#------------------------------------------------------------------------------ #$Date: 2021-06-11 08:04:54 +0300 (Fri, 11 Jun 2021) $ #$Revision: 266390 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/23/2022391.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022391 loop_ _publ_author_name 'Thomsen, Maria Storm' 'Madsen, Anders \/O.' 'S\/orensen, Thomas Just' _publ_section_title ; Crystal structure and optical properties of a two-sited Eu^III^ compound: an Eu^III^ ion coordinated by two [Eu^III^(DOTA)]^{-^} complexes (DOTA is 1,4,7,10-tetraazacyclododecane-1,4,7,10-tetraacetate) ; _journal_coeditor_code YD3018 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229621005647 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac ; Na [Eu O5 (O H) (H2 O)2] [Eu (C16 H24 N4 O8) (H2 O)]2 Cl, xH2 O1 ; _chemical_formula_moiety ; C32 H55 Eu3 N8 O21, Cl, H4 Na O2, 2.101(O), 4(H2 O), H1.63 O0.505, H O0.25, H2 O2 ; _chemical_formula_sum 'C32 H72.64 Cl Eu3 N8 Na O32.04' _chemical_formula_weight 1596.65 _chemical_name_systematic ; Poly[sodium [tetraaquahydroxidopentaoxido\ bis(\m-1,4,7,10-tetrazacyclododecane-1,4,7,10-tetraacetato)trieuropium(III)] chloride hydrate] ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _cell_angle_alpha 96.37(3) _cell_angle_beta 92.39(3) _cell_angle_gamma 93.26(3) _cell_formula_units_Z 2 _cell_length_a 9.2252(18) _cell_length_b 16.937(3) _cell_length_c 17.274(4) _cell_measurement_reflns_used 5559 _cell_measurement_temperature 100 _cell_measurement_theta_max 32.087 _cell_measurement_theta_min 2.213 _cell_volume 2674.9(10) _computing_cell_refinement ; SAINT (Bruker, 2009) ; _computing_data_collection ; APEX2 (Bruker, 2009) ; _computing_data_reduction ; SAINT (Bruker, 2009) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009), CELL_NOW (Sheldrick, 2008) and TWINABS (Sheldrick, 2012) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296.15 _diffrn_measured_fraction_theta_full 0.985 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0765 _diffrn_reflns_av_unetI/netI 0.0407 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_number 9966 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.679 _diffrn_reflns_theta_min 1.598 _diffrn_source_current 1.0 _diffrn_source_power 0.05 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 3.634 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details ; (TWINABS; Sheldrick, 2012) ; _exptl_crystal_colour 'clear whiteish colourless' _exptl_crystal_density_diffrn 1.980 _exptl_crystal_description plate _exptl_crystal_F_000 1587 _exptl_crystal_size_max 1.198 _exptl_crystal_size_mid 0.711 _exptl_crystal_size_min 0.12 _refine_diff_density_max 3.468 _refine_diff_density_min -1.940 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 759 _refine_ls_number_reflns 9966 _refine_ls_number_restraints 907 _refine_ls_restrained_S_all 1.002 _refine_ls_R_factor_all 0.0813 _refine_ls_R_factor_gt 0.0622 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0915P)^2^+70.0229P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1576 _refine_ls_wR_factor_ref 0.1707 _reflns_number_gt 8308 _reflns_number_total 9966 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yd3018sup1.cif _cod_data_source_block I _cod_original_cell_volume 2674.9(9) _cod_database_code 2022391 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.098 _shelx_estimated_absorpt_t_max 0.670 _shelx_hkl_file ; 1 0 0 462.15 9.40 2 0 0 595.94 7.80 3 0 0 19.40 0.90 4 0 0 138.99 2.80 5 0 0 0.00 3.20 6 0 0 1453.65 21.90 7 0 0 4.50 3.70 8 0 0 388.76 9.40 9 0 0 133.89 11.00 10 0 0 75.19 5.90 11 0 0 100.89 10.80 -11 1 0 117.39 13.70 -10 1 0 85.79 15.20 -9 1 0 501.35 20.40 -8 1 0 3.00 5.70 -7 1 0 1238.78 24.00 -6 1 0 86.79 4.20 -5 1 0 1505.75 21.10 -4 1 0 3.90 1.00 -3 1 0 58.79 1.70 -2 1 0 519.25 7.50 -1 1 0 641.14 22.50 1 1 0 67.89 1.70 2 1 0 1019.70 13.00 3 1 0 505.55 6.70 4 1 0 3358.76 60.09 5 1 0 560.74 10.70 6 1 0 1250.17 18.80 7 1 0 114.69 4.30 8 1 0 265.17 6.80 9 1 0 8.10 5.90 10 1 0 1330.97 26.80 11 1 0 36.40 11.90 -11 2 0 17.50 36.40 -10 2 0 38.00 34.40 -9 2 0 942.51 28.80 -8 2 0 156.38 8.30 -7 2 0 72.69 7.60 -6 2 0 80.19 4.70 -5 2 0 941.01 13.90 -4 2 0 120.59 3.00 -3 2 0 4261.17 70.69 -2 2 0 95.39 2.20 -1 2 0 1578.24 20.80 0 2 0 1857.31 38.50 1 2 0 287.27 3.70 2 2 0 58.89 1.50 3 2 0 2641.84 36.60 4 2 0 177.08 4.10 5 2 0 982.40 15.70 6 2 0 14.90 2.00 7 2 0 107.09 6.80 8 2 0 451.95 10.70 9 2 0 12.90 4.70 10 2 0 40.70 9.60 11 2 0 28.30 80.59 -11 3 0 0.00 52.99 -10 3 0 1632.34 48.40 -9 3 0 102.59 9.70 -8 3 0 406.16 12.60 -7 3 0 26.00 5.00 -6 3 0 8.70 2.60 -5 3 0 78.09 3.10 -4 3 0 1213.18 20.80 -3 3 0 601.24 10.40 -2 3 0 172.08 3.20 -1 3 0 1112.89 14.60 0 3 0 127.69 2.30 1 3 0 3094.29 40.20 2 3 0 1647.74 27.80 3 3 0 337.47 5.90 4 3 0 6.00 1.10 5 3 0 1291.17 19.40 6 3 0 5.40 3.50 7 3 0 2805.12 42.80 8 3 0 282.07 10.00 9 3 0 1063.19 24.30 10 3 0 242.88 31.80 -11 4 0 20.20 12.70 -10 4 0 11.20 8.50 -9 4 0 0.00 7.90 -8 4 0 509.55 12.60 -7 4 0 21.10 3.50 -6 4 0 3920.51 113.29 -5 4 0 510.85 10.10 -4 4 0 827.42 20.60 -3 4 0 722.63 11.80 -2 4 0 140.19 3.10 -1 4 0 20.20 1.10 0 4 0 432.86 8.10 1 4 0 1130.29 14.40 2 4 0 40.70 1.20 3 4 0 326.47 5.60 4 4 0 281.67 6.40 5 4 0 410.46 11.50 6 4 0 272.47 5.80 7 4 0 60.39 5.30 8 4 0 51.19 3.80 9 4 0 318.97 33.10 10 4 0 40.70 14.60 -11 5 0 211.28 17.40 -10 5 0 54.69 12.50 -9 5 0 103.79 7.50 -8 5 0 42.90 6.70 -7 5 0 291.97 8.30 -6 5 0 13.90 3.60 -5 5 0 329.47 7.30 -4 5 0 4.90 1.70 -3 5 0 3.20 1.30 -2 5 0 2989.40 45.60 -1 5 0 169.38 3.90 0 5 0 63.09 2.30 1 5 0 32.70 1.20 2 5 0 2285.37 27.20 3 5 0 449.76 8.20 4 5 0 2704.63 43.20 5 5 0 1182.08 21.90 6 5 0 904.91 16.00 7 5 0 429.56 10.80 8 5 0 175.88 7.40 9 5 0 0.00 6.20 10 5 0 342.87 15.20 -10 6 0 55.99 16.60 -9 6 0 842.52 19.70 -8 6 0 610.94 13.60 -7 6 0 637.14 14.10 -6 6 0 665.73 12.50 -5 6 0 558.74 9.60 -4 6 0 47.40 2.70 -3 6 0 4186.88 60.29 -2 6 0 1489.45 31.40 -1 6 0 1041.00 15.90 0 6 0 1126.89 16.20 1 6 0 60.89 1.90 2 6 0 219.48 4.00 3 6 0 2.70 1.50 4 6 0 595.44 10.80 5 6 0 159.88 6.70 6 6 0 437.06 11.70 7 6 0 153.68 7.50 8 6 0 569.54 11.70 9 6 0 239.38 10.90 10 6 0 340.57 15.10 -10 7 0 230.28 20.50 -9 7 0 90.39 9.60 -8 7 0 292.07 16.60 -7 7 0 139.89 6.90 -6 7 0 436.06 9.00 -5 7 0 570.44 11.60 -4 7 0 211.78 8.30 -3 7 0 93.89 3.50 -2 7 0 76.79 2.60 -1 7 0 1194.68 17.50 0 7 0 612.84 9.40 1 7 0 3910.71 52.69 2 7 0 2939.71 37.10 3 7 0 1237.88 22.30 4 7 0 999.00 19.90 5 7 0 138.79 5.70 6 7 0 59.69 9.60 7 7 0 1117.39 23.80 8 7 0 332.37 12.30 9 7 0 237.48 15.30 10 7 0 110.39 55.69 -10 8 0 25.20 10.50 -9 8 0 44.00 11.40 -8 8 0 455.05 36.90 -7 8 0 349.17 15.90 -6 8 0 2092.69 42.80 -5 8 0 951.80 17.00 -4 8 0 381.16 9.60 -3 8 0 5.80 1.90 -2 8 0 6.90 1.30 -1 8 0 69.09 3.00 0 8 0 331.17 7.70 1 8 0 589.74 10.00 2 8 0 298.77 5.50 3 8 0 555.94 8.60 4 8 0 489.45 9.60 5 8 0 424.66 10.70 6 8 0 58.59 7.80 7 8 0 230.68 11.40 8 8 0 314.37 43.40 10 8 0 68.79 29.80 -10 9 0 13.00 14.40 -9 9 0 229.58 20.30 -8 9 0 469.65 19.60 -7 9 0 62.69 9.20 -6 9 0 183.38 6.10 -5 9 0 3.80 6.80 -4 9 0 938.31 17.20 -3 9 0 401.56 8.20 -2 9 0 4805.72 69.69 -1 9 0 3547.75 62.59 0 9 0 388.26 8.00 1 9 0 1789.22 27.60 2 9 0 524.35 8.40 3 9 0 22.90 1.90 4 9 0 1203.78 17.90 5 9 0 305.07 5.60 6 9 0 686.63 16.60 7 9 0 209.88 12.50 8 9 0 110.99 26.50 9 9 0 84.49 22.00 -10 10 0 113.89 36.50 -9 10 0 409.06 17.20 -8 10 0 1070.69 22.00 -7 10 0 164.28 6.80 -6 10 0 63.59 6.20 -5 10 0 6.60 5.10 -4 10 0 2.30 4.60 -3 10 0 397.36 14.60 -2 10 0 1113.69 18.70 -1 10 0 25.10 3.10 0 10 0 210.28 5.70 1 10 0 1615.94 24.10 2 10 0 422.76 7.50 3 10 0 363.96 11.30 4 10 0 163.48 4.60 5 10 0 96.09 8.10 6 10 0 153.28 7.70 7 10 0 685.83 19.50 8 10 0 510.55 19.20 9 10 0 902.81 37.30 -9 11 0 0.00 10.90 -8 11 0 8.20 6.00 -7 11 0 232.08 9.70 -6 11 0 514.35 11.50 -5 11 0 484.65 10.20 -4 11 0 986.90 16.70 -3 11 0 405.86 8.00 -2 11 0 955.60 19.60 -1 11 0 167.98 6.60 0 11 0 200.88 6.30 1 11 0 1699.13 29.00 2 11 0 1818.62 27.70 3 11 0 174.68 5.70 4 11 0 520.75 19.70 5 11 0 59.29 5.00 6 11 0 110.29 6.10 7 11 0 0.00 10.80 8 11 0 199.48 14.40 9 11 0 62.79 22.90 -9 12 0 279.07 17.70 -8 12 0 28.70 11.50 -7 12 0 22.60 5.70 -6 12 0 292.97 11.00 -5 12 0 279.37 8.90 -4 12 0 161.38 5.80 -3 12 0 16.70 7.70 -2 12 0 549.25 10.90 -1 12 0 569.14 11.10 0 12 0 68.49 6.20 1 12 0 33.40 5.10 2 12 0 80.69 14.60 3 12 0 391.06 12.20 4 12 0 582.24 20.10 5 12 0 954.40 23.10 6 12 0 1320.37 29.10 7 12 0 147.09 9.20 8 12 0 575.34 46.70 -9 13 0 324.27 30.60 -8 13 0 262.37 25.40 -7 13 0 736.63 21.30 -6 13 0 0.00 9.30 -5 13 0 429.76 13.50 -4 13 0 259.77 9.10 -3 13 0 309.17 7.80 -2 13 0 1175.18 19.50 -1 13 0 2019.50 31.90 0 13 0 288.17 7.40 1 13 0 536.45 10.80 2 13 0 0.50 3.30 3 13 0 342.57 8.60 4 13 0 0.00 8.30 5 13 0 283.27 15.30 6 13 0 91.49 10.50 7 13 0 55.49 21.70 -8 14 0 569.24 33.40 -7 14 0 52.89 9.20 -6 14 0 109.59 23.20 -5 14 0 294.97 11.70 -4 14 0 6.30 7.00 -3 14 0 654.43 21.00 -2 14 0 241.48 8.70 -1 14 0 54.49 6.30 0 14 0 266.17 10.50 1 14 0 1305.17 22.40 2 14 0 310.67 8.20 3 14 0 1936.51 29.10 4 14 0 140.89 5.20 5 14 0 1112.29 21.80 6 14 0 188.78 14.30 7 14 0 99.19 87.19 -8 15 0 168.88 12.30 -7 15 0 219.18 13.20 -6 15 0 361.46 15.70 -5 15 0 387.16 18.20 -4 15 0 1895.51 43.50 -3 15 0 21.50 7.90 -2 15 0 806.52 16.20 -1 15 0 0.00 10.20 0 15 0 5.00 8.60 1 15 0 72.99 9.90 2 15 0 357.96 14.20 3 15 0 2.50 6.60 4 15 0 50.79 7.80 5 15 0 197.78 9.50 6 15 0 10.10 17.30 7 15 0 712.13 23.90 -7 16 0 51.19 16.30 -6 16 0 44.60 13.20 -5 16 0 66.29 10.40 -4 16 0 0.00 8.10 -3 16 0 158.48 16.30 -2 16 0 665.93 21.70 -1 16 0 206.88 9.60 0 16 0 1737.13 51.69 1 16 0 119.59 12.90 2 16 0 939.61 19.60 3 16 0 335.37 10.90 4 16 0 266.27 18.60 5 16 0 137.99 10.70 6 16 0 897.81 29.70 -6 17 0 0.00 11.60 -5 17 0 334.87 12.60 -4 17 0 191.98 12.60 -3 17 0 148.69 12.30 -2 17 0 27.20 7.50 -1 17 0 600.04 17.30 0 17 0 18.90 6.90 1 17 0 164.48 22.30 2 17 0 306.17 12.50 4 17 0 202.78 24.10 5 17 0 33.00 9.90 -6 18 0 33.70 17.70 -5 18 0 448.86 21.10 -4 18 0 16.40 19.10 -3 18 0 883.81 24.40 -2 18 0 0.00 10.40 -1 18 0 418.46 12.20 0 18 0 334.87 12.50 1 18 0 353.66 17.20 2 18 0 2.40 20.70 3 18 0 1543.65 43.70 4 18 0 134.59 13.60 -4 19 0 833.92 40.10 -3 19 0 58.59 14.20 -2 19 0 132.69 9.80 -1 19 0 162.28 11.70 0 19 0 2.70 16.70 1 19 0 409.06 22.10 2 19 0 17.50 12.00 3 19 0 12.00 10.50 -3 20 0 222.98 24.20 -2 20 0 392.86 57.59 -1 20 0 86.69 55.99 0 20 0 1512.25 81.29 1 20 0 15.80 12.50 -2 -20 1 13.60 11.20 -1 -20 1 14.70 12.50 0 -20 1 442.66 29.60 2 -20 1 179.08 37.20 3 -20 1 0.00 17.10 -3 -19 1 39.90 9.70 -2 -19 1 34.20 12.20 -1 -19 1 947.51 32.10 0 -19 1 26.60 20.70 1 -19 1 1482.35 30.90 2 -19 1 126.49 11.50 3 -19 1 6.60 15.40 4 -19 1 0.80 19.10 -4 -18 1 48.80 11.30 -3 -18 1 430.26 18.20 -2 -18 1 19.90 18.30 -1 -18 1 32.90 13.80 0 -18 1 0.00 10.30 1 -18 1 87.79 9.50 2 -18 1 25.60 10.30 3 -18 1 1049.20 27.20 4 -18 1 124.79 19.70 5 -18 1 565.44 70.79 6 -18 1 218.28 18.70 -5 -17 1 0.00 10.70 -4 -17 1 1197.08 88.29 -2 -17 1 1139.79 26.60 -1 -17 1 67.59 6.90 0 -17 1 72.69 7.60 1 -17 1 20.90 8.20 2 -17 1 544.65 16.10 3 -17 1 4.20 10.00 4 -17 1 356.86 17.40 5 -17 1 0.00 7.80 6 -17 1 36.50 14.80 -6 -16 1 108.59 9.00 -5 -16 1 30.40 7.40 -4 -16 1 319.97 19.30 -3 -16 1 89.29 15.50 -2 -16 1 116.89 10.10 -1 -16 1 0.00 11.20 0 -16 1 1495.95 35.80 1 -16 1 206.98 8.70 2 -16 1 1120.79 28.00 3 -16 1 297.97 10.70 4 -16 1 12.90 6.60 5 -16 1 25.60 10.20 6 -16 1 904.01 26.10 7 -16 1 41.40 12.50 -7 -15 1 1328.77 39.70 -6 -15 1 369.56 16.90 -5 -15 1 791.12 18.00 -4 -15 1 456.05 11.60 -3 -15 1 23.50 5.60 -2 -15 1 0.00 6.30 -1 -15 1 662.23 18.10 0 -15 1 48.70 14.80 1 -15 1 728.43 20.40 2 -15 1 124.19 9.90 3 -15 1 422.06 13.30 4 -15 1 0.00 12.30 5 -15 1 27.40 7.90 6 -15 1 353.36 15.80 7 -15 1 28.80 9.70 8 -15 1 26.90 9.00 -7 -14 1 3.70 20.90 -6 -14 1 72.39 13.00 -5 -14 1 40.40 7.40 -4 -14 1 11.90 3.40 -3 -14 1 561.64 11.90 -2 -14 1 518.85 10.60 -1 -14 1 865.81 15.90 0 -14 1 511.45 12.00 1 -14 1 11.10 5.00 2 -14 1 123.59 7.10 3 -14 1 1373.66 36.10 4 -14 1 793.12 21.50 5 -14 1 808.82 21.30 6 -14 1 349.67 18.10 7 -14 1 47.40 8.20 8 -14 1 44.00 14.50 -7 -13 1 273.17 21.60 -6 -13 1 17.00 8.40 -5 -13 1 4.80 4.70 -4 -13 1 1102.09 22.30 -3 -13 1 274.17 7.70 -2 -13 1 1032.20 19.10 -1 -13 1 320.27 11.30 0 -13 1 387.86 8.60 1 -13 1 100.89 7.00 2 -13 1 23.90 3.60 3 -13 1 260.17 10.30 4 -13 1 16.30 7.40 5 -13 1 25.70 7.70 6 -13 1 19.70 11.20 7 -13 1 510.25 17.90 8 -13 1 318.57 37.90 9 -13 1 432.96 50.49 -8 -12 1 0.00 16.30 -7 -12 1 171.08 11.90 -6 -12 1 987.00 22.50 -5 -12 1 588.54 14.40 -4 -12 1 348.67 13.40 -3 -12 1 365.76 9.30 -2 -12 1 83.49 5.20 -1 -12 1 59.89 3.80 0 -12 1 1574.94 24.50 1 -12 1 1172.38 18.70 2 -12 1 2010.80 32.70 3 -12 1 673.23 14.90 4 -12 1 6.20 4.40 5 -12 1 117.29 7.00 6 -12 1 440.76 12.00 7 -12 1 310.57 17.50 8 -12 1 176.58 16.10 9 -12 1 23.30 17.00 -9 -11 1 71.29 19.00 -8 -11 1 9.80 10.40 -7 -11 1 569.34 15.50 -6 -11 1 483.85 14.60 -5 -11 1 629.24 15.60 -4 -11 1 262.07 15.80 -3 -11 1 594.54 12.20 -2 -11 1 53.69 5.60 -1 -11 1 163.88 6.70 0 -11 1 259.07 5.90 1 -11 1 2.10 3.00 2 -11 1 36.80 4.50 3 -11 1 419.96 8.70 4 -11 1 1169.18 21.90 5 -11 1 432.76 9.30 6 -11 1 438.56 10.10 7 -11 1 648.64 14.90 8 -11 1 12.80 6.80 9 -11 1 70.19 12.40 -9 -10 1 131.49 14.60 -8 -10 1 221.18 16.40 -7 -10 1 81.09 13.70 -6 -10 1 62.09 5.60 -5 -10 1 58.69 4.00 -4 -10 1 68.09 5.00 -3 -10 1 2446.46 40.20 -2 -10 1 2574.54 34.20 -1 -10 1 1689.63 25.80 0 -10 1 966.10 15.80 1 -10 1 2.20 3.60 2 -10 1 162.98 5.30 3 -10 1 792.02 18.00 4 -10 1 1663.03 27.20 5 -10 1 295.47 7.20 6 -10 1 139.09 7.00 7 -10 1 489.25 10.40 8 -10 1 24.40 10.40 9 -10 1 0.30 13.30 10 -10 1 135.29 45.90 -9 -9 1 785.92 42.10 -8 -9 1 329.17 36.20 -7 -9 1 414.56 18.70 -6 -9 1 207.78 7.50 -5 -9 1 0.00 2.80 -4 -9 1 29.80 4.40 -3 -9 1 59.39 2.60 -2 -9 1 54.99 2.30 -1 -9 1 8.40 1.60 0 -9 1 521.65 12.00 1 -9 1 1118.09 24.50 2 -9 1 2491.45 46.60 3 -9 1 545.95 10.90 4 -9 1 1473.35 25.70 5 -9 1 23.70 6.30 6 -9 1 41.50 3.70 7 -9 1 968.10 17.90 8 -9 1 614.94 18.00 9 -9 1 370.36 21.20 10 -9 1 687.03 21.80 -10 -8 1 16.10 30.30 -9 -8 1 0.00 46.00 -8 -8 1 12.20 29.20 -7 -8 1 303.77 12.80 -6 -8 1 1098.59 19.50 -5 -8 1 1993.40 40.40 -4 -8 1 186.18 4.30 -3 -8 1 1635.94 22.10 -2 -8 1 1.40 1.40 -1 -8 1 7.10 1.60 0 -8 1 2335.07 43.30 1 -8 1 1363.96 20.10 2 -8 1 888.11 12.40 3 -8 1 1364.66 20.40 4 -8 1 273.67 8.20 5 -8 1 0.00 7.10 6 -8 1 0.00 12.00 7 -8 1 291.77 17.70 8 -8 1 124.09 28.30 9 -8 1 4.10 15.80 10 -8 1 74.09 9.20 -10 -7 1 572.94 79.79 -9 -7 1 14.20 21.10 -8 -7 1 8.60 8.70 -7 -7 1 33.20 9.40 -6 -7 1 854.21 20.90 -5 -7 1 24.10 6.80 -4 -7 1 247.78 5.70 -3 -7 1 412.46 9.60 -2 -7 1 128.89 3.10 -1 -7 1 1571.34 22.50 0 -7 1 692.73 10.80 1 -7 1 1217.48 17.50 2 -7 1 21.90 1.80 3 -7 1 4.50 2.60 4 -7 1 1158.38 19.20 5 -7 1 2154.58 31.70 6 -7 1 396.66 9.70 7 -7 1 2089.79 38.00 8 -7 1 50.39 21.50 9 -7 1 23.20 10.70 10 -7 1 30.70 16.80 -10 -6 1 136.29 12.80 -9 -6 1 495.65 13.40 -8 -6 1 2439.36 37.40 -7 -6 1 77.59 10.10 -6 -6 1 2236.78 45.30 -5 -6 1 26.20 5.60 -4 -6 1 78.49 3.70 -3 -6 1 354.16 7.90 -2 -6 1 7655.13 106.19 -1 -6 1 53.99 1.80 0 -6 1 3079.39 42.80 1 -6 1 378.16 6.90 2 -6 1 3690.73 59.19 3 -6 1 392.06 14.90 4 -6 1 275.67 6.00 5 -6 1 158.38 4.10 6 -6 1 42.80 3.70 7 -6 1 319.47 8.80 8 -6 1 78.49 7.30 9 -6 1 874.21 22.30 10 -6 1 214.18 27.10 -10 -5 1 27.80 6.20 -9 -5 1 135.09 10.50 -8 -5 1 8.70 7.60 -7 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2 1990.80 28.20 0 1 2 335.47 5.90 1 1 2 5321.57 89.59 2 1 2 53.29 1.40 3 1 2 1083.29 19.70 4 1 2 1329.47 19.00 5 1 2 1944.01 31.20 6 1 2 40.30 2.50 7 1 2 1749.72 29.70 8 1 2 570.04 11.40 9 1 2 435.86 10.10 10 1 2 75.09 7.20 11 1 2 28.60 15.30 -11 2 2 151.98 37.70 -10 2 2 0.00 33.40 -9 2 2 354.66 13.80 -8 2 2 1006.70 16.30 -7 2 2 46.50 4.30 -6 2 2 2100.29 29.20 -5 2 2 711.33 11.50 -4 2 2 314.57 5.30 -3 2 2 839.32 14.10 -2 2 2 105.19 2.50 -1 2 2 183.88 3.10 0 2 2 4338.87 55.69 1 2 2 321.57 5.00 2 2 2 350.46 9.20 3 2 2 51.69 2.30 4 2 2 842.72 14.30 5 2 2 870.01 17.90 6 2 2 9.30 2.10 7 2 2 178.38 5.10 8 2 2 85.89 5.80 9 2 2 415.76 13.60 10 2 2 239.78 10.40 -11 3 2 190.48 38.20 -10 3 2 21.40 12.20 -9 3 2 0.00 12.20 -8 3 2 33.20 6.50 -7 3 2 14.80 5.50 -6 3 2 46.10 3.60 -5 3 2 143.59 6.40 -4 3 2 745.33 13.90 -3 3 2 806.12 13.70 -2 3 2 6445.86 90.39 -1 3 2 1175.88 16.70 0 3 2 639.94 8.90 1 3 2 215.58 5.30 2 3 2 3934.51 69.39 3 3 2 134.49 3.50 4 3 2 4086.99 56.69 5 3 2 1124.59 19.80 6 3 2 1523.25 30.60 7 3 2 342.67 8.00 8 3 2 0.00 4.10 9 3 2 50.89 13.10 10 3 2 68.39 21.80 -11 4 2 637.14 23.50 -10 4 2 43.10 12.00 -9 4 2 1565.04 33.90 -8 4 2 1010.20 27.80 -7 4 2 250.47 8.40 -6 4 2 227.18 8.60 -5 4 2 133.99 7.20 -4 4 2 1075.19 23.00 -3 4 2 2792.02 38.20 -2 4 2 674.93 9.80 -1 4 2 397.96 6.60 0 4 2 2277.97 34.90 1 4 2 360.26 9.60 2 4 2 661.83 9.30 3 4 2 74.29 2.10 4 4 2 56.49 2.20 5 4 2 3.10 3.60 6 4 2 1796.42 35.20 7 4 2 273.97 7.60 8 4 2 1014.10 29.00 9 4 2 386.96 53.79 10 4 2 251.37 17.30 -11 5 2 21.40 13.70 -10 5 2 73.19 14.00 -9 5 2 63.29 6.80 -8 5 2 87.29 10.50 -7 5 2 377.26 9.70 -6 5 2 447.76 9.40 -5 5 2 1323.87 27.50 -4 5 2 155.48 4.10 -3 5 2 18.70 2.10 -2 5 2 314.47 5.80 -1 5 2 814.62 23.40 0 5 2 237.68 4.40 1 5 2 2898.01 41.00 2 5 2 1589.14 20.20 3 5 2 2920.71 39.00 4 5 2 225.38 4.20 5 5 2 9.30 1.50 6 5 2 196.38 5.20 7 5 2 791.82 15.80 8 5 2 277.27 14.00 9 5 2 359.96 15.30 10 5 2 30.00 10.30 -10 6 2 2.20 11.00 -9 6 2 190.48 8.70 -8 6 2 547.25 11.30 -7 6 2 18.30 4.30 -6 6 2 1970.20 36.00 -5 6 2 1428.66 20.30 -4 6 2 241.38 5.90 -3 6 2 12.10 3.50 -2 6 2 947.91 19.10 -1 6 2 0.00 2.40 0 6 2 1212.28 17.60 1 6 2 1107.49 16.50 2 6 2 16.30 1.80 3 6 2 1310.47 29.30 4 6 2 1676.63 28.70 5 6 2 1341.57 23.20 6 6 2 778.02 16.10 7 6 2 268.57 7.60 8 6 2 683.53 17.80 9 6 2 112.69 5.60 10 6 2 142.79 16.20 -10 7 2 220.78 15.90 -9 7 2 278.87 15.70 -8 7 2 512.85 11.20 -7 7 2 234.78 9.10 -6 7 2 15.90 3.20 -5 7 2 7.30 3.40 -4 7 2 1011.20 21.00 -3 7 2 464.65 11.60 -2 7 2 3880.11 55.99 -1 7 2 3262.47 46.60 0 7 2 359.96 6.30 1 7 2 1634.54 34.60 2 7 2 121.89 5.60 3 7 2 226.48 10.10 4 7 2 300.87 8.10 5 7 2 1146.79 22.10 6 7 2 246.38 6.20 7 7 2 85.29 7.70 8 7 2 76.49 4.90 9 7 2 188.98 14.00 -10 8 2 62.69 14.70 -9 8 2 710.93 59.69 -8 8 2 1421.26 58.79 -7 8 2 246.08 13.50 -6 8 2 17.70 4.90 -5 8 2 12.60 4.10 -4 8 2 58.99 4.60 -3 8 2 6.40 2.10 -2 8 2 459.95 8.70 -1 8 2 446.06 8.00 0 8 2 476.85 31.60 1 8 2 1337.17 21.30 2 8 2 250.57 10.80 3 8 2 1669.43 25.20 4 8 2 462.05 11.50 5 8 2 444.16 10.70 6 8 2 618.44 13.40 7 8 2 387.16 10.90 8 8 2 536.95 31.00 9 8 2 396.46 52.69 -10 9 2 204.38 33.20 -9 9 2 4.60 16.10 -8 9 2 54.49 17.20 -7 9 2 702.23 20.40 -6 9 2 1395.56 23.60 -5 9 2 1020.10 30.10 -4 9 2 2690.23 38.40 -3 9 2 42.80 2.60 -2 9 2 766.72 13.10 -1 9 2 147.29 5.20 0 9 2 151.48 4.40 1 9 2 866.61 14.00 2 9 2 811.02 12.20 3 9 2 558.84 9.20 4 9 2 239.38 12.40 5 9 2 28.90 2.80 6 9 2 78.99 5.20 7 9 2 155.98 9.20 9 9 2 8.90 21.00 -10 10 2 32.30 31.90 -9 10 2 123.19 12.30 -8 10 2 35.30 7.00 -7 10 2 274.07 9.00 -6 10 2 0.30 6.90 -5 10 2 131.39 8.30 -4 10 2 74.69 5.00 -3 10 2 188.98 16.30 -2 10 2 1129.09 21.30 -1 10 2 429.66 12.50 0 10 2 1231.78 19.80 1 10 2 105.39 3.50 2 10 2 397.96 9.40 3 10 2 727.73 12.10 4 10 2 881.31 14.20 5 10 2 912.21 15.40 6 10 2 2330.37 45.80 7 10 2 266.57 11.10 8 10 2 392.46 22.60 9 10 2 5.60 13.80 -9 11 2 515.45 16.20 -8 11 2 331.77 11.80 -7 11 2 1723.83 31.70 -6 11 2 11.00 4.60 -5 11 2 312.87 11.70 -4 11 2 65.19 6.30 -3 11 2 668.73 12.20 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-4 14 2 99.19 7.00 -3 14 2 1.50 6.10 -2 14 2 1184.68 20.00 -1 14 2 135.19 5.10 0 14 2 1921.31 30.60 1 14 2 26.00 3.90 2 14 2 772.22 19.20 3 14 2 114.59 7.40 4 14 2 307.67 9.40 5 14 2 111.69 8.00 6 14 2 741.43 64.59 7 14 2 3.10 16.90 -8 15 2 109.39 15.90 -7 15 2 1264.87 31.90 -6 15 2 119.49 15.80 -5 15 2 477.05 22.90 -4 15 2 6.90 12.60 -3 15 2 12.70 8.90 -2 15 2 14.50 6.90 -1 15 2 140.89 7.60 0 15 2 16.90 4.70 1 15 2 11.30 6.30 2 15 2 396.16 9.30 3 15 2 9.40 4.80 4 15 2 1181.38 26.60 5 15 2 0.00 15.60 6 15 2 198.38 23.80 -7 16 2 0.00 20.40 -6 16 2 48.50 24.90 -5 16 2 828.82 25.80 -4 16 2 24.30 7.20 -3 16 2 1638.74 46.00 -2 16 2 3.30 10.30 -1 16 2 591.64 19.80 0 16 2 544.65 23.40 1 16 2 338.87 9.00 2 16 2 8.90 6.60 3 16 2 1060.29 23.80 4 16 2 13.20 14.60 5 16 2 363.36 14.40 6 16 2 22.30 9.00 -6 17 2 12.40 12.70 -5 17 2 0.00 7.30 -4 17 2 267.47 15.10 -3 17 2 2.80 12.20 -2 17 2 49.20 13.10 -1 17 2 567.24 18.40 0 17 2 0.30 9.70 1 17 2 1052.89 22.90 2 17 2 84.79 13.10 3 17 2 51.09 33.60 4 17 2 71.59 13.10 5 17 2 397.56 16.90 -5 18 2 62.89 13.40 -4 18 2 96.19 18.80 -3 18 2 228.58 17.00 -2 18 2 320.07 13.90 -1 18 2 29.60 6.90 0 18 2 1482.75 34.20 1 18 2 23.10 15.20 2 18 2 753.72 46.20 3 18 2 5.90 18.90 4 18 2 36.30 24.00 -4 19 2 127.59 22.10 -3 19 2 13.50 13.10 -2 19 2 602.14 17.70 -1 19 2 56.59 12.50 0 19 2 97.39 16.80 1 19 2 15.30 16.10 2 19 2 536.05 29.70 3 19 2 3.10 15.80 -2 20 2 77.79 17.70 -1 20 2 623.14 35.10 0 20 2 40.20 18.80 -2 -20 3 43.60 16.20 -1 -20 3 144.39 19.80 0 -20 3 51.99 23.00 1 -20 3 2.80 52.89 2 -20 3 27.30 26.70 3 -20 3 1122.79 31.30 -3 -19 3 82.39 10.90 -2 -19 3 671.73 21.40 -1 -19 3 160.18 20.60 0 -19 3 20.80 51.29 1 -19 3 0.00 31.50 2 -19 3 122.69 18.00 3 -19 3 100.99 24.80 4 -19 3 14.80 49.10 -4 -18 3 130.09 7.80 -3 -18 3 195.08 10.60 -2 -18 3 173.58 14.30 -1 -18 3 1.20 10.50 0 -18 3 1630.34 31.90 1 -18 3 554.04 15.20 2 -18 3 452.75 15.60 3 -18 3 585.64 29.60 4 -18 3 12.00 40.80 5 -18 3 74.99 36.50 6 -18 3 716.53 28.60 -5 -17 3 652.73 20.20 -4 -17 3 166.88 14.10 -3 -17 3 31.10 6.30 -2 -17 3 0.00 8.30 -1 -17 3 75.59 5.90 0 -17 3 42.30 6.00 1 -17 3 26.20 8.80 2 -17 3 29.80 8.30 3 -17 3 168.68 15.40 4 -17 3 311.97 13.90 5 -17 3 104.89 12.20 6 -17 3 361.96 22.50 -6 -16 3 41.70 36.30 -5 -16 3 64.19 11.10 -4 -16 3 42.80 12.80 -3 -16 3 1787.82 32.40 -2 -16 3 673.63 14.10 -1 -16 3 1200.98 21.90 0 -16 3 405.26 16.50 1 -16 3 57.79 6.20 2 -16 3 0.00 9.10 3 -16 3 1297.37 26.20 4 -16 3 126.59 8.00 5 -16 3 269.77 13.10 6 -16 3 64.09 15.10 7 -16 3 138.39 24.00 -7 -15 3 400.36 20.80 -6 -15 3 20.00 11.30 -5 -15 3 2.10 9.00 -4 -15 3 598.14 13.80 -3 -15 3 774.72 16.30 -2 -15 3 262.97 10.50 -1 -15 3 3.90 9.40 0 -15 3 323.77 10.10 1 -15 3 392.46 12.20 2 -15 3 353.06 11.60 3 -15 3 193.58 13.30 4 -15 3 81.19 12.10 5 -15 3 41.40 6.30 6 -15 3 29.20 10.90 7 -15 3 780.82 27.10 8 -15 3 400.26 14.30 -7 -14 3 170.28 21.10 -6 -14 3 997.50 24.50 -5 -14 3 923.51 16.80 -4 -14 3 286.47 6.00 -3 -14 3 465.45 10.50 -2 -14 3 40.90 4.20 -1 -14 3 3.50 11.20 0 -14 3 1276.37 28.90 1 -14 3 975.20 19.50 2 -14 3 639.44 17.10 3 -14 3 327.77 13.60 4 -14 3 336.97 10.90 5 -14 3 127.79 10.60 6 -14 3 0.00 12.50 7 -14 3 239.68 13.20 8 -14 3 46.10 14.10 -8 -13 3 45.10 20.20 -7 -13 3 195.78 14.90 -6 -13 3 471.35 13.10 -5 -13 3 320.47 7.40 -4 -13 3 340.47 9.60 -3 -13 3 372.96 7.90 -2 -13 3 546.55 9.30 -1 -13 3 203.28 7.30 0 -13 3 296.07 7.40 1 -13 3 89.09 10.70 2 -13 3 70.39 5.20 3 -13 3 95.29 7.30 4 -13 3 821.72 17.60 5 -13 3 1119.89 20.50 6 -13 3 402.96 14.20 7 -13 3 583.64 21.60 8 -13 3 29.30 31.30 9 -13 3 90.19 25.70 -8 -12 3 1050.69 46.30 -7 -12 3 223.88 12.10 -6 -12 3 432.36 17.10 -5 -12 3 206.18 10.60 -4 -12 3 46.50 3.30 -3 -12 3 1730.63 25.00 -2 -12 3 2425.26 36.00 -1 -12 3 801.12 14.10 0 -12 3 848.02 15.30 1 -12 3 0.00 3.00 2 -12 3 60.49 4.30 3 -12 3 318.17 14.10 4 -12 3 947.01 18.90 5 -12 3 296.07 13.70 6 -12 3 0.00 17.30 7 -12 3 406.46 19.40 8 -12 3 59.89 11.80 9 -12 3 130.19 32.50 -9 -11 3 479.05 36.40 -8 -11 3 285.47 17.60 -7 -11 3 90.09 11.50 -6 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1549.94 30.10 6 -9 3 369.36 12.10 7 -9 3 1798.62 32.80 8 -9 3 6.20 9.90 9 -9 3 30.80 19.60 10 -9 3 0.00 16.10 -10 -8 3 204.08 35.50 -9 -8 3 320.17 50.49 -8 -8 3 1470.05 43.30 -7 -8 3 87.99 9.10 -6 -8 3 915.11 16.70 -5 -8 3 49.20 4.20 -4 -8 3 91.89 3.40 -3 -8 3 119.99 3.70 -2 -8 3 1328.87 21.80 -1 -8 3 13.90 7.20 0 -8 3 191.78 7.10 1 -8 3 1112.59 16.30 2 -8 3 32.90 2.10 3 -8 3 770.62 13.00 4 -8 3 334.47 9.30 5 -8 3 222.08 6.90 6 -8 3 0.00 10.00 7 -8 3 20.20 7.00 8 -8 3 60.59 14.30 9 -8 3 907.21 23.10 10 -8 3 46.10 8.10 -10 -7 3 76.39 28.20 -8 -7 3 0.00 10.00 -7 -7 3 19.40 12.30 -6 -7 3 360.36 10.50 -5 -7 3 32.30 5.50 -4 -7 3 1440.36 23.10 -3 -7 3 344.17 8.50 -2 -7 3 2269.07 33.00 -1 -7 3 522.65 8.60 0 -7 3 237.28 4.40 1 -7 3 1061.29 15.00 2 -7 3 1923.41 29.30 3 -7 3 522.25 10.30 4 -7 3 1921.81 32.20 5 -7 3 6.40 7.40 6 -7 3 21.00 26.80 7 -7 3 39.00 24.90 8 -7 3 294.27 12.60 9 -7 3 30.60 14.70 10 -7 3 125.89 10.60 -10 -6 3 22.80 11.00 -9 -6 3 598.24 17.50 -8 -6 3 0.00 7.30 -7 -6 3 18.00 9.40 -6 -6 3 994.80 26.40 -5 -6 3 2808.92 51.39 -4 -6 3 28.00 2.60 -3 -6 3 2354.66 42.90 -2 -6 3 174.18 3.10 -1 -6 3 40.30 1.80 0 -6 3 1904.81 25.90 1 -6 3 3.10 1.10 2 -6 3 1336.57 21.30 3 -6 3 114.69 3.60 4 -6 3 1507.15 22.40 5 -6 3 189.58 5.50 6 -6 3 1437.86 39.30 7 -6 3 159.88 8.20 8 -6 3 1732.93 30.70 9 -6 3 203.78 12.10 10 -6 3 24.10 24.10 -10 -5 3 37.70 7.90 -9 -5 3 504.25 13.50 -8 -5 3 3.20 3.00 -7 -5 3 925.01 17.70 -6 -5 3 0.00 7.10 -5 -5 3 1778.52 31.40 -4 -5 3 684.43 14.20 -3 -5 3 788.02 14.80 -2 -5 3 0.00 1.40 -1 -5 3 5158.48 70.49 0 -5 3 15.50 1.60 1 -5 3 3791.02 57.69 2 -5 3 11.70 1.50 3 -5 3 817.92 12.90 4 -5 3 13.70 1.70 5 -5 3 531.35 10.30 6 -5 3 9.10 2.80 7 -5 3 790.02 15.30 8 -5 3 25.50 6.80 9 -5 3 15.40 13.20 10 -5 3 352.06 22.10 -10 -4 3 20.00 8.20 -9 -4 3 206.48 11.00 -8 -4 3 1186.98 24.70 -7 -4 3 77.39 4.50 -6 -4 3 1419.46 25.20 -5 -4 3 4.50 2.20 -4 -4 3 226.78 6.20 -3 -4 3 17.40 1.00 -2 -4 3 498.45 8.80 -1 -4 3 1476.35 23.20 0 -4 3 817.82 19.90 1 -4 3 1446.96 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34.20 9 -2 3 188.88 15.10 10 -2 3 15.10 16.60 11 -2 3 71.89 48.30 -11 -1 3 106.39 14.00 -10 -1 3 99.59 9.60 -9 -1 3 101.49 7.10 -8 -1 3 10.10 5.80 -7 -1 3 3048.90 48.10 -6 -1 3 79.89 5.10 -5 -1 3 2090.29 41.10 -4 -1 3 503.25 11.70 -3 -1 3 330.97 5.90 -2 -1 3 501.85 6.80 -1 -1 3 2756.72 41.50 0 -1 3 177.78 4.20 1 -1 3 3441.76 54.19 2 -1 3 95.89 3.70 3 -1 3 1007.60 15.40 4 -1 3 733.73 11.50 5 -1 3 76.29 3.70 6 -1 3 596.34 9.50 7 -1 3 9.70 5.20 8 -1 3 69.09 9.30 10 -1 3 846.92 27.80 11 -1 3 25.60 18.80 -11 0 3 23.30 8.00 -10 0 3 13.30 5.70 -9 0 3 0.00 6.80 -8 0 3 553.14 13.80 -7 0 3 193.88 5.40 -6 0 3 133.99 5.00 -5 0 3 362.56 9.30 -4 0 3 736.13 12.30 -3 0 3 1316.97 18.80 -2 0 3 730.43 11.60 -1 0 3 1100.69 16.80 0 0 3 1079.59 19.00 1 0 3 20.70 3.10 2 0 3 59.69 1.50 3 0 3 3221.78 47.00 4 0 3 411.26 7.30 5 0 3 4391.96 56.69 6 0 3 814.32 20.30 7 0 3 262.57 7.20 8 0 3 20.40 4.30 9 0 3 259.27 13.10 10 0 3 0.00 9.40 11 0 3 425.96 21.20 -11 1 3 11.50 11.90 -10 1 3 1308.57 36.20 -9 1 3 186.48 8.10 -8 1 3 1051.19 18.10 -7 1 3 404.26 8.00 -6 1 3 52.29 5.00 -5 1 3 5.40 1.60 -4 1 3 3018.50 42.20 -3 1 3 3107.69 45.60 -2 1 3 656.03 11.10 -1 1 3 669.63 22.00 0 1 3 423.96 7.50 1 1 3 142.69 5.70 2 1 3 115.99 2.20 3 1 3 41.60 1.60 4 1 3 141.29 3.60 5 1 3 129.89 5.40 6 1 3 9.70 2.60 7 1 3 901.91 17.70 8 1 3 333.57 12.50 9 1 3 565.94 13.80 10 1 3 246.28 11.90 -10 2 3 186.98 28.80 -9 2 3 285.67 8.90 -8 2 3 40.10 4.20 -7 2 3 137.69 5.30 -6 2 3 545.95 9.20 -5 2 3 522.15 8.70 -4 2 3 1909.31 26.50 -3 2 3 139.69 3.90 -2 2 3 3243.78 57.99 -1 2 3 123.29 2.30 0 2 3 2677.73 38.90 1 2 3 604.44 11.90 2 2 3 7372.26 103.09 3 2 3 1759.02 30.60 4 2 3 60.89 2.80 5 2 3 9.40 2.30 6 2 3 711.53 13.40 7 2 3 1.70 3.50 8 2 3 958.40 16.10 9 2 3 162.68 6.90 10 2 3 33.60 6.90 -10 3 3 211.88 15.10 -9 3 3 43.00 9.40 -8 3 3 0.00 7.40 -7 3 3 1703.43 30.00 -6 3 3 537.15 10.90 -5 3 3 2244.28 36.10 -4 3 3 1892.61 31.00 -3 3 3 209.78 5.80 -2 3 3 349.57 5.90 -1 3 3 71.19 1.70 0 3 3 637.14 9.90 1 3 3 4.80 3.90 2 3 3 400.86 10.20 3 3 3 21.50 2.50 4 3 3 1461.55 26.00 5 3 3 1043.80 21.80 6 3 3 659.33 15.10 7 3 3 640.54 18.30 8 3 3 13.40 5.20 9 3 3 4.90 4.80 10 3 3 594.64 45.20 -11 4 3 58.19 20.10 -10 4 3 253.97 13.50 -9 4 3 133.99 12.60 -8 4 3 231.98 13.10 -7 4 3 255.67 11.40 -6 4 3 1244.58 25.50 -5 4 3 259.37 10.70 -4 4 3 678.43 12.10 -3 4 3 1839.42 27.70 -2 4 3 2077.99 30.80 -1 4 3 2904.61 38.80 0 4 3 1363.66 29.50 1 4 3 4.90 3.00 2 4 3 2.90 1.30 3 4 3 1251.67 19.00 4 4 3 419.66 8.50 5 4 3 830.52 14.10 6 4 3 568.04 10.40 7 4 3 207.68 7.30 8 4 3 8.90 8.40 9 4 3 108.59 18.30 10 4 3 257.77 13.40 -10 5 3 697.43 25.80 -9 5 3 762.22 20.30 -8 5 3 614.94 14.60 -7 5 3 593.34 14.50 -6 5 3 5.70 4.80 -5 5 3 155.68 7.60 -4 5 3 1.50 1.60 -3 5 3 732.13 12.10 -2 5 3 369.16 6.50 -1 5 3 265.87 9.80 0 5 3 396.86 6.60 1 5 3 337.77 5.40 2 5 3 799.32 11.20 3 5 3 821.22 12.10 4 5 3 279.37 11.00 5 5 3 15.10 1.90 6 5 3 68.49 4.10 7 5 3 994.00 22.60 8 5 3 1012.30 35.20 9 5 3 1012.30 31.80 10 5 3 467.65 15.60 -10 6 3 4.60 9.10 -9 6 3 66.49 7.60 -8 6 3 266.87 11.40 -7 6 3 101.79 5.20 -6 6 3 1665.13 30.70 -5 6 3 1179.08 19.10 -4 6 3 2078.89 31.50 -3 6 3 1866.41 57.89 -2 6 3 6.30 4.00 -1 6 3 4.20 3.60 0 6 3 233.78 4.70 1 6 3 2585.14 36.50 2 6 3 1592.24 22.80 3 6 3 245.78 5.90 4 6 3 301.07 6.00 5 6 3 0.00 3.20 6 6 3 94.09 6.20 7 6 3 108.49 4.90 8 6 3 50.79 7.50 9 6 3 7.80 5.30 10 6 3 30.10 12.40 -10 7 3 178.18 11.40 -9 7 3 0.70 5.50 -8 7 3 12.20 6.10 -7 7 3 111.49 6.60 -6 7 3 284.97 8.00 -5 7 3 256.97 6.80 -4 7 3 0.00 6.60 -3 7 3 99.09 4.50 -2 7 3 643.24 13.60 -1 7 3 1086.69 16.70 0 7 3 622.24 11.00 1 7 3 605.64 20.50 2 7 3 403.66 6.90 3 7 3 806.62 13.30 4 7 3 1063.39 24.00 5 7 3 1556.34 28.80 6 7 3 598.64 12.00 7 7 3 1226.78 21.00 8 7 3 9.80 4.70 9 7 3 37.50 6.40 10 7 3 246.68 26.50 -10 8 3 294.17 12.60 -9 8 3 324.07 32.50 -8 8 3 866.61 21.30 -7 8 3 361.96 10.30 -6 8 3 687.73 17.00 -5 8 3 222.08 6.30 -4 8 3 16.40 4.00 -3 8 3 693.23 11.30 -2 8 3 702.93 11.70 -1 8 3 1120.19 17.00 0 8 3 2215.38 40.90 1 8 3 75.09 2.80 2 8 3 36.10 10.10 3 8 3 48.80 2.20 4 8 3 761.22 20.80 5 8 3 2.90 8.30 6 8 3 88.29 4.50 7 8 3 346.97 9.40 8 8 3 358.66 21.50 9 8 3 292.07 50.39 -10 9 3 118.09 23.50 -9 9 3 83.69 22.10 -8 9 3 25.70 30.70 -7 9 3 172.08 15.10 -6 9 3 362.06 10.20 -5 9 3 14.30 7.10 -4 9 3 700.23 13.00 -3 9 3 31.00 2.50 -2 9 3 558.24 12.50 -1 9 3 376.26 10.10 0 9 3 20.40 2.50 1 9 3 1937.21 27.40 2 9 3 2976.50 42.10 3 9 3 1853.51 27.70 4 9 3 1849.21 41.20 5 9 3 0.00 2.60 6 9 3 55.39 6.80 7 9 3 274.97 29.90 9 9 3 64.79 22.20 -9 10 3 474.45 48.70 -8 10 3 118.59 10.00 -7 10 3 125.49 8.20 -6 10 3 1015.50 22.10 -5 10 3 1380.16 27.30 -4 10 3 347.67 10.70 -3 10 3 1073.19 31.60 -2 10 3 315.97 8.10 -1 10 3 56.49 4.40 0 10 3 20.60 2.70 1 10 3 109.29 3.60 2 10 3 71.99 5.20 3 10 3 0.30 4.30 4 10 3 8.00 2.60 5 10 3 258.37 6.20 6 10 3 2025.20 53.29 7 10 3 40.00 17.40 8 10 3 197.88 13.90 9 10 3 14.00 14.70 -9 11 3 197.28 11.60 -8 11 3 33.10 8.80 -7 11 3 419.16 14.80 -6 11 3 105.39 8.10 -5 11 3 51.79 9.50 -4 11 3 111.79 7.90 -3 11 3 821.92 14.10 -2 11 3 515.85 14.70 -1 11 3 2003.10 36.40 0 11 3 366.46 8.70 1 11 3 1962.00 29.90 2 11 3 10.20 3.20 3 11 3 47.40 3.90 4 11 3 759.12 13.80 5 11 3 946.11 18.90 6 11 3 295.97 11.50 7 11 3 601.94 16.90 8 11 3 63.19 8.80 -9 12 3 163.28 12.30 -8 12 3 796.02 20.60 -7 12 3 120.29 8.90 -6 12 3 2051.59 37.70 -5 12 3 147.09 7.30 -4 12 3 0.00 4.80 -3 12 3 162.28 7.30 -2 12 3 563.34 18.10 -1 12 3 108.99 8.10 0 12 3 877.81 19.00 1 12 3 300.57 7.50 2 12 3 254.37 9.20 3 12 3 1995.80 63.39 4 12 3 30.30 4.40 5 12 3 528.05 14.00 6 12 3 21.60 4.50 7 12 3 55.29 5.70 8 12 3 216.08 18.40 -8 13 3 58.79 11.80 -7 13 3 6.20 9.60 -6 13 3 261.97 9.90 -5 13 3 464.55 11.20 -4 13 3 2226.68 39.70 -3 13 3 5.60 3.60 -2 13 3 1046.00 17.90 -1 13 3 32.20 4.00 0 13 3 3.80 3.50 1 13 3 272.47 9.50 2 13 3 1775.22 50.69 3 13 3 16.40 6.10 4 13 3 1881.81 38.60 5 13 3 23.00 7.00 6 13 3 72.49 8.30 7 13 3 39.50 10.40 -8 14 3 104.39 16.80 -7 14 3 0.00 10.20 -6 14 3 0.00 11.10 -5 14 3 536.45 15.10 -4 14 3 145.19 7.20 -3 14 3 805.02 16.40 -2 14 3 30.30 5.10 -1 14 3 31.10 4.40 0 14 3 629.34 15.20 1 14 3 35.10 4.00 2 14 3 176.68 10.20 3 14 3 17.70 8.60 4 14 3 195.98 6.50 5 14 3 24.70 11.10 7 14 3 0.00 54.49 -7 15 3 978.20 39.30 -6 15 3 41.50 13.40 -5 15 3 957.70 27.00 -4 15 3 239.68 20.10 -3 15 3 14.20 5.70 -2 15 3 90.19 7.60 -1 15 3 1332.17 22.10 0 15 3 11.00 4.80 1 15 3 1456.45 23.30 2 15 3 142.89 8.30 3 15 3 65.39 4.90 4 15 3 19.70 8.20 5 15 3 56.69 17.80 6 15 3 1.70 39.10 -7 16 3 27.80 29.40 -6 16 3 477.45 28.50 -5 16 3 50.69 15.90 -4 16 3 6.20 6.70 -3 16 3 298.87 19.40 -2 16 3 0.00 10.40 -1 16 3 223.48 25.00 0 16 3 134.29 9.50 1 16 3 133.69 7.00 2 16 3 46.80 6.90 3 16 3 2125.89 38.70 4 16 3 70.09 17.90 5 16 3 759.02 23.00 -6 17 3 85.79 15.40 -5 17 3 2.60 8.80 -4 17 3 1197.88 32.30 -3 17 3 0.00 12.10 -2 17 3 1520.15 52.09 -1 17 3 74.69 13.60 0 17 3 13.80 11.00 1 17 3 29.80 10.10 2 17 3 523.45 20.10 3 17 3 20.40 15.40 4 17 3 142.19 12.30 5 17 3 42.90 12.30 -5 18 3 51.59 15.40 -4 18 3 37.40 14.60 -3 18 3 10.10 14.90 -2 18 3 67.39 11.00 -1 18 3 0.00 8.70 0 18 3 1623.04 38.90 1 18 3 88.39 15.00 2 18 3 1273.87 61.09 3 18 3 315.77 26.50 4 18 3 13.30 14.90 -4 19 3 331.27 20.50 -3 19 3 8.30 10.60 -2 19 3 3.40 9.00 -1 19 3 389.76 18.10 0 19 3 41.50 19.60 1 19 3 390.16 31.30 2 19 3 22.90 19.30 -2 -20 4 104.69 16.80 -1 -20 4 0.00 29.50 0 -20 4 180.08 30.50 1 -20 4 23.80 57.09 2 -20 4 176.18 25.20 3 -20 4 25.20 12.60 -3 -19 4 46.50 12.40 -2 -19 4 691.53 23.40 -1 -19 4 286.97 36.40 0 -19 4 98.59 31.50 1 -19 4 109.79 23.80 2 -19 4 351.26 17.30 3 -19 4 75.29 29.50 4 -19 4 968.60 39.50 -4 -18 4 227.08 11.00 -3 -18 4 495.75 17.10 -2 -18 4 193.58 18.20 -1 -18 4 405.46 18.60 0 -18 4 171.98 9.60 1 -18 4 38.10 8.70 2 -18 4 587.44 22.60 3 -18 4 0.00 17.10 4 -18 4 54.39 79.89 5 -18 4 14.30 34.60 -5 -17 4 568.54 16.20 -4 -17 4 482.55 23.60 -3 -17 4 23.30 7.20 -2 -17 4 137.29 10.30 -1 -17 4 514.25 12.60 0 -17 4 262.77 8.40 1 -17 4 987.80 24.10 2 -17 4 775.42 22.40 3 -17 4 314.77 23.70 4 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664.33 23.30 -8 -13 4 0.00 18.00 -7 -13 4 251.97 13.20 -6 -13 4 588.64 14.90 -5 -13 4 1182.08 20.90 -4 -13 4 1630.14 23.40 -3 -13 4 109.19 4.50 -2 -13 4 140.79 5.10 -1 -13 4 441.86 12.50 0 -13 4 322.67 8.20 1 -13 4 744.63 20.10 2 -13 4 436.96 13.30 3 -13 4 102.99 10.20 4 -13 4 4.30 8.80 5 -13 4 337.57 14.10 6 -13 4 27.60 12.00 7 -13 4 96.29 15.20 8 -13 4 14.00 46.40 -8 -12 4 0.00 21.30 -7 -12 4 151.38 11.70 -6 -12 4 119.09 12.80 -5 -12 4 150.68 12.40 -4 -12 4 428.26 10.10 -3 -12 4 95.99 4.10 -2 -12 4 1114.89 17.90 -1 -12 4 457.65 9.40 0 -12 4 1497.05 24.80 1 -12 4 2.60 2.90 2 -12 4 260.27 7.60 3 -12 4 930.81 21.70 4 -12 4 679.93 15.20 5 -12 4 1194.28 33.10 6 -12 4 2464.55 50.29 7 -12 4 75.99 9.40 8 -12 4 117.19 17.60 9 -12 4 3.90 24.70 -9 -11 4 692.93 31.30 -8 -11 4 367.46 22.60 -7 -11 4 1757.82 39.60 -6 -11 4 39.90 13.50 -5 -11 4 191.58 9.30 -4 -11 4 174.08 7.80 -3 -11 4 204.48 5.40 -2 -11 4 658.33 13.90 -1 -11 4 1871.91 27.00 0 -11 4 128.29 4.20 1 -11 4 340.07 8.20 2 -11 4 184.18 5.90 3 -11 4 322.57 8.50 4 -11 4 178.78 6.50 5 -11 4 149.69 6.50 6 -11 4 31.50 9.20 7 -11 4 430.16 17.90 8 -11 4 739.03 19.80 9 -11 4 179.18 17.50 -9 -10 4 33.90 14.40 -8 -10 4 21.00 12.80 -7 -10 4 45.00 9.20 -6 -10 4 162.18 8.60 -5 -10 4 647.04 13.60 -4 -10 4 450.25 9.80 -3 -10 4 1659.13 26.50 -2 -10 4 0.00 4.30 -1 -10 4 66.79 3.70 0 -10 4 358.16 8.50 1 -10 4 643.14 11.60 2 -10 4 593.34 12.80 3 -10 4 2617.54 39.20 4 -10 4 16.60 2.90 5 -10 4 303.67 9.40 6 -10 4 162.18 11.00 7 -10 4 27.60 5.40 8 -10 4 163.48 10.80 9 -10 4 496.65 35.00 -9 -9 4 30.70 13.40 -8 -9 4 52.49 13.50 -7 -9 4 637.54 20.30 -6 -9 4 1828.72 34.30 -5 -9 4 213.58 6.20 -4 -9 4 2145.49 39.70 -3 -9 4 266.47 5.80 -2 -9 4 284.97 5.70 -1 -9 4 264.17 7.70 0 -9 4 219.18 6.10 1 -9 4 302.57 7.60 2 -9 4 88.19 6.50 3 -9 4 64.09 3.00 4 -9 4 60.09 3.90 5 -9 4 460.55 9.60 6 -9 4 233.88 8.40 7 -9 4 2394.76 40.50 8 -9 4 84.69 7.90 9 -9 4 131.39 29.10 10 -9 4 433.06 23.20 -10 -8 4 96.99 24.40 -9 -8 4 12.90 32.00 -8 -8 4 428.86 16.80 -7 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4 790.52 12.90 3 -6 4 3493.75 54.79 4 -6 4 4.10 2.40 5 -6 4 265.77 6.60 6 -6 4 0.00 5.60 7 -6 4 0.00 8.70 8 -6 4 149.39 11.00 9 -6 4 40.90 10.60 10 -6 4 21.90 28.20 -10 -5 4 1236.38 31.40 -9 -5 4 1.50 5.90 -8 -5 4 36.50 12.60 -7 -5 4 3.40 3.40 -6 -5 4 35.10 4.60 -5 -5 4 65.89 2.30 -4 -5 4 74.89 3.30 -3 -5 4 1.20 1.80 -2 -5 4 642.04 10.90 -1 -5 4 1023.50 15.90 0 -5 4 0.20 2.20 1 -5 4 2069.89 31.80 2 -5 4 122.29 3.80 3 -5 4 119.99 3.30 4 -5 4 408.06 7.50 5 -5 4 1960.00 29.60 6 -5 4 298.07 6.70 7 -5 4 2361.26 40.50 8 -5 4 14.10 8.20 9 -5 4 334.87 26.90 10 -5 4 75.19 32.20 -10 -4 4 15.30 6.80 -9 -4 4 32.40 11.00 -8 -4 4 1422.26 26.10 -7 -4 4 0.00 4.20 -6 -4 4 3147.39 51.99 -5 -4 4 640.34 10.10 -4 -4 4 539.15 10.60 -3 -4 4 177.88 3.80 -2 -4 4 2542.55 37.60 -1 -4 4 685.73 10.80 0 -4 4 3932.91 69.19 1 -4 4 294.47 6.70 2 -4 4 1059.29 16.00 3 -4 4 2.80 1.20 4 -4 4 19.30 3.50 5 -4 4 236.88 5.80 6 -4 4 587.34 11.40 7 -4 4 24.20 3.90 8 -4 4 9.50 4.90 9 -4 4 923.71 23.70 10 -4 4 25.70 10.30 -10 -3 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24.50 1.40 -2 -1 4 18.10 1.00 -1 -1 4 587.94 10.10 0 -1 4 265.87 6.80 1 -1 4 1555.44 24.20 2 -1 4 640.24 19.10 3 -1 4 1424.46 22.80 4 -1 4 906.91 15.20 5 -1 4 512.95 13.90 6 -1 4 147.19 4.70 7 -1 4 1015.30 21.60 8 -1 4 385.26 25.90 9 -1 4 526.55 55.99 10 -1 4 24.60 22.40 -11 0 4 306.57 11.80 -10 0 4 34.90 7.00 -9 0 4 152.38 7.80 -8 0 4 1403.46 29.50 -7 0 4 109.69 7.20 -6 0 4 3425.36 66.99 -5 0 4 549.65 24.00 -4 0 4 1108.39 16.10 -3 0 4 46.90 1.80 -2 0 4 123.29 2.50 -1 0 4 281.67 4.90 0 0 4 1168.58 20.60 1 0 4 6.60 1.80 2 0 4 51.49 1.60 3 0 4 806.92 15.50 4 0 4 282.97 8.90 5 0 4 2961.10 42.70 6 0 4 105.69 6.20 7 0 4 142.89 6.00 8 0 4 568.04 33.90 9 0 4 751.62 23.40 10 0 4 66.39 9.30 -11 1 4 55.29 11.70 -10 1 4 97.19 16.70 -9 1 4 121.39 11.00 -8 1 4 291.87 7.70 -7 1 4 15.10 2.80 -6 1 4 50.69 4.50 -5 1 4 253.97 5.00 -4 1 4 3727.83 57.59 -3 1 4 2774.12 45.60 -2 1 4 2595.74 46.90 -1 1 4 873.41 17.00 0 1 4 473.55 9.60 1 1 4 65.19 3.10 2 1 4 539.75 11.60 3 1 4 216.78 3.90 4 1 4 4585.54 65.29 5 1 4 958.10 14.40 6 1 4 666.53 10.70 7 1 4 13.40 3.30 8 1 4 0.00 6.00 9 1 4 219.98 7.90 10 1 4 0.00 8.90 -10 2 4 11.70 12.80 -9 2 4 1541.05 29.40 -8 2 4 1062.79 22.00 -7 2 4 27.00 3.90 -6 2 4 69.99 4.00 -5 2 4 46.00 2.30 -4 2 4 276.07 5.60 -3 2 4 1494.05 22.50 -2 2 4 322.67 5.60 -1 2 4 20.90 1.20 0 2 4 381.16 6.90 1 2 4 3338.87 80.19 2 2 4 925.01 15.80 3 2 4 85.39 10.10 4 2 4 847.92 17.00 5 2 4 369.36 7.30 6 2 4 1249.18 20.50 7 2 4 307.77 7.70 8 2 4 992.60 20.40 9 2 4 572.94 12.80 10 2 4 358.56 12.60 -10 3 4 15.00 14.00 -9 3 4 0.00 7.80 -8 3 4 10.10 7.30 -7 3 4 1015.80 18.80 -6 3 4 236.08 6.00 -5 3 4 2175.38 33.50 -4 3 4 2434.66 45.30 -3 3 4 156.28 3.80 -2 3 4 1070.59 16.40 -1 3 4 3919.81 55.69 0 3 4 633.44 10.50 1 3 4 7592.34 148.99 2 3 4 861.71 15.50 3 3 4 3354.46 63.09 4 3 4 246.48 6.70 5 3 4 34.60 2.70 6 3 4 135.39 5.60 7 3 4 12.20 4.80 8 3 4 115.79 6.30 9 3 4 193.88 7.60 10 3 4 95.89 10.20 -10 4 4 38.00 11.00 -9 4 4 0.00 10.10 -8 4 4 38.50 7.40 -7 4 4 221.58 11.20 -6 4 4 609.94 12.50 -5 4 4 262.17 5.70 -4 4 4 370.56 7.90 -3 4 4 157.78 3.60 -2 4 4 604.54 9.40 -1 4 4 1670.43 23.90 0 4 4 470.25 16.90 1 4 4 22.40 1.80 2 4 4 21.50 1.80 3 4 4 2212.68 42.00 4 4 4 1416.86 26.30 5 4 4 1508.75 27.00 6 4 4 1784.62 29.00 7 4 4 78.29 4.90 8 4 4 665.93 20.70 9 4 4 67.29 10.50 10 4 4 198.78 9.70 -10 5 4 446.36 19.50 -9 5 4 595.14 19.60 -8 5 4 653.33 16.90 -7 5 4 1114.09 27.30 -6 5 4 0.00 4.60 -5 5 4 64.29 11.00 -4 5 4 780.22 13.50 -3 5 4 1032.60 17.10 -2 5 4 4060.39 64.29 -1 5 4 2220.98 30.20 0 5 4 514.95 9.20 1 5 4 135.39 3.20 2 5 4 474.65 8.30 3 5 4 442.26 7.10 4 5 4 147.79 8.70 5 5 4 277.57 5.70 6 5 4 175.78 5.80 7 5 4 105.99 5.50 8 5 4 670.03 21.80 9 5 4 337.07 13.60 10 5 4 422.26 33.90 -10 6 4 86.29 12.20 -9 6 4 232.98 9.70 -8 6 4 725.23 13.20 -7 6 4 151.88 7.20 -6 6 4 42.90 3.80 -5 6 4 341.47 8.00 -4 6 4 378.26 8.40 -3 6 4 819.22 41.60 -2 6 4 504.25 9.70 -1 6 4 145.09 6.20 0 6 4 1138.29 17.00 1 6 4 2472.75 35.00 2 6 4 655.23 11.90 3 6 4 2352.96 34.30 4 6 4 359.06 7.10 5 6 4 699.43 12.30 6 6 4 201.68 7.90 7 6 4 520.55 11.80 8 6 4 649.93 15.70 9 6 4 701.53 16.10 10 6 4 437.06 25.50 -10 7 4 639.34 19.90 -9 7 4 34.90 5.90 -8 7 4 96.29 7.20 -7 7 4 398.86 10.60 -6 7 4 957.20 20.10 -5 7 4 475.35 10.70 -4 7 4 2766.52 45.60 -3 7 4 566.34 10.80 -2 7 4 881.31 16.40 -1 7 4 189.18 4.20 0 7 4 794.02 14.00 1 7 4 98.29 13.20 2 7 4 1389.76 20.00 3 7 4 208.58 4.40 4 7 4 6.20 2.10 5 7 4 433.66 10.00 6 7 4 153.88 5.10 7 7 4 820.22 15.80 8 7 4 0.00 5.30 9 7 4 54.49 6.80 -10 8 4 13.50 10.00 -9 8 4 10.90 15.30 -8 8 4 119.09 10.20 -7 8 4 94.69 6.30 -6 8 4 0.00 7.10 -5 8 4 0.00 4.60 -4 8 4 7.10 4.70 -3 8 4 330.57 7.40 -2 8 4 1268.87 18.60 -1 8 4 156.98 4.20 0 8 4 2298.57 53.79 1 8 4 52.19 4.50 2 8 4 697.63 16.50 3 8 4 994.40 18.90 4 8 4 719.73 21.80 5 8 4 323.87 9.60 6 8 4 1194.78 19.30 7 8 4 201.08 6.40 8 8 4 179.68 10.00 9 8 4 0.50 8.50 -10 9 4 502.85 41.20 -9 9 4 497.75 42.50 -8 9 4 516.75 19.20 -7 9 4 1659.33 34.10 -6 9 4 51.09 4.80 -5 9 4 452.95 9.80 -4 9 4 348.37 9.00 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0.60 14.80 2 -3 20 84.59 26.00 3 -3 20 194.58 13.30 -3 -2 20 331.37 17.80 -2 -2 20 339.67 15.60 -1 -2 20 0.00 27.30 1 -2 20 126.99 18.80 2 -2 20 399.16 17.50 3 -2 20 0.00 18.30 -3 -1 20 88.39 10.50 -2 -1 20 601.54 78.99 0 -1 20 16.90 12.50 1 -1 20 7.00 11.00 2 -1 20 210.78 16.90 -2 0 20 348.07 27.10 -1 0 20 473.65 18.30 0 0 20 115.99 9.50 1 0 20 0.00 11.50 2 0 20 5.40 47.70 -3 1 20 61.29 28.50 -2 1 20 55.19 11.20 -1 1 20 125.29 10.50 0 1 20 172.28 13.50 1 1 20 976.00 65.69 -3 2 20 297.77 25.10 -2 2 20 76.49 21.00 -1 2 20 209.08 24.70 1 2 20 48.00 23.50 2 2 20 99.89 11.30 -2 3 20 972.90 64.79 1 3 20 105.09 50.09 -1 4 20 100.69 55.19 0 4 20 9.40 20.80 -1 -3 21 119.29 15.50 0 -3 21 0.00 27.90 -1 -2 21 0.90 24.00 0 -1 21 82.99 20.40 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 12817 _shelx_res_file ; TITL flubbi-copy_a.res in P-1 flubbi-copy-copy.res created by SHELXL-2018/3 at 17:44:04 on 08-Jun-2021 REM Old TITL flubbi_a.res in P-1 REM SHELXT solution in P-1: R1 0.106, Rweak 0.007, Alpha 0.161 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C81 Cl2 Eu6 N28 Na2 O42 CELL 0.71073 9.2252 16.9373 17.2739 96.366 92.395 93.259 ZERR 2 0.0018 0.0034 0.0035 0.03 0.03 0.03 LATT 1 SFAC C H Cl Eu N Na O UNIT 64 147.09 2 6 16 2 63.72 RIGU 0.001 0.001 Eu11 O1 O17 O3 O2 O5 H5a H5b O13 O4 O25 N1 N4 N2 N3 C1 H1a = H1B C3 C8 C17 H17A H17B C22 H22A H22B C23 C24 H24A H24B C25 H25A H25B C26 = H26A H26B C27 H27A H27B C28 H28A H28B C29 H29A H29B C30 H30A H30B C31 H31A = H31B C32 O11 C11 RIGU 0.001 0.001 Eu12 O6 O10 H10a H10b O20 O9 N5 N8 C4 H4a H4b C5 C7 H7a = H7B C9 C13 H13A H13B O8 O16 O23 O7 O15 N7 N6 C2 H2A C6 H6A H6B C10 H10C = H10D C12 C14 H14A H14B C15 H15A H15B C16 C18 H18C H18D C19 C20 H20A H20B = C21 H21B H21A H2B DELU 0.0001 0.0002 O31 ISOR 0.005 0.01 O32 ISOR 0.005 0.01 O33 ISOR 0.001 0.002 O31 DFIX -1.83 0.01 H26c H27c DFIX -1.85 0.01 H24c H26d DFIX -1.85 0.01 H18b H35b ISOR 0.001 0.002 O30 H30c H30d O30A O35 H35a H35b O35A L.S. 20 PLAN 6 SIZE 0.12 0.711 1.198 TEMP 23 CONF BOND LIST 6 MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.091500 70.022896 FVAR 0.24703 0.77303 0.49802 0.71464 EU11 4 0.797417 0.472486 0.692377 11.00000 0.00967 0.00505 = 0.01449 -0.00420 0.00180 0.00058 EU12 4 0.847808 0.026353 0.307581 11.00000 0.01156 0.00528 = 0.01115 -0.00183 0.00497 0.00149 EU2 4 0.321063 0.223222 0.466265 11.00000 0.01282 0.00752 = 0.01182 -0.00096 0.00002 -0.00343 CL1 3 0.999147 0.748896 1.004013 11.00000 0.01554 0.02274 = 0.02052 -0.00540 0.00441 -0.00157 NA1 6 1.660242 0.991905 0.978781 11.00000 0.02350 0.02800 = 0.03808 0.00688 -0.00531 -0.00065 O1 7 0.607880 0.413640 0.603434 11.00000 0.01887 0.01331 = 0.02029 -0.00022 -0.00003 -0.00313 O6 7 0.662083 0.076882 0.385760 11.00000 0.02297 0.01136 = 0.01102 -0.00128 0.00644 0.00734 O10 7 0.922660 0.045618 0.452068 11.00000 0.02301 0.01266 = 0.01303 0.00167 0.00204 0.00273 AFIX 7 H10A 2 0.975157 0.090150 0.461149 11.00000 -1.50000 H10B 2 0.848062 0.032416 0.474068 11.00000 -1.50000 AFIX 0 O17 7 0.574846 0.676534 0.608719 11.00000 0.01835 0.01260 = 0.02265 0.00124 0.00087 0.00015 O3 7 1.038806 0.531399 0.693934 11.00000 0.01464 0.01336 = 0.02438 -0.00313 0.00046 0.00125 O20 7 0.550000 0.182393 0.433369 11.00000 0.02869 0.00989 = 0.01682 -0.00049 0.01067 0.00799 O8 7 1.087184 -0.017531 0.318008 11.00000 0.01448 0.01446 = 0.01823 -0.00307 0.00154 0.00287 O2 7 0.741917 0.595924 0.644123 11.00000 0.01449 0.01093 = 0.02081 -0.00222 0.00311 0.00132 O16 7 0.607380 -0.152263 0.422038 11.00000 0.02820 0.01511 = 0.02581 0.00412 0.00908 -0.00457 O5 7 0.874267 0.469170 0.553290 11.00000 0.01565 0.01840 = 0.02508 -0.00979 0.00414 -0.00011 AFIX 7 H5A 2 0.834349 0.428059 0.526160 11.00000 -1.50000 H5B 2 0.839985 0.508119 0.532689 11.00000 -1.50000 AFIX 0 O23 7 1.215376 -0.126430 0.311537 11.00000 0.02243 0.02235 = 0.04250 0.00079 -0.00143 0.01060 O19 7 1.345100 0.499541 0.980684 11.00000 0.02456 0.01355 = 0.03464 0.00499 0.01991 0.00144 O7 7 0.977789 0.151463 0.345737 11.00000 0.03025 0.00806 = 0.01708 -0.00146 0.00299 -0.00414 O13 7 1.164018 0.648918 0.703009 11.00000 0.02841 0.01658 = 0.03433 0.00052 0.00710 -0.00431 O15 7 1.201500 0.206683 0.338222 11.00000 0.03601 0.02491 = 0.01813 0.00289 -0.00820 -0.01658 O9 7 0.788321 -0.092566 0.366161 11.00000 0.02149 0.00861 = 0.02479 0.00200 0.00814 0.00041 O4 7 0.905760 0.351392 0.656856 11.00000 0.02326 0.01128 = 0.04255 -0.00781 0.00004 0.00590 O14 7 0.291704 0.078801 0.415406 11.00000 0.03250 0.01413 = 0.04779 -0.00485 -0.01897 -0.00378 AFIX 7 H14 2 0.303222 0.058361 0.458846 11.00000 -1.50000 AFIX 0 O12 7 0.154820 0.328050 0.477964 11.00000 0.03113 0.03232 = 0.05298 0.01979 0.02456 0.01765 AFIX 7 H12A 2 0.066589 0.312759 0.454574 11.00000 -1.50000 H12B 2 0.183319 0.369489 0.452303 11.00000 -1.50000 AFIX 0 O18 7 0.099491 0.172173 0.517999 11.00000 0.02704 0.01825 = 0.06393 0.01652 0.01421 -0.00336 AFIX 7 H18A 2 0.115760 0.137601 0.556717 11.00000 -1.50000 H18B 2 0.047533 0.211552 0.547371 11.00000 -1.50000 AFIX 6 O21 7 0.772690 0.544266 0.406926 11.00000 0.05283 0.02539 = 0.05339 -0.02139 0.00331 0.00212 H21C 2 0.853930 0.525269 0.416632 11.00000 -1.50000 H21D 2 0.780492 0.594676 0.416728 11.00000 -1.50000 AFIX 6 O22 7 1.714350 0.663043 1.070726 11.00000 0.02516 0.04813 = 0.03136 0.00379 0.01106 -0.00037 H22C 2 1.696344 0.711204 1.084205 11.00000 -1.50000 H22D 2 1.788823 0.666071 1.043679 11.00000 -1.50000 AFIX 0 O11 7 0.454545 0.313230 0.555422 11.00000 0.04674 0.01943 = 0.03514 -0.00138 -0.01924 -0.00854 O24 7 1.294043 0.845076 1.065541 11.00000 0.03102 0.05118 = 0.03975 -0.01408 0.01530 -0.00772 AFIX 7 H24C 2 1.302028 0.860025 1.011801 11.00000 -1.50000 H24D 2 1.268319 0.898325 1.104070 11.00000 -1.50000 AFIX 0 O25 7 1.093256 0.276636 0.669833 11.00000 0.03764 0.02194 = 0.06196 -0.00055 0.00492 0.01743 AFIX 6 O26 7 1.501909 0.747566 1.005558 11.00000 0.01927 0.02735 = 0.07747 0.01159 0.00743 0.00242 H26C 2 1.452881 0.786514 1.021813 11.00000 -1.50000 H26D 2 1.550551 0.764171 0.969271 11.00000 -1.50000 AFIX 0 O27 7 1.715241 0.830054 0.933764 11.00000 0.02456 0.10016 = 0.02616 0.01563 0.00997 0.00278 AFIX 7 H27C 2 1.686663 0.801493 0.874445 11.00000 -1.50000 H27D 2 1.815642 0.807525 0.939840 11.00000 -1.50000 AFIX 6 O29 7 1.270218 0.645200 0.939430 11.00000 0.02503 0.05127 = 0.05594 -0.01641 -0.01327 0.01432 H29C 2 1.339871 0.672136 0.965652 11.00000 -1.50000 H29D 2 1.199591 0.675272 0.942475 11.00000 -1.50000 AFIX 6 PART 1 O30 7 -0.268163 0.361168 0.437770 31.00000 0.02300 0.02406 = 0.02170 0.00229 0.00140 0.00077 H30C 2 -0.326439 0.321937 0.444052 21.00000 -1.50000 H30D 2 -0.215836 0.343515 0.401124 21.00000 -1.50000 AFIX 0 PART 2 O30A 7 -0.224071 0.331902 0.452304 -31.00000 0.02446 0.02420 = 0.02402 0.00206 0.00235 0.00066 PART 0 AFIX 6 O31 7 -0.500000 0.000000 0.500000 10.25000 0.03054 0.03051 = 0.03010 0.00356 0.00284 0.00370 H31C 2 -0.443528 0.041239 0.498838 10.50000 -1.50000 H31D 2 -0.555484 -0.000789 0.459272 10.50000 -1.50000 AFIX 0 O32 7 -0.302492 0.075989 0.547944 10.55000 0.02528 0.06763 = 0.03175 -0.00243 0.00933 0.00029 O33 7 -0.238057 0.160166 0.541559 10.45000 0.03672 0.03964 = 0.03750 0.00222 0.00575 0.00658 O34 7 0.562876 0.496742 0.480818 0.61075 0.05537 0.04780 = 0.06739 0.00521 0.02727 0.01359 PART 1 AFIX 6 O35 7 -0.068685 0.267673 0.528296 41.00000 0.01823 0.01530 = 0.01625 0.00015 0.00579 0.00040 PART 0 H35A 2 -0.127689 0.273876 0.490594 11.00000 -1.50000 H35B 2 -0.120082 0.270766 0.568083 11.00000 -1.50000 AFIX 0 N5 5 0.645519 0.108701 0.239167 11.00000 0.01855 0.00875 = 0.01181 -0.00186 0.00551 0.00254 N7 5 0.922060 -0.072459 0.188203 11.00000 0.01341 0.00874 = 0.01653 -0.00533 0.00491 0.00053 N6 5 0.947691 0.101285 0.192839 11.00000 0.01391 0.01107 = 0.01457 -0.00115 0.00196 -0.00234 N8 5 0.625985 -0.065885 0.242569 11.00000 0.01588 0.00729 = 0.02075 -0.00321 0.00754 -0.00016 N1 5 0.581582 0.551133 0.759513 11.00000 0.02952 0.02386 = 0.02356 0.00376 0.01402 0.01316 N4 5 0.883116 0.572103 0.817795 11.00000 0.03491 0.01961 = 0.01654 -0.00879 0.00329 -0.01030 N2 5 0.594480 0.376343 0.748795 11.00000 0.02707 0.02123 = 0.02200 -0.00095 0.00263 -0.00944 N3 5 0.900942 0.398976 0.808855 11.00000 0.02817 0.02595 = 0.03442 0.01111 -0.00273 0.00927 C1 1 0.555770 0.312311 0.686063 11.00000 0.01702 0.01530 = 0.02342 0.00241 -0.00231 -0.00614 AFIX 23 H1A 2 0.464745 0.284714 0.696288 11.00000 -1.20000 H1B 2 0.630550 0.274223 0.683170 11.00000 -1.20000 AFIX 0 C2 1 0.851612 0.166226 0.176801 11.00000 0.01819 0.01282 = 0.01621 0.00196 0.00482 0.00107 AFIX 23 H2A 2 0.880254 0.187259 0.129344 11.00000 -1.20000 H2B 2 0.865714 0.209036 0.219123 11.00000 -1.20000 AFIX 0 C3 1 0.615172 0.621894 0.645195 11.00000 0.01428 0.00785 = 0.01212 -0.00628 0.00235 0.00017 C4 1 0.620644 0.174661 0.299639 11.00000 0.02043 0.00981 = 0.01334 -0.00149 0.00420 0.00579 AFIX 23 H4A 2 0.531766 0.199128 0.286324 11.00000 -1.20000 H4B 2 0.700467 0.214831 0.302136 11.00000 -1.20000 AFIX 0 C5 1 0.608861 0.143222 0.378945 11.00000 0.01657 0.00854 = 0.01324 -0.00306 0.00336 0.00331 C6 1 1.017647 -0.031710 0.136141 11.00000 0.01155 0.01578 = 0.01456 -0.00285 0.00241 -0.00060 AFIX 23 H6A 2 1.023513 -0.065533 0.087380 11.00000 -1.20000 H6B 2 1.114819 -0.022788 0.160378 11.00000 -1.20000 AFIX 0 C7 1 0.693524 0.139366 0.168104 11.00000 0.01746 0.01359 = 0.01341 0.00081 0.00486 0.00194 AFIX 23 H7A 2 0.636813 0.183735 0.157301 11.00000 -1.20000 H7B 2 0.677673 0.098075 0.124468 11.00000 -1.20000 AFIX 0 C8 1 1.067693 0.602959 0.723727 11.00000 0.01831 0.01232 = 0.01382 0.00117 -0.00453 0.00125 C9 1 0.527917 -0.025607 0.190872 11.00000 0.01503 0.01020 = 0.02151 -0.00112 0.00858 -0.00060 AFIX 23 H9A 2 0.434558 -0.055484 0.183618 11.00000 -1.20000 H9B 2 0.569225 -0.025181 0.140184 11.00000 -1.20000 AFIX 0 C10 1 0.960978 0.047150 0.119715 11.00000 0.00613 0.01562 = 0.01413 -0.00134 0.00423 -0.00277 AFIX 23 H10C 2 1.026407 0.072540 0.086130 11.00000 -1.20000 H10D 2 0.866529 0.037819 0.092355 11.00000 -1.20000 AFIX 0 C11 1 0.540657 0.348678 0.608353 11.00000 0.02521 0.01491 = 0.02242 0.00088 -0.00339 -0.00606 C12 1 1.113626 -0.088849 0.289350 11.00000 0.01587 0.01421 = 0.02215 -0.00111 0.00546 0.00492 C13 1 0.505370 0.059538 0.224526 11.00000 0.01749 0.01077 = 0.01788 -0.00080 0.00608 0.00233 AFIX 23 H13A 2 0.443010 0.083833 0.188519 11.00000 -1.20000 H13B 2 0.456562 0.058792 0.273124 11.00000 -1.20000 AFIX 0 C14 1 0.548864 -0.091924 0.308895 11.00000 0.02141 0.00851 = 0.02032 -0.00329 0.00843 -0.00108 AFIX 23 H14A 2 0.482363 -0.137279 0.290862 11.00000 -1.20000 H14B 2 0.492269 -0.049280 0.331218 11.00000 -1.20000 AFIX 0 C15 1 0.796331 -0.115547 0.142972 11.00000 0.01494 0.01393 = 0.01861 -0.00774 0.00524 -0.00167 AFIX 23 H15A 2 0.827811 -0.163815 0.114744 11.00000 -1.20000 H15B 2 0.759344 -0.082555 0.105094 11.00000 -1.20000 AFIX 0 C16 1 1.087560 0.168402 0.308790 11.00000 0.02549 0.01082 = 0.01507 -0.00042 -0.00156 -0.00557 C17 1 0.505744 0.583123 0.694207 11.00000 0.02158 0.02064 = 0.03102 0.00835 0.01359 0.00687 AFIX 23 H17A 2 0.439366 0.621962 0.714279 11.00000 -1.20000 H17B 2 0.449522 0.540407 0.662321 11.00000 -1.20000 AFIX 0 C18 1 0.676887 -0.136668 0.194891 11.00000 0.01699 0.00849 = 0.02676 -0.00679 0.00877 -0.00171 AFIX 23 H18C 2 0.595522 -0.163173 0.162988 11.00000 -1.20000 H18D 2 0.711526 -0.173714 0.229396 11.00000 -1.20000 AFIX 0 C19 1 0.655927 -0.114941 0.371507 11.00000 0.02205 0.01114 = 0.02472 0.00233 0.00859 -0.00073 C20 1 1.089736 0.136648 0.222478 11.00000 0.01673 0.01068 = 0.01553 0.00026 -0.00083 -0.00481 AFIX 23 H20A 2 1.118033 0.179861 0.192724 11.00000 -1.20000 H20B 2 1.161324 0.096967 0.215753 11.00000 -1.20000 AFIX 0 C21 1 1.009100 -0.129877 0.225933 11.00000 0.01759 0.01080 = 0.02232 -0.00333 0.00647 0.00481 AFIX 23 H21A 2 1.063316 -0.159569 0.186826 11.00000 -1.20000 H21B 2 0.944103 -0.167427 0.248125 11.00000 -1.20000 AFIX 0 C22 1 0.972819 0.636370 0.788103 11.00000 0.02443 0.01592 = 0.02129 -0.00991 0.00055 -0.00725 AFIX 23 H22A 2 1.034082 0.664456 0.830557 11.00000 -1.20000 H22B 2 0.909892 0.674116 0.767999 11.00000 -1.20000 AFIX 0 C23 1 1.011257 0.326750 0.696535 11.00000 0.02200 0.01036 = 0.04981 -0.00069 -0.00047 0.00301 C24 1 0.653543 0.624662 0.815281 11.00000 0.04770 0.02741 = 0.02319 -0.00090 0.01777 0.00664 AFIX 23 H24A 2 0.691126 0.664559 0.783904 11.00000 -1.20000 H24B 2 0.579766 0.648202 0.847267 11.00000 -1.20000 AFIX 0 C25 1 1.036336 0.365679 0.779575 11.00000 0.02760 0.02092 = 0.04899 -0.00022 -0.00447 0.00521 AFIX 23 H25A 2 1.068167 0.326699 0.812682 11.00000 -1.20000 H25B 2 1.112357 0.407951 0.781629 11.00000 -1.20000 AFIX 0 C26 1 0.986411 0.525017 0.870857 11.00000 0.04775 0.03949 = 0.02508 0.00120 -0.00028 0.00018 AFIX 23 H26A 2 1.079411 0.520442 0.847068 11.00000 -1.20000 H26B 2 1.003635 0.555778 0.921537 11.00000 -1.20000 AFIX 0 C27 1 0.773322 0.601830 0.866663 11.00000 0.04464 0.02728 = 0.02642 -0.00177 0.01251 -0.00293 AFIX 23 H27A 2 0.812168 0.647688 0.901523 11.00000 -1.20000 H27B 2 0.737946 0.561229 0.897848 11.00000 -1.20000 AFIX 0 C28 1 0.791827 0.326803 0.818255 11.00000 0.04341 0.03475 = 0.04313 0.01665 0.00283 0.00013 AFIX 23 H28A 2 0.801987 0.285505 0.775556 11.00000 -1.20000 H28B 2 0.817718 0.305279 0.866359 11.00000 -1.20000 AFIX 0 C29 1 0.641295 0.346613 0.819500 11.00000 0.03960 0.03550 = 0.02567 0.00291 -0.00390 -0.00880 AFIX 23 H29A 2 0.580730 0.299552 0.826793 11.00000 -1.20000 H29B 2 0.629469 0.386480 0.863243 11.00000 -1.20000 AFIX 0 C30 1 0.455379 0.425417 0.763763 11.00000 0.03681 0.03474 = 0.03853 0.00004 0.01435 0.00111 AFIX 23 H30A 2 0.405451 0.429659 0.713989 11.00000 -1.20000 H30B 2 0.389876 0.396078 0.794297 11.00000 -1.20000 AFIX 0 C31 1 0.486311 0.504755 0.803846 11.00000 0.04233 0.03142 = 0.02641 0.00637 0.01518 0.00461 AFIX 23 H31A 2 0.396187 0.530873 0.811108 11.00000 -1.20000 H31B 2 0.531864 0.501265 0.854888 11.00000 -1.20000 AFIX 0 C32 1 0.927073 0.445798 0.881714 11.00000 0.04273 0.03766 = 0.03661 0.00580 -0.00010 0.00694 AFIX 23 H32A 2 0.994972 0.420398 0.913888 11.00000 -1.20000 H32B 2 0.836883 0.449861 0.908393 11.00000 -1.20000 AFIX 0 PART 2 O35A 7 -0.165298 0.241971 0.537919 -41.00000 0.01593 0.01656 = 0.01602 0.00075 0.00003 0.00125 HKLF 4 REM flubbi-copy_a.res in P-1 REM wR2 = 0.1707, GooF = S = 1.038, Restrained GooF = 1.002 for all data REM R1 = 0.0622 for 8308 Fo > 4sig(Fo) and 0.0813 for all 9966 data REM 759 parameters refined using 907 restraints END WGHT 0.0915 69.9896 REM Highest difference peak 3.468, deepest hole -1.940, 1-sigma level 0.317 Q1 1 0.8616 0.0020 0.2646 11.00000 0.05 3.47 Q2 1 0.8152 0.4453 0.6452 11.00000 0.05 3.05 Q3 1 0.3140 0.2526 0.5143 11.00000 0.05 2.81 Q4 1 -0.3278 0.1216 0.5361 11.00000 0.05 2.70 Q5 1 0.7816 0.4946 0.7353 11.00000 0.05 2.69 Q6 1 0.3325 0.1996 0.4232 11.00000 0.05 2.20 ; _shelx_res_checksum 74685 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Eu Eu11 0.79742(5) 0.47249(3) 0.69238(3) 0.01010(14) Uani d 1 . . Eu Eu12 0.84781(5) 0.02635(3) 0.30758(3) 0.00938(14) Uani d 1 . . Eu Eu2 0.32106(5) 0.22322(3) 0.46627(3) 0.01105(14) Uani d 1 . . Cl Cl1 0.9991(3) 0.74890(15) 1.00401(15) 0.0202(5) Uani d 1 . . Na Na1 1.6602(5) 0.9919(3) 0.9788(3) 0.0299(10) Uani d 1 . . O O1 0.6079(8) 0.4136(4) 0.6034(4) 0.0178(11) Uani d 1 . . O O6 0.6621(8) 0.0769(4) 0.3858(4) 0.0149(10) Uani d 1 . . O O10 0.9227(8) 0.0456(4) 0.4521(4) 0.0161(11) Uani d 1 . . H H10A 0.975157 0.090150 0.461149 0.024 Uiso d 1 . . H H10B 0.848062 0.032416 0.474068 0.024 Uiso d 1 . . O O17 0.5748(8) 0.6765(4) 0.6087(4) 0.0180(14) Uani d 1 . . O O3 1.0388(7) 0.5314(4) 0.6939(4) 0.0179(11) Uani d 1 . . O O13 0.5500(8) 0.1824(4) 0.4334(4) 0.0181(14) Uani d 1 . . O O8 1.0872(7) -0.0175(4) 0.3180(4) 0.0160(10) Uani d 1 . . O O2 0.7419(7) 0.5959(4) 0.6441(4) 0.0156(10) Uani d 1 . . O O16 0.6074(8) -0.1523(4) 0.4220(5) 0.0229(15) Uani d 1 . . O O5 0.8743(7) 0.4692(4) 0.5533(4) 0.0206(12) Uani d 1 . . H H5A 0.834349 0.428059 0.526160 0.031 Uiso d 1 . . H H5B 0.839985 0.508119 0.532689 0.031 Uiso d 1 . . O O23 1.2154(9) -0.1264(5) 0.3115(5) 0.0290(17) Uani d 1 . . O O19 1.3451(8) 0.4995(4) 0.9807(5) 0.0236(17) Uani d 1 . . O O7 0.9778(8) 0.1515(4) 0.3457(4) 0.0188(11) Uani d 1 . . O O20 1.1640(9) 0.6489(4) 0.7030(5) 0.0267(17) Uani d 1 . . O O15 1.2015(9) 0.2067(5) 0.3382(4) 0.0273(17) Uani d 1 . . O O9 0.7883(8) -0.0926(4) 0.3662(4) 0.0181(11) Uani d 1 . . O O4 0.9058(8) 0.3514(4) 0.6569(5) 0.0264(12) Uani d 1 . . O O14 0.2917(9) 0.0788(5) 0.4154(6) 0.033(2) Uani d 1 . . H H14 0.303222 0.058361 0.458846 0.049 Uiso d 1 . . O O12 0.1548(10) 0.3280(5) 0.4780(6) 0.036(2) Uani d 1 . . H H12A 0.066589 0.312759 0.454574 0.055 Uiso d 1 . . H H12B 0.183319 0.369489 0.452303 0.055 Uiso d 1 . . O O18 0.0995(9) 0.1722(5) 0.5180(6) 0.035(2) Uani d 1 . . H H18A 0.115760 0.137601 0.556717 0.053 Uiso d 1 . . H H18B 0.047533 0.211552 0.547371 0.053 Uiso d 1 . . O O21 0.7727(11) 0.5443(6) 0.4069(6) 0.046(3) Uani d 1 . . H H21C 0.853930 0.525269 0.416632 0.069 Uiso d 1 . . H H21D 0.780492 0.594676 0.416728 0.069 Uiso d 1 . . O O22 1.7143(9) 0.6630(6) 1.0707(5) 0.035(2) Uani d 1 . . H H22C 1.696344 0.711204 1.084205 0.052 Uiso d 1 . . H H22D 1.788823 0.666071 1.043679 0.052 Uiso d 1 . . O O11 0.4545(10) 0.3132(5) 0.5554(5) 0.035(2) Uani d 1 . . O O24 1.2940(10) 0.8451(6) 1.0655(6) 0.042(2) Uani d 1 . . H H24C 1.302028 0.860025 1.011801 0.063 Uiso d 1 . . H H24D 1.268319 0.898325 1.104070 0.063 Uiso d 1 . . O O25 1.0933(10) 0.2766(5) 0.6698(6) 0.040(2) Uani d 1 . . O O26 1.5019(9) 0.7476(5) 1.0056(7) 0.041(2) Uani d 1 . . H H26C 1.452881 0.786514 1.021813 0.061 Uiso d 1 . . H H26D 1.550551 0.764171 0.969271 0.061 Uiso d 1 . . O O27 1.7152(10) 0.8301(7) 0.9338(5) 0.049(3) Uani d 1 . . H H27C 1.686663 0.801493 0.874445 0.074 Uiso d 1 . . H H27D 1.815642 0.807525 0.939840 0.074 Uiso d 1 . . O O29 1.2702(10) 0.6452(6) 0.9394(6) 0.046(3) Uani d 1 . . H H29C 1.339871 0.672136 0.965652 0.069 Uiso d 1 . . H H29D 1.199591 0.675272 0.942475 0.069 Uiso d 1 . . O O30 -0.268(2) 0.3612(13) 0.4378(10) 0.023(6) Uani d 0.50(5) A 1 H H30C -0.326439 0.321937 0.444052 0.034 Uiso d 0.77(17) B 1 H H30D -0.215836 0.343515 0.401124 0.034 Uiso d 0.77(17) B 1 O O30A -0.224(2) 0.3319(13) 0.4523(11) 0.024(6) Uani d 0.50(5) A 2 O O31 -0.500000 0.000000 0.500000 0.030(5) Uani d 0.5 . . H H31C -0.443528 0.041239 0.498838 0.045 Uiso d 0.5 . . H H31D -0.555484 -0.000789 0.459272 0.045 Uiso d 0.5 . . O O32 -0.3025(17) 0.0760(12) 0.5479(10) 0.042(4) Uani d 0.55 C . O O33 -0.238(2) 0.1602(12) 0.5416(12) 0.038(5) Uani d 0.45 . . O O34 0.563(2) 0.4967(11) 0.4808(12) 0.056(7) Uani d 0.61(3) . . O O35 -0.0687(11) 0.2677(6) 0.5283(6) 0.017(3) Uani d 0.71(3) C 1 H H35A -0.127689 0.273876 0.490594 0.025 Uiso d 1 . . H H35B -0.120082 0.270766 0.568083 0.025 Uiso d 1 . . N N5 0.6455(9) 0.1087(5) 0.2392(5) 0.0131(10) Uani d 1 . . N N7 0.9221(9) -0.0725(5) 0.1882(5) 0.0133(10) Uani d 1 . . N N6 0.9477(9) 0.1013(5) 0.1928(5) 0.0135(10) Uani d 1 . . N N8 0.6260(9) -0.0659(5) 0.2426(5) 0.0148(10) Uani d 1 . . N N1 0.5816(11) 0.5511(6) 0.7595(6) 0.0248(12) Uani d 1 . . N N4 0.8831(11) 0.5721(5) 0.8178(5) 0.0249(12) Uani d 1 . . N N2 0.5945(10) 0.3763(6) 0.7488(6) 0.0241(12) Uani d 1 . . N N3 0.9009(11) 0.3990(6) 0.8089(6) 0.0288(12) Uani d 1 . . C C1 0.5558(11) 0.3123(6) 0.6861(6) 0.0189(17) Uani d 1 . . H H1A 0.464745 0.284714 0.696288 0.023 Uiso calc 1 . . H H1B 0.630550 0.274223 0.683170 0.023 Uiso calc 1 . . C C2 0.8516(11) 0.1662(6) 0.1768(6) 0.0156(15) Uani d 1 . . H H2A 0.880254 0.187259 0.129344 0.019 Uiso calc 1 . . H H2B 0.865714 0.209036 0.219123 0.019 Uiso calc 1 . . C C3 0.6152(10) 0.6219(5) 0.6452(6) 0.0119(15) Uani d 1 . . C C4 0.6206(11) 0.1747(6) 0.2996(6) 0.0145(16) Uani d 1 . . H H4A 0.531766 0.199128 0.286324 0.017 Uiso calc 1 . . H H4B 0.700467 0.214831 0.302136 0.017 Uiso calc 1 . . C C5 0.6089(11) 0.1432(6) 0.3789(6) 0.0129(14) Uani d 1 . . C C6 1.0176(10) -0.0317(6) 0.1361(6) 0.0143(15) Uani d 1 . . H H6A 1.023513 -0.065533 0.087380 0.017 Uiso calc 1 . . H H6B 1.114819 -0.022788 0.160378 0.017 Uiso calc 1 . . C C7 0.6935(11) 0.1394(6) 0.1681(6) 0.0147(15) Uani d 1 . . H H7A 0.636813 0.183735 0.157301 0.018 Uiso calc 1 . . H H7B 0.677673 0.098075 0.124468 0.018 Uiso calc 1 . . C C8 1.0677(11) 0.6030(6) 0.7237(6) 0.0150(13) Uani d 1 . . C C9 0.5279(11) -0.0256(6) 0.1909(6) 0.0156(15) Uani d 1 . . H H9A 0.434558 -0.055484 0.183618 0.019 Uiso calc 1 . . H H9B 0.569225 -0.025181 0.140184 0.019 Uiso calc 1 . . C C10 0.9610(10) 0.0471(6) 0.1197(6) 0.0122(14) Uani d 1 . . H H10C 1.026407 0.072540 0.086130 0.015 Uiso calc 1 . . H H10D 0.866529 0.037819 0.092355 0.015 Uiso calc 1 . . C C11 0.5407(12) 0.3487(6) 0.6084(7) 0.0213(16) Uani d 1 . . C C12 1.1136(11) -0.0888(6) 0.2894(6) 0.0174(14) Uani d 1 . . C C13 0.5054(11) 0.0595(6) 0.2245(6) 0.0154(16) Uani d 1 . . H H13A 0.443010 0.083833 0.188519 0.018 Uiso calc 1 . . H H13B 0.456562 0.058792 0.273124 0.018 Uiso calc 1 . . C C14 0.5489(11) -0.0919(6) 0.3089(6) 0.0170(15) Uani d 1 . . H H14A 0.482363 -0.137279 0.290862 0.020 Uiso calc 1 . . H H14B 0.492269 -0.049280 0.331218 0.020 Uiso calc 1 . . C C15 0.7963(11) -0.1155(6) 0.1430(6) 0.0165(16) Uani d 1 . . H H15A 0.827811 -0.163815 0.114744 0.020 Uiso calc 1 . . H H15B 0.759344 -0.082555 0.105094 0.020 Uiso calc 1 . . C C16 1.0876(12) 0.1684(6) 0.3088(6) 0.0176(13) Uani d 1 . . C C17 0.5057(12) 0.5831(7) 0.6942(7) 0.0234(18) Uani d 1 . . H H17A 0.439366 0.621962 0.714279 0.028 Uiso calc 1 . . H H17B 0.449522 0.540407 0.662321 0.028 Uiso calc 1 . . C C18 0.6769(11) -0.1367(6) 0.1949(6) 0.0180(17) Uani d 1 . . H H18C 0.595522 -0.163173 0.162988 0.022 Uiso calc 1 . . H H18D 0.711526 -0.173714 0.229396 0.022 Uiso calc 1 . . C C19 0.6559(12) -0.1149(6) 0.3715(6) 0.0191(14) Uani d 1 . . C C20 1.0897(11) 0.1366(6) 0.2225(6) 0.0147(15) Uani d 1 . . H H20A 1.118033 0.179861 0.192724 0.018 Uiso calc 1 . . H H20B 1.161324 0.096967 0.215753 0.018 Uiso calc 1 . . C C21 1.0091(11) -0.1299(6) 0.2259(6) 0.0170(15) Uani d 1 . . H H21A 1.063316 -0.159569 0.186826 0.020 Uiso calc 1 . . H H21B 0.944103 -0.167427 0.248125 0.020 Uiso calc 1 . . C C22 0.9728(12) 0.6364(6) 0.7881(6) 0.0218(18) Uani d 1 . . H H22A 1.034082 0.664456 0.830557 0.026 Uiso calc 1 . . H H22B 0.909892 0.674116 0.767999 0.026 Uiso calc 1 . . C C23 1.0113(12) 0.3267(6) 0.6965(8) 0.0277(16) Uani d 1 . . C C24 0.6535(15) 0.6247(7) 0.8153(7) 0.0324(19) Uani d 1 . . H H24A 0.691126 0.664559 0.783904 0.039 Uiso calc 1 . . H H24B 0.579766 0.648202 0.847267 0.039 Uiso calc 1 . . C C25 1.0363(13) 0.3657(7) 0.7796(8) 0.033(2) Uani d 1 . . H H25A 1.068167 0.326699 0.812682 0.039 Uiso calc 1 . . H H25B 1.112357 0.407951 0.781629 0.039 Uiso calc 1 . . C C26 0.9864(16) 0.5250(8) 0.8709(8) 0.038(2) Uani d 1 . . H H26A 1.079411 0.520442 0.847068 0.045 Uiso calc 1 . . H H26B 1.003635 0.555778 0.921537 0.045 Uiso calc 1 . . C C27 0.7733(14) 0.6018(8) 0.8667(7) 0.0330(19) Uani d 1 . . H H27A 0.812168 0.647688 0.901523 0.040 Uiso calc 1 . . H H27B 0.737946 0.561229 0.897848 0.040 Uiso calc 1 . . C C28 0.7918(15) 0.3268(8) 0.8183(9) 0.040(2) Uani d 1 . . H H28A 0.801987 0.285505 0.775556 0.047 Uiso calc 1 . . H H28B 0.817718 0.305279 0.866359 0.047 Uiso calc 1 . . C C29 0.6413(14) 0.3466(8) 0.8195(7) 0.034(2) Uani d 1 . . H H29A 0.580730 0.299552 0.826793 0.041 Uiso calc 1 . . H H29B 0.629469 0.386480 0.863243 0.041 Uiso calc 1 . . C C30 0.4554(15) 0.4254(8) 0.7638(8) 0.037(2) Uani d 1 . . H H30A 0.405451 0.429659 0.713989 0.044 Uiso calc 1 . . H H30B 0.389876 0.396078 0.794297 0.044 Uiso calc 1 . . C C31 0.4863(15) 0.5048(7) 0.8038(7) 0.033(2) Uani d 1 . . H H31A 0.396187 0.530873 0.811108 0.039 Uiso calc 1 . . H H31B 0.531864 0.501265 0.854888 0.039 Uiso calc 1 . . C C32 0.9271(16) 0.4458(8) 0.8817(8) 0.039(2) Uani d 1 . . H H32A 0.994972 0.420398 0.913888 0.047 Uiso calc 1 . . H H32B 0.836883 0.449861 0.908393 0.047 Uiso calc 1 . . O O35A -0.165(3) 0.2420(15) 0.5379(15) 0.016(8) Uani d 0.29(3) C 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Eu11 0.0097(2) 0.0051(2) 0.0145(3) 0.00058(17) 0.00180(18) -0.00420(17) Eu12 0.0116(2) 0.0053(2) 0.0111(2) 0.00149(17) 0.00497(18) -0.00183(17) Eu2 0.0128(3) 0.0075(2) 0.0118(3) -0.00343(17) 0.00002(18) -0.00096(18) Cl1 0.0155(12) 0.0227(13) 0.0205(13) -0.0016(10) 0.0044(10) -0.0054(10) Na1 0.023(2) 0.028(2) 0.038(3) -0.0006(19) -0.005(2) 0.007(2) O1 0.019(2) 0.013(2) 0.020(3) -0.0031(18) 0.000(2) -0.0002(19) O6 0.023(2) 0.011(2) 0.011(2) 0.0073(18) 0.006(2) -0.0013(18) O10 0.023(3) 0.013(3) 0.013(2) 0.003(2) 0.0020(19) 0.0017(18) O17 0.018(3) 0.013(3) 0.023(3) 0.000(2) 0.001(3) 0.001(2) O3 0.015(2) 0.013(2) 0.024(3) 0.0013(17) 0.0005(19) -0.0031(19) O13 0.029(4) 0.010(3) 0.017(3) 0.008(3) 0.011(3) 0.000(2) O8 0.014(2) 0.014(2) 0.018(3) 0.0029(17) 0.0015(18) -0.0031(19) O2 0.014(2) 0.011(2) 0.021(3) 0.0013(17) 0.0031(18) -0.002(2) O16 0.028(3) 0.015(3) 0.026(3) -0.005(3) 0.009(3) 0.004(2) O5 0.016(3) 0.018(3) 0.025(3) 0.000(2) 0.004(2) -0.0098(19) O23 0.022(3) 0.022(3) 0.042(4) 0.011(3) -0.001(3) 0.001(3) O19 0.025(4) 0.014(4) 0.035(5) 0.001(3) 0.020(3) 0.005(3) O7 0.030(2) 0.008(2) 0.017(2) -0.0041(19) 0.003(2) -0.0015(19) O20 0.028(3) 0.017(3) 0.034(4) -0.004(2) 0.007(3) 0.001(3) O15 0.036(3) 0.025(4) 0.018(3) -0.017(3) -0.008(3) 0.003(3) O9 0.021(2) 0.009(2) 0.025(3) 0.0004(17) 0.0081(18) 0.002(2) O4 0.023(2) 0.011(2) 0.043(3) 0.006(2) 0.000(2) -0.008(2) O14 0.032(5) 0.014(4) 0.048(6) -0.004(3) -0.019(4) -0.005(4) O12 0.031(5) 0.032(5) 0.053(6) 0.018(4) 0.025(4) 0.020(4) O18 0.027(4) 0.018(4) 0.064(6) -0.003(3) 0.014(4) 0.017(4) O21 0.053(6) 0.025(5) 0.053(6) 0.002(4) 0.003(5) -0.021(5) O22 0.025(5) 0.048(6) 0.031(5) 0.000(4) 0.011(4) 0.004(4) O11 0.047(4) 0.019(4) 0.035(3) -0.009(3) -0.019(3) -0.001(3) O24 0.031(5) 0.051(6) 0.040(6) -0.008(4) 0.015(4) -0.014(5) O25 0.038(4) 0.022(4) 0.062(5) 0.017(3) 0.005(4) -0.001(3) O26 0.019(4) 0.027(5) 0.077(8) 0.002(4) 0.007(4) 0.012(5) O27 0.025(5) 0.100(9) 0.026(5) 0.003(5) 0.010(4) 0.016(5) O29 0.025(5) 0.051(6) 0.056(7) 0.014(4) -0.013(4) -0.016(5) O30 0.023(7) 0.024(7) 0.022(7) 0.001(2) 0.001(2) 0.002(2) O30A 0.024(7) 0.024(7) 0.024(7) 0.001(2) 0.002(2) 0.002(2) O31 0.031(6) 0.031(6) 0.030(6) 0.004(2) 0.003(2) 0.004(2) O32 0.025(7) 0.068(8) 0.032(7) 0.000(6) 0.009(6) -0.002(6) O33 0.037(6) 0.040(6) 0.038(6) 0.007(5) 0.006(5) 0.002(5) O34 0.055(12) 0.048(12) 0.067(14) 0.014(9) 0.027(9) 0.005(9) O35 0.018(4) 0.015(4) 0.016(4) 0.0004(19) 0.0058(18) 0.0001(19) N5 0.019(2) 0.009(2) 0.012(2) 0.0025(18) 0.0055(18) -0.0019(18) N7 0.013(2) 0.009(2) 0.017(2) 0.0005(18) 0.0049(16) -0.0053(18) N6 0.014(2) 0.011(2) 0.015(2) -0.0023(17) 0.0020(17) -0.0011(17) N8 0.016(2) 0.007(2) 0.021(2) -0.0002(18) 0.0075(18) -0.0032(18) N1 0.030(2) 0.024(3) 0.024(3) 0.013(2) 0.014(2) 0.0038(19) N4 0.035(3) 0.020(2) 0.017(3) -0.010(2) 0.0033(19) -0.009(2) N2 0.027(2) 0.021(2) 0.022(2) -0.009(2) 0.003(2) -0.001(2) N3 0.028(3) 0.026(3) 0.034(3) 0.009(2) -0.003(2) 0.011(2) C1 0.017(5) 0.015(3) 0.023(3) -0.006(3) -0.002(2) 0.002(2) C2 0.018(3) 0.013(3) 0.016(4) 0.001(2) 0.005(2) 0.002(3) C3 0.014(2) 0.008(3) 0.012(4) 0.000(2) 0.002(2) -0.006(2) C4 0.020(4) 0.010(3) 0.013(2) 0.006(3) 0.004(2) -0.0015(18) C5 0.017(3) 0.009(2) 0.013(2) 0.003(2) 0.003(2) -0.003(2) C6 0.012(3) 0.016(3) 0.015(4) -0.001(2) 0.002(3) -0.003(2) C7 0.017(3) 0.014(4) 0.013(3) 0.002(3) 0.005(2) 0.001(3) C8 0.018(2) 0.012(2) 0.014(3) 0.0013(19) -0.005(2) 0.001(2) C9 0.015(3) 0.010(3) 0.022(3) -0.001(2) 0.009(3) -0.001(2) C10 0.006(4) 0.016(3) 0.014(3) -0.003(2) 0.004(3) -0.0013(19) C11 0.025(3) 0.015(3) 0.022(3) -0.006(2) -0.003(2) 0.001(2) C12 0.016(2) 0.014(2) 0.022(3) 0.0049(19) 0.005(2) -0.001(2) C13 0.017(3) 0.011(3) 0.018(4) 0.0023(19) 0.006(3) -0.001(2) C14 0.021(3) 0.009(4) 0.020(3) -0.001(3) 0.008(2) -0.003(3) C15 0.015(3) 0.014(4) 0.019(3) -0.002(2) 0.0052(19) -0.008(3) C16 0.025(2) 0.011(2) 0.015(3) -0.006(2) -0.0016(19) 0.000(2) C17 0.022(3) 0.021(5) 0.031(3) 0.007(3) 0.014(2) 0.008(3) C18 0.017(3) 0.008(3) 0.027(4) -0.002(2) 0.009(3) -0.007(3) C19 0.022(2) 0.011(3) 0.025(3) -0.001(2) 0.009(2) 0.002(3) C20 0.017(3) 0.011(4) 0.016(3) -0.005(2) -0.001(2) 0.000(2) C21 0.018(3) 0.011(3) 0.022(3) 0.005(2) 0.006(3) -0.003(2) C22 0.024(4) 0.016(3) 0.021(4) -0.007(3) 0.001(3) -0.010(2) C23 0.022(3) 0.010(3) 0.050(3) 0.003(2) 0.000(3) -0.001(3) C24 0.048(4) 0.027(4) 0.023(4) 0.007(3) 0.018(3) -0.001(3) C25 0.028(3) 0.021(5) 0.049(4) 0.005(3) -0.004(3) 0.000(3) C26 0.048(5) 0.039(4) 0.025(5) 0.000(3) 0.000(4) 0.001(3) C27 0.045(4) 0.027(5) 0.026(4) -0.003(3) 0.013(2) -0.002(3) C28 0.043(3) 0.035(4) 0.043(7) 0.000(3) 0.003(3) 0.017(4) C29 0.040(3) 0.036(6) 0.026(3) -0.009(3) -0.004(3) 0.003(3) C30 0.037(4) 0.035(3) 0.039(6) 0.001(3) 0.014(4) 0.000(3) C31 0.042(5) 0.031(3) 0.026(5) 0.005(3) 0.015(4) 0.006(3) C32 0.043(6) 0.038(3) 0.037(3) 0.007(3) 0.000(3) 0.006(2) O35A 0.016(8) 0.017(8) 0.016(8) 0.001(2) 0.000(2) 0.001(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0.00 -1.00 0.00 0.2610 0.00 1.00 0.00 0.3520 0.00 0.00 1.00 0.0600 0.00 0.00 -1.00 0.0120 1.00 0.00 0.00 0.5820 -1.00 0.00 0.00 0.4480 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Eu11 O3 . . 140.7(2) ? O1 Eu11 O2 . . 85.6(2) ? O1 Eu11 O5 . . 69.2(2) ? O1 Eu11 N1 . . 83.7(3) ? O1 Eu11 N4 . . 149.5(3) ? O1 Eu11 N2 . . 63.0(3) ? O1 Eu11 N3 . . 122.3(3) ? O1 Eu11 C8 . . 146.6(2) ? O1 Eu11 C11 . . 18.3(3) ? O1 Eu11 C23 . . 101.3(3) ? O3 Eu11 O2 . . 81.5(2) ? O3 Eu11 O5 . . 71.5(2) ? O3 Eu11 N1 . . 121.6(3) ? O3 Eu11 N4 . . 63.8(3) ? O3 Eu11 N2 . . 151.4(3) ? O3 Eu11 N3 . . 84.2(3) ? O3 Eu11 C8 . . 19.9(2) ? O3 Eu11 C11 . . 149.7(3) ? O3 Eu11 C23 . . 74.1(3) ? O2 Eu11 O5 . . 71.2(2) ? O2 Eu11 N1 . . 63.2(3) ? O2 Eu11 N4 . . 81.0(3) ? O2 Eu11 N2 . . 122.7(3) ? O2 Eu11 N3 . . 148.1(3) ? O2 Eu11 C8 . . 68.6(2) ? O2 Eu11 C11 . . 102.6(3) ? O2 Eu11 C23 . . 149.0(3) ? O5 Eu11 N1 . . 128.2(3) ? O5 Eu11 N4 . . 130.1(3) ? O5 Eu11 N2 . . 127.6(3) ? O5 Eu11 N3 . . 130.0(3) ? O5 Eu11 C8 . . 82.3(2) ? O5 Eu11 C11 . . 81.3(3) ? O5 Eu11 C23 . . 82.9(3) ? O4 Eu11 O1 . . 82.9(3) ? O4 Eu11 O3 . . 85.0(3) ? O4 Eu11 O2 . . 142.1(3) ? O4 Eu11 O5 . . 70.9(3) ? O4 Eu11 N1 . . 149.6(3) ? O4 Eu11 N4 . . 123.5(3) ? O4 Eu11 N2 . . 83.1(3) ? O4 Eu11 N3 . . 63.8(3) ? O4 Eu11 C8 . . 104.4(3) ? O4 Eu11 C11 . . 73.4(3) ? O4 Eu11 C23 . . 19.2(3) ? N1 Eu11 N2 . . 66.6(3) ? N1 Eu11 C8 . . 101.8(3) ? N1 Eu11 C11 . . 85.7(3) ? N1 Eu11 C23 . . 147.1(3) ? N4 Eu11 N1 . . 65.9(3) ? N4 Eu11 N2 . . 102.2(3) ? N4 Eu11 C8 . . 48.6(3) ? N4 Eu11 C11 . . 146.3(3) ? N4 Eu11 C23 . . 104.3(3) ? N2 Eu11 C8 . . 149.3(3) ? N2 Eu11 C11 . . 47.4(3) ? N2 Eu11 C23 . . 86.6(3) ? N3 Eu11 N1 . . 101.8(3) ? N3 Eu11 N4 . . 67.1(3) ? N3 Eu11 N2 . . 67.2(3) ? N3 Eu11 C8 . . 89.2(3) ? N3 Eu11 C11 . . 104.1(3) ? N3 Eu11 C23 . . 48.0(3) ? C8 Eu11 C11 . . 163.3(3) ? C8 Eu11 C23 . . 91.7(3) ? C23 Eu11 C11 . . 89.7(3) ? O6 Eu12 O10 . . 67.3(2) ? O6 Eu12 O8 . . 141.1(2) ? O6 Eu12 O7 . . 86.0(2) ? O6 Eu12 O9 . . 82.7(2) ? O6 Eu12 N5 . . 62.6(2) ? O6 Eu12 N7 . . 148.3(2) ? O6 Eu12 N6 . . 121.8(2) ? O6 Eu12 N8 . . 81.0(2) ? O6 Eu12 C12 . . 147.7(3) ? O6 Eu12 C16 . . 105.9(3) ? O6 Eu12 C19 . . 68.7(2) ? O10 Eu12 N5 . . 124.8(2) ? O10 Eu12 N7 . . 133.6(2) ? O10 Eu12 N6 . . 129.7(2) ? O10 Eu12 N8 . . 125.7(2) ? O10 Eu12 C12 . . 85.8(2) ? O10 Eu12 C16 . . 80.5(2) ? O10 Eu12 C19 . . 78.3(3) ? O8 Eu12 O10 . . 73.8(2) ? O8 Eu12 O7 . . 80.7(2) ? O8 Eu12 O9 . . 82.6(2) ? O8 Eu12 N5 . . 151.2(2) ? O8 Eu12 N7 . . 64.8(2) ? O8 Eu12 N6 . . 84.5(2) ? O8 Eu12 N8 . . 122.8(2) ? O8 Eu12 C12 . . 20.3(2) ? O8 Eu12 C16 . . 68.0(3) ? O8 Eu12 C19 . . 102.5(3) ? O7 Eu12 O10 . . 67.7(2) ? O7 Eu12 O9 . . 136.9(3) ? O7 Eu12 N5 . . 86.8(2) ? O7 Eu12 N7 . . 122.1(2) ? O7 Eu12 N6 . . 64.2(2) ? O7 Eu12 N8 . . 154.1(3) ? O7 Eu12 C12 . . 100.5(3) ? O7 Eu12 C16 . . 20.5(3) ? O7 Eu12 C19 . . 143.6(3) ? O9 Eu12 O10 . . 69.6(2) ? O9 Eu12 N5 . . 122.9(2) ? O9 Eu12 N7 . . 84.7(2) ? O9 Eu12 N6 . . 152.0(2) ? O9 Eu12 N8 . . 63.4(3) ? O9 Eu12 C12 . . 71.0(2) ? O9 Eu12 C16 . . 142.9(3) ? O9 Eu12 C19 . . 20.1(3) ? N5 Eu12 C12 . . 148.6(3) ? N5 Eu12 C16 . . 92.0(3) ? N5 Eu12 C19 . . 102.9(3) ? N7 Eu12 N5 . . 101.6(2) ? N7 Eu12 C12 . . 48.8(3) ? N7 Eu12 C16 . . 101.6(3) ? N7 Eu12 C19 . . 90.6(3) ? N6 Eu12 N5 . . 66.7(2) ? N6 Eu12 N7 . . 67.3(2) ? N6 Eu12 C12 . . 88.9(3) ? N6 Eu12 C16 . . 49.2(3) ? N6 Eu12 C19 . . 151.7(3) ? N8 Eu12 N5 . . 67.3(2) ? N8 Eu12 N7 . . 67.4(2) ? N8 Eu12 N6 . . 104.4(3) ? N8 Eu12 C12 . . 102.5(3) ? N8 Eu12 C16 . . 152.6(3) ? N8 Eu12 C19 . . 48.7(3) ? C16 Eu12 C12 . . 85.8(3) ? C16 Eu12 C19 . . 158.5(3) ? C19 Eu12 C12 . . 89.2(3) ? O17 Eu2 O16 2_666 2_656 138.4(2) ? O17 Eu2 O14 2_666 . 122.7(3) ? O17 Eu2 H14 2_666 . 137.2 ? O13 Eu2 O17 . 2_666 73.9(2) ? O13 Eu2 O16 . 2_656 77.8(2) ? O13 Eu2 O15 . 1_455 99.3(3) ? O13 Eu2 O14 . . 72.5(3) ? O13 Eu2 H14 . . 73.8 ? O13 Eu2 O12 . . 148.3(3) ? O13 Eu2 O18 . . 139.9(3) ? O16 Eu2 O14 2_656 . 75.1(3) ? O16 Eu2 H14 2_656 . 57.4 ? O15 Eu2 O17 1_455 2_666 71.5(2) ? O15 Eu2 O16 1_455 2_656 143.9(3) ? O15 Eu2 O14 1_455 . 69.9(3) ? O15 Eu2 H14 1_455 . 86.9 ? O15 Eu2 O18 1_455 . 89.0(3) ? O14 Eu2 H14 . . 17.9 ? O12 Eu2 O17 . 2_666 75.6(3) ? O12 Eu2 O16 . 2_656 122.1(3) ? O12 Eu2 O15 . 1_455 78.6(3) ? O12 Eu2 O14 . . 133.1(3) ? O12 Eu2 H14 . . 136.8 ? O12 Eu2 O18 . . 71.7(3) ? O18 Eu2 O17 . 2_666 144.6(3) ? O18 Eu2 O16 . 2_656 73.0(3) ? O18 Eu2 O14 . . 73.9(3) ? O18 Eu2 H14 . . 67.6 ? O11 Eu2 O17 . 2_666 74.4(3) ? O11 Eu2 O13 . . 83.1(3) ? O11 Eu2 O16 . 2_656 72.5(3) ? O11 Eu2 O15 . 1_455 143.5(3) ? O11 Eu2 O14 . . 142.7(3) ? O11 Eu2 H14 . . 127.9 ? O11 Eu2 O12 . . 80.8(3) ? O11 Eu2 O18 . . 112.6(3) ? O24 Na1 Na1 2_877 2_877 95.7(3) ? O27 Na1 Na1 . 2_877 111.0(3) ? O27 Na1 O24 . 2_877 143.2(3) ? C11 O1 Eu11 . . 124.9(7) ? C5 O6 Eu12 . . 123.2(6) ? Eu12 O10 H10A . . 107.5 ? Eu12 O10 H10B . . 104.5 ? H10A O10 H10B . . 127.3 ? C3 O17 Eu2 . 2_666 139.0(6) ? C8 O3 Eu11 . . 120.5(6) ? C5 O13 Eu2 . . 139.6(7) ? C12 O8 Eu12 . . 120.0(6) ? C3 O2 Eu11 . . 122.6(6) ? C19 O16 Eu2 . 2_656 143.0(7) ? Eu11 O5 H5A . . 109.5 ? Eu11 O5 H5B . . 109.4 ? H5A O5 H5B . . 104.3 ? C16 O7 Eu12 . . 117.7(6) ? C16 O15 Eu2 . 1_655 134.1(7) ? C19 O9 Eu12 . . 119.4(6) ? C23 O4 Eu11 . . 123.4(7) ? Eu2 O14 H14 . . 99.3 ? Eu2 O12 H12A . . 112.5 ? Eu2 O12 H12B . . 112.4 ? H12A O12 H12B . . 102.2 ? Eu2 O18 H18A . . 113.4 ? Eu2 O18 H18B . . 114.4 ? H18A O18 H18B . . 99.6 ? H21C O21 H21D . . 109.7 ? H22C O22 H22D . . 104.5 ? C11 O11 Eu2 . . 167.1(8) ? Na1 O24 H24C 2_877 . 53.5 ? Na1 O24 H24D 2_877 . 57.6 ? H24C O24 H24D . . 108.3 ? H26C O26 H26D . . 104.7 ? Na1 O27 H27C . . 121.3 ? Na1 O27 H27D . . 123.6 ? H27C O27 H27D . . 97.3 ? H29C O29 H29D . . 104.6 ? H30C O30 H30D . . 104.4 ? H31C O31 H31C . 2_456 180.0 ? H31C O31 H31D 2_456 2_456 103.7 ? H31C O31 H31D . . 103.7 ? H31C O31 H31D . 2_456 76.3 ? H31D O31 H31C . 2_456 76.3 ? H31D O31 H31D . 2_456 180.0 ? O35A O33 O32 . . 176(2) ? H35A O35 H35B . . 104.5 ? C4 N5 Eu12 . . 103.7(6) ? C4 N5 C13 . . 107.0(7) ? C7 N5 Eu12 . . 113.2(6) ? C7 N5 C4 . . 110.7(7) ? C7 N5 C13 . . 111.4(8) ? C13 N5 Eu12 . . 110.5(6) ? C6 N7 Eu12 . . 111.7(5) ? C6 N7 C21 . . 107.8(7) ? C15 N7 Eu12 . . 113.6(5) ? C15 N7 C6 . . 110.5(8) ? C15 N7 C21 . . 109.6(8) ? C21 N7 Eu12 . . 103.2(6) ? C2 N6 Eu12 . . 110.1(6) ? C10 N6 Eu12 . . 112.8(5) ? C10 N6 C2 . . 109.4(8) ? C20 N6 Eu12 . . 104.7(6) ? C20 N6 C2 . . 108.9(7) ? C20 N6 C10 . . 110.7(7) ? C9 N8 Eu12 . . 114.0(5) ? C14 N8 Eu12 . . 104.2(6) ? C14 N8 C9 . . 111.1(8) ? C14 N8 C18 . . 109.3(8) ? C18 N8 Eu12 . . 110.9(6) ? C18 N8 C9 . . 107.2(8) ? C17 N1 Eu11 . . 104.0(6) ? C17 N1 C24 . . 107.2(9) ? C24 N1 Eu11 . . 107.6(7) ? C31 N1 Eu11 . . 115.3(7) ? C31 N1 C17 . . 113.3(10) ? C31 N1 C24 . . 108.9(9) ? C22 N4 Eu11 . . 105.2(6) ? C22 N4 C26 . . 108.2(9) ? C26 N4 Eu11 . . 107.0(7) ? C27 N4 Eu11 . . 117.3(7) ? C27 N4 C22 . . 112.6(9) ? C27 N4 C26 . . 106.3(9) ? C1 N2 Eu11 . . 105.9(6) ? C1 N2 C30 . . 107.8(9) ? C29 N2 Eu11 . . 113.5(7) ? C29 N2 C1 . . 112.2(9) ? C29 N2 C30 . . 109.4(10) ? C30 N2 Eu11 . . 107.7(7) ? C25 N3 Eu11 . . 104.2(7) ? C25 N3 C28 . . 107.1(9) ? C28 N3 Eu11 . . 107.6(7) ? C32 N3 Eu11 . . 116.5(8) ? C32 N3 C25 . . 111.5(10) ? C32 N3 C28 . . 109.5(11) ? N2 C1 H1A . . 109.9 ? N2 C1 H1B . . 109.9 ? N2 C1 C11 . . 108.8(8) ? H1A C1 H1B . . 108.3 ? C11 C1 H1A . . 109.9 ? C11 C1 H1B . . 109.9 ? N6 C2 H2A . . 108.9 ? N6 C2 H2B . . 108.9 ? N6 C2 C7 . . 113.3(8) ? H2A C2 H2B . . 107.7 ? C7 C2 H2A . . 108.9 ? C7 C2 H2B . . 108.9 ? O17 C3 O2 . . 124.7(9) ? O17 C3 C17 . . 117.7(9) ? O2 C3 C17 . . 117.6(9) ? N5 C4 H4A . . 109.7 ? N5 C4 H4B . . 109.7 ? N5 C4 C5 . . 109.9(8) ? H4A C4 H4B . . 108.2 ? C5 C4 H4A . . 109.7 ? C5 C4 H4B . . 109.7 ? O6 C5 Eu12 . . 37.7(4) ? O6 C5 C4 . . 116.5(8) ? O13 C5 Eu12 . . 153.7(7) ? O13 C5 O6 . . 123.0(9) ? O13 C5 C4 . . 120.5(8) ? C4 C5 Eu12 . . 81.6(5) ? N7 C6 H6A . . 109.4 ? N7 C6 H6B . . 109.4 ? N7 C6 C10 . . 111.3(8) ? H6A C6 H6B . . 108.0 ? C10 C6 H6A . . 109.4 ? C10 C6 H6B . . 109.4 ? N5 C7 C2 . . 110.5(8) ? N5 C7 H7A . . 109.5 ? N5 C7 H7B . . 109.5 ? C2 C7 H7A . . 109.5 ? C2 C7 H7B . . 109.5 ? H7A C7 H7B . . 108.1 ? O3 C8 Eu11 . . 39.6(5) ? O3 C8 C22 . . 117.7(9) ? O20 C8 Eu11 . . 153.7(7) ? O20 C8 O3 . . 125.4(10) ? O20 C8 C22 . . 116.9(9) ? C22 C8 Eu11 . . 81.8(6) ? N8 C9 H9A . . 109.2 ? N8 C9 H9B . . 109.2 ? N8 C9 C13 . . 112.0(8) ? H9A C9 H9B . . 107.9 ? C13 C9 H9A . . 109.2 ? C13 C9 H9B . . 109.2 ? N6 C10 C6 . . 111.7(8) ? N6 C10 H10C . . 109.3 ? N6 C10 H10D . . 109.3 ? C6 C10 H10C . . 109.3 ? C6 C10 H10D . . 109.3 ? H10C C10 H10D . . 107.9 ? O1 C11 Eu11 . . 36.8(5) ? O1 C11 O11 . . 124.0(10) ? O1 C11 C1 . . 117.8(9) ? O11 C11 Eu11 . . 159.5(8) ? O11 C11 C1 . . 118.0(9) ? C1 C11 Eu11 . . 82.0(5) ? O8 C12 Eu12 . . 39.7(4) ? O8 C12 C21 . . 117.3(9) ? O23 C12 Eu12 . . 156.5(8) ? O23 C12 O8 . . 124.9(10) ? O23 C12 C21 . . 117.8(9) ? C21 C12 Eu12 . . 80.1(5) ? N5 C13 C9 . . 112.2(8) ? N5 C13 H13A . . 109.2 ? N5 C13 H13B . . 109.2 ? C9 C13 H13A . . 109.2 ? C9 C13 H13B . . 109.2 ? H13A C13 H13B . . 107.9 ? N8 C14 H14A . . 109.4 ? N8 C14 H14B . . 109.4 ? N8 C14 C19 . . 111.0(8) ? H14A C14 H14B . . 108.0 ? C19 C14 H14A . . 109.4 ? C19 C14 H14B . . 109.4 ? N7 C15 H15A . . 109.3 ? N7 C15 H15B . . 109.3 ? N7 C15 C18 . . 111.6(8) ? H15A C15 H15B . . 108.0 ? C18 C15 H15A . . 109.3 ? C18 C15 H15B . . 109.3 ? O7 C16 Eu12 . . 41.8(5) ? O7 C16 O15 . . 125.0(10) ? O7 C16 C20 . . 118.7(9) ? O15 C16 Eu12 . . 150.7(7) ? O15 C16 C20 . . 116.2(9) ? C20 C16 Eu12 . . 82.0(5) ? N1 C17 C3 . . 109.8(9) ? N1 C17 H17A . . 109.7 ? N1 C17 H17B . . 109.7 ? C3 C17 H17A . . 109.7 ? C3 C17 H17B . . 109.7 ? H17A C17 H17B . . 108.2 ? N8 C18 C15 . . 112.7(8) ? N8 C18 H18C . . 109.1 ? N8 C18 H18D . . 109.1 ? C15 C18 H18C . . 109.1 ? C15 C18 H18D . . 109.1 ? H18C C18 H18D . . 107.8 ? O16 C19 Eu12 . . 154.5(8) ? O16 C19 O9 . . 125.8(11) ? O16 C19 C14 . . 117.8(9) ? O9 C19 Eu12 . . 40.5(5) ? O9 C19 C14 . . 116.4(9) ? C14 C19 Eu12 . . 80.1(5) ? N6 C20 C16 . . 111.3(8) ? N6 C20 H20A . . 109.4 ? N6 C20 H20B . . 109.4 ? C16 C20 H20A . . 109.4 ? C16 C20 H20B . . 109.4 ? H20A C20 H20B . . 108.0 ? N7 C21 C12 . . 112.0(8) ? N7 C21 H21A . . 109.2 ? N7 C21 H21B . . 109.2 ? C12 C21 H21A . . 109.2 ? C12 C21 H21B . . 109.2 ? H21A C21 H21B . . 107.9 ? N4 C22 C8 . . 111.1(8) ? N4 C22 H22A . . 109.4 ? N4 C22 H22B . . 109.4 ? C8 C22 H22A . . 109.4 ? C8 C22 H22B . . 109.4 ? H22A C22 H22B . . 108.0 ? O4 C23 Eu11 . . 37.4(5) ? O4 C23 C25 . . 116.1(10) ? O25 C23 Eu11 . . 156.3(10) ? O25 C23 O4 . . 123.8(12) ? O25 C23 C25 . . 120.1(11) ? C25 C23 Eu11 . . 80.2(6) ? N1 C24 H24A . . 109.1 ? N1 C24 H24B . . 109.1 ? H24A C24 H24B . . 107.9 ? C27 C24 N1 . . 112.3(10) ? C27 C24 H24A . . 109.1 ? C27 C24 H24B . . 109.1 ? N3 C25 C23 . . 110.6(10) ? N3 C25 H25A . . 109.5 ? N3 C25 H25B . . 109.5 ? C23 C25 H25A . . 109.5 ? C23 C25 H25B . . 109.5 ? H25A C25 H25B . . 108.1 ? N4 C26 H26A . . 108.8 ? N4 C26 H26B . . 108.8 ? H26A C26 H26B . . 107.7 ? C32 C26 N4 . . 113.7(11) ? C32 C26 H26A . . 108.8 ? C32 C26 H26B . . 108.8 ? N4 C27 C24 . . 107.4(10) ? N4 C27 H27A . . 110.2 ? N4 C27 H27B . . 110.2 ? C24 C27 H27A . . 110.2 ? C24 C27 H27B . . 110.2 ? H27A C27 H27B . . 108.5 ? N3 C28 H28A . . 108.8 ? N3 C28 H28B . . 108.8 ? H28A C28 H28B . . 107.7 ? C29 C28 N3 . . 114.0(11) ? C29 C28 H28A . . 108.8 ? C29 C28 H28B . . 108.8 ? N2 C29 C28 . . 111.6(11) ? N2 C29 H29A . . 109.3 ? N2 C29 H29B . . 109.3 ? C28 C29 H29A . . 109.3 ? C28 C29 H29B . . 109.3 ? H29A C29 H29B . . 108.0 ? N2 C30 H30A . . 108.7 ? N2 C30 H30B . . 108.7 ? H30A C30 H30B . . 107.6 ? C31 C30 N2 . . 114.4(11) ? C31 C30 H30A . . 108.7 ? C31 C30 H30B . . 108.7 ? N1 C31 C30 . . 110.5(10) ? N1 C31 H31A . . 109.5 ? N1 C31 H31B . . 109.5 ? C30 C31 H31A . . 109.5 ? C30 C31 H31B . . 109.5 ? H31A C31 H31B . . 108.1 ? N3 C32 C26 . . 110.5(11) ? N3 C32 H32A . . 109.6 ? N3 C32 H32B . . 109.6 ? C26 C32 H32A . . 109.6 ? C26 C32 H32B . . 109.6 ? H32A C32 H32B . . 108.1 ? O33 O35A H35A . . 133.8 ? O33 O35A H35B . . 132.4 ? H35A O35A H35B . . 91.4 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Eu11 O1 . 2.377(7) ? Eu11 O3 . 2.386(7) ? Eu11 O2 . 2.408(7) ? Eu11 O5 . 2.529(7) ? Eu11 O4 . 2.364(7) ? Eu11 N1 . 2.690(9) ? Eu11 N4 . 2.657(9) ? Eu11 N2 . 2.695(9) ? Eu11 N3 . 2.653(10) ? Eu11 C8 . 3.223(10) ? Eu11 C11 . 3.254(10) ? Eu11 C23 . 3.251(11) ? Eu12 O6 . 2.365(7) ? Eu12 O10 . 2.542(7) ? Eu12 O8 . 2.376(7) ? Eu12 O7 . 2.387(7) ? Eu12 O9 . 2.399(7) ? Eu12 N5 . 2.702(8) ? Eu12 N7 . 2.647(8) ? Eu12 N6 . 2.639(8) ? Eu12 N8 . 2.635(8) ? Eu12 C12 . 3.224(10) ? Eu12 C16 . 3.172(10) ? Eu12 C19 . 3.217(10) ? Eu2 O17 2_666 2.427(7) ? Eu2 O13 . 2.333(7) ? Eu2 O16 2_656 2.470(8) ? Eu2 O15 1_455 2.411(8) ? Eu2 O14 . 2.501(8) ? Eu2 H14 . 2.7762 ? Eu2 O12 . 2.409(8) ? Eu2 O18 . 2.418(8) ? Eu2 O11 . 2.306(8) ? Na1 Na1 2_877 3.096(9) ? Na1 O24 2_877 2.958(11) ? Na1 O27 . 2.845(13) ? O1 C11 . 1.245(12) ? O6 C5 . 1.267(12) ? O10 H10A . 0.8683 ? O10 H10B . 0.8314 ? O17 C3 . 1.241(12) ? O3 C8 . 1.272(12) ? O13 C5 . 1.251(12) ? O8 C12 . 1.294(12) ? O2 C3 . 1.273(12) ? O16 C19 . 1.219(13) ? O5 H5A . 0.8510 ? O5 H5B . 0.8534 ? O23 C12 . 1.235(13) ? O7 C16 . 1.256(13) ? O20 C8 . 1.238(13) ? O15 C16 . 1.260(13) ? O9 C19 . 1.268(13) ? O4 C23 . 1.283(14) ? O14 H14 . 0.8656 ? O12 H12A . 0.9045 ? O12 H12B . 0.9033 ? O18 H18A . 0.9493 ? O18 H18B . 0.9559 ? O21 H21C . 0.8498 ? O21 H21D . 0.8502 ? O22 H22C . 0.8507 ? O22 H22D . 0.8492 ? O11 C11 . 1.261(13) ? O24 H24C . 0.9935 ? O24 H24D . 1.1032 ? O25 C23 . 1.233(14) ? O26 H26C . 0.8497 ? O26 H26D . 0.8495 ? O27 H27C . 1.0984 ? O27 H27D . 1.0274 ? O29 H29C . 0.8501 ? O29 H29D . 0.8493 ? O30 H30C . 0.8500 ? O30 H30D . 0.8504 ? O31 H31C 2_456 0.8498 ? O31 H31C . 0.8499 ? O31 H31D 2_456 0.8510(10) ? O31 H31D . 0.8510 ? O32 O33 . 1.53(3) ? O33 O35A . 1.51(3) ? O34 O34 2_666 1.36(3) ? O35 H35A . 0.8506 ? O35 H35B . 0.8497 ? N5 C4 . 1.477(12) ? N5 C7 . 1.461(12) ? N5 C13 . 1.494(13) ? N7 C6 . 1.482(12) ? N7 C15 . 1.480(12) ? N7 C21 . 1.484(13) ? N6 C2 . 1.493(13) ? N6 C10 . 1.490(12) ? N6 C20 . 1.458(12) ? N8 C9 . 1.490(14) ? N8 C14 . 1.469(13) ? N8 C18 . 1.488(12) ? N1 C17 . 1.473(15) ? N1 C24 . 1.583(16) ? N1 C31 . 1.445(15) ? N4 C22 . 1.480(14) ? N4 C26 . 1.600(17) ? N4 C27 . 1.424(16) ? N2 C1 . 1.463(14) ? N2 C29 . 1.431(16) ? N2 C30 . 1.583(16) ? N3 C25 . 1.484(16) ? N3 C28 . 1.566(16) ? N3 C32 . 1.415(17) ? C1 H1A . 0.9700 ? C1 H1B . 0.9700 ? C1 C11 . 1.542(15) ? C2 H2A . 0.9700 ? C2 H2B . 0.9700 ? C2 C7 . 1.499(14) ? C3 C17 . 1.512(14) ? C4 H4A . 0.9700 ? C4 H4B . 0.9700 ? C4 C5 . 1.530(14) ? C6 H6A . 0.9700 ? C6 H6B . 0.9700 ? C6 C10 . 1.513(14) ? C7 H7A . 0.9700 ? C7 H7B . 0.9700 ? C8 C22 . 1.523(15) ? C9 H9A . 0.9700 ? C9 H9B . 0.9700 ? C9 C13 . 1.523(13) ? C10 H10C . 0.9700 ? C10 H10D . 0.9700 ? C12 C21 . 1.510(15) ? C13 H13A . 0.9700 ? C13 H13B . 0.9700 ? C14 H14A . 0.9700 ? C14 H14B . 0.9700 ? C14 C19 . 1.531(15) ? C15 H15A . 0.9700 ? C15 H15B . 0.9700 ? C15 C18 . 1.502(14) ? C16 C20 . 1.529(14) ? C17 H17A . 0.9700 ? C17 H17B . 0.9700 ? C18 H18C . 0.9700 ? C18 H18D . 0.9700 ? C20 H20A . 0.9700 ? C20 H20B . 0.9700 ? C21 H21A . 0.9700 ? C21 H21B . 0.9700 ? C22 H22A . 0.9700 ? C22 H22B . 0.9700 ? C23 C25 . 1.514(18) ? C24 H24A . 0.9700 ? C24 H24B . 0.9700 ? C24 C27 . 1.484(19) ? C25 H25A . 0.9700 ? C25 H25B . 0.9700 ? C26 H26A . 0.9700 ? C26 H26B . 0.9700 ? C26 C32 . 1.455(19) ? C27 H27A . 0.9700 ? C27 H27B . 0.9700 ? C28 H28A . 0.9700 ? C28 H28B . 0.9700 ? C28 C29 . 1.448(19) ? C29 H29A . 0.9700 ? C29 H29B . 0.9700 ? C30 H30A . 0.9700 ? C30 H30B . 0.9700 ? C30 C31 . 1.449(18) ? C31 H31A . 0.9700 ? C31 H31B . 0.9700 ? C32 H32A . 0.9700 ? C32 H32B . 0.9700 ? O35A H35A . 1.0868 ? O35A H35B . 0.7653 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Eu11 O1 C11 O11 . . . . -170.0(9) ? Eu11 O1 C11 C1 . . . . 14.3(14) ? Eu11 O3 C8 O20 . . . . -150.1(8) ? Eu11 O3 C8 C22 . . . . 27.4(12) ? Eu11 O2 C3 O17 . . . . -166.1(7) ? Eu11 O2 C3 C17 . . . . 13.6(12) ? Eu11 O4 C23 O25 . . . . -160.0(9) ? Eu11 O4 C23 C25 . . . . 17.3(14) ? Eu11 N1 C17 C3 . . . . -47.0(9) ? Eu11 N1 C24 C27 . . . . -48.4(10) ? Eu11 N1 C31 C30 . . . . -40.5(13) ? Eu11 N4 C22 C8 . . . . -39.6(10) ? Eu11 N4 C26 C32 . . . . -47.2(12) ? Eu11 N4 C27 C24 . . . . -44.2(12) ? Eu11 N2 C1 C11 . . . . -42.9(9) ? Eu11 N2 C29 C28 . . . . -39.0(13) ? Eu11 N2 C30 C31 . . . . -46.2(12) ? Eu11 N3 C25 C23 . . . . -44.7(10) ? Eu11 N3 C28 C29 . . . . -47.8(13) ? Eu11 N3 C32 C26 . . . . -38.7(14) ? Eu11 C8 C22 N4 . . . . 30.8(8) ? Eu11 C23 C25 N3 . . . . 34.4(8) ? Eu12 O6 C5 O13 . . . . -155.3(7) ? Eu12 O6 C5 C4 . . . . 24.3(11) ? Eu12 O8 C12 O23 . . . . -155.6(9) ? Eu12 O8 C12 C21 . . . . 22.3(12) ? Eu12 O7 C16 O15 . . . . -144.4(9) ? Eu12 O7 C16 C20 . . . . 31.6(12) ? Eu12 O9 C19 O16 . . . . -150.4(9) ? Eu12 O9 C19 C14 . . . . 29.0(11) ? Eu12 N5 C4 C5 . . . . -43.9(8) ? Eu12 N5 C7 C2 . . . . -37.4(9) ? Eu12 N5 C13 C9 . . . . -44.2(9) ? Eu12 N7 C6 C10 . . . . -45.4(9) ? Eu12 N7 C15 C18 . . . . -36.6(10) ? Eu12 N7 C21 C12 . . . . -43.3(8) ? Eu12 N6 C2 C7 . . . . -49.3(9) ? Eu12 N6 C10 C6 . . . . -40.0(8) ? Eu12 N6 C20 C16 . . . . -38.7(9) ? Eu12 N8 C9 C13 . . . . -39.5(9) ? Eu12 N8 C14 C19 . . . . -43.2(8) ? Eu12 N8 C18 C15 . . . . -46.5(10) ? Eu12 C12 C21 N7 . . . . 33.8(7) ? Eu12 C16 C20 N6 . . . . 30.5(7) ? Eu2 O17 C3 O2 2_666 . . . -9.8(16) ? Eu2 O17 C3 C17 2_666 . . . 170.4(7) ? Eu2 O13 C5 Eu12 . . . . -147.8(10) ? Eu2 O13 C5 O6 . . . . -112.5(11) ? Eu2 O13 C5 C4 . . . . 67.9(13) ? Eu2 O16 C19 Eu12 2_656 . . . -56(2) ? Eu2 O16 C19 O9 2_656 . . . -7.6(19) ? Eu2 O16 C19 C14 2_656 . . . 172.9(7) ? Eu2 O15 C16 Eu12 1_655 . . . -24(2) ? Eu2 O15 C16 O7 1_655 . . . 28.2(17) ? Eu2 O15 C16 C20 1_655 . . . -148.0(8) ? Eu2 O11 C11 Eu11 . . . . 122(3) ? Eu2 O11 C11 O1 . . . . 140(3) ? Eu2 O11 C11 C1 . . . . -45(4) ? O17 C3 C17 N1 . . . . -152.5(9) ? O3 C8 C22 N4 . . . . 13.5(14) ? O8 C12 C21 N7 . . . . 19.6(13) ? O2 C3 C17 N1 . . . . 27.7(13) ? O23 C12 C21 N7 . . . . -162.4(9) ? O7 C16 C20 N6 . . . . 9.9(13) ? O20 C8 C22 N4 . . . . -168.7(9) ? O15 C16 C20 N6 . . . . -173.7(9) ? O4 C23 C25 N3 . . . . 23.8(15) ? O25 C23 C25 N3 . . . . -158.8(11) ? N5 C4 C5 Eu12 . . . . 34.6(7) ? N5 C4 C5 O6 . . . . 19.9(12) ? N5 C4 C5 O13 . . . . -160.5(9) ? N7 C6 C10 N6 . . . . 58.2(10) ? N7 C15 C18 N8 . . . . 56.9(12) ? N6 C2 C7 N5 . . . . 59.8(11) ? N8 C9 C13 N5 . . . . 57.5(11) ? N8 C14 C19 Eu12 . . . . 33.5(6) ? N8 C14 C19 O16 . . . . -165.7(9) ? N8 C14 C19 O9 . . . . 14.9(12) ? N1 C24 C27 N4 . . . . 62.3(12) ? N4 C26 C32 N3 . . . . 58.7(15) ? N2 C1 C11 Eu11 . . . . 33.2(7) ? N2 C1 C11 O1 . . . . 24.6(14) ? N2 C1 C11 O11 . . . . -151.4(10) ? N2 C30 C31 N1 . . . . 59.5(15) ? N3 C28 C29 N2 . . . . 60.4(15) ? C1 N2 C29 C28 . . . . 81.0(13) ? C1 N2 C30 C31 . . . . -160.1(10) ? C2 N6 C10 C6 . . . . -162.9(7) ? C2 N6 C20 C16 . . . . 79.0(10) ? C4 N5 C7 C2 . . . . 78.5(10) ? C4 N5 C13 C9 . . . . -156.4(8) ? C6 N7 C15 C18 . . . . -163.2(8) ? C6 N7 C21 C12 . . . . 75.0(10) ? C7 N5 C4 C5 . . . . -165.6(8) ? C7 N5 C13 C9 . . . . 82.5(10) ? C9 N8 C14 C19 . . . . -166.5(8) ? C9 N8 C18 C15 . . . . 78.6(10) ? C10 N6 C2 C7 . . . . 75.2(10) ? C10 N6 C20 C16 . . . . -160.6(8) ? C13 N5 C4 C5 . . . . 72.9(10) ? C13 N5 C7 C2 . . . . -162.5(8) ? C14 N8 C9 C13 . . . . 77.9(10) ? C14 N8 C18 C15 . . . . -160.9(9) ? C15 N7 C6 C10 . . . . 82.1(9) ? C15 N7 C21 C12 . . . . -164.6(8) ? C17 N1 C24 C27 . . . . -159.8(9) ? C17 N1 C31 C30 . . . . 79.2(13) ? C18 N8 C9 C13 . . . . -162.7(8) ? C18 N8 C14 C19 . . . . 75.4(10) ? C20 N6 C2 C7 . . . . -163.6(8) ? C20 N6 C10 C6 . . . . 77.0(9) ? C21 N7 C6 C10 . . . . -158.1(8) ? C21 N7 C15 C18 . . . . 78.2(10) ? C22 N4 C26 C32 . . . . -160.0(11) ? C22 N4 C27 C24 . . . . 78.0(12) ? C24 N1 C17 C3 . . . . 66.8(10) ? C24 N1 C31 C30 . . . . -161.6(11) ? C25 N3 C28 C29 . . . . -159.4(11) ? C25 N3 C32 C26 . . . . 80.7(14) ? C26 N4 C22 C8 . . . . 74.4(11) ? C26 N4 C27 C24 . . . . -163.7(10) ? C27 N4 C22 C8 . . . . -168.5(10) ? C27 N4 C26 C32 . . . . 78.9(13) ? C28 N3 C25 C23 . . . . 69.1(12) ? C28 N3 C32 C26 . . . . -161.0(11) ? C29 N2 C1 C11 . . . . -167.3(9) ? C29 N2 C30 C31 . . . . 77.7(13) ? C30 N2 C1 C11 . . . . 72.2(11) ? C30 N2 C29 C28 . . . . -159.4(11) ? C31 N1 C17 C3 . . . . -173.0(9) ? C31 N1 C24 C27 . . . . 77.3(12) ? C32 N3 C25 C23 . . . . -171.2(10) ? C32 N3 C28 C29 . . . . 79.6(14) ? _cod_database_fobs_code 2022391