 -7 35.64 1.75 0 -7 7 37.39 2.18 0 -7 -8 8.85 0.91 0 -7 -8 9.35 0.94 0 -7 8 8.50 1.11 0 -6 0 105.74 3.30 0 -6 0 104.28 2.69 0 -6 -1 16.43 1.07 0 -6 -1 15.23 1.22 0 -6 1 15.07 1.30 0 -6 1 15.58 1.09 0 -6 2 29.82 1.52 0 -6 -2 30.97 1.68 0 -6 -2 29.89 1.42 0 -6 2 29.84 1.92 0 -6 -3 106.01 2.64 0 -6 3 106.28 3.67 0 -6 3 107.66 2.96 0 -6 -3 108.04 3.04 0 -6 -4 19.44 1.14 0 -6 4 19.56 1.68 0 -6 4 18.27 1.27 0 -6 5 17.86 1.31 0 -6 -5 20.17 1.15 0 -6 5 19.10 1.69 0 -6 -5 18.69 1.37 0 -6 6 3.16 0.61 0 -6 -6 4.58 0.61 0 -6 6 3.64 0.88 0 -6 -6 3.84 0.70 0 -6 7 14.67 1.64 0 -6 -7 15.09 1.04 0 -6 7 16.02 1.33 0 -6 -7 17.24 1.32 0 -6 8 12.21 1.22 0 -6 -8 12.43 1.18 0 -6 8 10.87 1.53 0 -6 -8 12.35 0.96 0 -6 9 13.85 1.37 0 -6 -9 16.35 1.06 0 -6 10 12.33 1.34 0 -5 0 0.28 0.23 0 -5 0 -0.11 0.33 0 -5 1 5.40 0.75 0 -5 1 3.99 0.51 0 -5 -1 3.81 0.48 0 -5 -1 4.52 0.59 0 -5 -2 8.82 0.68 0 -5 2 8.90 0.79 0 -5 -2 7.08 0.75 0 -5 2 8.45 0.95 0 -5 3 164.34 3.30 0 -5 -3 165.58 3.56 0 -5 3 172.28 4.21 0 -5 -3 165.03 2.93 0 -5 -4 57.96 2.11 0 -5 4 53.95 2.50 0 -5 -4 57.54 1.74 0 -5 4 56.84 2.03 0 -5 -5 174.27 3.64 0 -5 5 176.69 4.64 0 -5 -5 175.55 3.04 0 -5 5 172.44 3.66 0 -5 -6 87.55 2.19 0 -5 -6 87.32 2.62 0 -5 6 85.21 2.67 0 -5 6 88.25 3.37 0 -5 7 167.88 4.89 0 -5 -7 168.46 3.15 0 -5 7 162.48 3.86 0 -5 -7 167.87 3.62 0 -5 -8 52.83 2.10 0 -5 8 52.36 2.84 0 -5 -8 58.66 1.89 0 -5 8 49.04 2.22 0 -5 -9 7.36 0.68 0 -5 9 5.50 0.83 0 -5 -9 5.93 0.78 0 -5 9 7.57 1.29 0 -5 10 25.08 2.19 0 -5 10 25.79 1.75 0 -5 -10 22.66 1.39 0 -5 -10 26.79 1.18 0 -5 11 6.68 1.00 0 -5 -11 5.60 0.77 0 -5 12 0.71 0.56 0 -4 0 186.32 3.44 0 -4 0 181.23 2.79 0 -4 -1 83.29 2.22 0 -4 1 77.68 2.32 0 -4 -1 79.55 1.82 0 -4 1 78.90 1.91 0 -4 2 44.75 1.85 0 -4 -2 43.49 1.61 0 -4 -2 41.52 1.31 0 -4 2 42.73 1.46 0 -4 3 195.92 4.06 0 -4 -3 194.46 2.80 0 -4 3 189.90 3.22 0 -4 -3 200.35 3.43 0 -4 4 49.58 1.73 0 -4 -4 49.71 1.45 0 -4 -4 53.01 1.78 0 -4 4 54.96 2.24 0 -4 -5 9.43 0.65 0 -4 -5 8.34 0.72 0 -4 5 9.80 0.81 0 -4 5 8.70 1.00 0 -4 -6 11.65 0.76 0 -4 6 11.40 0.91 0 -4 6 12.89 1.23 0 -4 -6 13.30 0.91 0 -4 7 85.30 2.59 0 -4 -7 90.97 2.39 0 -4 7 88.68 3.30 0 -4 -8 4.75 0.59 0 -4 8 5.41 0.92 0 -4 8 5.51 0.76 0 -4 -8 5.81 0.60 0 -4 9 8.26 0.92 0 -4 -9 10.96 0.79 0 -4 9 10.50 1.32 0 -4 -9 9.80 0.83 0 -4 10 4.94 1.03 0 -4 -10 5.36 0.65 0 -4 10 4.51 0.72 0 -4 -10 5.19 0.54 0 -4 11 6.31 0.88 0 -4 11 7.42 1.24 0 -4 -11 7.55 0.74 0 -4 -11 8.75 0.69 0 -4 12 11.27 1.19 0 -4 13 1.31 0.67 0 -3 0 0.35 0.25 0 -3 0 -0.23 0.19 0 -3 1 21.44 1.09 0 -3 -1 23.01 0.84 0 -3 1 21.85 0.89 0 -3 -1 24.52 1.03 0 -3 -2 108.35 2.17 0 -3 -2 105.81 1.75 0 -3 2 105.58 2.47 0 -3 2 105.80 2.02 0 -3 3 9.92 0.67 0 -3 -3 9.95 0.56 0 -3 3 8.51 0.82 0 -3 -3 11.10 0.71 0 -3 4 53.78 2.01 0 -3 -4 53.32 1.53 0 -3 4 56.45 1.63 0 -3 -4 51.58 1.26 0 -3 -5 83.58 1.74 0 -3 -5 85.46 1.98 0 -3 5 82.85 2.65 0 -3 6 103.98 2.21 0 -3 6 105.39 3.12 0 -3 -6 102.70 2.20 0 -3 -6 103.89 2.06 0 -3 -7 25.23 1.10 0 -3 -7 24.18 1.04 0 -3 7 23.49 1.09 0 -3 7 23.82 1.61 0 -3 -8 11.98 0.78 0 -3 -8 11.77 0.79 0 -3 8 10.99 1.21 0 -3 9 32.45 2.01 0 -3 -9 32.91 1.31 0 -3 -9 32.41 1.31 0 -3 9 29.18 0.79 0 -3 10 4.27 0.34 0 -3 -10 4.01 0.54 0 -3 -10 5.21 0.54 0 -3 10 5.84 0.73 0 -3 10 4.80 0.91 0 -3 11 5.89 1.06 0 -3 -11 4.82 0.60 0 -3 11 4.25 0.72 0 -3 -11 4.02 0.49 0 -3 12 0.14 0.62 0 -3 -12 0.15 0.24 0 -3 -12 0.80 0.36 0 -3 12 0.67 0.44 0 -3 13 1.33 0.60 0 -3 13 1.96 0.84 0 -3 14 1.24 0.71 0 -2 -1 139.63 1.97 0 -2 1 134.10 2.22 0 -2 -1 138.37 1.64 0 -2 1 130.77 1.81 0 -2 -2 2.40 0.30 0 -2 -2 1.99 0.22 0 -2 -3 46.14 0.99 0 -2 3 49.69 1.20 0 -2 3 50.68 1.61 0 -2 -3 48.83 1.22 0 -2 4 103.41 1.79 0 -2 4 107.37 2.52 0 -2 -4 103.92 1.80 0 -2 4 100.97 1.08 0 -2 -4 103.59 1.66 0 -2 -5 88.41 1.69 0 -2 5 84.89 2.41 0 -2 5 86.95 1.71 0 -2 -5 87.45 1.66 0 -2 -6 59.75 1.50 0 -2 -6 60.36 1.46 0 -2 6 58.93 2.16 0 -2 6 58.85 1.04 0 -2 6 59.74 1.48 0 -2 7 32.36 0.86 0 -2 -7 34.26 1.14 0 -2 7 33.70 1.16 0 -2 -7 35.30 1.25 0 -2 7 34.75 1.77 0 -2 8 29.71 1.67 0 -2 -8 26.80 1.03 0 -2 8 26.51 1.08 0 -2 8 26.73 0.87 0 -2 -8 30.11 1.24 0 -2 9 28.15 1.72 0 -2 9 25.46 1.08 0 -2 9 23.55 0.90 0 -2 -9 25.33 1.02 0 -2 -9 26.48 1.24 0 -2 -10 20.55 1.15 0 -2 10 23.79 1.07 0 -2 10 23.47 0.96 0 -2 10 22.23 1.61 0 -2 -10 21.99 0.97 0 -2 -11 9.31 0.84 0 -2 11 9.83 0.67 0 -2 11 9.09 0.82 0 -2 11 9.65 1.15 0 -2 -11 9.70 0.65 0 -2 -12 6.55 0.76 0 -2 12 7.68 0.65 0 -2 12 6.69 0.83 0 -2 12 6.09 1.06 0 -2 -12 6.35 0.51 0 -2 13 5.88 1.10 0 -2 13 8.23 0.94 0 -2 -13 7.15 0.82 0 -2 14 3.29 0.68 0 -1 -1 146.21 1.42 0 -1 -1 141.36 1.13 0 -1 1 143.36 1.72 0 -1 1 143.49 1.37 0 -1 2 154.75 1.54 0 -1 2 157.12 2.11 0 -1 -2 153.34 1.54 0 -1 3 62.98 1.06 0 -1 -3 61.32 1.09 0 -1 3 62.62 0.75 0 -1 3 64.80 1.54 0 -1 -3 63.60 1.06 0 -1 -4 264.77 2.30 0 -1 -4 264.73 2.56 0 -1 4 258.76 1.91 0 -1 4 261.26 2.33 0 -1 5 76.44 2.06 0 -1 -5 77.38 1.59 0 -1 5 71.71 1.17 0 -1 -5 72.13 1.30 0 -1 5 73.73 1.34 0 -1 6 96.74 1.54 0 -1 -6 100.71 2.03 0 -1 6 96.20 2.44 0 -1 -6 98.07 1.60 0 -1 6 99.50 1.65 0 -1 -7 35.17 1.31 0 -1 7 35.58 1.05 0 -1 -7 34.06 1.00 0 -1 7 31.82 0.99 0 -1 7 34.58 1.58 0 -1 8 104.13 1.88 0 -1 -8 106.20 1.85 0 -1 8 101.55 1.91 0 -1 8 102.81 2.83 0 -1 -8 106.36 2.44 0 -1 -9 64.53 1.50 0 -1 -9 64.46 2.03 0 -1 9 65.24 1.56 0 -1 9 61.19 1.60 0 -1 9 64.41 2.37 0 -1 10 44.30 2.10 0 -1 10 45.18 1.33 0 -1 -10 45.61 1.27 0 -1 -10 42.90 1.78 0 -1 10 46.66 1.50 0 -1 -11 24.56 1.41 0 -1 11 24.64 0.99 0 -1 11 26.17 1.20 0 -1 -11 25.81 0.96 0 -1 11 23.21 1.59 0 -1 -12 1.44 0.45 0 -1 12 1.30 0.38 0 -1 12 1.33 0.29 0 -1 12 0.68 0.49 0 -1 -12 1.24 0.26 0 -1 13 2.94 0.84 0 -1 -13 3.64 0.70 0 -1 13 1.54 0.64 0 -1 13 2.56 0.50 0 -1 14 1.47 0.52 0 0 -2 213.30 1.88 0 0 -2 223.53 1.48 0 0 3 25.71 0.62 0 0 3 23.90 0.53 0 0 3 29.21 0.85 0 0 -3 29.59 0.86 0 0 -3 27.83 0.58 0 0 4 170.52 1.62 0 0 -4 170.41 1.66 0 0 4 167.09 1.84 0 0 4 173.45 2.39 0 0 5 167.19 1.83 0 0 5 168.45 2.09 0 0 -5 166.90 1.86 0 0 -5 174.45 2.66 0 0 5 174.27 2.68 0 0 6 13.17 0.55 0 0 -6 13.08 0.82 0 0 -6 13.24 0.57 0 0 6 12.82 0.67 0 0 6 13.65 0.84 0 0 7 13.32 0.71 0 0 -7 13.31 0.62 0 0 -7 13.80 0.91 0 0 7 14.28 0.90 0 0 7 15.20 0.63 0 0 -8 0.65 0.35 0 0 -8 0.17 0.15 0 0 8 0.22 0.20 0 0 8 0.04 0.26 0 0 8 0.11 0.12 0 0 -9 97.07 2.69 0 0 9 99.63 2.25 0 0 -9 103.17 1.88 0 0 9 98.94 1.76 0 0 9 98.47 2.71 0 0 10 92.51 1.74 0 0 10 89.09 2.29 0 0 -10 93.93 1.84 0 0 -10 87.65 2.66 0 0 10 86.68 2.68 0 0 11 55.55 2.29 0 0 -11 54.54 1.41 0 0 11 57.83 1.97 0 0 11 53.62 1.34 0 0 -11 52.91 2.20 0 0 -12 8.93 0.57 0 0 12 9.99 0.58 0 0 12 11.10 0.95 0 0 -12 11.73 1.11 0 0 12 9.18 1.07 0 0 -13 13.20 1.25 0 0 13 14.13 1.09 0 0 13 11.38 1.18 0 0 14 0.22 0.36 0 1 1 139.91 1.14 0 1 -1 145.45 1.37 0 1 1 144.33 1.42 0 1 -1 141.14 1.73 0 1 2 155.92 1.54 0 1 -2 154.92 2.09 0 1 -2 154.11 1.53 0 1 3 64.96 1.06 0 1 -3 61.63 1.07 0 1 -3 61.21 0.70 0 1 3 63.08 1.20 0 1 -3 61.95 1.50 0 1 3 61.09 1.02 0 1 -4 269.31 3.43 0 1 4 272.69 2.76 0 1 4 264.21 2.26 0 1 -4 245.37 1.77 0 1 -4 254.48 2.34 0 1 4 254.07 2.51 0 1 -5 71.33 1.36 0 1 5 69.97 1.51 0 1 5 72.98 1.28 0 1 -5 75.12 1.97 0 1 5 73.15 1.56 0 1 6 92.41 1.52 0 1 -6 93.11 1.65 0 1 6 93.85 1.91 0 1 -6 92.25 2.38 0 1 6 93.07 1.89 0 1 7 34.74 1.26 0 1 -7 35.10 1.07 0 1 7 34.77 0.99 0 1 -7 35.27 1.55 0 1 7 36.70 1.30 0 1 8 106.56 2.38 0 1 -8 104.55 2.83 0 1 8 105.67 1.78 0 1 8 101.78 2.31 0 1 -8 101.40 1.93 0 1 9 60.61 1.94 0 1 9 62.48 1.41 0 1 -9 64.26 1.61 0 1 9 62.15 1.94 0 1 -9 64.52 2.36 0 1 -10 43.40 1.38 0 1 10 41.73 1.69 0 1 10 43.78 1.74 0 1 -10 45.78 2.09 0 1 10 46.26 1.24 0 1 11 25.68 0.92 0 1 -11 27.25 1.09 0 1 -11 25.35 1.67 0 1 11 25.38 1.37 0 1 11 26.47 1.43 0 1 12 0.93 0.40 0 1 -12 1.00 0.28 0 1 12 0.59 0.17 0 1 -12 0.19 0.41 0 1 12 0.45 0.31 0 1 13 2.40 0.55 0 1 -13 2.39 0.37 0 1 -13 2.75 0.36 0 1 14 1.60 0.59 0 1 14 0.31 0.77 0 2 1 138.78 1.61 0 2 -1 139.60 1.73 0 2 -1 141.62 2.04 0 2 -1 140.06 1.87 0 2 1 137.57 1.97 0 2 2 2.44 0.29 0 2 -2 2.54 0.20 0 2 2 1.87 0.25 0 2 2 2.06 0.22 0 2 -2 1.89 0.26 0 2 -3 45.81 1.14 0 2 -3 48.60 1.55 0 2 3 46.21 0.94 0 2 3 45.93 1.20 0 2 3 48.07 1.20 0 2 4 98.45 1.88 0 2 -4 99.26 1.80 0 2 -4 105.80 2.47 0 2 4 106.58 1.79 0 2 4 103.68 1.44 0 2 -5 87.53 2.39 0 2 -5 84.72 1.71 0 2 5 85.39 1.66 0 2 5 83.87 1.44 0 2 5 88.69 1.94 0 2 6 61.05 1.44 0 2 -6 59.66 2.10 0 2 6 58.19 1.34 0 2 6 54.27 1.66 0 2 -6 56.77 1.48 0 2 7 32.39 1.07 0 2 7 34.27 1.10 0 2 7 32.36 1.36 0 2 -7 31.35 1.16 0 2 -7 33.61 1.68 0 2 -8 27.37 1.61 0 2 -8 29.30 1.18 0 2 8 26.58 1.31 0 2 8 27.79 1.06 0 2 8 29.88 1.07 0 2 9 26.57 1.12 0 2 9 23.27 1.30 0 2 -9 23.38 1.56 0 2 9 25.16 1.00 0 2 -9 27.72 1.18 0 2 -10 22.60 1.11 0 2 -10 23.44 1.62 0 2 10 21.47 1.30 0 2 10 21.30 1.05 0 2 10 22.64 0.95 0 2 -11 10.18 0.77 0 2 -11 10.10 1.15 0 2 11 9.80 0.96 0 2 11 10.88 0.66 0 2 11 10.44 0.80 0 2 -12 6.47 0.62 0 2 -12 7.31 0.67 0 2 12 6.05 0.82 0 2 12 7.29 0.52 0 2 12 7.28 0.73 0 2 13 8.24 0.97 0 2 -13 7.09 0.66 0 2 14 3.80 0.76 0 3 0 -0.11 0.17 0 3 0 0.18 0.15 0 3 -1 23.92 0.96 0 3 -1 23.05 0.95 0 3 1 23.57 0.82 0 3 1 23.54 1.01 0 3 -1 22.92 1.00 0 3 -2 101.20 1.70 0 3 2 108.89 1.92 0 3 -2 105.06 2.05 0 3 2 108.07 1.69 0 3 2 107.19 2.14 0 3 -2 107.53 2.21 0 3 3 8.95 0.49 0 3 -3 9.29 0.40 0 3 -3 8.46 0.60 0 3 3 10.95 0.69 0 3 -3 9.65 0.71 0 3 3 7.64 0.56 0 3 4 54.93 1.56 0 3 -4 52.79 1.65 0 3 4 56.05 1.24 0 3 -4 55.93 1.57 0 3 4 56.49 1.58 0 3 5 82.89 1.53 0 3 -5 83.50 1.97 0 3 5 80.70 1.91 0 3 5 79.81 2.02 0 3 6 100.77 2.15 0 3 6 102.53 2.43 0 3 -6 104.26 3.05 0 3 6 101.88 1.73 0 3 -6 96.73 2.20 0 3 7 23.51 0.88 0 3 7 23.10 1.04 0 3 7 24.35 1.25 0 3 -7 22.89 1.50 0 3 -7 21.33 1.08 0 3 -8 11.87 1.17 0 3 -8 12.15 0.85 0 3 8 12.87 0.69 0 3 8 12.10 0.77 0 3 8 14.39 1.03 0 3 -9 29.34 1.45 0 3 9 28.87 1.19 0 3 -9 32.11 1.40 0 3 9 28.39 1.53 0 3 9 32.91 1.12 0 3 -10 4.62 0.62 0 3 10 5.02 0.52 0 3 10 4.87 0.46 0 3 -10 5.20 0.63 0 3 10 4.45 0.66 0 3 11 4.39 0.73 0 3 11 4.84 0.51 0 3 -11 4.46 0.57 0 3 11 4.16 0.49 0 3 -11 4.86 0.63 0 3 -12 0.37 0.36 0 3 12 0.34 0.41 0 3 12 0.38 0.28 0 3 -12 0.32 0.31 0 3 12 0.30 0.23 0 3 13 1.77 0.56 0 4 0 186.05 3.07 0 4 0 179.97 3.26 0 4 1 81.10 1.75 0 4 -1 83.23 2.11 0 4 1 80.08 1.78 0 4 1 82.08 2.20 0 4 -1 80.21 2.21 0 4 -1 77.06 2.00 0 4 -2 40.02 1.47 0 4 2 44.03 1.28 0 4 2 43.36 1.36 0 4 2 42.23 1.57 0 4 -2 46.60 1.68 0 4 -2 41.64 1.36 0 4 3 192.80 2.61 0 4 -3 196.19 3.53 0 4 -3 182.84 3.19 0 4 3 193.44 3.35 0 4 3 188.13 3.02 0 4 -3 200.54 2.52 0 4 -4 50.75 0.87 0 4 -4 51.65 1.72 0 4 4 51.39 1.33 0 4 4 51.39 1.74 0 4 -4 53.67 1.89 0 4 4 50.76 1.68 0 4 5 9.88 0.78 0 4 -5 8.84 0.73 0 4 -5 8.64 0.79 0 4 5 9.04 0.56 0 4 5 9.92 0.78 0 4 6 11.73 0.85 0 4 6 13.14 0.68 0 4 -6 11.94 0.93 0 4 6 12.90 0.97 0 4 -6 11.19 0.87 0 4 -7 91.88 2.62 0 4 -7 91.50 2.47 0 4 7 94.13 2.66 0 4 7 94.54 1.81 0 4 7 88.96 2.32 0 4 -8 4.57 0.68 0 4 8 5.88 0.47 0 4 8 6.14 0.63 0 4 8 4.66 0.65 0 4 -8 6.11 0.69 0 4 9 9.10 0.94 0 4 9 11.71 0.67 0 4 -9 9.23 0.85 0 4 9 8.91 0.76 0 4 -9 8.16 0.88 0 4 10 4.88 0.57 0 4 10 4.88 0.74 0 4 -10 5.99 0.76 0 4 10 5.92 0.48 0 4 -10 5.90 0.73 0 4 -11 7.48 0.86 0 4 11 7.38 0.98 0 4 -11 7.86 0.84 0 4 11 6.91 0.68 0 4 11 6.85 0.51 0 4 12 13.10 1.28 0 4 -12 12.04 1.09 0 4 -12 12.18 1.08 0 5 0 0.03 0.16 0 5 0 0.13 0.21 0 5 0 -0.34 0.27 0 5 0 0.20 0.30 0 5 -1 3.90 0.55 0 5 1 4.22 0.55 0 5 1 3.50 0.57 0 5 -1 4.86 0.67 0 5 -1 4.04 0.41 0 5 -1 3.77 0.65 0 5 1 3.36 0.42 0 5 1 3.73 0.67 0 5 -2 8.44 0.79 0 5 2 7.75 0.63 0 5 2 7.58 0.65 0 5 -2 8.71 0.52 0 5 2 7.65 0.79 0 5 -2 8.20 0.83 0 5 -2 7.12 0.71 0 5 3 163.90 3.49 0 5 -3 171.83 3.70 0 5 -3 166.00 2.84 0 5 -3 163.46 3.41 0 5 3 172.75 3.18 0 5 3 165.95 2.77 0 5 -3 164.00 1.98 0 5 -4 52.99 0.95 0 5 -4 56.23 2.17 0 5 4 56.16 1.57 0 5 4 56.48 2.05 0 5 4 51.50 1.84 0 5 -4 55.19 2.00 0 5 -4 55.01 1.29 0 5 5 180.35 2.77 0 5 -5 179.41 3.66 0 5 5 177.02 3.64 0 5 -5 188.05 4.02 0 5 5 176.47 3.55 0 5 6 87.01 2.62 0 5 -6 86.48 2.77 0 5 6 88.02 2.58 0 5 -6 86.06 2.59 0 5 6 87.05 1.88 0 5 -7 168.42 3.72 0 5 7 160.65 3.49 0 5 7 160.59 3.71 0 5 7 168.31 2.57 0 5 -7 167.47 3.94 0 5 8 51.28 1.97 0 5 -8 53.55 2.28 0 5 8 53.67 1.44 0 5 8 52.98 2.26 0 5 -8 49.93 2.07 0 5 -9 7.02 0.85 0 5 -9 6.05 0.89 0 5 9 6.99 0.85 0 5 9 6.47 0.51 0 5 9 6.55 0.75 0 5 -10 24.61 1.55 0 5 10 25.90 0.93 0 5 10 26.38 1.45 0 5 10 23.72 1.66 0 5 -10 26.59 1.66 0 5 11 7.36 1.01 0 5 11 6.52 0.76 0 5 -11 7.49 0.96 0 5 -11 7.14 0.94 0 5 -12 0.12 0.48 0 5 -12 1.02 0.59 0 6 0 105.88 2.31 0 6 0 110.73 3.25 0 6 0 107.77 3.29 0 6 0 103.00 2.92 0 6 -1 15.53 0.83 0 6 1 15.94 0.97 0 6 -1 14.87 1.24 0 6 -1 15.13 1.13 0 6 1 16.82 1.37 0 6 1 18.36 1.24 0 6 1 17.12 1.28 0 6 2 26.06 1.29 0 6 -2 23.57 1.46 0 6 2 26.17 1.55 0 6 2 27.63 1.49 0 6 -2 26.87 1.04 0 6 -2 28.76 1.69 0 6 2 30.81 1.94 0 6 -2 27.41 1.53 0 6 -3 104.27 3.03 0 6 3 108.94 3.16 0 6 -3 109.44 2.62 0 6 3 104.90 2.92 0 6 3 110.79 3.78 0 6 3 104.77 2.70 0 6 -3 107.57 1.84 0 6 -3 112.36 3.34 0 6 4 19.12 1.36 0 6 4 20.13 1.06 0 6 -4 20.18 1.35 0 6 -4 20.73 1.47 0 6 -4 20.21 0.94 0 6 -4 20.27 0.69 0 6 4 19.77 1.24 0 6 -5 18.22 1.32 0 6 -5 18.14 0.51 0 6 -5 20.09 1.48 0 6 5 19.80 1.36 0 6 5 19.18 1.02 0 6 5 19.98 1.29 0 6 -6 3.73 0.72 0 6 6 3.81 0.69 0 6 6 3.78 0.47 0 6 -6 4.15 0.71 0 6 6 4.50 0.72 0 6 -7 17.08 1.39 0 6 7 17.47 1.30 0 6 7 17.73 0.93 0 6 7 16.99 1.32 0 6 -7 19.79 1.45 0 6 8 13.01 1.25 0 6 -8 11.26 1.20 0 6 -8 12.98 1.20 0 6 8 14.06 0.80 0 6 8 11.35 1.08 0 6 -9 14.46 1.34 0 6 -9 13.52 1.27 0 6 9 14.77 0.78 0 6 9 15.44 1.22 0 6 9 15.89 1.41 0 6 -10 12.73 1.23 0 6 10 11.76 1.09 0 6 -10 11.97 1.26 0 6 10 13.99 1.33 0 6 -11 17.39 1.48 0 6 -11 21.16 1.69 0 7 0 0.14 0.27 0 7 0 -0.08 0.30 0 7 0 0.51 0.46 0 7 0 0.76 0.51 0 7 1 2.65 0.49 0 7 -1 3.36 0.75 0 7 1 3.57 0.92 0 7 -1 2.14 0.53 0 7 -1 3.34 0.47 0 7 1 2.60 0.57 0 7 -1 2.78 0.73 0 7 1 2.91 0.67 0 7 -2 19.14 1.45 0 7 2 16.65 1.37 0 7 2 15.62 1.26 0 7 2 18.51 1.18 0 7 -2 18.47 1.51 0 7 2 18.05 1.65 0 7 -2 18.86 1.42 0 7 -2 16.20 0.90 0 7 -3 42.96 1.90 0 7 -3 48.32 2.28 0 7 3 43.53 2.61 0 7 -3 43.22 1.33 0 7 -3 48.77 2.42 0 7 3 45.41 2.13 0 7 3 46.36 1.96 0 7 3 43.84 2.22 0 7 4 7.39 1.25 0 7 4 7.32 0.92 0 7 4 8.19 0.88 0 7 4 7.77 0.92 0 7 -4 8.88 0.75 0 7 -4 8.86 0.53 0 7 -4 8.54 1.12 0 7 -4 7.84 0.94 0 7 5 28.66 2.36 0 7 5 27.11 1.63 0 7 -5 27.26 1.86 0 7 -5 27.90 1.79 0 7 -5 28.04 0.80 0 7 5 28.45 1.81 0 7 5 27.37 1.70 0 7 6 17.50 1.44 0 7 6 20.51 1.47 0 7 -6 23.02 1.67 0 7 6 18.32 1.39 0 7 -6 22.97 1.75 0 7 6 17.46 1.93 0 7 7 42.45 2.19 0 7 -7 37.14 2.15 0 7 -7 40.38 2.37 0 7 7 34.92 1.95 0 7 7 41.00 2.16 0 7 8 10.10 1.10 0 7 -8 10.83 1.31 0 7 -8 7.97 1.07 0 7 8 8.92 1.02 0 7 8 8.76 1.07 0 7 9 4.18 0.75 0 7 9 3.65 0.75 0 7 -9 5.99 1.00 0 7 10 15.47 1.37 0 7 -10 17.00 1.60 0 7 -11 1.81 0.78 0 8 0 6.16 0.68 0 8 0 7.35 1.09 0 8 0 7.20 1.04 0 8 0 6.22 1.07 0 8 -1 13.02 0.96 0 8 1 12.68 1.35 0 8 -1 11.99 1.29 0 8 1 10.65 1.47 0 8 1 11.68 1.00 0 8 -1 11.05 1.38 0 8 -1 15.54 1.52 0 8 1 12.04 1.26 0 8 2 15.63 1.50 0 8 -2 17.02 1.01 0 8 2 16.56 1.24 0 8 2 17.12 1.49 0 8 -2 15.08 1.52 0 8 -2 14.24 1.35 0 8 -2 14.95 1.39 0 8 2 15.95 1.70 0 8 3 14.98 1.20 0 8 -3 14.89 1.23 0 8 3 11.80 1.66 0 8 3 12.85 1.27 0 8 -3 15.77 1.60 0 8 -3 15.12 0.86 0 8 3 14.44 1.47 0 8 -4 5.51 0.66 0 8 -4 3.35 0.84 0 8 4 4.70 0.82 0 8 4 5.78 0.82 0 8 4 5.97 1.31 0 8 -4 5.66 0.48 0 8 4 4.29 0.85 0 8 5 10.17 1.11 0 8 -5 9.59 1.30 0 8 -5 10.01 0.53 0 8 5 8.54 1.05 0 8 5 11.30 1.30 0 8 6 0.33 0.46 0 8 -6 1.01 0.68 0 8 6 1.27 0.53 0 8 7 1.65 0.72 0 8 7 2.29 0.80 0 8 -7 1.21 0.67 0 8 8 4.18 0.92 0 8 -8 3.87 0.95 0 8 9 8.92 1.24 0 9 0 -0.09 0.38 0 9 0 0.38 0.59 0 9 0 1.02 0.87 0 9 1 1.34 0.65 0 9 1 1.54 0.92 0 9 1 0.18 0.35 0 9 -1 0.35 0.33 0 9 -1 0.97 0.82 0 9 -1 0.70 0.66 0 9 2 11.86 1.45 0 9 -2 10.68 1.33 0 9 2 10.43 1.63 0 9 2 12.86 1.19 0 9 -2 12.57 1.56 0 9 -2 10.47 0.88 0 9 3 2.52 0.88 0 9 3 3.23 0.73 0 9 -3 3.15 0.50 0 9 4 1.22 0.64 0 9 4 1.17 0.63 0 10 0 46.89 2.19 0 10 1 8.60 1.04 0 10 2 4.87 0.94 1 -10 -3 1.98 0.78 -1 -10 0 18.00 1.65 -1 -10 -1 12.23 1.42 -1 -10 -2 10.98 1.28 1 -9 -6 17.57 1.52 1 -9 -5 11.51 1.39 1 -9 -5 10.69 1.19 1 -9 -4 5.07 0.86 1 -9 -4 6.65 1.18 -1 -9 4 6.24 1.02 1 -9 -3 20.38 1.89 -1 -9 3 18.02 1.64 1 -9 -3 19.74 1.60 1 -9 -2 26.70 2.19 -1 -9 2 31.04 2.00 1 -9 -2 32.95 2.02 -1 -9 1 57.18 2.63 1 -9 -1 56.87 2.66 -1 -9 0 28.43 2.28 -1 -9 0 29.44 1.91 1 -9 0 26.37 1.87 -1 -9 -1 1.12 0.83 1 -9 1 1.93 0.74 -1 -9 -1 0.85 0.52 -1 -9 -2 -0.03 0.61 1 -9 2 0.17 0.47 -1 -9 -2 0.37 0.48 -1 -9 -3 4.68 0.82 -1 -9 -3 4.34 0.91 1 -9 3 5.32 0.99 -1 -9 -4 1.91 0.68 -1 -9 -4 2.40 0.86 1 -8 -7 5.42 0.85 1 -8 -7 4.82 0.84 1 -8 -6 0.97 0.55 1 -8 -6 1.14 0.54 -1 -8 6 1.31 0.53 -1 -8 5 1.23 0.58 1 -8 -5 0.38 0.51 1 -8 -5 1.14 0.47 -1 -8 4 2.59 0.88 -1 -8 4 2.88 0.67 1 -8 -4 4.08 0.92 1 -8 -4 1.75 0.55 1 -8 -3 1.58 0.51 1 -8 -3 2.05 0.72 -1 -8 3 0.57 0.70 -1 -8 3 1.76 0.56 -1 -8 2 29.61 1.78 1 -8 -2 28.98 2.07 1 -8 -2 29.29 1.75 -1 -8 2 28.39 2.18 1 -8 -1 10.23 1.31 -1 -8 1 12.05 1.44 1 -8 -1 10.49 1.10 -1 -8 1 11.38 1.11 1 -8 0 18.70 1.47 -1 -8 0 14.91 1.23 -1 -8 0 15.47 1.57 1 -8 0 16.45 1.67 -1 -8 -1 34.08 1.79 -1 -8 -1 35.83 2.24 1 -8 1 32.94 1.96 1 -8 1 32.02 2.38 1 -8 2 54.83 3.09 -1 -8 -2 52.70 2.62 -1 -8 -2 51.70 2.18 1 -8 2 51.73 2.47 -1 -8 -3 24.21 1.51 -1 -8 -3 25.66 1.81 1 -8 3 24.85 1.75 -1 -8 -4 10.38 1.14 -1 -8 -4 9.76 0.97 1 -8 4 9.36 1.15 -1 -8 -5 2.44 0.67 1 -8 5 3.25 0.83 -1 -8 -5 2.92 0.61 -1 -8 -6 4.28 0.78 -1 -8 -6 5.14 0.75 -1 -7 9 7.47 1.06 1 -7 -9 8.17 1.12 1 -7 -9 7.45 0.95 1 -7 -8 6.09 0.86 -1 -7 8 4.96 0.89 1 -7 -7 19.53 1.40 1 -7 -7 19.78 1.64 -1 -7 7 19.76 1.60 -1 -7 6 16.70 1.41 1 -7 -6 16.53 1.46 1 -7 -6 15.45 1.23 -1 -7 5 4.13 0.98 1 -7 -5 3.33 0.75 -1 -7 5 4.35 0.76 1 -7 -5 4.17 0.70 -1 -7 4 16.69 1.31 1 -7 -4 21.35 1.36 1 -7 -4 21.64 1.62 -1 -7 4 18.62 1.76 1 -7 -3 16.34 1.23 -1 -7 3 16.48 1.26 -1 -7 3 16.53 1.62 -1 -7 2 20.95 1.39 1 -7 -2 25.59 1.73 1 -7 -2 19.97 1.32 -1 -7 2 21.32 1.69 -1 -7 1 44.73 1.94 1 -7 -1 47.29 2.03 -1 -7 1 47.36 2.48 1 -7 -1 48.37 2.48 1 -7 0 36.28 2.20 -1 -7 0 34.38 2.03 -1 -7 0 30.85 1.61 1 -7 0 33.35 1.74 -1 -7 -1 2.60 0.72 1 -7 1 2.50 0.60 -1 -7 -1 3.38 0.57 1 -7 1 3.07 0.81 -1 -7 -2 4.43 0.78 1 -7 2 2.18 0.56 1 -7 2 3.86 0.91 -1 -7 -2 2.92 0.53 -1 -7 -3 14.89 1.24 1 -7 3 13.47 1.48 1 -7 3 12.38 1.17 -1 -7 -3 12.84 1.01 1 -7 4 13.55 1.57 1 -7 4 10.90 1.10 -1 -7 -4 12.50 0.95 -1 -7 -4 11.90 1.08 1 -7 5 17.52 1.45 1 -7 5 16.24 1.81 -1 -7 -5 15.91 1.07 -1 -7 -5 15.70 1.18 1 -7 6 25.38 1.76 -1 -7 -6 25.76 1.43 -1 -7 -6 24.90 1.34 -1 -7 -7 19.20 1.15 1 -7 7 17.86 1.55 -1 -7 -7 16.93 1.09 1 -7 8 21.03 1.71 1 -6 -11 4.59 0.91 1 -6 -10 15.50 1.20 1 -6 -10 14.47 1.31 -1 -6 10 13.61 1.35 1 -6 -9 9.35 1.05 1 -6 -9 8.92 0.91 -1 -6 9 9.32 1.12 1 -6 -8 37.97 1.84 -1 -6 8 38.24 2.65 -1 -6 8 36.79 2.04 1 -6 -8 40.53 2.07 -1 -6 7 20.58 1.88 -1 -6 7 21.35 1.51 1 -6 -7 20.61 1.49 1 -6 -7 19.84 1.33 -1 -6 6 1.77 0.51 1 -6 -6 2.17 0.46 1 -6 -6 2.96 0.65 -1 -6 6 1.83 0.74 1 -6 -5 2.62 0.49 -1 -6 5 4.18 0.87 -1 -6 5 3.12 0.59 1 -6 -5 2.80 0.61 1 -6 -4 6.24 0.80 1 -6 -4 7.58 0.76 -1 -6 4 5.88 0.76 -1 -6 4 7.42 1.05 1 -6 -3 -0.18 0.38 -1 -6 3 -0.46 0.45 -1 -6 3 -0.08 0.30 1 -6 -3 0.00 0.28 -1 -6 2 10.89 0.92 1 -6 -2 12.09 1.09 -1 -6 2 11.54 1.20 1 -6 -2 11.96 0.95 1 -6 -1 15.17 1.07 -1 -6 1 16.13 1.33 -1 -6 1 16.24 1.07 -1 -6 0 10.38 1.08 1 -6 0 12.90 1.22 -1 -6 0 11.00 0.88 1 -6 0 10.48 0.90 1 -6 1 2.88 0.68 -1 -6 -1 2.18 0.48 1 -6 1 2.85 0.54 -1 -6 -1 2.40 0.46 1 -6 2 150.35 4.23 -1 -6 -2 150.89 3.55 -1 -6 -2 148.02 3.00 1 -6 2 147.64 3.44 -1 -6 -3 79.71 2.49 -1 -6 -3 76.26 2.12 1 -6 3 79.94 2.60 1 -6 3 80.45 3.22 -1 -6 -4 18.40 1.04 1 -6 4 21.17 1.76 -1 -6 -4 20.20 1.24 1 -6 4 18.93 1.33 -1 -6 -5 9.87 0.84 1 -6 5 9.52 1.29 -1 -6 -5 10.39 0.79 1 -6 5 8.21 0.91 1 -6 6 11.10 1.41 1 -6 6 11.27 1.09 -1 -6 -6 9.79 0.80 -1 -6 -6 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15.79 0.51 1 1 13 0.52 0.38 1 1 13 0.19 0.73 1 1 14 1.55 0.53 -1 2 15 0.98 0.55 -1 2 14 3.23 0.72 -1 2 13 23.53 1.58 1 2 -13 22.36 1.28 1 2 -13 21.88 1.83 -1 2 13 19.86 1.01 -1 2 13 19.82 1.26 -1 2 12 17.72 0.99 1 2 -12 18.30 1.13 -1 2 12 19.78 1.22 -1 2 12 18.59 1.36 1 2 -12 17.61 1.63 1 2 -11 8.61 0.79 -1 2 11 7.27 0.73 -1 2 11 7.27 0.83 1 2 -11 8.86 1.11 -1 2 11 7.95 0.67 1 2 -10 57.80 1.86 -1 2 10 56.72 2.06 -1 2 10 53.31 1.81 1 2 -10 53.50 2.47 -1 2 10 53.85 1.68 1 2 -9 93.47 2.30 -1 2 9 94.19 2.55 -1 2 9 96.19 2.14 -1 2 9 90.14 2.24 1 2 -9 91.35 3.03 1 2 -8 30.77 1.28 1 2 -8 33.23 1.76 -1 2 8 31.74 1.39 -1 2 8 31.03 1.23 -1 2 8 30.50 1.19 -1 2 7 31.19 1.16 1 2 -7 35.08 1.73 -1 2 7 33.23 1.33 1 2 -7 33.19 1.25 1 2 -7 30.90 0.85 -1 2 7 32.55 1.18 1 2 -6 153.95 3.40 -1 2 6 152.47 2.65 1 2 -6 150.18 2.51 1 2 -6 151.19 1.68 -1 2 6 148.14 2.35 -1 2 6 149.77 2.44 1 2 -5 29.16 1.06 -1 2 5 30.30 0.98 1 2 -5 28.32 0.66 -1 2 5 30.00 1.08 -1 2 5 30.05 1.10 1 2 -5 30.03 1.44 1 2 -4 169.05 1.59 1 2 -4 173.08 3.17 1 2 -4 163.10 2.39 -1 2 4 162.83 2.15 -1 2 4 170.78 2.45 -1 2 4 173.22 2.45 -1 2 3 235.09 2.79 1 2 -3 218.31 3.32 1 2 -3 235.50 2.08 -1 2 3 222.79 2.37 -1 2 3 225.27 2.56 1 2 -3 229.41 2.68 -1 2 1 88.73 1.66 -1 2 1 89.38 1.46 1 2 -1 85.98 1.65 -1 2 1 90.70 1.29 1 2 -1 87.87 1.54 1 2 -1 89.18 1.76 -1 2 0 71.75 1.35 -1 2 0 71.50 1.00 1 2 0 73.14 1.34 1 2 0 69.78 1.43 1 2 0 72.66 1.68 1 2 1 410.87 3.06 1 2 1 394.08 3.27 -1 2 -1 399.84 3.43 -1 2 -1 408.16 3.34 1 2 2 300.01 1.84 -1 2 -2 293.01 2.99 -1 2 -2 292.80 2.80 1 2 2 294.93 2.80 1 2 3 96.80 1.58 -1 2 -3 98.43 1.75 1 2 3 97.90 1.01 1 2 4 12.59 0.39 -1 2 -4 12.86 0.68 -1 2 -4 11.70 0.60 1 2 4 13.31 0.60 1 2 5 114.10 1.34 1 2 5 113.31 1.73 1 2 5 119.76 2.29 -1 2 -5 117.53 2.07 -1 2 -5 112.79 1.90 -1 2 -6 232.97 2.97 1 2 6 225.55 3.34 -1 2 -6 226.74 2.79 1 2 6 221.95 2.15 1 2 6 228.63 2.50 -1 2 -7 55.80 1.49 1 2 7 52.63 1.22 1 2 7 52.00 1.16 -1 2 -7 53.12 1.41 1 2 7 53.69 1.76 -1 2 -8 25.06 1.03 1 2 8 25.17 0.90 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2.02 1 3 -7 62.22 2.47 -1 3 7 65.16 1.62 1 3 -7 61.02 1.85 1 3 -6 59.92 2.30 1 3 -6 55.45 0.89 -1 3 6 55.19 1.45 -1 3 6 54.20 1.74 1 3 -6 57.90 1.73 -1 3 6 56.96 1.71 1 3 -5 56.64 2.16 -1 3 5 58.37 1.71 -1 3 5 59.03 1.43 -1 3 5 57.32 1.66 1 3 -5 55.65 1.64 1 3 -5 53.20 0.90 -1 3 4 199.56 2.93 -1 3 4 202.69 3.12 1 3 -4 209.12 2.10 1 3 -4 198.72 2.98 -1 3 4 204.87 2.61 1 3 -3 650.06 5.22 -1 3 3 646.33 5.48 1 3 -3 658.94 4.49 1 3 -3 638.21 6.40 -1 3 3 654.66 4.65 -1 3 3 630.09 4.82 -1 3 2 96.11 1.74 -1 3 2 93.59 2.07 -1 3 2 95.39 1.79 1 3 -2 93.51 1.92 1 3 -2 97.63 1.98 1 3 -2 97.84 2.34 -1 3 1 183.53 2.86 1 3 -1 189.39 2.92 -1 3 1 187.80 2.23 1 3 -1 180.22 2.63 -1 3 1 186.03 2.51 1 3 0 157.57 2.94 -1 3 0 158.35 1.82 1 3 0 152.92 2.37 -1 3 0 148.25 2.34 1 3 0 150.28 2.53 -1 3 0 150.25 2.62 1 3 1 38.40 1.53 -1 3 -1 37.40 0.77 1 3 1 36.28 1.15 1 3 1 36.00 1.22 -1 3 -1 38.41 1.22 -1 3 -1 38.48 1.31 -1 3 -2 30.28 0.78 1 3 2 32.18 0.83 1 3 2 33.66 1.17 -1 3 -2 27.63 0.52 -1 3 -2 31.23 1.13 -1 3 -2 34.85 1.25 1 3 3 0.65 0.23 1 3 3 0.56 0.13 -1 3 -3 0.72 0.23 -1 3 -3 0.35 0.19 1 3 4 12.09 0.47 -1 3 -4 11.08 0.70 1 3 4 11.87 0.70 -1 3 -4 10.98 0.75 1 3 5 20.52 0.61 1 3 5 19.05 0.89 -1 3 -5 18.72 0.99 1 3 5 19.62 1.04 -1 3 -5 19.64 0.93 -1 3 -6 186.11 2.95 1 3 6 184.88 1.85 1 3 6 181.92 3.35 1 3 6 192.33 2.78 -1 3 -6 191.57 3.19 1 3 7 30.02 0.78 1 3 7 30.02 1.10 -1 3 -7 31.61 1.34 -1 3 -7 32.29 1.28 -1 3 -8 148.09 2.80 1 3 8 149.01 1.79 1 3 8 152.57 2.47 -1 3 -8 145.46 2.89 -1 3 -9 94.74 2.31 1 3 9 90.98 1.43 1 3 9 90.49 1.89 1 3 9 90.78 2.73 -1 3 -9 92.35 2.32 -1 3 -10 2.47 0.45 -1 3 -10 2.45 0.42 1 3 10 2.58 0.61 1 3 10 2.31 0.26 1 3 10 2.42 0.33 -1 3 -11 20.00 1.10 1 3 11 16.63 0.62 1 3 11 18.98 1.39 -1 3 -11 19.50 1.10 1 3 11 18.28 0.73 -1 3 -12 8.71 0.74 -1 3 -12 8.17 0.73 1 3 12 7.67 1.00 1 3 13 3.27 0.75 1 4 -13 9.48 1.06 -1 4 13 9.42 1.12 1 4 -13 9.12 1.04 -1 4 12 16.40 0.93 -1 4 12 14.72 1.33 1 4 -12 14.97 1.23 1 4 -12 15.34 1.31 -1 4 12 14.38 1.04 1 4 -11 4.47 0.72 -1 4 11 5.32 0.56 1 4 -11 5.31 0.74 -1 4 11 4.89 0.63 -1 4 11 5.16 0.82 -1 4 10 9.11 0.84 -1 4 10 10.99 0.76 -1 4 10 8.81 0.96 1 4 -10 9.96 1.03 1 4 -10 9.12 0.93 1 4 -9 43.62 2.42 -1 4 9 45.04 1.98 -1 4 9 43.06 1.45 1 4 -9 40.84 1.79 -1 4 9 40.76 1.68 1 4 -8 59.10 2.10 -1 4 8 58.07 1.98 -1 4 8 60.96 1.68 1 4 -8 59.54 2.71 -1 4 8 61.84 2.21 1 4 -7 34.07 1.57 -1 4 7 36.64 1.60 -1 4 7 37.74 1.30 1 4 -7 36.63 2.06 -1 4 7 34.89 1.52 -1 4 6 22.50 0.99 1 4 -6 19.78 0.50 -1 4 6 20.89 1.17 1 4 -6 22.24 1.53 1 4 -6 20.57 1.18 -1 4 5 55.87 1.87 -1 4 5 56.51 1.82 -1 4 5 56.54 1.54 1 4 -5 51.96 1.78 1 4 -5 55.95 1.07 1 4 -4 87.65 2.47 -1 4 4 85.17 2.09 1 4 -4 84.12 2.20 1 4 -4 86.95 1.68 -1 4 4 87.41 1.92 -1 4 4 85.31 2.30 1 4 -3 40.92 1.34 -1 4 3 42.10 1.34 1 4 -3 41.47 1.66 -1 4 3 39.26 1.55 -1 4 3 40.90 1.38 1 4 -3 40.69 1.50 -1 4 2 339.40 3.78 1 4 -2 344.73 4.36 1 4 -2 332.97 4.22 -1 4 2 338.54 3.67 -1 4 2 334.21 4.48 1 4 -2 344.74 4.65 1 4 -1 48.17 1.71 1 4 -1 48.76 1.75 -1 4 1 48.52 1.30 -1 4 1 49.94 1.51 1 4 -1 51.77 1.63 -1 4 1 47.87 1.70 -1 4 0 51.64 1.79 -1 4 0 50.86 1.56 -1 4 0 50.06 1.22 1 4 0 51.39 1.74 1 4 0 53.81 1.96 1 4 0 51.24 1.61 -1 4 -1 309.96 4.32 -1 4 -1 311.93 2.68 1 4 1 301.78 4.86 1 4 1 298.96 4.13 1 4 1 298.25 3.82 1 4 2 425.07 4.94 -1 4 -2 441.49 5.23 -1 4 -2 438.70 2.77 -1 4 -2 432.45 4.80 -1 4 -2 419.12 3.84 1 4 2 449.25 6.14 1 4 2 426.09 4.51 -1 4 -3 222.24 3.72 -1 4 -3 201.67 3.35 1 4 3 228.15 3.56 -1 4 -3 208.88 1.98 1 4 3 224.16 2.53 -1 4 -4 100.59 2.39 1 4 4 103.04 2.45 1 4 4 102.77 1.65 -1 4 -4 103.60 2.58 1 4 4 98.58 2.34 -1 4 -5 103.82 2.48 -1 4 -5 108.45 2.70 1 4 5 108.79 2.46 1 4 5 109.80 1.66 1 4 5 109.63 2.66 -1 4 -6 151.11 3.04 1 4 6 151.97 2.91 1 4 6 159.39 1.92 -1 4 -6 159.22 3.29 1 4 6 154.99 3.31 1 4 7 49.42 1.97 1 4 7 53.07 1.07 -1 4 -7 51.66 1.84 -1 4 -7 53.80 1.94 1 4 7 52.68 1.71 -1 4 -8 3.78 0.59 1 4 8 5.00 0.32 1 4 8 5.27 0.72 -1 4 -8 5.51 0.67 1 4 8 4.64 0.53 1 4 9 10.04 0.75 1 4 9 9.65 0.98 1 4 9 9.87 0.41 -1 4 -9 10.72 0.94 -1 4 -9 9.64 0.85 1 4 10 1.38 0.13 1 4 10 2.53 0.59 1 4 10 1.48 0.91 -1 4 -10 2.95 0.57 1 4 10 2.58 0.41 -1 4 -10 2.58 0.54 1 4 11 4.71 0.47 1 4 11 5.01 0.52 -1 4 -11 5.13 0.69 1 4 11 5.32 0.85 -1 4 -11 4.60 0.67 1 4 12 2.95 0.72 1 5 -12 16.58 1.45 1 5 -12 17.54 1.47 -1 5 12 17.36 1.24 -1 5 11 0.45 0.28 1 5 -11 0.19 0.45 -1 5 11 -0.21 0.38 1 5 -11 0.28 0.53 -1 5 11 0.23 0.48 -1 5 10 10.45 1.12 -1 5 10 12.84 1.05 -1 5 10 10.84 0.76 1 5 -10 9.90 1.04 1 5 -10 11.28 1.12 1 5 -9 20.37 1.46 -1 5 9 17.99 1.24 -1 5 9 18.97 0.98 -1 5 9 16.79 1.33 1 5 -9 17.58 1.30 -1 5 8 15.07 0.88 1 5 -8 14.81 1.18 1 5 -8 15.04 1.25 -1 5 8 15.51 1.12 -1 5 8 13.13 1.12 -1 5 7 5.92 0.56 -1 5 7 5.83 0.71 1 5 -7 5.91 0.82 1 5 -7 4.84 0.68 -1 5 7 7.18 0.81 -1 5 6 24.48 1.12 1 5 -6 24.13 1.52 1 5 -6 23.96 1.40 1 5 -6 20.54 0.54 -1 5 6 22.04 1.31 -1 5 6 22.00 1.34 -1 5 5 12.40 0.92 -1 5 5 12.27 1.00 1 5 -5 13.99 1.15 -1 5 5 12.57 0.80 1 5 -5 11.18 0.94 1 5 -5 13.32 0.64 -1 5 4 152.08 2.78 1 5 -4 151.07 3.32 -1 5 4 150.53 3.03 1 5 -4 147.69 3.58 -1 5 4 148.24 3.40 1 5 -4 154.89 2.66 1 5 -3 156.34 3.30 -1 5 3 154.36 2.92 1 5 -3 159.73 3.07 -1 5 3 155.43 3.44 -1 5 3 158.14 2.90 1 5 -3 159.13 3.61 1 5 -2 5.47 0.71 -1 5 2 4.33 0.60 -1 5 2 4.53 0.52 1 5 -2 4.44 0.64 -1 5 2 5.10 0.52 1 5 -2 4.75 0.61 1 5 -1 7.57 0.84 1 5 -1 7.57 0.73 1 5 -1 7.63 0.80 -1 5 1 8.59 0.83 -1 5 1 6.70 0.62 -1 5 1 6.90 0.56 1 5 0 12.19 0.91 1 5 0 12.00 0.98 1 5 0 11.03 1.02 -1 5 0 11.61 0.68 -1 5 -1 1.87 0.41 1 5 1 1.51 0.54 1 5 1 1.47 0.38 -1 5 -1 0.96 0.19 -1 5 -1 1.27 0.41 1 5 1 1.82 0.42 -1 5 -1 1.26 0.41 -1 5 -2 11.15 0.96 1 5 2 11.70 0.95 1 5 2 11.37 1.15 1 5 2 12.61 0.90 -1 5 -2 9.60 0.74 -1 5 -2 12.81 0.96 -1 5 -2 12.64 0.58 1 5 3 9.78 1.10 1 5 3 9.56 0.86 -1 5 -3 8.82 0.83 -1 5 -3 10.25 0.93 -1 5 -3 8.85 0.40 1 5 3 9.48 0.80 -1 5 -3 8.25 0.57 1 5 3 10.44 0.81 1 5 4 13.62 0.94 1 5 4 14.87 1.04 1 5 4 12.95 1.32 -1 5 -4 13.45 1.01 1 5 4 14.83 1.05 -1 5 -4 14.83 1.13 1 5 5 11.74 1.36 1 5 5 11.17 0.93 -1 5 -5 11.10 0.92 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1.38 1 6 -6 1.15 0.16 -1 6 6 1.70 0.37 -1 6 6 2.10 0.51 -1 6 6 1.42 0.44 1 6 -6 2.06 0.57 1 6 -6 1.69 0.19 1 6 -6 1.39 0.49 -1 6 5 3.33 0.64 1 6 -5 3.75 0.76 -1 6 5 2.67 0.52 -1 6 5 2.44 0.41 1 6 -5 3.24 0.31 1 6 -5 2.59 0.38 1 6 -5 3.00 0.54 -1 6 4 7.05 0.86 1 6 -4 6.03 0.82 -1 6 4 6.23 0.71 1 6 -4 6.96 0.70 1 6 -4 6.44 0.78 -1 6 4 6.65 0.68 1 6 -3 -0.05 0.30 -1 6 3 0.51 0.35 1 6 -3 0.40 0.32 1 6 -3 0.45 0.40 -1 6 3 0.42 0.30 -1 6 3 -0.14 0.26 -1 6 2 11.18 0.83 -1 6 2 11.61 1.07 1 6 -2 9.50 1.00 1 6 -2 10.53 0.99 -1 6 2 9.46 0.81 1 6 -2 11.20 1.11 -1 6 1 14.38 1.20 1 6 -1 14.16 1.26 1 6 -1 14.60 1.18 1 6 -1 15.55 1.17 -1 6 1 15.17 0.89 -1 6 1 13.60 1.08 1 6 0 11.12 1.03 -1 6 0 10.94 1.04 -1 6 0 10.78 0.71 -1 6 0 9.89 1.00 1 6 0 10.55 0.97 1 6 0 9.95 1.11 -1 6 -1 2.07 0.54 1 6 1 2.21 0.68 1 6 1 1.99 0.48 -1 6 -1 1.34 0.49 1 6 1 1.71 0.48 -1 6 -1 2.23 0.34 1 6 1 2.49 0.44 -1 6 -1 2.43 0.52 -1 6 -2 146.06 3.21 1 6 2 145.17 3.64 1 6 2 152.30 3.48 -1 6 -2 157.44 3.92 1 6 2 156.14 3.23 -1 6 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0.96 1 7 -8 6.68 1.00 1 7 -8 6.40 1.05 -1 7 8 7.83 0.74 -1 7 8 8.41 1.07 -1 7 7 17.82 1.44 1 7 -7 18.20 1.65 -1 7 7 19.32 1.17 -1 7 7 18.88 1.48 1 7 -7 18.11 1.53 1 7 -6 15.23 0.58 -1 7 6 17.59 1.46 -1 7 6 15.78 1.27 -1 7 6 15.39 1.08 1 7 -6 17.77 1.54 1 7 -6 16.07 1.39 -1 7 5 3.16 0.64 1 7 -5 4.07 0.51 1 7 -5 3.90 0.74 -1 7 5 3.56 0.56 1 7 -5 3.00 0.34 -1 7 5 3.27 0.74 1 7 -5 3.45 0.77 1 7 -4 16.77 1.37 1 7 -4 21.97 1.30 1 7 -4 20.96 0.91 -1 7 4 21.80 1.28 -1 7 4 21.89 1.60 -1 7 4 21.25 1.36 1 7 -4 21.49 1.69 -1 7 3 16.50 1.38 1 7 -3 16.95 1.33 1 7 -3 16.78 0.91 1 7 -3 19.25 1.56 -1 7 3 17.13 1.34 1 7 -3 16.93 1.30 -1 7 3 18.15 1.18 -1 7 2 21.50 1.25 -1 7 2 20.87 1.45 1 7 -2 17.79 1.37 1 7 -2 20.85 1.55 1 7 -2 23.02 1.14 -1 7 2 20.66 1.61 -1 7 2 20.22 1.67 1 7 -2 21.46 1.60 1 7 -1 44.46 2.39 -1 7 1 48.68 2.39 -1 7 1 45.47 1.68 1 7 -1 46.16 1.69 1 7 -1 47.15 2.17 1 7 -1 46.99 2.36 -1 7 1 46.57 2.16 -1 7 1 44.75 2.42 1 7 0 30.58 1.90 -1 7 0 29.98 1.87 1 7 0 33.71 1.51 -1 7 0 29.37 1.74 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1.58 1 7 8 20.24 1.52 1 7 9 26.72 1.74 -1 7 -9 27.55 2.03 -1 7 -10 1.61 0.79 -1 8 8 21.42 1.81 1 8 -8 21.64 1.99 -1 8 7 5.70 0.97 1 8 -7 7.79 1.25 -1 8 7 6.49 0.98 -1 8 6 1.17 0.57 1 8 -6 1.35 0.68 -1 8 6 1.64 0.65 -1 8 5 1.73 0.65 1 8 -5 0.68 0.60 -1 8 5 1.75 1.03 1 8 -5 0.88 0.26 -1 8 5 0.44 0.45 1 8 -5 0.97 0.36 1 8 -4 2.93 0.80 1 8 -4 3.01 0.62 -1 8 4 5.34 0.88 1 8 -4 3.28 0.43 -1 8 4 3.11 0.74 -1 8 4 4.13 1.10 -1 8 4 2.92 0.60 -1 8 3 1.94 0.56 -1 8 3 2.16 0.66 1 8 -3 1.34 0.66 -1 8 3 0.76 0.67 1 8 -3 2.01 0.61 1 8 -3 1.84 0.42 -1 8 3 1.66 0.69 1 8 -2 29.29 1.37 1 8 -2 33.20 2.22 -1 8 2 31.45 2.06 -1 8 2 26.61 1.83 1 8 -2 32.03 2.06 -1 8 2 28.85 2.20 -1 8 2 29.92 1.59 -1 8 1 10.95 0.94 -1 8 1 13.23 1.40 1 8 -1 13.77 1.38 1 8 -1 12.44 1.37 1 8 -1 12.21 0.96 -1 8 1 11.68 1.41 1 8 -1 12.47 1.40 -1 8 1 11.61 1.24 1 8 0 15.85 1.64 -1 8 0 15.97 1.06 -1 8 0 17.18 1.48 1 8 0 15.09 1.44 -1 8 0 17.15 1.58 -1 8 0 15.27 1.50 1 8 0 13.52 1.32 1 8 0 16.23 1.14 1 8 1 32.73 1.99 1 8 1 38.17 2.25 1 8 1 31.01 2.35 -1 8 -1 35.03 1.45 1 8 1 36.68 1.78 -1 8 -1 29.68 2.01 -1 8 -1 33.77 2.21 -1 8 -1 34.92 2.09 1 8 2 53.74 2.24 1 8 2 53.70 2.70 -1 8 -2 56.35 2.83 -1 8 -2 51.45 1.62 -1 8 -2 52.75 2.65 1 8 2 49.74 2.44 1 8 2 47.21 2.98 -1 8 -2 55.12 2.42 1 8 3 24.09 1.72 1 8 3 25.05 2.29 -1 8 -3 26.17 1.04 1 8 3 28.13 1.71 1 8 3 24.50 1.80 -1 8 -3 25.73 1.98 -1 8 -3 26.71 1.45 1 8 4 9.76 1.21 1 8 4 9.32 1.50 -1 8 -4 9.01 1.19 1 8 4 8.60 1.08 1 8 4 10.87 1.12 -1 8 -4 10.66 0.68 -1 8 -4 9.93 0.52 1 8 5 1.49 0.58 1 8 5 1.71 0.57 -1 8 -5 3.19 0.81 1 8 5 2.57 0.67 1 8 6 6.02 1.01 -1 8 -6 5.04 1.09 1 8 6 4.34 0.81 1 8 6 4.29 0.83 -1 8 -7 4.27 0.99 1 8 7 4.94 0.95 1 8 8 3.80 0.84 -1 8 -8 4.50 1.07 -1 9 5 13.05 1.35 -1 9 4 7.33 0.98 -1 9 4 8.02 1.21 -1 9 3 16.91 1.38 -1 9 3 21.53 2.22 1 9 -3 17.19 1.08 -1 9 3 18.41 1.79 1 9 -3 16.32 1.50 -1 9 2 26.96 2.36 1 9 -2 29.45 1.52 -1 9 2 30.97 1.72 1 9 -2 31.62 2.36 -1 9 2 31.63 2.32 1 9 -2 26.66 2.04 -1 9 1 55.28 3.17 -1 9 1 61.76 2.30 1 9 -1 60.80 3.19 1 9 -1 64.63 2.29 1 9 -1 52.84 3.07 -1 9 1 62.65 3.22 -1 9 0 27.08 1.48 1 9 0 28.70 2.36 1 9 0 32.17 2.37 -1 9 0 32.55 2.36 -1 9 0 28.24 2.23 1 9 0 29.14 1.67 1 9 1 1.21 0.53 -1 9 -1 1.06 0.43 -1 9 -1 1.24 0.70 -1 9 -1 1.13 0.75 1 9 1 1.08 0.69 1 9 1 0.65 0.81 1 9 2 0.22 0.42 1 9 2 0.44 0.66 -1 9 -2 0.66 0.34 -1 9 -2 1.53 0.90 1 9 3 4.51 0.98 1 9 3 4.95 0.85 1 9 4 2.58 0.82 1 9 4 2.77 0.76 1 9 5 9.37 1.35 -1 10 3 2.07 0.71 -1 10 2 1.10 0.57 -1 10 1 11.79 1.13 1 10 0 17.97 1.46 1 10 1 13.48 1.29 1 10 2 11.39 1.24 -2 -10 0 3.18 0.89 -2 -10 -1 5.70 0.96 2 -9 -7 0.68 0.64 2 -9 -6 3.05 0.83 2 -9 -5 7.77 1.30 2 -9 -5 6.78 1.07 2 -9 -4 6.39 1.01 -2 -9 4 5.19 0.92 -2 -9 3 14.94 1.41 2 -9 -3 14.17 1.41 -2 -9 2 12.92 1.30 2 -9 -2 13.78 1.39 -2 -9 1 34.53 2.49 2 -9 -1 33.56 2.12 -2 -9 1 31.54 1.98 2 -9 0 18.47 1.64 -2 -9 0 18.51 1.80 -2 -9 0 18.72 1.50 2 -9 1 15.68 1.52 -2 -9 -1 17.35 1.40 -2 -9 -1 14.07 1.52 -2 -9 -2 2.30 0.73 -2 -9 -2 3.75 0.78 -2 -9 -3 2.15 0.80 -2 -9 -3 0.94 0.43 2 -8 -8 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1.58 0.59 -2 -7 6 1.62 0.87 2 -7 -6 0.66 0.41 -2 -7 5 5.83 0.88 -2 -7 5 7.43 1.21 2 -7 -5 4.87 0.84 2 -7 -5 5.78 0.77 2 -7 -4 9.43 0.98 2 -7 -4 9.94 1.13 -2 -7 4 10.91 1.38 -2 -7 4 9.65 1.00 2 -7 -3 21.68 1.64 -2 -7 3 21.81 1.44 2 -7 -3 20.16 1.40 -2 -7 3 22.24 1.82 2 -7 -2 26.01 1.77 -2 -7 2 24.79 1.83 -2 -7 2 23.27 1.41 2 -7 -2 23.77 1.49 -2 -7 1 2.67 0.68 -2 -7 1 2.78 0.53 2 -7 -1 3.50 0.76 2 -7 -1 2.79 0.56 2 -7 0 18.69 1.66 -2 -7 0 18.55 1.21 2 -7 0 16.76 1.28 -2 -7 0 15.44 1.33 2 -7 1 22.34 1.51 -2 -7 -1 23.23 1.32 -2 -7 -1 23.50 1.60 2 -7 1 25.27 1.98 -2 -7 -2 31.54 1.49 -2 -7 -2 31.25 1.77 2 -7 2 31.24 1.82 2 -7 2 33.39 2.29 2 -7 3 14.74 1.60 2 -7 3 14.15 1.24 -2 -7 -3 14.16 1.15 -2 -7 -3 14.27 0.99 -2 -7 -4 23.41 1.42 -2 -7 -4 24.28 1.25 2 -7 4 25.21 1.70 -2 -7 -5 13.68 0.95 2 -7 5 14.83 1.34 -2 -7 -5 14.68 1.05 2 -7 5 14.58 1.72 -2 -7 -6 2.35 0.47 -2 -7 -6 2.57 0.45 2 -7 6 2.17 0.54 2 -7 7 0.47 0.50 -2 -7 -7 0.12 0.21 2 -6 -11 18.62 1.51 2 -6 -11 14.52 1.37 -2 -6 11 15.78 1.54 -2 -6 10 10.10 1.19 2 -6 -10 10.68 1.20 2 -6 -10 13.73 1.25 -2 -6 9 41.35 2.23 2 -6 -9 41.95 2.05 2 -6 -9 39.70 2.11 -2 -6 8 5.13 0.84 2 -6 -8 6.84 0.96 2 -6 -8 5.27 0.75 -2 -6 8 7.21 1.28 2 -6 -7 30.96 1.69 -2 -6 7 30.51 1.81 2 -6 -7 28.72 1.79 -2 -6 7 34.08 2.37 -2 -6 6 51.77 2.24 2 -6 -6 51.04 2.32 2 -6 -6 51.96 2.10 -2 -6 6 49.14 2.73 -2 -6 5 73.05 3.16 2 -6 -5 72.44 2.73 -2 -6 5 74.26 2.56 2 -6 -5 72.23 2.44 -2 -6 4 84.99 3.35 -2 -6 4 86.12 2.67 2 -6 -4 86.84 2.63 -2 -6 3 25.44 1.40 2 -6 -3 23.73 1.55 -2 -6 3 26.07 1.77 2 -6 -3 23.68 1.39 2 -6 -2 15.12 1.25 2 -6 -2 15.87 1.13 -2 -6 2 13.79 0.99 -2 -6 2 13.62 1.26 -2 -6 1 40.99 1.67 2 -6 -1 47.52 2.20 -2 -6 1 45.95 2.15 2 -6 -1 46.18 1.91 -2 -6 0 40.06 1.60 -2 -6 0 45.02 2.06 2 -6 0 39.53 1.78 -2 -6 -1 11.52 1.02 2 -6 1 13.81 1.32 2 -6 1 13.78 1.09 -2 -6 -1 13.95 0.92 2 -6 2 42.26 2.33 -2 -6 -2 39.24 1.77 -2 -6 -2 39.60 1.49 2 -6 2 35.30 1.74 -2 -6 -3 22.64 1.28 2 -6 3 20.76 1.37 -2 -6 -3 21.57 1.07 2 -6 3 22.05 1.75 -2 -6 -4 71.60 1.90 2 -6 4 72.31 2.60 -2 -6 -4 70.80 2.11 2 -6 4 68.58 3.11 2 -6 5 68.21 3.25 2 -6 5 63.28 2.51 -2 -6 -5 69.85 1.94 -2 -6 -5 64.89 1.74 -2 -6 -6 143.01 2.46 -2 -6 -6 149.20 2.53 2 -6 6 147.89 3.98 2 -6 6 152.03 4.97 -2 -6 -7 0.96 0.19 2 -6 7 0.82 0.62 2 -6 7 0.26 0.40 2 -6 8 4.72 0.88 2 -6 9 5.84 0.98 2 -5 -12 16.31 1.36 2 -5 -12 19.11 1.42 -2 -5 12 16.79 1.55 -2 -5 11 7.54 1.02 2 -5 -11 8.26 0.98 2 -5 -11 7.54 0.93 -2 -5 10 4.79 1.06 2 -5 -10 3.85 0.75 2 -5 -10 3.04 0.64 -2 -5 9 1.30 0.60 2 -5 -9 1.18 0.43 2 -5 -9 1.33 0.46 -2 -5 8 71.78 3.31 2 -5 -8 81.23 2.61 2 -5 -8 75.95 2.63 2 -5 -7 58.21 2.29 2 -5 -7 58.78 2.14 -2 -5 7 61.06 2.93 2 -5 -6 0.40 0.33 -2 -5 6 0.65 0.56 2 -5 -6 1.30 0.40 -2 -5 5 31.02 1.92 -2 -5 5 30.80 1.55 2 -5 -5 31.89 1.65 2 -5 -5 30.60 1.45 2 -5 -4 96.46 2.80 -2 -5 4 99.54 3.28 2 -5 -4 96.51 2.52 -2 -5 4 89.54 2.49 2 -5 -3 50.10 1.81 -2 -5 3 50.84 1.80 -2 -5 3 53.65 2.29 2 -5 -3 52.22 2.07 2 -5 -2 96.72 2.48 -2 -5 2 94.41 2.34 -2 -5 2 93.03 2.89 2 -5 -2 91.12 2.71 2 -5 -1 60.27 2.19 2 -5 -1 59.24 1.96 -2 -5 1 54.05 1.72 -2 -5 1 56.14 2.16 2 -5 0 33.96 1.50 2 -5 0 33.07 1.62 -2 -5 0 34.03 1.30 -2 -5 0 32.35 1.57 2 -5 1 47.51 1.81 -2 -5 -1 49.92 1.51 -2 -5 -1 49.37 1.82 2 -5 1 54.18 2.09 2 -5 2 104.53 3.30 2 -5 2 102.22 2.68 -2 -5 -2 99.37 2.07 -2 -5 -2 97.80 2.43 2 -5 3 15.21 1.33 -2 -5 -3 14.08 0.88 -2 -5 -3 15.31 0.78 2 -5 3 16.31 1.10 2 -5 4 19.83 1.26 -2 -5 -4 21.81 1.00 -2 -5 -4 21.27 0.88 2 -5 4 20.36 1.58 -2 -5 -5 44.34 1.22 -2 -5 -5 46.64 1.31 2 -5 5 45.67 1.96 -2 -5 -6 20.62 0.76 2 -5 6 23.50 1.82 2 -5 6 23.08 1.46 -2 -5 -6 22.87 0.79 2 -5 7 5.77 0.98 2 -5 7 5.77 0.80 2 -5 8 2.06 0.54 2 -5 8 1.82 0.73 2 -5 9 17.96 1.82 2 -5 9 18.11 1.45 2 -5 10 29.85 1.93 2 -5 11 19.11 1.64 2 -4 -13 10.90 1.13 2 -4 -13 10.09 1.05 -2 -4 12 9.99 1.00 2 -4 -12 11.40 1.12 2 -4 -12 10.00 1.01 2 -4 -11 14.53 1.16 2 -4 -11 16.43 1.25 -2 -4 11 13.88 1.12 -2 -4 11 14.38 1.57 2 -4 -10 25.79 1.48 -2 -4 10 24.09 1.42 2 -4 -10 26.74 1.59 -2 -4 10 23.19 1.91 2 -4 -9 62.37 2.22 -2 -4 9 57.56 2.83 -2 -4 9 57.55 2.12 2 -4 -9 64.26 2.33 2 -4 -8 5.18 0.67 2 -4 -8 3.93 0.60 -2 -4 8 3.94 0.58 -2 -4 8 3.35 0.39 -2 -4 8 4.43 0.86 2 -4 -7 44.95 1.82 -2 -4 7 39.74 1.29 -2 -4 7 45.43 2.36 2 -4 -7 45.15 1.84 -2 -4 7 43.55 1.77 2 -4 -6 33.74 1.56 -2 -4 6 30.03 1.17 -2 -4 6 32.11 1.88 -2 -4 6 33.22 1.51 2 -4 -6 32.73 1.44 2 -4 -5 18.46 1.07 -2 -4 5 17.59 0.98 -2 -4 5 18.62 1.10 2 -4 -5 19.65 1.18 -2 -4 5 20.17 1.46 -2 -4 4 46.16 1.68 -2 -4 4 45.54 2.07 -2 -4 4 47.59 1.59 2 -4 -4 49.98 1.66 -2 -4 3 10.45 0.96 -2 -4 3 7.64 0.69 2 -4 -3 8.62 0.71 -2 -4 3 9.83 0.77 2 -4 -3 9.30 0.79 -2 -4 2 74.01 1.85 2 -4 -2 75.34 2.21 2 -4 -2 78.81 2.05 -2 -4 2 74.47 2.32 -2 -4 1 155.16 2.54 -2 -4 1 163.32 3.22 2 -4 -1 166.65 2.93 2 -4 -1 162.57 3.19 -2 -4 0 183.52 2.62 -2 -4 0 185.06 3.22 2 -4 0 185.21 3.39 -2 -4 -1 65.29 1.80 -2 -4 -1 63.83 1.47 2 -4 1 64.93 1.91 2 -4 1 63.76 2.01 2 -4 2 88.01 2.73 -2 -4 -2 87.95 1.92 -2 -4 -2 91.06 1.67 -2 -4 -3 138.49 1.93 -2 -4 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170.75 3.09 2 2 2 18.00 1.08 -2 2 -2 16.64 0.76 2 2 2 16.23 0.64 2 2 2 15.77 0.60 -2 2 -2 15.92 0.72 -2 2 -3 171.65 2.17 -2 2 -3 175.54 2.33 2 2 3 172.56 2.04 2 2 3 177.63 3.57 2 2 3 174.19 1.91 -2 2 -4 16.51 0.73 2 2 4 16.37 0.61 2 2 4 14.65 1.17 2 2 4 16.24 0.57 -2 2 -4 15.47 0.68 2 2 5 62.30 1.08 -2 2 -5 59.54 1.39 2 2 5 59.22 2.33 -2 2 -5 57.42 1.31 2 2 5 60.56 1.13 -2 2 -6 0.46 0.18 2 2 6 0.38 0.07 2 2 6 -0.05 0.34 2 2 6 0.57 0.24 2 2 6 0.32 0.06 2 2 6 0.60 0.14 -2 2 -6 0.41 0.17 2 2 6 0.52 0.12 2 2 7 43.38 0.76 2 2 7 44.57 2.29 2 2 7 45.23 0.85 -2 2 -7 48.29 1.28 -2 2 -7 47.49 1.24 2 2 7 50.04 1.76 2 2 7 44.74 0.90 2 2 8 88.89 1.08 2 2 8 87.60 1.10 2 2 8 89.92 1.26 -2 2 -8 99.15 1.83 -2 2 -8 97.29 1.83 2 2 8 85.35 3.35 2 2 8 89.20 1.16 2 2 8 97.15 2.53 2 2 9 30.98 2.07 2 2 9 27.79 0.76 -2 2 -9 30.48 1.01 2 2 9 27.65 0.70 -2 2 -9 31.21 1.02 2 2 9 31.51 1.51 -2 2 -10 4.30 0.38 2 2 10 3.34 0.27 2 2 10 4.54 0.66 -2 2 -10 3.53 0.34 2 2 10 3.84 0.31 2 2 11 1.63 0.20 -2 2 -11 1.42 0.20 2 2 11 1.17 0.47 2 2 11 0.98 0.72 2 2 11 1.50 0.22 -2 2 -11 1.40 0.19 2 2 12 1.10 0.89 2 2 12 1.25 0.54 2 2 13 3.61 0.80 -2 3 14 1.15 0.56 2 3 -14 1.53 0.86 -2 3 13 4.30 0.65 -2 3 13 5.77 0.73 2 3 -13 6.15 1.09 -2 3 13 5.89 0.91 2 3 -13 4.83 0.74 2 3 -12 24.86 2.00 -2 3 12 25.06 1.35 2 3 -12 26.09 1.53 -2 3 12 25.10 1.36 -2 3 12 24.41 1.62 -2 3 11 5.85 0.69 -2 3 11 6.40 0.81 -2 3 11 6.40 0.70 2 3 -11 7.13 1.12 2 3 -11 6.07 0.74 -2 3 10 7.97 0.75 2 3 -10 6.75 0.99 2 3 -10 6.76 0.76 -2 3 10 6.82 0.71 -2 3 10 4.95 0.70 2 3 -10 5.68 0.44 2 3 -9 1.95 0.25 -2 3 9 2.36 0.44 -2 3 9 1.47 0.36 2 3 -9 2.92 0.65 -2 3 9 2.45 0.41 2 3 -9 2.30 0.44 2 3 -8 25.89 0.83 -2 3 8 28.20 1.41 2 3 -8 26.99 1.73 -2 3 8 29.38 1.34 2 3 -8 28.07 1.37 -2 3 8 28.61 1.24 2 3 -7 86.11 1.45 2 3 -7 81.39 2.23 -2 3 7 87.53 2.31 2 3 -7 86.29 2.91 -2 3 7 84.18 2.06 -2 3 7 78.87 2.16 2 3 -6 4.43 0.52 2 3 -6 4.50 0.70 2 3 -6 4.48 0.34 -2 3 6 4.46 0.54 -2 3 6 4.28 0.51 -2 3 6 3.47 0.42 2 3 -5 4.13 0.37 2 3 -5 3.56 0.45 -2 3 5 3.72 0.47 -2 3 5 3.97 0.47 2 3 -5 4.08 0.65 -2 3 5 3.51 0.45 2 3 -4 161.67 2.79 2 3 -4 169.59 3.52 -2 3 4 169.81 2.60 -2 3 4 170.11 2.99 -2 3 4 171.04 2.70 2 3 -3 21.02 0.96 -2 3 3 22.02 1.06 -2 3 3 21.72 0.91 2 3 -3 20.79 1.14 -2 3 3 23.17 0.97 2 3 -3 20.66 0.97 2 3 -2 48.61 1.43 -2 3 2 45.35 1.51 -2 3 2 48.23 1.40 2 3 -2 45.88 1.60 2 3 -2 46.20 1.52 -2 3 2 46.39 1.22 -2 3 1 270.57 3.56 2 3 -1 277.09 4.02 -2 3 1 270.19 2.67 2 3 -1 265.85 3.54 2 3 -1 272.93 3.27 -2 3 1 278.62 3.35 -2 3 0 12.17 0.71 -2 3 0 13.24 0.79 2 3 0 14.28 0.81 -2 3 0 12.72 0.54 2 3 0 12.53 0.71 2 3 0 14.43 1.00 -2 3 -1 45.68 1.44 2 3 1 44.99 1.85 2 3 1 44.75 1.27 2 3 1 43.38 1.34 -2 3 -1 44.92 0.85 2 3 2 32.26 1.06 -2 3 -2 32.57 1.22 -2 3 -2 32.73 1.24 2 3 2 32.17 1.64 -2 3 -2 31.50 0.61 2 3 2 32.96 1.17 -2 3 -3 44.71 1.45 -2 3 -3 49.82 1.45 2 3 3 48.13 1.38 2 3 3 49.74 2.10 2 3 3 46.85 1.26 2 3 4 0.49 0.39 -2 3 -4 0.11 0.19 2 3 4 0.34 0.18 2 3 4 0.29 0.17 -2 3 -4 0.20 0.19 -2 3 -5 43.00 1.44 2 3 5 39.81 1.22 2 3 5 41.48 1.17 2 3 5 43.65 2.17 -2 3 -5 40.67 1.35 -2 3 -6 1.12 0.28 2 3 6 1.21 0.45 2 3 6 2.23 0.30 2 3 6 1.77 0.27 2 3 6 1.64 0.39 -2 3 -6 2.10 0.33 -2 3 -7 10.81 0.72 -2 3 -7 11.11 0.76 2 3 7 9.97 0.88 2 3 7 10.71 1.30 2 3 7 11.46 0.63 2 3 7 11.28 0.59 2 3 8 53.10 1.22 -2 3 -8 51.71 1.63 2 3 8 54.97 1.31 2 3 8 49.43 1.96 -2 3 -8 53.55 1.62 2 3 9 3.29 0.87 2 3 9 4.58 0.36 -2 3 -9 5.18 0.54 -2 3 -9 4.96 0.55 2 3 9 5.29 0.70 2 3 9 4.83 0.35 2 3 10 5.69 0.30 2 3 10 7.43 0.87 -2 3 -10 6.27 0.60 -2 3 -10 6.13 0.57 2 3 11 13.49 1.19 -2 3 -11 14.23 0.83 -2 3 -11 13.87 0.83 2 3 12 15.20 1.40 2 3 13 9.05 1.12 2 4 -13 10.36 1.16 -2 4 13 9.63 0.94 -2 4 13 9.66 1.18 -2 4 12 9.30 0.83 2 4 -12 9.40 1.02 -2 4 12 10.63 0.99 2 4 -12 11.71 1.55 -2 4 12 10.65 1.19 2 4 -11 14.08 1.62 2 4 -11 15.11 1.24 -2 4 11 13.48 1.21 -2 4 11 13.30 0.98 -2 4 11 13.42 1.06 -2 4 10 23.41 1.20 -2 4 10 25.99 1.42 -2 4 10 22.41 1.50 2 4 -10 24.70 1.96 2 4 -10 24.42 1.48 -2 4 9 60.08 2.29 2 4 -9 55.17 2.77 -2 4 9 53.86 2.01 2 4 -9 57.99 2.18 -2 4 9 60.06 1.87 2 4 -8 3.33 0.54 2 4 -8 3.79 0.77 -2 4 8 4.23 0.59 2 4 -8 3.08 0.27 -2 4 8 3.06 0.45 -2 4 8 3.30 0.54 2 4 -7 48.91 2.39 -2 4 7 47.49 1.83 -2 4 7 48.41 1.60 2 4 -7 44.10 1.01 2 4 -7 44.28 1.82 -2 4 7 43.53 1.76 -2 4 6 33.70 1.34 2 4 -6 31.69 1.49 -2 4 6 32.83 1.52 -2 4 6 33.33 1.47 2 4 -6 34.52 1.00 2 4 -5 18.82 1.11 2 4 -5 17.93 1.36 -2 4 5 17.47 0.95 -2 4 5 17.57 1.10 -2 4 5 17.60 1.01 2 4 -5 18.94 0.85 2 4 -4 48.40 1.54 -2 4 4 47.18 1.55 2 4 -4 46.53 2.03 -2 4 4 47.40 1.76 2 4 -4 42.28 1.62 -2 4 4 45.73 1.53 -2 4 3 7.94 0.66 2 4 -3 8.83 0.74 2 4 -3 10.04 0.93 -2 4 3 8.93 0.65 -2 4 3 9.37 0.80 2 4 -3 10.54 0.80 2 4 -2 79.92 2.29 2 4 -2 73.87 2.21 -2 4 2 74.73 1.94 -2 4 2 76.46 2.20 -2 4 2 76.54 1.75 2 4 -2 70.12 1.98 2 4 -1 151.87 2.82 -2 4 1 152.74 2.32 2 4 -1 158.22 3.11 -2 4 1 160.07 2.83 2 4 -1 162.64 3.43 -2 4 0 184.64 3.37 -2 4 0 193.26 2.33 2 4 0 183.12 3.29 -2 4 0 183.83 3.11 2 4 0 188.61 3.08 2 4 0 185.13 3.91 -2 4 -1 63.77 1.87 -2 4 -1 62.53 1.99 2 4 1 64.27 1.78 2 4 1 64.66 1.92 -2 4 -1 68.23 1.25 2 4 2 87.20 2.06 2 4 2 86.06 2.20 -2 4 -2 84.79 2.31 2 4 2 88.03 2.95 -2 4 -2 87.58 1.19 -2 4 -3 138.77 2.97 -2 4 -3 136.63 2.78 2 4 3 132.11 2.69 2 4 3 137.34 2.56 2 4 3 132.93 3.78 2 4 4 189.36 2.96 -2 4 -4 189.75 3.30 2 4 4 189.75 3.18 -2 4 -4 188.16 3.44 -2 4 -5 147.15 3.06 2 4 5 150.49 2.81 2 4 5 146.65 2.60 -2 4 -5 144.20 2.89 -2 4 -6 173.01 3.39 2 4 6 179.15 3.62 -2 4 -6 172.99 3.23 2 4 6 166.81 2.75 2 4 6 178.18 3.01 2 4 6 175.59 4.91 2 4 7 5.69 0.72 2 4 7 5.08 0.94 -2 4 -7 5.82 0.65 2 4 7 6.24 0.60 -2 4 -7 6.38 0.67 2 4 7 5.83 0.52 2 4 8 35.70 1.24 2 4 8 33.75 2.42 -2 4 -8 36.30 1.59 2 4 8 33.46 1.27 -2 4 -8 35.75 1.53 2 4 8 33.24 1.75 2 4 9 13.68 1.80 2 4 9 13.88 0.77 2 4 9 13.79 1.19 2 4 9 13.15 0.78 -2 4 -9 15.10 1.08 -2 4 -9 14.29 1.00 -2 4 -10 0.38 0.32 2 4 10 0.51 0.47 2 4 10 0.66 0.21 2 4 10 1.48 0.30 -2 4 -10 0.55 0.35 2 4 10 -0.53 0.83 -2 4 -11 1.65 0.43 -2 4 -11 1.58 0.45 2 4 11 1.38 0.60 2 5 -13 14.74 1.46 2 5 -12 16.24 1.43 2 5 -12 17.48 1.55 -2 5 12 16.71 1.27 -2 5 12 16.21 1.52 2 5 -11 7.86 1.00 2 5 -11 8.39 1.11 -2 5 11 8.55 0.77 -2 5 11 7.91 0.90 -2 5 11 7.38 1.02 2 5 -10 2.77 0.71 -2 5 10 2.77 0.48 -2 5 10 3.17 0.61 2 5 -10 3.17 0.68 -2 5 10 2.83 0.69 2 5 -9 1.82 0.54 -2 5 9 1.57 0.38 -2 5 9 1.63 0.51 -2 5 9 1.56 0.47 2 5 -8 75.55 2.62 -2 5 8 72.40 2.52 -2 5 8 77.62 2.18 -2 5 8 75.68 2.62 2 5 -7 54.17 2.18 -2 5 7 54.54 2.09 -2 5 7 58.72 1.88 -2 5 7 56.87 2.21 2 5 -7 55.05 1.14 -2 5 6 0.87 0.35 2 5 -6 0.78 0.22 -2 5 6 0.98 0.39 2 5 -6 1.15 0.43 -2 5 6 0.98 0.34 2 5 -5 31.54 1.72 -2 5 5 32.79 1.64 -2 5 5 29.24 1.31 2 5 -5 32.56 1.26 -2 5 5 28.94 1.41 2 5 -5 28.15 1.48 -2 5 4 95.80 2.37 2 5 -4 90.56 2.59 2 5 -4 94.93 2.41 2 5 -4 97.57 2.93 -2 5 4 91.92 2.35 -2 5 4 95.43 2.77 -2 5 3 53.94 2.09 -2 5 3 51.58 1.75 2 5 -3 48.60 1.88 -2 5 3 49.92 1.65 2 5 -3 51.05 1.92 2 5 -3 55.18 2.18 -2 5 2 94.48 2.72 2 5 -2 90.72 2.48 2 5 -2 94.89 2.78 2 5 -2 92.90 2.77 -2 5 2 96.13 2.40 -2 5 2 93.40 2.10 2 5 -1 55.51 1.92 -2 5 1 59.36 2.16 -2 5 1 60.38 1.95 -2 5 1 57.46 1.56 2 5 -1 56.47 2.09 2 5 -1 51.90 2.20 2 5 0 33.81 1.86 2 5 0 32.94 1.46 -2 5 0 32.15 1.11 2 5 0 34.70 1.63 -2 5 0 31.73 1.43 -2 5 0 34.42 1.66 2 5 1 46.89 1.87 2 5 1 52.30 2.42 2 5 1 50.94 1.80 -2 5 -1 50.32 2.01 -2 5 -1 51.66 1.25 2 5 2 99.37 2.50 2 5 2 99.88 3.43 -2 5 -2 100.25 2.10 -2 5 -2 100.61 2.83 -2 5 -2 104.01 1.55 2 5 2 98.14 2.66 2 5 3 13.46 1.38 -2 5 -3 15.06 1.05 -2 5 -3 13.67 0.44 -2 5 -3 15.51 1.13 2 5 3 13.86 1.00 -2 5 -3 13.64 0.58 2 5 3 15.05 0.97 2 5 4 19.47 1.72 2 5 4 22.27 1.27 -2 5 -4 22.51 1.37 -2 5 -4 20.99 1.25 2 5 4 21.53 1.14 2 5 5 46.54 1.79 2 5 5 46.27 2.66 -2 5 -5 46.84 1.89 -2 5 -5 46.52 1.99 2 5 5 46.28 1.69 2 5 5 47.46 1.93 2 5 6 22.84 1.26 2 5 6 22.18 1.93 2 5 6 23.67 1.45 2 5 6 24.28 1.23 -2 5 -6 23.69 1.43 -2 5 -6 23.09 1.34 2 5 7 5.61 1.06 -2 5 -7 5.56 0.71 2 5 7 4.45 0.59 2 5 7 5.14 0.78 -2 5 -7 5.83 0.78 2 5 7 5.10 0.62 2 5 8 2.47 0.61 -2 5 -8 2.17 0.53 -2 5 -8 2.23 0.52 2 5 8 2.20 0.45 2 5 8 1.42 0.74 2 5 8 1.65 0.37 2 5 9 16.13 0.95 -2 5 -9 18.28 1.26 -2 5 -9 17.96 1.32 2 5 9 15.23 1.34 2 5 9 18.01 1.08 2 5 10 28.82 1.90 -2 5 -10 29.02 1.64 2 5 10 27.60 1.28 -2 5 -10 28.14 1.57 2 6 -13 3.25 0.93 -2 6 12 4.33 0.78 2 6 -12 3.55 0.89 2 6 -11 17.84 1.64 -2 6 11 14.88 1.34 2 6 -11 18.84 1.63 2 6 -10 14.44 1.44 -2 6 10 11.49 1.14 -2 6 10 13.81 1.36 -2 6 10 12.53 0.96 2 6 -10 10.54 1.22 2 6 -9 40.69 2.31 -2 6 9 44.27 1.76 -2 6 9 38.54 2.03 -2 6 9 42.28 2.19 2 6 -9 42.23 2.22 2 6 -8 6.05 0.98 -2 6 8 6.25 0.84 2 6 -8 4.62 0.77 -2 6 8 4.38 0.74 -2 6 8 5.52 0.65 -2 6 7 30.66 1.79 2 6 -7 29.03 0.86 2 6 -7 33.34 2.02 -2 6 7 33.20 1.52 2 6 -7 29.20 1.74 -2 6 7 33.77 1.80 -2 6 6 49.01 2.04 2 6 -6 51.94 1.48 -2 6 6 50.93 1.88 -2 6 6 49.94 2.27 2 6 -6 47.75 2.19 2 6 -6 49.08 2.38 2 6 -5 70.70 2.77 -2 6 5 72.45 2.36 -2 6 5 66.09 2.13 2 6 -5 68.23 2.53 -2 6 5 70.49 2.64 2 6 -5 72.99 2.10 -2 6 4 85.29 2.44 -2 6 4 85.84 2.91 2 6 -4 83.95 2.98 -2 6 4 86.55 2.46 2 6 -4 91.31 2.65 2 6 -4 79.13 2.67 -2 6 3 23.23 1.23 2 6 -3 21.76 1.50 -2 6 3 24.02 1.33 -2 6 3 23.83 1.56 2 6 -3 23.01 1.42 2 6 -3 23.44 1.48 2 6 -2 14.23 1.10 2 6 -2 13.55 1.22 -2 6 2 13.43 1.18 2 6 -2 13.03 1.19 -2 6 2 14.51 0.92 -2 6 2 14.24 1.05 2 6 -1 42.17 2.19 2 6 -1 48.52 2.15 2 6 -1 45.72 1.94 -2 6 1 49.07 2.18 -2 6 1 45.19 1.85 -2 6 1 47.37 1.57 -2 6 0 43.48 2.05 2 6 0 39.42 1.80 -2 6 0 42.58 1.37 2 6 0 41.50 2.00 2 6 0 40.84 2.22 -2 6 -1 11.13 0.97 2 6 1 14.73 1.41 -2 6 -1 13.40 0.74 -2 6 -1 13.56 1.16 2 6 1 14.98 1.18 -2 6 -1 13.77 1.09 2 6 1 13.91 1.07 2 6 2 39.60 1.77 2 6 2 40.97 1.96 -2 6 -2 42.91 1.95 -2 6 -2 39.39 1.98 -2 6 -2 40.09 1.12 2 6 2 39.72 2.41 -2 6 -2 36.22 1.50 2 6 3 20.65 1.30 -2 6 -3 23.71 0.70 -2 6 -3 21.90 1.52 2 6 3 18.34 1.71 -2 6 -3 21.35 0.90 -2 6 -3 22.59 1.43 2 6 3 23.12 1.45 2 6 4 68.97 2.32 2 6 4 70.39 2.50 2 6 4 71.41 3.47 2 6 4 72.63 2.48 -2 6 -4 71.90 2.59 -2 6 -4 72.86 2.70 2 6 5 63.23 2.42 -2 6 -5 67.32 2.62 2 6 5 60.44 2.29 2 6 5 67.02 3.45 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4 3 11 0.38 0.41 4 4 -14 8.75 1.20 -4 4 14 9.10 1.06 -4 4 13 37.80 2.19 -4 4 13 37.22 1.90 4 4 -13 41.36 2.83 -4 4 13 35.14 1.90 4 4 -13 34.80 2.08 -4 4 12 23.05 1.53 -4 4 12 21.69 1.45 4 4 -12 20.34 1.57 4 4 -12 23.46 2.15 -4 4 12 23.56 1.66 -4 4 11 20.89 1.52 -4 4 11 21.26 1.44 4 4 -11 22.83 2.01 -4 4 11 22.08 1.43 4 4 -11 17.28 0.88 4 4 -11 21.10 1.53 4 4 -10 27.75 2.11 -4 4 10 25.23 1.54 -4 4 10 27.82 1.50 4 4 -10 30.87 1.80 4 4 -10 26.91 1.08 -4 4 10 27.29 1.64 4 4 -9 9.69 0.99 -4 4 9 8.79 0.92 -4 4 9 9.76 0.91 -4 4 9 11.52 1.02 4 4 -9 8.90 1.25 4 4 -9 8.97 0.65 4 4 -8 16.92 1.23 4 4 -8 19.27 0.96 -4 4 8 17.25 1.23 -4 4 8 18.77 1.19 -4 4 8 17.14 1.19 4 4 -7 55.60 2.60 -4 4 7 54.46 2.13 4 4 -7 56.94 1.71 -4 4 7 59.54 2.04 -4 4 7 59.36 2.08 4 4 -7 55.24 2.11 4 4 -6 44.33 2.23 -4 4 6 44.83 1.90 -4 4 6 42.19 1.69 -4 4 6 39.47 1.61 4 4 -6 38.72 1.73 4 4 -6 39.93 1.53 4 4 -5 16.96 1.31 -4 4 5 17.15 1.18 -4 4 5 18.37 1.12 4 4 -5 18.34 1.12 -4 4 5 17.66 1.04 4 4 -5 17.41 1.12 4 4 -4 78.75 2.46 -4 4 4 70.72 1.96 4 4 -4 68.62 2.49 -4 4 4 71.64 2.32 -4 4 4 74.90 2.18 4 4 -4 71.21 2.16 -4 4 3 30.17 1.50 -4 4 3 29.99 1.39 4 4 -3 32.91 1.70 4 4 -3 32.02 1.62 -4 4 3 30.35 1.24 4 4 -3 31.87 1.42 4 4 -2 11.12 1.05 -4 4 2 13.69 1.00 -4 4 2 13.79 0.96 4 4 -2 12.63 0.95 4 4 -2 13.17 0.89 -4 4 2 12.78 0.77 4 4 -1 112.88 3.28 4 4 -1 108.99 2.60 -4 4 1 113.82 2.69 -4 4 1 107.69 2.72 -4 4 1 114.28 2.12 4 4 -1 110.21 2.49 -4 4 0 12.00 0.93 4 4 0 12.06 1.17 -4 4 0 12.06 0.91 -4 4 0 11.20 0.65 4 4 0 14.02 0.88 4 4 1 9.76 1.09 4 4 1 10.93 0.77 4 4 1 10.28 0.82 -4 4 -1 9.68 0.83 -4 4 -1 10.69 0.87 -4 4 -1 10.16 0.60 -4 4 -2 17.55 0.73 -4 4 -2 16.11 1.08 4 4 2 15.30 0.94 -4 4 -2 16.38 1.06 4 4 2 14.71 1.37 4 4 2 15.68 0.90 4 4 3 23.22 1.80 4 4 3 24.80 1.09 -4 4 -3 26.05 1.31 4 4 3 25.47 1.18 -4 4 -4 67.48 2.02 4 4 4 67.83 1.87 -4 4 -4 67.09 2.07 4 4 4 70.02 1.79 -4 4 -5 5.93 0.65 4 4 5 4.07 1.02 -4 4 -5 5.84 0.66 4 4 5 5.80 0.55 4 4 5 6.35 0.54 -4 4 -6 62.14 1.92 4 4 6 59.40 3.15 -4 4 -6 62.18 1.98 4 4 6 62.57 1.59 4 4 6 61.03 1.62 4 4 7 25.37 2.16 -4 4 -7 21.65 1.20 4 4 7 23.44 0.94 -4 4 -7 20.96 1.12 4 4 7 22.22 0.88 4 4 8 11.32 1.11 4 4 8 9.78 1.65 -4 4 -8 8.88 0.80 4 4 8 9.59 0.53 4 4 8 9.54 0.50 -4 4 -8 9.74 0.78 -4 4 -9 37.47 1.47 -4 4 -9 38.23 1.46 4 4 9 41.11 2.10 4 4 10 13.46 1.35 -4 5 13 1.55 0.58 4 5 -12 9.60 1.54 -4 5 12 10.23 1.03 -4 5 12 10.46 1.13 4 5 -12 9.63 1.20 -4 5 12 9.39 1.20 4 5 -11 7.00 1.00 4 5 -11 6.14 1.18 -4 5 11 6.51 0.81 -4 5 11 6.88 0.92 4 5 -11 4.95 0.45 -4 5 11 6.04 0.93 4 5 -10 7.63 0.99 -4 5 10 8.42 0.98 4 5 -10 8.02 0.60 -4 5 10 7.04 0.92 -4 5 10 7.56 0.84 4 5 -9 6.43 0.56 4 5 -9 6.45 0.85 -4 5 9 6.27 0.83 -4 5 9 6.23 0.75 -4 5 9 8.30 0.95 4 5 -9 8.30 1.24 4 5 -8 5.79 0.84 4 5 -8 5.64 0.55 -4 5 8 5.32 0.74 4 5 -8 6.64 1.03 -4 5 8 6.24 0.79 -4 5 8 6.20 0.75 -4 5 7 12.83 1.15 -4 5 7 13.20 1.03 4 5 -7 12.36 0.88 4 5 -7 11.62 1.11 -4 5 7 12.82 1.04 4 5 -7 11.24 1.26 4 5 -6 50.67 2.13 -4 5 6 51.39 1.98 -4 5 6 54.76 2.30 4 5 -6 52.48 2.58 -4 5 6 52.65 1.97 4 5 -6 52.80 1.90 4 5 -5 25.04 1.44 4 5 -5 20.68 1.57 -4 5 5 20.73 1.20 -4 5 5 22.69 1.31 -4 5 5 22.54 1.46 4 5 -5 23.98 1.43 4 5 -4 126.12 3.32 4 5 -4 119.31 3.51 -4 5 4 127.94 3.06 -4 5 4 128.65 3.38 4 5 -4 116.56 3.05 -4 5 4 120.25 2.74 4 5 -3 16.83 1.15 -4 5 3 15.86 1.11 -4 5 3 15.75 1.18 4 5 -3 16.25 1.25 -4 5 3 17.79 1.01 4 5 -3 16.43 1.29 4 5 -2 36.41 1.98 -4 5 2 37.03 1.66 -4 5 2 35.25 1.75 -4 5 2 36.06 1.35 4 5 -2 36.88 1.64 4 5 -1 18.16 1.45 4 5 -1 18.55 1.24 -4 5 1 19.61 1.21 -4 5 1 20.20 1.33 -4 5 1 18.99 0.93 4 5 -1 17.82 1.13 4 5 0 0.94 0.31 -4 5 0 1.25 0.26 4 5 0 1.44 0.51 -4 5 0 0.97 0.38 -4 5 0 1.63 0.43 4 5 0 1.27 0.39 4 5 1 12.09 0.91 4 5 1 10.45 0.89 -4 5 -1 12.63 1.04 -4 5 -1 13.48 1.06 -4 5 -1 12.97 0.70 4 5 1 11.47 1.27 -4 5 -2 0.84 0.21 4 5 2 1.23 0.36 -4 5 -2 1.41 0.43 4 5 2 1.11 0.37 -4 5 -2 0.44 0.32 4 5 2 0.86 0.56 4 5 3 50.40 1.78 4 5 3 53.22 2.82 -4 5 -3 49.31 1.95 4 5 3 52.52 1.93 -4 5 -3 52.76 2.10 4 5 4 27.18 2.16 4 5 4 29.15 1.44 -4 5 -4 28.06 1.53 -4 5 -4 28.81 1.49 4 5 4 28.23 1.32 -4 5 -5 78.15 2.49 4 5 5 70.76 3.57 4 5 5 75.32 2.23 -4 5 -5 79.14 2.55 4 5 5 75.92 2.10 -4 5 -6 5.29 0.68 4 5 6 5.37 1.24 -4 5 -6 5.44 0.72 4 5 6 6.39 0.66 4 5 6 6.69 0.63 -4 5 -7 5.83 0.73 4 5 7 3.26 1.09 4 5 7 5.07 0.56 -4 5 -7 4.47 0.67 4 5 7 5.61 0.84 4 5 7 5.09 0.56 4 5 8 13.66 0.81 -4 5 -8 14.63 1.14 4 5 8 13.48 0.85 4 5 8 11.60 1.25 -4 5 -8 11.23 0.98 -4 5 -9 13.46 1.06 4 5 9 13.15 1.30 -4 5 -9 14.88 1.14 -4 6 13 6.89 1.05 -4 6 12 19.05 1.60 -4 6 11 16.55 1.51 4 6 -11 18.24 2.02 -4 6 11 18.99 1.38 -4 6 11 15.44 1.43 -4 6 10 6.07 0.84 4 6 -10 5.12 1.21 -4 6 10 4.34 0.77 4 6 -10 4.04 0.39 -4 6 10 6.45 0.99 4 6 -10 5.26 0.96 4 6 -9 19.13 1.93 -4 6 9 18.12 1.32 -4 6 9 16.08 1.42 4 6 -9 15.07 0.81 -4 6 9 14.99 1.34 4 6 -9 14.74 1.37 -4 6 8 37.38 2.09 4 6 -8 32.90 2.34 -4 6 8 36.32 1.82 -4 6 8 32.86 1.87 4 6 -8 30.65 1.89 4 6 -8 34.23 1.36 4 6 -7 0.86 0.39 4 6 -7 0.26 0.53 -4 6 7 0.55 0.36 -4 6 7 0.35 0.29 -4 6 7 0.77 0.47 4 6 -7 0.91 0.48 4 6 -6 10.95 1.11 -4 6 6 13.26 1.08 -4 6 6 14.28 1.30 -4 6 6 13.87 1.12 4 6 -6 15.40 1.50 4 6 -6 14.55 1.12 -4 6 5 0.25 0.27 4 6 -5 0.45 0.35 -4 6 5 -0.52 0.36 -4 6 5 0.11 0.31 4 6 -5 -0.41 0.44 4 6 -4 15.62 1.34 4 6 -4 18.06 1.43 4 6 -4 16.33 1.27 -4 6 4 18.35 1.27 -4 6 4 20.69 1.49 -4 6 4 16.56 1.12 4 6 -3 17.13 1.46 4 6 -3 17.70 1.43 -4 6 3 18.33 1.27 -4 6 3 19.41 1.47 -4 6 3 18.21 1.11 4 6 -3 16.89 1.26 4 6 -2 47.91 2.44 4 6 -2 53.03 2.35 -4 6 2 55.20 2.20 -4 6 2 51.87 2.33 -4 6 2 53.32 1.78 4 6 -2 47.44 2.04 4 6 -1 151.26 4.47 4 6 -1 153.09 3.91 -4 6 1 161.37 3.80 -4 6 1 169.36 4.16 4 6 -1 162.63 3.71 -4 6 1 163.78 2.93 4 6 0 41.91 1.87 -4 6 0 45.97 1.47 4 6 0 43.76 2.53 -4 6 0 46.07 2.04 4 6 0 40.13 1.99 -4 6 0 45.56 2.17 4 6 1 10.39 0.90 4 6 1 11.54 1.39 -4 6 -1 12.45 1.11 4 6 1 12.97 1.13 -4 6 -1 14.17 1.22 -4 6 -1 13.67 0.75 4 6 2 16.42 1.71 -4 6 -2 12.82 0.82 -4 6 -2 15.06 1.19 4 6 2 14.99 1.18 -4 6 -2 14.66 1.25 4 6 2 14.54 1.09 -4 6 -2 16.82 0.75 4 6 3 21.69 2.05 -4 6 -3 24.29 1.52 4 6 3 24.41 1.50 -4 6 -3 22.96 1.56 4 6 3 21.25 1.31 -4 6 -4 32.73 1.75 4 6 4 37.62 2.73 4 6 4 33.24 1.61 4 6 4 35.02 1.75 -4 6 -4 31.80 1.80 4 6 5 16.03 1.12 4 6 5 19.62 1.29 -4 6 -5 17.39 1.31 4 6 5 15.46 1.86 4 6 6 20.44 1.26 -4 6 -6 21.09 1.49 4 6 6 21.72 1.35 4 6 6 22.35 1.61 -4 6 -6 21.52 1.48 4 6 7 0.28 0.32 -4 6 -7 0.25 0.38 -4 6 -7 0.87 0.52 4 6 7 0.31 0.33 4 6 7 -0.12 0.41 -4 6 -8 3.85 0.74 -4 6 -8 6.43 0.89 -4 7 11 13.94 1.45 4 7 -10 10.16 1.43 -4 7 10 9.80 1.06 -4 7 10 10.52 1.28 4 7 -9 4.12 0.91 -4 7 9 4.02 0.74 -4 7 9 4.51 0.83 -4 7 9 3.53 0.78 4 7 -8 42.52 2.62 -4 7 8 41.28 2.04 4 7 -8 43.24 1.57 -4 7 8 44.67 2.46 -4 7 8 43.29 2.24 4 7 -7 47.14 2.68 -4 7 7 49.30 2.21 -4 7 7 45.95 2.49 -4 7 7 47.41 2.26 4 7 -7 51.77 1.96 4 7 -6 38.66 2.39 -4 7 6 36.25 1.91 -4 7 6 39.02 2.27 4 7 -6 38.18 1.88 4 7 -6 31.91 1.99 -4 7 6 38.05 1.93 4 7 -5 10.32 1.16 -4 7 5 7.73 0.88 4 7 -5 8.34 1.16 -4 7 5 8.59 0.93 -4 7 5 8.38 1.11 4 7 -5 7.94 1.01 4 7 -4 10.43 1.21 4 7 -4 10.49 1.21 -4 7 4 9.90 1.01 -4 7 4 10.22 1.18 -4 7 4 9.69 0.90 4 7 -4 9.31 1.09 4 7 -3 4.05 0.86 4 7 -3 3.23 0.71 -4 7 3 3.41 0.71 -4 7 3 4.38 0.78 4 7 -3 3.52 0.71 -4 7 3 4.07 0.63 4 7 -2 64.91 3.08 4 7 -2 58.62 2.67 -4 7 2 60.83 2.51 -4 7 2 60.33 2.75 -4 7 2 59.80 2.01 4 7 -2 54.97 2.43 4 7 -1 11.64 1.42 -4 7 1 10.49 1.08 4 7 -1 10.62 1.17 -4 7 1 10.69 1.21 -4 7 1 10.17 0.81 4 7 -1 10.54 1.09 4 7 0 4.58 0.70 4 7 0 6.66 1.18 -4 7 0 5.56 0.84 4 7 0 4.60 0.81 -4 7 0 3.92 0.75 -4 7 0 5.19 0.59 4 7 1 0.21 0.65 -4 7 -1 1.37 0.56 -4 7 -1 0.56 0.38 4 7 1 1.20 0.58 -4 7 -1 1.52 0.60 4 7 1 0.79 0.35 -4 7 -1 1.00 0.30 -4 7 -2 0.83 0.25 4 7 2 0.39 0.38 -4 7 -2 1.03 0.38 -4 7 -2 1.38 0.59 4 7 2 0.13 0.43 -4 7 -2 0.28 0.48 4 7 3 13.90 1.73 -4 7 -3 12.41 1.24 4 7 3 14.23 1.26 -4 7 -3 15.42 1.40 4 7 3 13.49 1.15 -4 7 -4 10.60 1.16 4 7 4 9.31 1.04 -4 7 -4 9.14 1.14 4 7 4 9.29 1.02 4 7 5 11.14 1.06 4 7 5 12.84 1.19 -4 7 -5 12.87 1.36 4 7 5 12.34 1.24 -4 7 -5 9.92 1.17 4 7 6 4.34 0.85 -4 7 -6 3.50 0.76 -4 7 -6 3.68 0.80 4 7 6 3.75 0.72 4 7 6 2.68 0.58 -4 7 -7 13.69 1.42 4 7 7 13.65 1.18 -4 7 -7 13.06 1.33 -4 7 -8 23.73 1.76 -4 8 8 16.17 1.40 -4 8 8 15.24 1.61 -4 8 8 18.76 1.61 4 8 -7 6.75 1.28 -4 8 7 5.28 0.88 -4 8 7 4.36 0.93 -4 8 7 6.43 0.96 4 8 -6 7.87 0.94 4 8 -6 7.28 1.22 -4 8 6 5.66 0.83 -4 8 6 5.91 0.89 -4 8 6 7.61 1.17 4 8 -5 8.42 1.09 -4 8 5 7.47 1.01 4 8 -5 8.06 1.25 -4 8 5 6.14 1.03 -4 8 5 6.53 0.89 -4 8 4 9.55 1.09 4 8 -4 7.56 1.15 4 8 -4 9.44 1.25 -4 8 4 7.77 1.12 -4 8 4 8.50 0.93 4 8 -3 3.09 0.88 4 8 -3 2.63 0.75 -4 8 3 2.12 0.63 -4 8 3 2.81 0.85 -4 8 3 2.64 0.58 4 8 -2 11.94 1.51 -4 8 2 12.86 1.30 4 8 -2 16.39 1.55 -4 8 2 18.12 1.70 -4 8 2 14.71 1.09 4 8 -1 61.99 2.95 -4 8 1 63.32 3.04 -4 8 1 59.22 2.06 4 8 0 30.56 1.97 -4 8 0 31.94 1.92 4 8 0 34.07 2.21 -4 8 0 38.40 2.40 -4 8 0 35.98 1.52 4 8 0 32.51 2.54 4 8 1 14.16 1.82 -4 8 -1 16.51 1.29 4 8 1 16.45 1.58 -4 8 -1 14.18 1.55 -4 8 -1 17.44 1.01 4 8 1 13.97 1.34 4 8 2 3.52 0.74 -4 8 -2 3.24 0.53 4 8 2 5.48 0.97 -4 8 -2 4.59 0.94 -4 8 -2 4.54 0.47 4 8 3 4.38 0.78 4 8 3 5.90 0.96 4 8 3 5.26 0.87 -4 8 -3 5.53 1.02 4 8 4 2.09 0.66 4 8 4 2.20 0.64 -4 8 -4 3.13 0.86 4 8 4 2.52 0.69 4 8 5 3.55 0.78 4 8 5 3.46 0.80 -4 8 -5 2.60 0.88 -4 8 -6 6.70 1.17 4 8 6 7.53 1.06 -4 8 -7 2.07 0.84 -4 9 6 13.48 1.39 -4 9 5 8.85 1.12 4 9 -4 4.68 1.04 -4 9 4 5.57 0.86 4 9 -3 13.84 1.69 -4 9 3 14.35 1.26 4 9 -2 16.61 1.82 -4 9 2 16.28 1.85 -4 9 2 17.54 1.29 -4 9 1 5.05 1.03 -4 9 1 6.08 0.78 4 9 0 12.24 1.24 4 9 1 5.66 1.05 4 9 1 4.66 0.87 4 9 2 6.37 1.16 -5 -9 5 14.25 1.43 -5 -9 4 11.22 1.27 -5 -9 3 8.68 1.09 -5 -9 2 12.69 1.60 -5 -9 2 10.74 1.17 -5 -9 1 17.21 1.75 -5 -9 1 18.87 1.49 -5 -9 0 19.61 1.42 5 -8 -10 17.24 1.85 5 -8 -9 10.69 1.43 5 -8 -8 4.00 0.96 5 -8 -7 3.69 1.12 -5 -8 7 1.08 0.67 -5 -8 6 11.94 1.31 5 -8 -6 11.67 1.42 5 -8 -5 7.84 1.09 -5 -8 5 7.26 0.99 5 -8 -4 3.30 0.79 -5 -8 4 2.52 0.61 -5 -8 4 4.42 0.99 -5 -8 3 1.81 0.58 -5 -8 3 3.40 0.92 5 -8 -3 2.81 0.81 -5 -8 2 5.60 0.99 -5 -8 2 3.33 0.64 5 -8 -2 4.36 0.90 -5 -8 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0.65 5 7 -6 12.44 1.24 5 7 -6 10.93 1.37 -5 7 6 12.97 1.21 -5 7 6 11.06 1.29 -5 7 6 10.54 1.08 5 7 -6 8.94 1.14 5 7 -5 33.77 2.09 5 7 -5 29.82 2.07 -5 7 5 31.94 1.87 -5 7 5 29.17 2.01 -5 7 5 31.84 1.72 5 7 -5 30.04 1.94 5 7 -4 35.72 2.22 5 7 -4 35.40 2.21 -5 7 4 36.25 1.96 -5 7 4 35.79 2.20 -5 7 4 34.96 1.74 5 7 -4 34.18 2.02 5 7 -3 27.13 1.99 5 7 -3 26.51 1.90 -5 7 3 24.02 1.63 -5 7 3 26.66 1.88 -5 7 3 25.68 1.41 5 7 -3 23.71 1.65 -5 7 2 4.55 0.66 5 7 -2 4.65 0.78 5 7 -2 4.07 0.94 5 7 -2 4.72 0.87 -5 7 2 4.38 0.75 -5 7 2 4.74 0.84 5 7 -1 7.29 1.27 -5 7 1 6.67 0.97 5 7 -1 6.62 0.94 -5 7 1 6.39 0.99 5 7 -1 6.78 0.92 -5 7 1 6.89 0.74 5 7 0 3.18 0.64 5 7 0 2.83 0.98 5 7 0 3.85 0.75 -5 7 0 3.99 0.78 -5 7 0 3.58 0.79 -5 7 0 4.36 0.55 -5 7 -1 2.92 0.47 5 7 1 2.79 0.68 5 7 1 2.89 0.95 5 7 1 2.39 0.58 -5 7 -1 2.44 0.64 5 7 2 3.05 0.69 -5 7 -2 3.39 0.40 5 7 2 4.53 1.26 -5 7 -2 2.50 0.42 -5 7 -2 4.44 0.82 5 7 2 2.81 0.75 -5 7 -2 3.02 0.73 -5 7 -3 15.77 1.43 5 7 3 15.21 1.34 -5 7 -3 15.92 1.44 5 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10.80 1.39 -5 8 -6 4.81 1.09 -5 9 6 3.98 0.86 -5 9 5 11.72 1.27 5 9 -4 10.93 1.55 -5 9 4 15.90 1.38 -5 9 3 10.82 1.12 5 9 -3 12.56 1.70 -5 9 2 12.88 1.16 -6 -9 4 1.70 0.67 -6 -9 3 16.75 1.45 -6 -9 2 5.82 0.88 -6 -9 1 6.33 0.87 6 -8 -9 10.27 1.48 6 -8 -8 27.97 2.25 6 -8 -7 23.43 2.03 -6 -8 7 22.21 1.77 -6 -8 6 10.27 1.20 6 -8 -6 11.78 1.49 -6 -8 5 19.87 1.54 6 -8 -5 19.34 1.85 6 -8 -4 8.43 1.18 -6 -8 4 9.09 1.08 -6 -8 4 9.48 1.34 -6 -8 3 12.88 1.19 6 -8 -3 14.04 1.51 -6 -8 3 12.20 1.47 -6 -8 2 27.21 1.62 6 -8 -2 23.30 1.84 -6 -8 2 25.11 1.94 -6 -8 1 23.37 1.47 6 -8 -1 24.91 1.91 -6 -8 1 24.02 1.81 -6 -8 0 16.46 1.17 6 -8 0 15.60 1.58 -6 -8 0 17.87 1.52 -6 -8 -1 14.23 1.02 6 -7 -12 13.42 1.81 6 -7 -11 6.70 1.37 6 -7 -10 3.46 0.90 -6 -7 9 3.35 0.78 -6 -7 9 2.12 0.72 6 -7 -9 4.11 0.99 -6 -7 8 1.44 0.62 6 -7 -8 2.59 0.94 -6 -7 7 3.71 0.83 6 -7 -7 5.22 1.00 6 -7 -6 6.24 0.98 -6 -7 6 6.64 1.19 -6 -7 5 11.18 1.08 6 -7 -5 10.82 1.35 -6 -7 5 8.32 1.20 6 -7 -5 11.08 1.25 -6 -7 4 43.06 2.04 6 -7 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34.12 1.59 7 5 3 12.34 1.61 7 5 3 16.29 1.12 -7 5 -3 15.16 1.22 7 5 3 14.28 1.01 -7 5 -4 25.57 1.51 7 5 4 27.10 1.38 -7 5 -4 28.17 1.59 7 5 4 28.22 1.35 -7 5 -5 7.15 0.83 7 5 5 9.34 0.76 -7 5 -5 7.91 0.86 7 5 5 8.08 0.69 -7 5 -6 2.35 0.55 -7 5 -6 2.38 0.55 -7 6 11 2.63 0.81 7 6 -11 1.47 0.53 7 6 -10 7.37 1.32 -7 6 10 8.66 1.23 -7 6 10 6.93 0.99 -7 6 10 5.35 0.92 7 6 -10 5.71 0.76 -7 6 9 20.09 1.61 -7 6 9 21.05 1.71 7 6 -9 20.07 2.00 -7 6 9 20.97 1.62 7 6 -9 22.62 1.51 -7 6 8 31.45 1.96 -7 6 8 29.33 1.99 7 6 -8 25.19 2.14 -7 6 8 29.28 1.85 7 6 -8 27.84 1.75 -7 6 7 19.88 1.49 -7 6 7 20.94 1.59 -7 6 7 23.33 1.76 7 6 -7 22.60 1.97 7 6 -7 22.21 1.68 7 6 -7 22.25 1.64 -7 6 6 38.37 2.09 -7 6 6 37.99 2.24 7 6 -6 35.39 2.06 7 6 -6 39.17 2.44 -7 6 6 39.55 1.98 7 6 -6 40.35 2.27 7 6 -5 91.16 3.55 -7 6 5 96.84 3.29 -7 6 5 98.21 3.50 7 6 -5 96.10 3.29 -7 6 5 94.00 2.99 7 6 -5 96.29 3.61 7 6 -4 44.35 2.60 7 6 -4 39.33 2.22 -7 6 4 40.79 2.13 -7 6 4 42.16 2.32 7 6 -4 40.65 2.12 -7 6 4 40.30 1.91 7 6 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1.04 -7 7 6 5.99 0.92 7 7 -6 6.41 1.13 7 7 -5 5.08 1.03 -7 7 5 5.58 1.07 -7 7 5 5.04 0.78 7 7 -4 23.27 2.05 7 7 -4 26.04 1.99 -7 7 4 27.40 2.00 -7 7 4 26.15 1.61 7 7 -3 13.04 1.65 7 7 -3 10.28 1.28 -7 7 3 13.51 1.44 7 7 -3 8.50 1.06 -7 7 3 12.39 1.13 7 7 -2 4.18 0.81 7 7 -2 4.51 1.03 7 7 -2 4.90 0.91 -7 7 2 3.28 0.85 -7 7 2 3.61 0.64 7 7 -1 22.55 2.15 7 7 -1 23.23 1.75 7 7 -1 21.10 1.58 -7 7 1 21.17 1.73 -7 7 1 24.93 1.47 7 7 0 9.49 1.15 -7 7 0 10.84 1.27 7 7 0 9.76 1.10 -7 7 0 9.13 0.89 -7 7 -1 18.80 1.17 7 7 1 18.67 1.55 -7 7 -1 19.87 1.63 7 7 1 17.25 1.40 7 7 2 4.69 0.83 -7 7 -2 2.50 0.72 7 7 2 4.51 0.79 -7 7 -2 4.29 0.93 7 7 3 6.65 0.93 7 7 3 6.89 0.94 -7 7 -3 6.08 0.97 7 7 4 6.06 0.93 -7 7 -4 6.47 1.02 -7 7 -5 2.16 0.69 -7 8 7 28.42 2.00 7 8 -7 29.93 2.11 7 8 -6 5.46 1.17 -7 8 6 5.49 0.93 7 8 -5 8.03 1.38 -7 8 5 7.15 1.06 7 8 -4 5.43 1.11 -7 8 4 4.93 0.88 -7 8 3 5.19 0.85 7 8 -3 3.41 0.90 -7 8 3 3.26 0.80 7 8 -2 4.54 0.95 -7 8 2 2.58 0.83 -7 8 2 3.20 0.70 7 8 -1 12.33 1.48 -7 8 1 13.48 1.60 -7 8 1 14.45 1.21 7 8 0 6.63 1.18 -7 8 0 4.94 1.07 7 8 1 0.39 0.60 -7 8 -1 0.55 0.66 7 8 2 11.94 1.36 -7 8 -2 11.95 1.44 7 8 3 1.38 0.71 -7 9 5 0.93 0.63 -7 9 4 0.87 0.56 -8 -8 6 3.93 0.86 -8 -8 5 32.70 1.99 -8 -8 4 18.99 1.52 -8 -8 4 17.50 1.76 -8 -8 3 0.41 0.67 -8 -8 3 1.76 0.58 -8 -8 2 16.18 1.27 -8 -8 2 16.89 1.65 8 -7 -9 14.92 1.81 -8 -7 9 5.04 1.20 8 -7 -8 22.47 2.07 -8 -7 8 13.71 1.68 8 -7 -7 15.79 1.72 -8 -7 7 16.23 1.59 -8 -7 6 21.69 1.79 -8 -7 6 17.46 1.80 8 -7 -6 16.63 1.33 -8 -7 6 18.23 1.84 8 -7 -6 18.64 1.85 -8 -7 5 9.72 1.34 8 -7 -5 8.83 1.22 -8 -7 5 10.89 1.55 -8 -7 5 10.57 1.21 8 -7 -5 8.98 0.95 -8 -7 4 12.36 1.41 8 -7 -4 12.39 1.07 8 -7 -4 14.26 1.51 -8 -7 3 5.94 0.96 8 -7 -3 6.97 1.14 -8 -7 3 7.60 0.84 8 -7 -2 6.52 1.14 -8 -7 2 4.69 0.69 -8 -7 2 4.64 0.87 -8 -7 1 15.23 1.06 8 -7 -1 16.85 1.60 -8 -7 0 9.27 0.97 -8 -7 0 9.65 0.79 8 -7 0 8.97 1.20 8 -7 1 12.16 1.40 8 -6 -12 6.04 1.40 -8 -6 11 -0.08 0.66 8 -6 -11 0.77 0.82 -8 -6 10 1.10 0.59 -8 -6 10 0.34 0.76 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1.02 -8 -4 10 7.10 1.19 -8 -4 9 3.34 0.68 -8 -4 9 4.80 0.97 8 -4 -9 4.54 0.86 8 -4 -9 4.40 0.95 8 -4 -9 4.44 0.76 -8 -4 9 4.59 0.99 -8 -4 8 7.27 0.92 -8 -4 8 6.00 1.08 8 -4 -8 8.49 1.19 8 -4 -8 7.30 0.98 -8 -4 8 8.15 1.23 8 -4 -8 9.73 1.00 -8 -4 7 43.84 2.10 -8 -4 7 45.26 2.54 8 -4 -7 48.86 2.52 8 -4 -7 43.98 2.27 -8 -4 7 44.52 2.47 8 -4 -7 46.07 2.00 -8 -4 6 3.70 0.65 -8 -4 6 2.65 0.78 8 -4 -6 4.24 0.74 8 -4 -6 3.60 0.71 8 -4 -6 3.94 0.61 -8 -4 6 4.31 0.86 8 -4 -5 61.36 2.70 -8 -4 5 65.87 2.43 -8 -4 5 58.46 3.01 8 -4 -5 64.46 2.61 -8 -4 5 64.18 2.66 8 -4 -5 58.85 2.10 -8 -4 4 52.02 2.13 -8 -4 4 59.99 3.07 8 -4 -4 53.70 2.37 -8 -4 4 54.11 2.33 8 -4 -4 52.73 1.90 8 -4 -4 55.38 2.53 -8 -4 3 40.19 1.80 -8 -4 3 42.50 2.61 -8 -4 3 39.15 1.90 8 -4 -3 38.96 1.96 8 -4 -3 40.26 1.60 8 -4 -3 43.60 2.15 -8 -4 2 98.56 2.79 -8 -4 2 96.63 3.96 -8 -4 2 103.81 2.87 8 -4 -2 95.05 3.00 8 -4 -2 98.15 2.40 8 -4 -2 97.78 3.15 -8 -4 1 33.88 1.58 -8 -4 1 35.65 1.54 -8 -4 1 36.76 2.52 8 -4 -1 36.34 1.83 8 -4 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-6 43.28 2.74 -13 3 6 50.84 2.67 -13 3 5 3.85 1.12 13 3 -5 1.83 0.68 -13 3 5 2.47 0.72 13 3 -5 3.46 0.95 -13 3 4 1.24 0.90 13 3 -4 2.74 0.78 -13 3 4 2.30 0.73 13 3 -4 1.63 0.68 -13 3 3 1.48 0.91 13 3 -3 0.48 0.49 -13 3 3 1.37 0.58 13 3 -3 0.42 0.57 13 3 -2 1.77 0.67 -13 3 2 1.63 1.03 13 3 -2 1.04 0.58 -13 3 2 1.89 0.68 -13 3 1 0.22 0.81 13 3 -1 0.93 0.56 -13 3 1 0.61 0.52 -13 3 0 4.97 1.18 -13 3 0 8.18 1.03 -13 3 -1 0.94 0.85 13 4 -9 8.67 1.56 13 4 -8 23.23 2.22 -13 4 8 23.65 2.31 -13 4 7 3.62 1.18 13 4 -7 1.77 0.77 -13 4 6 4.67 1.24 13 4 -6 3.60 0.96 -13 4 6 3.48 0.95 -13 4 5 8.86 1.52 13 4 -5 5.76 1.11 -13 4 5 7.84 1.20 -13 4 4 6.13 1.18 13 4 -4 7.69 1.18 -13 4 4 8.84 1.17 -13 4 3 49.61 3.09 13 4 -3 49.42 2.55 13 4 -3 47.38 2.47 -13 4 3 52.72 2.68 -13 4 2 9.10 1.46 13 4 -2 7.07 1.03 -13 4 2 7.30 1.10 -13 4 1 0.59 0.80 -13 4 1 0.61 0.63 13 5 -8 3.04 1.09 13 5 -7 4.98 1.15 -13 5 6 3.06 1.20 13 5 -6 2.54 0.93 -13 5 5 2.04 1.06 13 5 -5 1.21 0.72 -13 5 4 8.80 1.49 -13 5 3 7.94 1.35 -13 5 2 1.54 0.79 -13 5 1 5.22 1.03 -14 -4 5 0.61 0.70 -14 -4 4 0.19 0.56 -14 -4 3 16.07 1.53 -14 -3 7 9.22 1.24 -14 -3 6 5.75 1.05 -14 -3 5 34.30 2.13 -14 -3 5 31.33 2.03 -14 -3 4 72.49 3.03 -14 -3 4 72.50 2.92 -14 -3 3 40.20 2.22 14 -3 -3 39.97 2.78 -14 -3 2 7.10 1.01 14 -3 -2 5.93 1.27 -14 -2 8 20.99 1.80 14 -2 -7 37.48 2.86 -14 -2 7 35.94 2.26 14 -2 -6 22.14 2.20 -14 -2 6 22.11 1.75 -14 -2 5 2.15 0.75 -14 -2 5 0.88 0.59 14 -2 -5 1.45 0.83 -14 -2 4 0.71 0.58 14 -2 -4 0.31 0.61 -14 -2 4 0.29 0.51 -14 -2 3 0.85 0.64 14 -2 -3 0.67 0.63 14 -2 -3 0.51 0.65 -14 -2 3 0.75 0.54 -14 -2 2 4.32 0.81 14 -2 -2 6.29 1.28 14 -2 -1 4.89 1.12 14 -2 0 6.56 1.21 14 -1 -8 6.23 1.32 -14 -1 8 6.84 1.07 -14 -1 7 4.72 0.90 -14 -1 7 4.52 1.38 14 -1 -7 3.72 1.04 -14 -1 6 7.40 1.09 -14 -1 6 5.44 1.50 14 -1 -6 8.59 1.42 -14 -1 5 4.91 0.83 -14 -1 5 5.64 1.48 14 -1 -5 3.73 0.99 -14 -1 5 2.68 0.68 -14 -1 4 15.94 2.14 14 -1 -4 17.03 1.84 14 -1 -4 13.15 1.45 -14 -1 4 15.76 1.43 -14 -1 4 16.54 1.42 -14 -1 3 6.06 1.50 14 -1 -3 7.23 1.06 -14 -1 3 8.34 1.05 14 -1 -3 7.74 1.25 -14 -1 3 8.92 1.07 -14 -1 2 2.88 0.67 14 -1 -2 2.57 0.74 14 -1 -2 2.95 0.97 -14 -1 2 1.34 0.56 14 -1 -1 2.00 0.87 14 0 -9 19.25 2.16 14 0 -8 29.25 2.53 -14 0 8 30.58 2.14 -14 0 7 35.62 2.96 14 0 -7 32.63 2.59 -14 0 7 33.28 2.12 14 0 -6 6.70 1.23 -14 0 6 4.78 1.18 -14 0 6 6.68 1.03 -14 0 5 3.77 1.21 -14 0 5 5.05 0.92 -14 0 5 5.62 0.96 14 0 -5 3.22 0.99 -14 0 4 3.64 1.21 14 0 -4 5.72 0.92 -14 0 4 4.71 0.81 14 0 -4 7.43 1.28 -14 0 4 7.46 1.01 -14 0 3 0.90 0.91 14 0 -3 1.34 0.75 -14 0 3 0.55 0.54 14 0 -3 -0.35 0.68 -14 0 3 0.68 0.51 -14 0 2 -0.13 0.49 -14 0 2 1.12 0.94 14 0 -2 -0.16 0.60 -14 0 2 0.38 0.52 14 0 -2 0.68 0.72 -14 0 1 0.59 0.45 -14 0 1 0.67 1.00 -14 0 1 0.32 0.48 14 0 -1 -0.53 0.76 14 1 -9 0.60 0.75 14 1 -8 7.18 1.40 -14 1 8 7.57 1.15 14 1 -7 3.27 0.95 -14 1 7 4.94 0.96 -14 1 6 6.36 1.42 14 1 -6 7.64 1.29 -14 1 6 7.03 1.07 -14 1 5 3.45 1.30 14 1 -5 3.75 0.94 -14 1 5 4.97 0.94 -14 1 4 12.01 1.86 14 1 -4 15.17 1.44 14 1 -4 12.67 1.55 -14 1 4 16.24 1.46 14 1 -3 5.68 1.18 14 1 -3 7.12 1.02 -14 1 3 8.39 1.07 14 1 -2 2.93 0.80 -14 1 2 -0.16 1.09 14 1 -2 1.16 0.63 -14 1 2 1.56 0.63 -14 1 2 1.74 0.61 -14 1 1 2.57 1.21 -14 1 1 2.95 0.68 -14 1 0 0.54 1.10 -14 1 -1 0.66 1.15 14 2 -9 23.35 2.27 14 2 -8 20.69 2.15 -14 2 7 38.44 2.44 14 2 -7 38.54 2.79 -14 2 6 21.85 2.25 -14 2 6 19.68 1.72 14 2 -6 21.45 2.05 -14 2 5 1.38 0.86 14 2 -5 0.21 0.67 -14 2 5 1.23 0.68 -14 2 4 0.33 0.89 14 2 -4 0.65 0.70 14 2 -4 0.36 0.57 -14 2 4 0.71 0.56 -14 2 3 0.33 0.93 14 2 -3 1.73 0.77 14 2 -3 1.22 0.62 -14 2 3 0.62 0.57 -14 2 2 1.80 1.15 -14 2 2 4.35 0.85 -14 2 1 0.94 1.11 -14 2 1 3.20 0.70 -14 2 0 4.56 1.31 14 3 -8 2.24 0.94 14 3 -7 7.48 1.38 -14 3 6 3.70 1.06 -14 3 6 5.86 1.02 14 3 -6 6.25 1.32 -14 3 5 38.15 2.92 14 3 -5 35.09 2.49 -14 3 5 31.93 2.22 -14 3 4 73.21 4.07 14 3 -4 69.84 3.33 -14 3 4 70.54 3.15 -14 3 3 34.35 2.85 -14 3 3 38.38 2.28 -14 3 2 6.39 1.52 -14 3 2 6.37 1.02 -14 3 1 0.70 1.01 14 4 -7 10.07 1.52 14 4 -6 10.69 1.60 -14 4 5 0.53 0.91 14 4 -5 0.33 0.69 -14 4 4 -1.37 1.17 -14 4 3 15.11 2.03 -14 4 3 14.31 1.55 -14 4 2 1.59 1.16 -14 4 2 2.21 0.87 -15 -3 4 17.77 1.67 -15 -2 5 1.85 0.78 -15 -2 4 8.21 1.18 -15 -2 3 2.48 0.76 -15 -1 6 14.52 1.49 -15 -1 5 1.38 0.63 15 -1 -5 2.93 1.08 -15 -1 4 0.35 0.55 15 -1 -4 0.82 0.84 15 -1 -3 9.65 1.50 -15 -1 3 8.73 1.15 15 -1 -2 24.18 2.22 15 0 -6 11.90 1.71 -15 0 6 9.93 1.26 15 0 -5 2.75 0.98 -15 0 5 5.09 0.95 -15 0 4 1.57 0.63 -15 0 3 3.04 0.87 15 0 -3 1.40 0.93 15 1 -7 3.87 1.19 15 1 -6 13.59 1.67 -15 1 6 13.23 1.45 15 1 -5 2.97 1.05 -15 1 5 3.53 0.89 15 1 -4 1.08 0.90 -15 1 4 1.84 0.76 -15 1 3 7.13 1.03 15 2 -7 39.62 2.90 15 2 -6 4.27 1.11 15 2 -5 -0.28 0.79 -15 2 5 1.21 0.71 -15 2 4 8.44 1.23 -15 2 3 3.14 0.93 15 3 -7 1.56 1.00 15 3 -6 4.22 1.21 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT2014 (Sheldrick, 2015a)' _computing_cell_refinement 'CrysAlis PRO (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlis PRO (Rigaku OD, 2015)' _cell_measurement_reflns_used 13845 _cell_measurement_theta_min 3.4120 _cell_measurement_theta_max 29.6790 _exptl_absorpt_correction_T_min 0.83842 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ) CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ) _computing_data_collection ) Rigaku CrystalClear-SM Expert 2.1 b32 (Rigaku, 2014) MSCServDetCCD = {5.7.3.4} ) _diffrn_source 'Rotating Anode MicroMax-007HF DW 1.2 kW' _diffrn_measurement_device_type 'AFC11 (Right): Eulerian 3 circle CCD' _diffrn_measurement_method 'Profile data from \w-scans' _exptl_crystal_description block _exptl_crystal_colour 'colourless' ; _shelx_hkl_checksum 9351 _shelx_res_file ; TITL (I) in P2(1) (I).res created by SHELXL-2018/3 at 13:22:11 on 27-Jul-2018 CELL 0.71073 11.3449 7.3527 11.8641 90.000 113.623 90.000 ZERR 2.00 0.0002 0.0001 0.0003 0.000 0.003 0.000 LATT -1 SYMM -X, 0.5+Y, -Z SFAC C H N O P UNIT 40 40 2 6 2 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! L.S. 4 BOND $H FMAP 2 PLAN 20 shel 999 0.83 acta temp -153 size 0.05 0.05 0.15 eqiv $1 -x, y-1/2, -z eqiv $2 -x+1, y-1/2, -z eqiv $3 x,y-1,z dfix 0.88 0.01 N1 H1N htab N1 O1_$1 htab C4 O1_$1 htab C7 O2_$2 htab C1 O2_$3 conf WGHT 0.036300 0.111600 FVAR 0.50065 P1 5 0.111630 0.558944 -0.042503 11.00000 0.01626 0.01870 = 0.02360 -0.00231 0.00990 -0.00115 C1 1 0.189509 0.111380 -0.171929 11.00000 0.04158 0.02660 = 0.02787 -0.00226 0.01477 0.00529 AFIX 137 H1A 2 0.117455 0.152536 -0.246310 11.00000 -1.50000 H1B 2 0.159520 0.017335 -0.131115 11.00000 -1.50000 H1C 2 0.257187 0.061177 -0.194363 11.00000 -1.50000 AFIX 0 O1 4 -0.002447 0.582678 -0.015084 11.00000 0.02058 0.02567 = 0.03569 -0.00625 0.01553 -0.00054 O2 4 0.109927 0.661158 -0.161374 11.00000 0.02067 0.02244 = 0.02850 0.00298 0.00918 -0.00158 C2 1 0.242925 0.271621 -0.084882 11.00000 0.02467 0.01969 = 0.02916 0.00308 0.01774 0.00320 AFIX 13 H2 2 0.271072 0.367118 -0.128810 11.00000 -1.20000 AFIX 0 C3 1 0.359103 0.214360 0.028940 11.00000 0.02377 0.01562 = 0.02984 -0.00312 0.01528 0.00000 O3 4 0.238810 0.659323 0.046343 11.00000 0.02320 0.02962 = 0.02649 -0.00618 0.01136 -0.00856 N1 3 0.139118 0.347322 -0.055254 11.00000 0.02009 0.01981 = 0.03134 0.00154 0.01647 0.00007 H1N 2 0.093105 0.273345 -0.030291 11.00000 -1.20000 C20 1 0.402842 0.571511 0.239247 11.00000 0.02415 0.02423 = 0.03963 -0.00664 0.01061 0.00046 AFIX 43 H20 2 0.448329 0.514285 0.196962 11.00000 -1.20000 AFIX 0 C19 1 0.453940 0.576552 0.366406 11.00000 0.03018 0.02754 = 0.03970 0.00289 0.00225 0.00094 AFIX 43 H19 2 0.534906 0.521430 0.412026 11.00000 -1.20000 AFIX 0 C18 1 0.387824 0.661427 0.427602 11.00000 0.04272 0.03750 = 0.02754 0.00138 0.00764 -0.00703 AFIX 43 H18 2 0.424179 0.666399 0.514934 11.00000 -1.20000 AFIX 0 C17 1 0.268677 0.739119 0.361572 11.00000 0.03817 0.04094 = 0.03142 -0.00716 0.01751 -0.00418 AFIX 43 H17 2 0.222697 0.794866 0.403915 11.00000 -1.20000 AFIX 0 C16 1 0.216070 0.736002 0.233908 11.00000 0.02357 0.02825 = 0.03137 -0.00461 0.01042 -0.00054 AFIX 43 H16 2 0.135014 0.790819 0.188194 11.00000 -1.20000 AFIX 0 C15 1 0.284150 0.651398 0.174649 11.00000 0.02225 0.02101 = 0.02608 -0.00256 0.00877 -0.00477 C4 1 0.344037 0.115236 0.122306 11.00000 0.02151 0.02331 = 0.02992 -0.00121 0.01265 -0.00160 AFIX 43 H4 2 0.260152 0.083866 0.115315 11.00000 -1.20000 AFIX 0 C5 1 0.450405 0.061915 0.225398 11.00000 0.02809 0.02593 = 0.02850 0.00001 0.01210 -0.00055 AFIX 43 H5 2 0.439074 -0.005717 0.288557 11.00000 -1.20000 AFIX 0 C6 1 0.573496 0.107145 0.236555 11.00000 0.02310 0.02669 = 0.03330 -0.00485 0.00696 0.00372 AFIX 43 H6 2 0.646440 0.071780 0.307487 11.00000 -1.20000 AFIX 0 C9 1 0.008491 0.646118 -0.276988 11.00000 0.02094 0.02291 = 0.02586 0.00439 0.00911 -0.00091 C8 1 0.482815 0.256749 0.039945 11.00000 0.02798 0.01835 = 0.03931 -0.00066 0.02194 0.00118 AFIX 43 H8 2 0.494569 0.322097 -0.023856 11.00000 -1.20000 AFIX 0 C7 1 0.588927 0.204265 0.143337 11.00000 0.02052 0.02397 = 0.04742 -0.00827 0.01754 -0.00141 AFIX 43 H7 2 0.672907 0.235115 0.150359 11.00000 -1.20000 AFIX 0 C10 1 -0.104064 0.742876 -0.301828 11.00000 0.03105 0.03228 = 0.03321 0.00125 0.01336 0.00754 AFIX 43 H10 2 -0.115946 0.810978 -0.239135 11.00000 -1.20000 AFIX 0 C11 1 -0.199206 0.737921 -0.420697 11.00000 0.02657 0.04595 = 0.03883 0.00776 0.00821 0.01081 AFIX 43 H11 2 -0.277448 0.802145 -0.439333 11.00000 -1.20000 AFIX 0 C13 1 -0.067836 0.544642 -0.485315 11.00000 0.04177 0.03789 = 0.02848 0.00227 0.01794 0.00236 AFIX 43 H13 2 -0.055745 0.477124 -0.548126 11.00000 -1.20000 AFIX 0 C14 1 0.027765 0.547228 -0.367066 11.00000 0.02852 0.02791 = 0.03265 0.00404 0.01657 0.00414 AFIX 43 H14 2 0.105535 0.481742 -0.348321 11.00000 -1.20000 AFIX 0 C12 1 -0.180855 0.640503 -0.511729 11.00000 0.03408 0.04735 = 0.02728 0.00629 0.00854 -0.00025 AFIX 43 H12 2 -0.246008 0.639184 -0.592845 11.00000 -1.20000 REM ##### AFIX 0 HKLF 4 REM (I) in P2(1) REM wR2 = 0.0612, GooF = S = 1.068, Restrained GooF = 1.068 for all data REM R1 = 0.0235 for 3245 Fo > 4sig(Fo) and 0.0244 for all 3322 data REM 230 parameters refined using 2 restraints END WGHT 0.0363 0.1116 REM Highest difference peak 0.161, deepest hole -0.230, 1-sigma level 0.030 Q1 1 0.1013 0.4411 -0.1023 11.00000 0.05 0.16 Q2 1 0.1040 0.6237 -0.1176 11.00000 0.05 0.13 Q3 1 0.0049 0.5622 -0.3227 11.00000 0.05 0.13 Q4 1 0.2126 0.1987 -0.1341 11.00000 0.05 0.12 Q5 1 0.3569 0.1526 0.0663 11.00000 0.05 0.12 Q6 1 0.3907 0.5572 0.3837 11.00000 0.05 0.12 Q7 1 0.2160 0.6876 0.2898 11.00000 0.05 0.12 Q8 1 0.2305 0.6515 0.2022 11.00000 0.05 0.11 Q9 1 0.4117 0.5393 0.2993 11.00000 0.05 0.11 Q10 1 -0.1655 0.7149 -0.3530 11.00000 0.05 0.11 Q11 1 0.4187 0.0527 0.1669 11.00000 0.05 0.11 Q12 1 0.1556 0.4329 -0.0024 11.00000 0.05 0.11 Q13 1 0.2989 0.5523 0.2038 11.00000 0.05 0.11 Q14 1 -0.0220 0.7369 -0.3012 11.00000 0.05 0.11 Q15 1 -0.0124 0.5560 -0.4271 11.00000 0.05 0.10 Q16 1 0.3087 0.2399 -0.0241 11.00000 0.05 0.10 Q17 1 0.2552 0.6448 0.1096 11.00000 0.05 0.10 Q18 1 0.1158 0.4941 -0.1549 11.00000 0.05 0.09 Q19 1 0.3377 0.6549 0.2016 11.00000 0.05 0.09 Q20 1 0.5395 0.2446 0.0975 11.00000 0.05 0.09 ; _shelx_res_checksum 76725 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy P P1 0.11163(4) 0.55894(6) -0.04250(4) 0.01891(13) Uani d 1 C C1 0.1895(2) 0.1114(3) -0.17193(19) 0.0317(5) Uani d 1 H H1A 0.117455 0.152536 -0.246310 0.048 Uiso calc 1 H H1B 0.159520 0.017335 -0.131115 0.048 Uiso calc 1 H H1C 0.257187 0.061177 -0.194363 0.048 Uiso calc 1 O O1 -0.00245(12) 0.5827(2) -0.01508(12) 0.0260(3) Uani d 1 O O2 0.10993(12) 0.66116(18) -0.16137(12) 0.0241(3) Uani d 1 C C2 0.24293(18) 0.2716(3) -0.08488(18) 0.0223(4) Uani d 1 H H2 0.271072 0.367118 -0.128810 0.027 Uiso calc 1 C C3 0.35910(18) 0.2144(3) 0.02894(17) 0.0216(4) Uani d 1 O O3 0.23881(13) 0.6593(2) 0.04634(12) 0.0260(3) Uani d 1 N N1 0.13912(15) 0.3473(2) -0.05525(15) 0.0218(3) Uani d 1 H H1N 0.0931(19) 0.273(3) -0.0303(19) 0.026 Uiso d 1 C C20 0.40284(18) 0.5715(3) 0.23925(19) 0.0300(4) Uani d 1 H H20 0.448329 0.514285 0.196962 0.036 Uiso calc 1 C C19 0.4539(2) 0.5766(3) 0.3664(2) 0.0362(5) Uani d 1 H H19 0.534906 0.521430 0.412026 0.043 Uiso calc 1 C C18 0.3878(2) 0.6614(3) 0.4276(2) 0.0380(5) Uani d 1 H H18 0.424179 0.666399 0.514934 0.046 Uiso calc 1 C C17 0.2687(2) 0.7391(3) 0.36157(19) 0.0357(5) Uani d 1 H H17 0.222697 0.794866 0.403915 0.043 Uiso calc 1 C C16 0.21607(19) 0.7360(3) 0.23391(19) 0.0279(4) Uani d 1 H H16 0.135014 0.790819 0.188194 0.033 Uiso calc 1 C C15 0.28415(18) 0.6514(3) 0.17465(18) 0.0234(4) Uani d 1 C C4 0.34404(18) 0.1152(3) 0.12231(17) 0.0242(4) Uani d 1 H H4 0.260152 0.083866 0.115315 0.029 Uiso calc 1 C C5 0.45040(17) 0.0619(3) 0.22540(17) 0.0273(4) Uani d 1 H H5 0.439074 -0.005717 0.288557 0.033 Uiso calc 1 C C6 0.57350(19) 0.1071(3) 0.23656(19) 0.0291(5) Uani d 1 H H6 0.646440 0.071780 0.307487 0.035 Uiso calc 1 C C9 0.00849(17) 0.6461(3) -0.27699(17) 0.0233(4) Uani d 1 C C8 0.4828(2) 0.2567(3) 0.0399(2) 0.0259(4) Uani d 1 H H8 0.494569 0.322097 -0.023856 0.031 Uiso calc 1 C C7 0.58893(19) 0.2043(3) 0.1433(2) 0.0294(5) Uani d 1 H H7 0.672907 0.235115 0.150359 0.035 Uiso calc 1 C C10 -0.1041(2) 0.7429(3) -0.3018(2) 0.0320(5) Uani d 1 H H10 -0.115946 0.810978 -0.239135 0.038 Uiso calc 1 C C11 -0.1992(2) 0.7379(4) -0.4207(2) 0.0387(5) Uani d 1 H H11 -0.277448 0.802145 -0.439333 0.046 Uiso calc 1 C C13 -0.0678(2) 0.5446(4) -0.48532(18) 0.0348(5) Uani d 1 H H13 -0.055745 0.477124 -0.548126 0.042 Uiso calc 1 C C14 0.02776(18) 0.5472(3) -0.36707(17) 0.0283(4) Uani d 1 H H14 0.105535 0.481742 -0.348321 0.034 Uiso calc 1 C C12 -0.1809(2) 0.6405(4) -0.5117(2) 0.0374(5) Uani d 1 H H12 -0.246008 0.639184 -0.592845 0.045 Uiso calc 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 P1 0.0163(2) 0.0187(2) 0.0236(2) -0.00115(19) 0.00990(17) -0.0023(2) C1 0.0416(11) 0.0266(12) 0.0279(10) 0.0053(9) 0.0148(9) -0.0023(8) O1 0.0206(6) 0.0257(7) 0.0357(7) -0.0005(6) 0.0155(5) -0.0062(6) O2 0.0207(6) 0.0224(7) 0.0285(7) -0.0016(5) 0.0092(6) 0.0030(6) C2 0.0247(10) 0.0197(9) 0.0292(9) 0.0032(7) 0.0177(8) 0.0031(8) C3 0.0238(9) 0.0156(9) 0.0298(10) 0.0000(7) 0.0153(8) -0.0031(7) O3 0.0232(7) 0.0296(8) 0.0265(7) -0.0086(6) 0.0114(6) -0.0062(6) N1 0.0201(8) 0.0198(8) 0.0313(8) 0.0001(7) 0.0165(7) 0.0015(7) C20 0.0241(9) 0.0242(10) 0.0396(10) 0.0005(9) 0.0106(8) -0.0066(10) C19 0.0302(10) 0.0275(11) 0.0397(11) 0.0009(10) 0.0022(9) 0.0029(10) C18 0.0427(12) 0.0375(13) 0.0275(11) -0.0070(11) 0.0076(10) 0.0014(10) C17 0.0382(12) 0.0409(13) 0.0314(11) -0.0042(11) 0.0175(10) -0.0072(10) C16 0.0236(10) 0.0283(11) 0.0314(10) -0.0005(9) 0.0104(9) -0.0046(9) C15 0.0223(9) 0.0210(9) 0.0261(9) -0.0048(8) 0.0088(8) -0.0026(8) C4 0.0215(9) 0.0233(10) 0.0299(10) -0.0016(7) 0.0127(8) -0.0012(7) C5 0.0281(9) 0.0259(9) 0.0285(9) -0.0005(10) 0.0121(8) 0.0000(10) C6 0.0231(9) 0.0267(11) 0.0333(10) 0.0037(8) 0.0070(8) -0.0048(8) C9 0.0209(9) 0.0229(9) 0.0259(9) -0.0009(8) 0.0091(8) 0.0044(8) C8 0.0280(10) 0.0184(9) 0.0393(11) 0.0012(8) 0.0219(9) -0.0007(9) C7 0.0205(9) 0.0240(10) 0.0474(12) -0.0014(8) 0.0175(9) -0.0083(9) C10 0.0311(11) 0.0323(11) 0.0332(11) 0.0075(9) 0.0134(9) 0.0012(9) C11 0.0266(11) 0.0460(14) 0.0388(12) 0.0108(10) 0.0082(10) 0.0078(11) C13 0.0418(11) 0.0379(13) 0.0285(10) 0.0024(11) 0.0179(9) 0.0023(10) C14 0.0285(9) 0.0279(10) 0.0326(9) 0.0041(9) 0.0166(8) 0.0040(10) C12 0.0341(11) 0.0474(13) 0.0273(10) -0.0003(10) 0.0085(9) 0.0063(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O1 P1 O3 116.47(8) O1 P1 O2 116.24(8) O3 P1 O2 93.09(7) O1 P1 N1 111.00(8) O3 P1 N1 110.73(8) O2 P1 N1 107.94(8) C2 C1 H1A 109.5 C2 C1 H1B 109.5 H1A C1 H1B 109.5 C2 C1 H1C 109.5 H1A C1 H1C 109.5 H1B C1 H1C 109.5 C9 O2 P1 123.04(11) N1 C2 C3 112.69(15) N1 C2 C1 108.45(16) C3 C2 C1 110.84(16) N1 C2 H2 108.2 C3 C2 H2 108.2 C1 C2 H2 108.2 C8 C3 C4 118.89(18) C8 C3 C2 120.26(16) C4 C3 C2 120.82(16) C15 O3 P1 122.91(12) C2 N1 P1 126.51(13) C2 N1 H1N 119.1(16) P1 N1 H1N 113.7(16) C19 C20 C15 118.8(2) C19 C20 H20 120.6 C15 C20 H20 120.6 C20 C19 C18 120.4(2) C20 C19 H19 119.8 C18 C19 H19 119.8 C19 C18 C17 120.0(2) C19 C18 H18 120.0 C17 C18 H18 120.0 C18 C17 C16 120.4(2) C18 C17 H17 119.8 C16 C17 H17 119.8 C15 C16 C17 118.59(19) C15 C16 H16 120.7 C17 C16 H16 120.7 C16 C15 C20 121.77(19) C16 C15 O3 119.84(17) C20 C15 O3 118.15(17) C5 C4 C3 120.58(17) C5 C4 H4 119.7 C3 C4 H4 119.7 C4 C5 C6 120.17(19) C4 C5 H5 119.9 C6 C5 H5 119.9 C7 C6 C5 119.41(19) C7 C6 H6 120.3 C5 C6 H6 120.3 C14 C9 C10 121.59(18) C14 C9 O2 118.55(16) C10 C9 O2 119.61(18) C7 C8 C3 120.43(18) C7 C8 H8 119.8 C3 C8 H8 119.8 C6 C7 C8 120.50(18) C6 C7 H7 119.8 C8 C7 H7 119.8 C9 C10 C11 118.5(2) C9 C10 H10 120.8 C11 C10 H10 120.8 C12 C11 C10 120.5(2) C12 C11 H11 119.7 C10 C11 H11 119.7 C12 C13 C14 120.0(2) C12 C13 H13 120.0 C14 C13 H13 120.0 C9 C14 C13 119.20(19) C9 C14 H14 120.4 C13 C14 H14 120.4 C11 C12 C13 120.2(2) C11 C12 H12 119.9 C13 C12 H12 119.9 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance P1 O1 1.4658(13) P1 O3 1.5871(14) P1 O2 1.5913(14) P1 N1 1.6059(17) C1 C2 1.523(3) C1 H1A 0.9800 C1 H1B 0.9800 C1 H1C 0.9800 O2 C9 1.397(2) C2 N1 1.467(2) C2 C3 1.520(3) C2 H2 1.0000 C3 C8 1.392(3) C3 C4 1.393(3) O3 C15 1.399(2) N1 H1N 0.883(13) C20 C19 1.383(3) C20 C15 1.385(3) C20 H20 0.9500 C19 C18 1.384(3) C19 H19 0.9500 C18 C17 1.385(3) C18 H18 0.9500 C17 C16 1.388(3) C17 H17 0.9500 C16 C15 1.383(3) C16 H16 0.9500 C4 C5 1.387(3) C4 H4 0.9500 C5 C6 1.389(3) C5 H5 0.9500 C6 C7 1.385(3) C6 H6 0.9500 C9 C14 1.381(3) C9 C10 1.386(3) C8 C7 1.385(3) C8 H8 0.9500 C7 H7 0.9500 C10 C11 1.391(3) C10 H10 0.9500 C11 C12 1.380(3) C11 H11 0.9500 C13 C12 1.385(3) C13 C14 1.388(3) C13 H13 0.9500 C14 H14 0.9500 C12 H12 0.9500 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1N O1 2_545 0.883(13) 1.938(13) 2.815(2) 172(2) yes C7 H7 O2 2_645 0.95 2.47 3.352(2) 153.4 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion O1 P1 O2 C9 -51.61(17) O3 P1 O2 C9 -173.24(15) N1 P1 O2 C9 73.80(16) N1 C2 C3 C8 -136.12(18) C1 C2 C3 C8 102.1(2) N1 C2 C3 C4 45.4(2) C1 C2 C3 C4 -76.3(2) O1 P1 O3 C15 47.65(17) O2 P1 O3 C15 169.09(15) N1 P1 O3 C15 -80.41(16) C3 C2 N1 P1 96.74(19) C1 C2 N1 P1 -140.17(16) O1 P1 N1 C2 178.56(15) O3 P1 N1 C2 -50.46(18) O2 P1 N1 C2 50.09(18) C15 C20 C19 C18 -0.6(4) C20 C19 C18 C17 1.2(4) C19 C18 C17 C16 -1.4(4) C18 C17 C16 C15 1.0(3) C17 C16 C15 C20 -0.4(3) C17 C16 C15 O3 -174.65(18) C19 C20 C15 C16 0.2(3) C19 C20 C15 O3 174.51(19) P1 O3 C15 C16 -68.4(2) P1 O3 C15 C20 117.13(18) C8 C3 C4 C5 0.9(3) C2 C3 C4 C5 179.40(19) C3 C4 C5 C6 0.0(3) C4 C5 C6 C7 -0.6(3) P1 O2 C9 C14 -107.98(18) P1 O2 C9 C10 77.7(2) C4 C3 C8 C7 -1.3(3) C2 C3 C8 C7 -179.78(18) C5 C6 C7 C8 0.3(3) C3 C8 C7 C6 0.7(3) C14 C9 C10 C11 0.4(3) O2 C9 C10 C11 174.5(2) C9 C10 C11 C12 -0.7(4) C10 C9 C14 C13 0.0(3) O2 C9 C14 C13 -174.23(19) C12 C13 C14 C9 0.0(3) C10 C11 C12 C13 0.8(4) C14 C13 C12 C11 -0.4(4) _cod_database_fobs_code 2021471