#------------------------------------------------------------------------------ #$Date: 2019-05-18 08:19:18 +0300 (Sat, 18 May 2019) $ #$Revision: 215301 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/16/2021633.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021633 _cell_angle_alpha 90.000 _cell_angle_beta 98.040 _cell_angle_gamma 90.000 _cell_length_a 30.1842 _cell_length_b 5.8907 _cell_length_c 7.7144 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.8384 _cod_data_source_file ov3125Isup2.hkl _cod_data_source_block I _shelx_title ' SIR92 run in space group C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 277.94 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 16 0 0 49.99 42.81 2.45 o 18 0 0 367.98 385.33 13.46 o 20 0 0 61.49 52.60 3.06 o 22 0 0 354.57 361.48 12.84 o 24 0 0 317.77 307.65 11.62 o 26 0 0 80.49 80.12 4.28 o 28 0 0 201.39 131.88 8.06 o 30 0 0 5.36 5.35 1.09 o 32 0 0 1.60 -0.29 3.38 o 34 0 0 8.18 8.32 1.36 o 3 1 0 5182.50 5147.17 104.05 o 5 1 0 1139.11 1016.04 28.75 o 15 1 0 28.12 26.03 1.30 o 17 1 0 6.54 6.12 0.61 o 19 1 0 3.75 5.83 0.86 o 21 1 0 5.13 7.34 1.83 o 23 1 0 13.25 11.82 1.47 o 25 1 0 243.69 250.16 9.79 o 27 1 0 0.63 2.42 1.05 o 29 1 0 2.51 2.17 1.28 o 31 1 0 0.55 -0.40 1.76 o 33 1 0 0.82 -0.32 1.31 o 35 1 0 0.37 0.19 0.55 o 0 2 0 5475.25 4498.00 147.41 o 2 2 0 689.39 628.14 16.72 o 4 2 0 212.98 211.97 4.64 o 6 2 0 1.37 1.02 0.48 o 8 2 0 14.62 13.46 1.02 o 10 2 0 2111.34 2392.74 104.59 o 12 2 0 370.45 343.95 11.32 o 14 2 0 1106.71 1085.06 30.70 o 16 2 0 772.61 753.36 20.89 o 18 2 0 8.02 9.37 1.02 o 20 2 0 105.21 100.76 3.14 o 22 2 0 3.55 2.22 0.78 o 24 2 0 16.10 14.51 1.37 o 26 2 0 2.78 3.30 0.67 o 28 2 0 25.42 26.89 4.17 o 30 2 0 6.22 4.65 1.64 o 32 2 0 2.97 0.00 2.75 o 34 2 0 0.19 -0.85 1.35 o 1 3 0 0.52 0.82 0.35 o 3 3 0 832.76 832.50 21.61 o 5 3 0 8.19 8.60 0.66 o 7 3 0 49.69 44.61 1.35 o 9 3 0 57.44 63.16 2.99 o 11 3 0 210.34 191.15 6.44 o 13 3 0 0.49 0.61 0.86 o 15 3 0 34.08 39.44 3.06 o 17 3 0 9.13 8.99 1.47 o 19 3 0 66.82 61.63 1.67 o 21 3 0 5.58 4.36 1.77 o 23 3 0 9.63 8.40 0.89 o 25 3 0 23.64 30.43 7.91 o 27 3 0 0.02 0.39 0.70 o 29 3 0 0.12 2.80 1.21 o 31 3 0 1.05 -0.12 0.92 o 0 4 0 322.37 326.62 11.62 o 2 4 0 44.21 38.25 1.73 o 4 4 0 5.47 1.63 1.53 o 6 4 0 63.94 63.66 2.16 o 8 4 0 5.14 7.34 1.22 o 10 4 0 229.97 238.54 9.17 o 12 4 0 19.77 21.35 1.00 o 14 4 0 224.48 229.87 4.68 o 16 4 0 186.30 184.69 3.57 o 18 4 0 154.94 156.45 2.84 o 20 4 0 16.99 17.81 1.03 o 22 4 0 6.65 6.53 0.89 o 24 4 0 6.43 5.59 1.02 o 26 4 0 0.49 -0.41 0.61 o 28 4 0 0.22 -0.61 0.61 o 1 5 0 0.99 0.92 0.65 o 3 5 0 0.34 0.51 0.39 o 5 5 0 8.24 8.11 0.78 o 7 5 0 121.47 111.66 2.76 o 9 5 0 1.57 1.69 0.51 o 11 5 0 105.80 112.05 2.71 o 13 5 0 12.37 10.26 0.97 o 15 5 0 8.89 7.78 0.88 o 17 5 0 1.40 2.34 0.54 o 19 5 0 10.19 10.97 0.80 o 21 5 0 3.65 2.71 0.50 o 23 5 0 7.09 5.83 0.86 o 25 5 0 0.06 1.83 1.22 o 0 6 0 38.17 46.81 2.16 o 2 6 0 11.16 15.62 1.32 o 4 6 0 0.59 2.67 0.66 o 6 6 0 0.03 0.31 0.65 o 8 6 0 0.66 1.22 0.73 o 10 6 0 19.61 23.09 1.09 o 12 6 0 11.72 12.16 2.14 o 14 6 0 12.32 12.23 1.83 o 16 6 0 9.44 9.79 1.83 o 1 7 0 1.82 1.83 0.61 o -35 1 1 0.01 0.72 0.86 o -33 1 1 2.72 -0.02 1.30 o -31 1 1 0.27 -2.81 6.73 o -29 1 1 10.75 7.23 3.15 o -27 1 1 21.12 23.49 6.73 o -25 1 1 0.04 1.22 1.83 o -23 1 1 543.09 537.34 18.04 o -21 1 1 13.89 14.47 1.09 o -19 1 1 71.64 81.52 2.94 o -17 1 1 58.40 55.05 3.06 o -15 1 1 1.54 3.67 0.61 o -7 1 1 859.29 763.94 25.08 o -5 1 1 162.05 134.56 4.89 o -3 1 1 13924.45 12905.60 417.75 o -1 1 1 2237.09 2378.67 77.07 o 5 1 1 1364.12 1277.72 55.66 o 7 1 1 1313.52 1320.53 57.49 o 13 1 1 261.92 263.62 9.17 o 15 1 1 1296.22 1309.21 31.86 o 17 1 1 7.86 11.01 1.22 o 19 1 1 11.66 13.45 1.16 o 21 1 1 23.84 24.45 1.26 o 23 1 1 0.23 -0.11 0.55 o 25 1 1 276.87 276.05 23.04 o 27 1 1 0.28 -0.08 1.13 o 29 1 1 0.01 -0.87 0.87 o 31 1 1 0.10 -1.54 1.54 o 33 1 1 0.59 0.77 1.37 o -34 2 1 0.00 -0.83 0.86 o -32 2 1 2.16 1.74 1.27 o -30 2 1 1.72 1.42 0.52 o -28 2 1 0.14 0.38 0.50 o -26 2 1 81.31 85.68 5.68 o -24 2 1 5.98 6.18 1.30 o -22 2 1 15.07 15.39 1.00 o -20 2 1 12.04 10.64 1.15 o -18 2 1 27.77 28.08 2.03 o -16 2 1 133.41 136.58 3.32 o -14 2 1 112.53 107.30 3.01 o -12 2 1 9.62 12.98 1.83 o -10 2 1 1.63 3.58 0.92 o -8 2 1 126.92 139.97 4.07 o -6 2 1 279.22 245.79 5.37 o -4 2 1 214.23 204.87 4.59 o -2 2 1 273.80 250.76 5.37 o 0 2 1 1245.52 1164.22 30.83 o 2 2 1 94.97 118.66 4.28 o 4 2 1 10.70 13.83 0.78 o 6 2 1 284.48 245.47 7.30 o 8 2 1 205.70 205.02 4.04 o 10 2 1 0.35 0.41 0.38 o 12 2 1 145.42 155.39 4.53 o 14 2 1 79.02 69.44 2.35 o 16 2 1 121.87 109.11 2.97 o 18 2 1 42.67 41.38 1.35 o 20 2 1 39.25 37.11 1.62 o 22 2 1 72.59 72.87 2.15 o 24 2 1 31.19 33.49 4.15 o 26 2 1 2.91 0.46 2.58 o 28 2 1 14.52 12.11 3.11 o 30 2 1 5.28 4.06 3.03 o 32 2 1 1.00 0.90 1.33 o -31 3 1 0.39 -0.56 0.56 o -29 3 1 3.99 2.67 3.06 o -27 3 1 3.01 2.36 0.79 o -25 3 1 1.61 1.53 0.50 o -23 3 1 72.65 80.01 2.03 o -21 3 1 0.32 1.35 0.48 o -19 3 1 59.41 54.17 1.64 o -17 3 1 24.11 27.43 1.91 o -15 3 1 5.43 5.31 0.72 o -13 3 1 12.54 9.88 0.92 o -11 3 1 28.61 24.87 1.28 o -9 3 1 153.98 143.62 3.64 o -7 3 1 169.07 163.28 4.00 o -5 3 1 22.67 23.50 0.97 o -3 3 1 951.52 972.29 17.60 o -1 3 1 223.78 231.72 5.15 o 1 3 1 985.25 1109.68 21.92 o 3 3 1 320.23 306.19 6.57 o 5 3 1 214.67 212.04 7.74 o 7 3 1 34.93 32.02 1.07 o 9 3 1 0.50 0.08 0.37 o 11 3 1 99.04 110.03 2.78 o 13 3 1 26.76 30.58 1.47 o 15 3 1 84.24 78.21 2.87 o 17 3 1 4.73 2.83 0.78 o 19 3 1 4.32 3.67 0.78 o 21 3 1 17.44 15.03 6.44 o 23 3 1 1.78 1.29 1.94 o 25 3 1 52.61 64.74 10.86 o 27 3 1 0.34 1.69 1.55 o 29 3 1 1.32 13.46 10.40 o -28 4 1 3.34 5.43 0.99 o -26 4 1 1.84 0.61 1.30 o -24 4 1 5.30 3.85 0.48 o -22 4 1 0.28 0.20 0.43 o -20 4 1 2.11 1.31 0.41 o -18 4 1 1.37 1.38 0.39 o -16 4 1 98.11 96.89 3.27 o -14 4 1 27.07 28.50 1.40 o -12 4 1 2.87 4.60 0.79 o -10 4 1 65.17 63.00 3.67 o -8 4 1 8.65 7.15 0.92 o -6 4 1 4.34 3.29 0.50 o -4 4 1 35.44 33.77 1.28 o -2 4 1 0.98 1.49 0.34 o 0 4 1 74.68 71.40 2.38 o 2 4 1 163.45 166.35 4.08 o 4 4 1 28.35 26.92 1.44 o 6 4 1 31.75 31.12 1.32 o 8 4 1 24.32 22.82 1.47 o 10 4 1 61.99 59.45 2.35 o 12 4 1 0.12 0.76 0.54 o 14 4 1 14.08 12.58 0.82 o 16 4 1 9.24 8.62 0.97 o 18 4 1 33.25 33.70 1.46 o 20 4 1 0.36 0.00 0.71 o 22 4 1 12.66 14.63 1.15 o 24 4 1 0.32 1.83 1.83 o 26 4 1 2.30 1.83 1.22 o 28 4 1 0.01 -0.61 1.22 o -25 5 1 2.86 1.83 1.22 o -23 5 1 1.20 0.00 0.61 o -21 5 1 2.30 3.54 0.90 o -19 5 1 5.76 6.30 0.62 o -17 5 1 23.83 26.25 1.03 o -15 5 1 21.26 21.20 1.68 o -13 5 1 122.89 125.27 2.96 o -11 5 1 19.81 21.75 1.33 o -9 5 1 11.54 9.94 0.75 o -7 5 1 191.25 198.85 4.58 o -5 5 1 126.36 123.02 2.63 o -3 5 1 38.72 34.88 1.43 o -1 5 1 21.61 20.34 1.12 o 1 5 1 0.06 1.02 0.71 o 3 5 1 18.79 21.77 1.93 o 5 5 1 11.18 11.46 0.71 o 7 5 1 201.33 199.29 3.71 o 9 5 1 144.37 147.54 3.68 o 11 5 1 17.81 16.06 0.92 o 13 5 1 38.34 42.70 2.06 o 15 5 1 39.94 40.87 1.74 o 17 5 1 21.39 20.58 1.85 o 19 5 1 1.19 1.27 0.63 o 21 5 1 0.01 -0.20 0.61 o 23 5 1 0.00 1.22 1.22 o -16 6 1 5.08 4.28 1.22 o -14 6 1 1.56 1.99 0.58 o -12 6 1 6.33 6.89 0.66 o -10 6 1 5.67 5.46 0.50 o -8 6 1 25.69 25.02 1.41 o -6 6 1 3.15 3.88 0.43 o -4 6 1 2.50 2.11 0.46 o -2 6 1 1.08 2.06 0.78 o 0 6 1 1.09 2.60 0.78 o 2 6 1 1.35 1.63 0.96 o 4 6 1 0.00 1.21 0.62 o 6 6 1 22.85 26.25 1.41 o 8 6 1 0.01 -0.25 0.63 o 10 6 1 3.20 1.45 1.57 o 12 6 1 19.21 16.34 2.14 o 14 6 1 0.19 0.20 1.09 o 16 6 1 13.94 11.82 1.47 o -32 0 2 0.77 1.53 0.86 o -30 0 2 0.87 0.61 1.02 o -28 0 2 45.84 53.73 3.36 o -24 0 2 69.41 58.72 4.28 o -22 0 2 140.31 133.95 7.34 o -20 0 2 266.63 261.17 12.23 o -18 0 2 23.93 23.03 1.47 o -16 0 2 1884.48 2067.34 74.62 o -14 0 2 15.75 12.23 1.22 o -12 0 2 2.30 3.67 0.61 o -10 0 2 247.11 263.62 9.17 o -6 0 2 156.14 154.74 5.50 o -4 0 2 5024.83 5144.50 167.59 o 0 0 2 2888.33 2893.67 94.19 o 2 0 2 77252.02 61164.00 1993.95 o 12 0 2 1517.70 1478.95 48.32 o 14 0 2 25.71 20.18 1.83 o 16 0 2 1.56 0.41 0.55 o 18 0 2 8.47 8.09 1.02 o 20 0 2 35.43 40.86 1.48 o 22 0 2 66.46 74.58 2.19 o 24 0 2 99.07 110.81 21.79 o 26 0 2 36.32 44.85 9.15 o 28 0 2 10.77 10.21 1.73 o 30 0 2 10.87 10.71 5.98 o 32 0 2 3.05 2.26 1.50 o -35 1 2 0.00 -0.31 3.67 o -33 1 2 0.06 -0.05 0.41 o -31 1 2 0.98 0.11 0.50 o -29 1 2 6.75 8.22 2.90 o -27 1 2 72.73 63.05 6.53 o -25 1 2 15.04 19.57 2.45 o -23 1 2 166.29 164.44 5.43 o -21 1 2 1.56 2.75 0.86 o -19 1 2 124.51 143.78 4.70 o -17 1 2 279.62 268.67 7.92 o -15 1 2 10.60 14.07 1.22 o -13 1 2 116.39 135.78 6.12 o -9 1 2 63.72 62.39 2.45 o -7 1 2 1001.65 869.14 28.75 o -5 1 2 26.09 30.58 1.22 o -3 1 2 12480.52 11914.43 272.90 o -1 1 2 15921.33 15674.70 316.63 o 1 1 2 7478.95 7649.17 247.71 o 11 1 2 1727.46 1633.69 53.21 o 13 1 2 148.31 153.95 3.53 o 15 1 2 87.19 76.22 1.97 o 17 1 2 3.66 4.68 0.62 o 19 1 2 4.60 5.57 0.62 o 21 1 2 55.12 52.50 1.48 o 23 1 2 12.90 11.96 2.66 o 25 1 2 13.29 13.81 1.60 o 27 1 2 128.88 128.58 8.34 o 29 1 2 1.15 -0.90 2.05 o 31 1 2 0.25 -1.29 2.10 o 33 1 2 0.29 -0.34 1.07 o -34 2 2 0.91 0.49 0.84 o -32 2 2 0.08 -0.70 0.97 o -30 2 2 0.69 0.63 0.98 o -28 2 2 7.30 8.33 1.50 o -26 2 2 25.03 26.44 1.98 o -24 2 2 16.86 20.08 1.26 o -22 2 2 21.98 25.81 1.62 o -20 2 2 5.30 7.70 1.93 o -18 2 2 36.90 28.94 1.62 o -16 2 2 49.97 52.37 2.79 o -14 2 2 683.93 683.15 18.16 o -12 2 2 1094.18 1137.25 29.41 o -10 2 2 1006.61 960.72 29.02 o -8 2 2 611.87 632.44 23.24 o -6 2 2 166.24 137.37 3.39 o -4 2 2 7.18 5.58 0.41 o -2 2 2 102.71 109.53 2.25 o 0 2 2 557.79 553.12 11.82 o 2 2 2 1584.51 1609.67 37.63 o 4 2 2 175.78 163.13 3.53 o 6 2 2 1.24 1.92 0.62 o 8 2 2 36.69 29.93 1.04 o 10 2 2 9.93 8.27 0.86 o 12 2 2 464.09 520.15 13.14 o 14 2 2 25.35 22.88 1.15 o 16 2 2 45.38 43.43 1.53 o 18 2 2 76.83 74.71 1.69 o 20 2 2 0.11 0.45 0.44 o 22 2 2 129.97 126.19 4.76 o 24 2 2 15.40 21.66 1.50 o 26 2 2 6.51 3.45 2.36 o 28 2 2 0.63 0.62 0.85 o 30 2 2 5.42 9.91 2.56 o 32 2 2 2.31 1.05 1.17 o -31 3 2 7.53 6.29 1.80 o -29 3 2 0.84 -0.76 0.76 o -27 3 2 0.09 0.59 0.74 o -25 3 2 4.16 4.40 1.04 o -23 3 2 38.69 37.15 1.85 o -21 3 2 10.44 7.67 0.60 o -19 3 2 0.15 0.55 0.56 o -17 3 2 335.46 331.41 6.44 o -15 3 2 3.92 7.46 0.80 o -13 3 2 87.71 88.63 2.25 o -11 3 2 179.43 182.22 7.34 o -9 3 2 5.65 5.65 1.53 o -7 3 2 34.81 32.97 1.46 o -5 3 2 18.73 19.34 0.88 o -3 3 2 0.07 1.06 0.92 o -1 3 2 450.35 473.78 8.99 o 1 3 2 3.26 5.40 0.41 o 3 3 2 14.75 17.16 1.15 o 5 3 2 117.92 132.65 2.89 o 7 3 2 95.22 98.26 2.28 o 9 3 2 0.06 1.02 0.50 o 11 3 2 420.49 458.25 11.84 o 13 3 2 452.00 492.31 9.36 o 15 3 2 19.43 20.36 1.20 o 17 3 2 104.05 101.43 2.13 o 19 3 2 23.94 27.71 3.17 o 21 3 2 37.64 34.64 3.08 o 23 3 2 0.34 0.39 0.86 o 25 3 2 0.28 1.03 2.09 o 27 3 2 1.55 1.10 0.89 o -28 4 2 0.10 0.06 1.74 o -26 4 2 0.05 0.12 0.41 o -24 4 2 0.11 -0.31 0.50 o -22 4 2 0.01 -0.73 0.89 o -20 4 2 7.02 7.58 1.21 o -18 4 2 0.74 0.67 0.42 o -16 4 2 188.20 186.71 3.44 o -14 4 2 248.22 231.88 5.62 o -12 4 2 133.74 136.30 3.32 o -10 4 2 0.26 0.61 0.86 o -8 4 2 150.70 150.93 3.85 o -6 4 2 140.49 131.32 3.37 o -4 4 2 58.81 55.62 1.66 o -2 4 2 34.99 38.00 1.59 o 0 4 2 107.03 108.02 2.93 o 2 4 2 119.93 116.61 3.44 o 4 4 2 5.31 4.75 0.66 o 6 4 2 103.59 98.06 2.39 o 8 4 2 34.58 35.10 1.35 o 10 4 2 24.00 22.50 1.70 o 12 4 2 76.33 75.03 2.28 o 14 4 2 12.96 11.12 1.06 o 16 4 2 55.45 54.96 1.74 o 18 4 2 55.09 59.30 2.88 o 20 4 2 30.06 32.48 1.86 o 22 4 2 37.83 50.49 2.75 o 24 4 2 2.80 4.53 1.22 o 26 4 2 6.59 7.05 1.22 o -23 5 2 0.46 0.20 0.35 o -21 5 2 0.98 0.49 0.41 o -19 5 2 11.19 8.46 0.48 o -17 5 2 30.35 31.06 1.32 o -15 5 2 13.43 15.82 0.94 o -13 5 2 2.33 0.61 0.46 o -11 5 2 10.28 7.56 0.73 o -9 5 2 41.45 44.21 1.54 o -7 5 2 3.74 2.45 0.50 o -5 5 2 27.84 24.46 1.14 o -3 5 2 7.25 5.83 0.62 o -1 5 2 12.37 11.15 0.76 o 1 5 2 0.75 1.35 0.46 o 3 5 2 1.38 0.85 0.60 o 5 5 2 0.00 0.27 0.88 o 7 5 2 8.82 7.74 1.06 o 9 5 2 55.17 48.16 4.51 o 11 5 2 0.80 0.00 0.86 o 13 5 2 56.87 61.20 2.21 o 15 5 2 1.10 1.96 0.72 o 17 5 2 9.58 9.64 1.06 o 19 5 2 6.20 6.46 1.22 o 21 5 2 0.65 0.20 0.55 o -16 6 2 3.75 6.73 1.83 o -14 6 2 1.06 1.22 0.92 o -12 6 2 9.29 9.15 0.79 o -10 6 2 47.92 51.30 2.12 o -8 6 2 1.37 1.93 0.68 o -6 6 2 1.29 1.53 0.61 o -4 6 2 7.25 11.20 1.41 o -2 6 2 0.57 1.08 0.57 o 0 6 2 0.61 0.31 0.50 o 2 6 2 25.40 31.73 1.64 o 4 6 2 24.75 26.83 1.77 o 6 6 2 0.57 -0.30 0.53 o 8 6 2 7.15 4.69 2.45 o 10 6 2 13.75 15.38 2.04 o 12 6 2 15.05 12.39 1.83 o 14 6 2 0.04 -0.20 1.22 o -33 1 3 0.00 0.82 0.55 o -31 1 3 0.09 0.00 0.71 o -29 1 3 0.73 1.11 0.66 o -27 1 3 22.97 25.90 1.62 o -25 1 3 32.74 35.30 2.35 o -23 1 3 19.73 23.78 1.91 o -21 1 3 208.27 219.60 7.05 o -19 1 3 0.02 -0.31 0.92 o -17 1 3 280.58 308.96 9.23 o -15 1 3 279.82 305.22 9.05 o -13 1 3 38.44 43.08 2.14 o -11 1 3 1600.21 1641.25 33.09 o -9 1 3 224.70 226.83 4.79 o -7 1 3 301.15 298.88 7.35 o -5 1 3 0.36 0.00 1.22 o -1 1 3 5521.26 5791.97 132.99 o 1 1 3 53.32 51.99 1.83 o 7 1 3 3.92 2.79 0.43 o 9 1 3 794.43 836.24 20.46 o 11 1 3 158.79 158.21 4.32 o 13 1 3 24.71 33.25 1.16 o 15 1 3 56.36 58.66 1.35 o 17 1 3 117.42 121.80 2.08 o 19 1 3 19.91 21.63 0.91 o 21 1 3 9.41 11.02 0.98 o 23 1 3 18.09 20.67 1.59 o 25 1 3 1.53 0.46 0.86 o 27 1 3 26.60 27.54 2.71 o 29 1 3 2.31 1.27 1.00 o 31 1 3 1.97 1.91 1.64 o -32 2 3 0.04 0.12 0.44 o -30 2 3 0.52 0.10 0.56 o -28 2 3 0.17 0.44 0.59 o -26 2 3 24.54 28.77 1.40 o -24 2 3 164.79 175.28 3.95 o -22 2 3 15.06 13.48 1.19 o -20 2 3 37.06 35.86 1.48 o -18 2 3 0.41 0.00 0.71 o -16 2 3 73.93 70.38 2.47 o -14 2 3 100.25 108.94 3.77 o -12 2 3 1.91 20.18 1.83 o -10 2 3 0.72 0.00 0.55 o -8 2 3 6.83 5.83 0.86 o -6 2 3 114.26 103.88 2.05 o -4 2 3 41.98 48.30 1.35 o -2 2 3 2497.56 2590.03 52.01 o 0 2 3 1566.35 1518.85 30.86 o 2 2 3 714.35 707.94 14.67 o 4 2 3 282.51 310.26 5.79 o 6 2 3 2.73 1.33 0.65 o 8 2 3 5.12 2.87 0.46 o 10 2 3 41.50 42.77 1.35 o 12 2 3 63.25 60.72 1.74 o 14 2 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