#------------------------------------------------------------------------------ #$Date: 2021-07-08 08:16:13 +0300 (Thu, 08 Jul 2021) $ #$Revision: 267370 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/23/2022399.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022399 _cell_angle_alpha 90.000 _cell_angle_beta 92.524 _cell_angle_gamma 90.000 _cell_length_a 10.5897 _cell_length_b 22.8595 _cell_length_c 14.3102 _exptl_crystal_F_000 1528.00 _reflns_d_resolution_high 0.7927 _cod_data_source_file ef3020Isup2.hkl _cod_data_source_block I _shelx_title ' ZK-M051-1 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 324.34 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 -23 0 1.08 -5.25 5.25 o 7 -23 0 66.57 53.23 7.86 o 6 -22 0 7.82 13.34 5.07 o 7 -22 0 8.93 11.10 5.27 o 8 -22 0 26.35 17.60 4.92 o 7 -21 0 466.47 529.52 33.84 o 8 -21 0 20.80 16.71 5.68 o 7 -20 0 41.89 36.83 10.71 o 8 -20 0 35.64 44.12 9.95 o 9 -20 0 37.66 43.85 7.79 o 7 -19 0 202.42 219.51 25.59 o 8 -19 0 56.69 41.08 10.52 o 9 -19 0 28.27 33.71 8.13 o 2 -18 0 280.13 274.96 45.59 o 3 -18 0 514.73 522.40 66.23 o 8 -18 0 164.12 169.29 22.29 o 9 -18 0 39.85 47.91 10.45 o 10 -18 0 217.24 229.33 16.92 o 1 -17 0 230.75 189.06 34.59 o 2 -17 0 206.40 196.24 37.80 o 3 -17 0 1406.02 1435.91 109.90 o 4 -17 0 75.41 44.80 21.41 o 8 -17 0 163.79 189.09 24.88 o 9 -17 0 76.64 83.82 14.74 o 10 -17 0 67.08 74.95 11.27 o 0 -16 0 2131.06 2260.41 118.16 o 1 -16 0 122.07 84.92 22.48 o 2 -16 0 1810.75 2000.87 84.60 o 3 -16 0 487.51 588.38 43.46 o 4 -16 0 610.40 673.21 49.80 o 5 -16 0 218.92 175.26 42.14 o 8 -16 0 92.09 91.68 18.05 o 9 -16 0 81.69 94.90 16.79 o 10 -16 0 223.66 263.98 22.74 o 1 -15 0 533.88 516.39 55.36 o 2 -15 0 732.41 825.27 59.50 o 3 -15 0 603.40 561.97 42.17 o 4 -15 0 571.49 609.31 47.11 o 5 -15 0 329.73 335.31 37.33 o 8 -15 0 40.49 37.42 12.91 o 9 -15 0 385.30 399.73 35.54 o 10 -15 0 11.75 9.33 6.85 o 0 -14 0 530.05 543.73 51.71 o 1 -14 0 719.59 684.97 41.95 o 2 -14 0 298.97 263.95 25.47 o 3 -14 0 27.22 7.93 17.73 o 4 -14 0 2454.72 2556.94 98.29 o 5 -14 0 35.49 29.49 13.09 o 6 -14 0 292.20 311.98 37.07 o 8 -14 0 470.14 527.85 44.85 o 9 -14 0 91.05 100.65 19.19 o 10 -14 0 127.98 128.83 18.68 o 1 -13 0 1688.48 1755.19 66.28 o 2 -13 0 478.43 549.23 36.00 o 3 -13 0 3233.10 3506.70 106.72 o 4 -13 0 595.52 667.29 47.54 o 5 -13 0 1781.09 1802.64 85.84 o 6 -13 0 81.91 72.83 9.38 o 8 -13 0 63.24 56.91 16.23 o 9 -13 0 615.81 666.63 49.71 o 10 -13 0 62.50 58.31 14.35 o 11 -13 0 81.54 79.44 12.85 o 0 -12 0 3315.56 3329.83 128.67 o 1 -12 0 149.65 155.98 18.16 o 2 -12 0 3472.34 3441.44 97.37 o 3 -12 0 120.73 110.58 17.34 o 4 -12 0 1908.57 1954.12 81.31 o 5 -12 0 25.54 33.06 12.14 o 6 -12 0 348.12 344.83 19.44 o 7 -12 0 9.03 0.81 17.90 o 8 -12 0 794.48 933.89 46.34 o 9 -12 0 148.92 167.58 15.04 o 10 -12 0 512.37 552.68 25.17 o 11 -12 0 88.28 89.54 8.21 o 12 -12 0 94.88 80.49 8.88 o 1 -11 0 2025.57 2143.95 82.03 o 2 -11 0 4633.17 5134.45 119.83 o 3 -11 0 8972.77 9059.62 183.45 o 4 -11 0 1291.63 1386.44 65.79 o 5 -11 0 4539.77 4944.04 167.95 o 6 -11 0 777.11 916.54 61.91 o 7 -11 0 43.87 37.14 8.70 o 8 -11 0 164.13 165.59 15.50 o 9 -11 0 47.24 43.25 8.78 o 10 -11 0 27.68 38.36 7.38 o 11 -11 0 9.48 5.78 3.67 o 12 -11 0 58.31 38.27 7.15 o 0 -10 0 12935.88 12551.14 294.49 o 1 -10 0 4338.36 4473.56 141.11 o 2 -10 0 6569.03 6677.64 137.25 o 3 -10 0 2245.51 2260.68 75.74 o 4 -10 0 2211.94 2318.91 84.71 o 5 -10 0 1549.22 1717.70 71.93 o 6 -10 0 128.26 118.16 22.09 o 7 -10 0 541.49 520.42 22.39 o 8 -10 0 973.94 1086.74 41.45 o 9 -10 0 5.77 13.36 4.95 o 10 -10 0 761.97 827.95 34.10 o 11 -10 0 139.31 152.43 12.62 o 12 -10 0 24.83 23.10 4.69 o 1 -9 0 4233.70 3860.72 89.06 o 2 -9 0 771.71 803.58 38.14 o 3 -9 0 5897.44 5321.56 123.09 o 4 -9 0 97.52 98.59 16.18 o 5 -9 0 4612.04 5184.55 119.16 o 6 -9 0 766.10 799.31 55.14 o 7 -9 0 431.83 463.61 21.06 o 8 -9 0 28.94 32.31 5.33 o 9 -9 0 83.60 80.57 11.76 o 10 -9 0 142.74 160.45 15.56 o 11 -9 0 282.01 301.17 22.77 o 12 -9 0 58.32 45.52 10.37 o 0 -8 0 4309.17 3619.46 114.34 o 1 -8 0 515.34 463.64 25.24 o 2 -8 0 2238.67 1809.44 56.51 o 3 -8 0 33.36 53.25 13.68 o 4 -8 0 1858.16 1778.34 90.83 o 5 -8 0 146.74 162.92 24.38 o 6 -8 0 900.48 815.41 73.01 o 7 -8 0 9.50 11.09 5.16 o 8 -8 0 1070.40 1191.61 32.12 o 9 -8 0 122.30 137.51 14.89 o 10 -8 0 491.24 536.80 28.56 o 11 -8 0 18.24 20.54 5.79 o 12 -8 0 169.05 171.24 18.01 o 1 -7 0 775.40 698.06 29.44 o 2 -7 0 918.14 871.95 46.38 o 3 -7 0 2492.98 2556.30 97.70 o 4 -7 0 462.02 453.62 43.23 o 5 -7 0 2181.27 2161.11 75.48 o 6 -7 0 299.56 309.15 43.86 o 7 -7 0 475.03 460.49 43.07 o 8 -7 0 9.64 1.09 8.04 o 9 -7 0 90.18 91.02 12.10 o 10 -7 0 355.38 382.72 24.07 o 11 -7 0 258.24 309.69 26.89 o 12 -7 0 23.31 11.96 6.65 o 0 -6 0 4018.26 3606.31 103.33 o 1 -6 0 2436.58 2188.16 52.92 o 2 -6 0 4132.45 4186.34 81.75 o 3 -6 0 399.61 453.95 36.68 o 4 -6 0 324.31 219.83 29.42 o 5 -6 0 952.56 931.47 45.84 o 6 -6 0 46.04 27.96 13.80 o 7 -6 0 487.44 497.81 59.10 o 8 -6 0 124.32 118.42 13.48 o 9 -6 0 210.09 208.00 18.05 o 10 -6 0 36.08 49.86 9.28 o 11 -6 0 90.40 93.37 15.62 o 12 -6 0 218.35 218.78 13.97 o 13 -6 0 10.37 7.06 3.13 o 1 -5 0 8658.89 7440.02 160.75 o 2 -5 0 13733.33 13271.53 193.67 o 3 -5 0 189.27 171.88 21.31 o 4 -5 0 216.06 175.47 17.32 o 5 -5 0 1978.72 1813.43 63.59 o 6 -5 0 945.06 974.67 74.95 o 7 -5 0 2375.28 2290.96 128.30 o 8 -5 0 590.36 633.06 22.34 o 9 -5 0 199.14 185.42 17.09 o 10 -5 0 52.10 52.18 9.57 o 11 -5 0 35.87 32.07 9.74 o 12 -5 0 16.00 8.11 6.36 o 13 -5 0 46.70 33.30 6.01 o 0 -4 0 8006.98 7441.82 158.69 o 1 -4 0 3935.55 3528.74 85.46 o 2 -4 0 8281.94 7342.39 165.89 o 3 -4 0 4656.91 4738.52 133.99 o 4 -4 0 160.44 128.62 14.17 o 5 -4 0 138.27 139.22 16.33 o 6 -4 0 1143.57 1115.54 78.65 o 7 -4 0 143.13 131.86 28.96 o 8 -4 0 634.91 643.31 23.41 o 9 -4 0 83.35 83.31 13.68 o 10 -4 0 44.05 54.98 9.59 o 11 -4 0 153.39 167.86 21.31 o 12 -4 0 225.60 216.66 17.38 o 13 -4 0 0.27 1.46 2.76 o 1 -3 0 3453.97 3190.99 74.69 o 2 -3 0 21074.54 18544.70 357.09 o 3 -3 0 127.80 113.54 23.96 o 4 -3 0 31.49 32.87 7.11 o 5 -3 0 5686.96 5546.16 117.63 o 6 -3 0 688.26 750.93 63.08 o 7 -3 0 2019.72 1924.92 113.05 o 8 -3 0 87.01 108.98 9.53 o 9 -3 0 486.36 511.77 28.12 o 10 -3 0 174.36 196.26 17.75 o 11 -3 0 563.56 552.05 39.20 o 12 -3 0 6.56 4.97 4.16 o 13 -3 0 208.24 182.31 14.23 o 0 -2 0 65477.26 61817.67 1069.31 o 1 -2 0 384.05 353.95 12.29 o 2 -2 0 2235.84 1957.27 61.95 o 3 -2 0 1244.54 1394.45 40.05 o 4 -2 0 3610.71 3635.68 80.87 o 5 -2 0 144.54 162.63 16.64 o 6 -2 0 3366.98 3036.63 132.39 o 7 -2 0 17.43 21.14 13.12 o 8 -2 0 1576.93 1781.35 33.96 o 9 -2 0 246.26 272.93 20.34 o 10 -2 0 263.40 321.18 31.54 o 11 -2 0 243.29 252.09 18.18 o 12 -2 0 47.81 46.74 7.11 o 13 -2 0 6.89 7.50 4.01 o 1 -1 0 5607.20 5106.58 104.72 o 2 -1 0 6117.58 5651.94 89.43 o 3 -1 0 50952.48 48253.54 1071.10 o 4 -1 0 8398.75 8652.84 146.68 o 5 -1 0 1959.04 2058.95 77.34 o 6 -1 0 12364.67 13667.20 343.88 o 7 -1 0 1670.99 1708.95 103.55 o 8 -1 0 10.57 264.31 16.57 o 9 -1 0 233.53 233.05 17.11 o 10 -1 0 245.89 284.03 29.62 o 11 -1 0 53.77 46.67 8.47 o 12 -1 0 24.34 30.13 6.07 o 13 -1 0 519.72 458.74 23.20 o 1 0 0 1075.55 1099.87 36.49 o 2 0 0 437.65 583.84 26.57 o 3 0 0 105194.99 101521.22 1256.76 o 4 0 0 2547.50 2486.66 62.20 o 5 0 0 52.42 57.13 10.87 o 6 0 0 4563.75 7630.50 234.43 o 7 0 0 1806.25 2419.48 124.42 o 8 0 0 1952.00 2223.22 37.52 o 9 0 0 470.78 500.85 19.58 o 10 0 0 1276.28 1496.77 69.85 o 11 0 0 353.48 440.88 34.27 o 12 0 0 50.28 63.73 8.10 o 13 0 0 51.63 66.84 8.74 o 1 1 0 5767.45 5824.49 120.99 o 2 1 0 6113.25 5973.05 142.87 o 3 1 0 50963.21 51525.94 655.40 o 4 1 0 8386.98 8696.58 327.14 o 5 1 0 1934.75 2096.56 92.36 o 6 1 0 12346.49 15799.73 378.40 o 7 1 0 1679.08 2600.89 126.87 o 8 1 0 10.80 527.28 23.99 o 9 1 0 249.10 305.55 23.18 o 10 1 0 248.49 340.72 22.15 o 11 1 0 38.68 42.06 7.88 o 12 1 0 25.54 29.96 10.28 o 13 1 0 521.22 747.81 28.70 o 1 2 0 382.89 379.22 16.85 o 2 2 0 2102.44 1833.89 57.60 o 3 2 0 1252.61 1575.89 62.16 o 4 2 0 3874.15 4015.72 125.79 o 5 2 0 144.10 171.71 25.59 o 6 2 0 3416.30 4701.06 167.05 o 7 2 0 19.36 401.74 50.17 o 8 2 0 1576.83 1721.15 36.19 o 9 2 0 246.88 272.91 15.43 o 10 2 0 267.92 323.01 21.22 o 11 2 0 244.00 252.08 17.53 o 12 2 0 56.88 63.65 7.79 o 2 3 0 21134.72 20423.73 382.80 o 3 3 0 106.79 84.12 13.62 o 4 3 0 30.37 29.51 10.49 o 5 3 0 5467.45 5562.68 169.78 o 6 3 0 693.99 812.87 61.23 o 7 3 0 2009.58 2022.80 108.70 o 8 3 0 87.07 138.95 11.22 o 9 3 0 500.01 507.99 18.06 o 10 3 0 176.66 205.78 15.76 o 11 3 0 512.92 486.86 38.06 o 12 3 0 7.17 10.47 5.37 o 3 4 0 4658.47 5347.96 136.90 o 4 4 0 182.69 162.49 21.61 o 5 4 0 139.61 145.20 23.68 o 6 4 0 1135.29 1091.23 71.37 o 7 4 0 139.07 137.37 27.15 o 8 4 0 623.81 593.77 22.36 o 9 4 0 83.25 74.73 7.04 o 10 4 0 31.82 29.35 6.37 o 11 4 0 153.58 188.36 14.32 o 12 4 0 221.87 212.65 17.38 o 8 5 0 590.07 598.30 17.24 o 9 5 0 219.32 207.56 10.57 o 10 5 0 51.69 45.91 5.64 o 11 5 0 44.67 36.77 6.58 o 12 5 0 15.71 6.82 3.56 o 8 6 0 136.26 112.87 8.66 o 9 6 0 205.75 204.86 10.47 o 10 6 0 21.85 18.96 4.02 o 11 6 0 91.66 93.04 12.70 o 8 7 0 9.82 12.37 4.62 o 9 7 0 64.12 61.26 7.58 o 10 7 0 356.43 348.35 20.88 o 11 7 0 282.74 305.89 25.61 o 8 8 0 1143.75 1237.05 41.25 o 9 8 0 120.03 142.66 13.93 o 10 8 0 491.74 561.37 33.67 o 11 8 0 18.75 20.05 7.89 o 7 9 0 407.96 392.48 21.42 o 8 9 0 28.51 28.21 6.96 o 9 9 0 67.80 58.26 9.03 o 10 9 0 140.93 137.04 12.97 o 11 9 0 311.06 361.97 26.71 o 7 10 0 535.67 491.92 25.03 o 8 10 0 1015.22 980.37 37.10 o 9 10 0 5.98 12.12 6.01 o 10 10 0 776.76 846.14 31.98 o 11 10 0 136.75 119.45 15.15 o 7 11 0 44.50 39.61 7.36 o 8 11 0 161.30 146.74 14.33 o 9 11 0 55.97 48.29 7.94 o 10 11 0 29.21 43.94 7.47 o 11 11 0 17.37 20.41 6.69 o 6 12 0 335.83 300.07 19.17 o 7 12 0 8.65 6.10 5.36 o 8 12 0 784.44 777.88 32.90 o 9 12 0 150.05 132.68 13.09 o 10 12 0 520.68 519.50 23.26 o 11 12 0 87.82 63.79 10.25 o 6 13 0 81.06 71.92 10.06 o 7 13 0 194.91 170.21 15.19 o 8 13 0 63.04 69.61 9.80 o 9 13 0 625.62 609.74 27.62 o 10 13 0 64.20 58.01 10.10 o 11 13 0 76.97 81.00 10.54 o 5 14 0 33.37 18.89 5.20 o 6 14 0 312.97 277.59 18.87 o 7 14 0 528.14 469.80 25.18 o 8 14 0 455.60 452.53 24.36 o 9 14 0 92.86 86.60 10.11 o 10 14 0 131.03 124.91 11.79 o 11 14 0 21.43 20.75 5.43 o 4 15 0 571.44 573.14 30.08 o 5 15 0 352.64 328.15 19.82 o 6 15 0 39.44 56.61 8.95 o 7 15 0 240.48 238.08 21.10 o 8 15 0 41.56 40.36 8.42 o 9 15 0 362.10 366.61 21.36 o 10 15 0 12.76 8.66 3.05 o 11 15 0 371.71 332.25 17.01 o 3 16 0 489.05 459.48 41.15 o 4 16 0 613.40 643.11 32.89 o 5 16 0 214.87 183.95 26.91 o 6 16 0 488.96 422.72 51.07 o 7 16 0 71.64 62.81 9.01 o 8 16 0 84.00 74.98 9.07 o 9 16 0 82.51 82.46 8.61 o 10 16 0 222.32 212.24 17.76 o 1 17 0 242.99 206.09 27.03 o 2 17 0 206.40 183.39 26.18 o 3 17 0 1405.67 1468.21 79.65 o 4 17 0 74.75 76.17 12.44 o 5 17 0 393.82 368.97 21.70 o 6 17 0 236.18 245.15 27.77 o 7 17 0 448.66 431.27 23.04 o 8 17 0 166.98 155.68 12.66 o 9 17 0 96.30 96.73 14.05 o 10 17 0 70.05 68.04 9.05 o 0 18 0 1529.69 1585.37 77.84 o 1 18 0 123.07 156.64 16.52 o 2 18 0 305.08 324.30 23.82 o 3 18 0 514.64 553.72 48.95 o 4 18 0 815.65 859.33 40.10 o 5 18 0 231.94 230.82 16.88 o 6 18 0 9.83 9.77 4.89 o 7 18 0 32.90 30.26 9.36 o 8 18 0 189.03 205.70 22.46 o 9 18 0 41.29 42.22 9.37 o 10 18 0 227.07 221.05 13.85 o 1 19 0 50.22 41.58 9.48 o 2 19 0 389.35 378.98 26.63 o 3 19 0 461.80 508.11 47.56 o 4 19 0 108.37 120.71 19.52 o 5 19 0 356.53 386.22 34.96 o 6 19 0 107.91 114.25 18.89 o 7 19 0 226.94 192.56 22.85 o 8 19 0 58.15 40.27 10.31 o 9 19 0 36.79 37.91 7.61 o 0 20 0 172.34 164.98 25.47 o 1 20 0 570.06 571.28 33.82 o 2 20 0 378.99 363.87 26.58 o 3 20 0 99.88 84.02 21.01 o 4 20 0 341.21 419.13 36.09 o 5 20 0 39.94 41.00 11.53 o 6 20 0 27.98 28.52 9.36 o 7 20 0 41.72 33.83 10.88 o 8 20 0 47.65 49.43 9.46 o 9 20 0 36.36 27.27 5.50 o 1 21 0 5.47 2.31 5.93 o 2 21 0 61.00 52.56 10.62 o 3 21 0 216.74 270.73 28.06 o 4 21 0 231.45 265.16 28.40 o 5 21 0 182.94 214.20 24.72 o 6 21 0 87.25 92.86 15.73 o 7 21 0 459.94 520.14 33.00 o 8 21 0 20.54 18.96 6.14 o 0 22 0 449.40 608.76 49.78 o 1 22 0 22.00 26.52 8.10 o 2 22 0 212.91 224.45 20.63 o 3 22 0 68.76 83.85 16.07 o 4 22 0 213.84 251.86 26.77 o 5 22 0 127.71 134.37 18.63 o 6 22 0 7.76 16.08 7.24 o 7 22 0 9.06 10.87 5.31 o 8 22 0 17.85 24.53 5.19 o 1 23 0 552.68 622.68 27.65 o 2 23 0 149.15 134.43 19.96 o 3 23 0 192.31 268.73 26.95 o 4 23 0 55.97 44.36 11.16 o 5 23 0 161.74 162.66 19.31 o 6 23 0 1.07 2.66 4.85 o 7 23 0 64.65 49.05 6.25 o 0 24 0 616.55 684.41 34.97 o 1 24 0 3.06 -0.28 9.03 o 2 24 0 87.89 105.63 11.77 o 3 24 0 60.55 51.83 11.95 o 4 24 0 301.37 304.34 25.92 o 5 24 0 15.11 15.68 6.90 o 6 24 0 54.46 61.44 13.21 o 1 25 0 225.87 248.26 25.03 o 2 25 0 91.85 95.77 14.53 o 3 25 0 35.77 30.66 8.96 o 4 25 0 52.78 53.13 10.04 o 5 25 0 217.61 257.39 15.24 o 6 25 0 14.45 9.11 3.02 o 0 26 0 247.43 272.06 26.47 o 1 26 0 118.87 137.44 17.03 o 2 26 0 21.63 17.88 5.30 o 3 26 0 34.16 48.48 12.12 o 4 26 0 189.15 211.97 13.58 o 5 26 0 12.55 12.27 4.43 o 1 27 0 101.23 112.19 10.12 o 2 27 0 23.78 22.08 5.15 o 3 27 0 60.55 70.17 7.53 o 4 27 0 89.02 85.03 7.12 o 0 28 0 187.16 220.28 15.81 o 1 28 0 5.92 4.21 2.92 o 2 28 0 44.87 53.97 7.00 o 6 -24 1 138.45 137.92 13.01 o 6 -23 1 45.39 59.88 10.41 o 7 -23 1 10.69 11.00 4.64 o -7 -22 1 94.24 92.64 11.46 o -6 -22 1 87.41 99.64 13.55 o 7 -22 1 153.72 156.83 16.36 o 8 -22 1 228.17 234.96 15.88 o -8 -21 1 136.01 127.70 12.67 o -7 -21 1 143.82 167.04 17.79 o -6 -21 1 13.06 2.86 5.34 o 7 -21 1 191.36 265.05 24.10 o 8 -21 1 63.45 62.79 10.38 o -9 -20 1 99.78 73.83 9.04 o -8 -20 1 211.45 221.04 20.00 o -7 -20 1 42.36 48.18 10.91 o 7 -20 1 128.15 163.87 21.41 o 8 -20 1 761.93 835.84 42.79 o 9 -20 1 9.73 5.50 4.10 o -9 -19 1 68.14 68.60 10.57 o -8 -19 1 517.33 583.02 25.77 o -7 -19 1 125.37 131.92 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