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Information card for entry 2022830
Preview
| Coordinates | 2022830.cif |
|---|---|
| Structure factors | 2022830.hkl |
| Original IUCr paper | HTML |
| Common name | <i>N</i>'-[(1<i>E</i>)-(4-Chloro-3-nitrophenyl)methylidene]acetohydrazide |
|---|---|
| Chemical name | (<i>E</i>)-<i>N</i>'-(4-Chloro-3-nitrobenzylidene)acetohydrazide |
| Formula | C9 H8 Cl N3 O3 |
| Calculated formula | C9 H8 Cl N3 O3 |
| Title of publication | Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitrobenzylidene)acetohydrazide and (E)-2-(4-chlorobenzylidene)-1-(quinolin-8-yl)hydrazine |
| Authors of publication | Nasr, Tamer; Kariuki, Benson M.; Elansary, Mai M.; Elhaggar, Radwan; Zaghary, Wafaa |
| Journal of publication | Acta Crystallographica Section E Crystallographic Communications |
| Year of publication | 2023 |
| Journal volume | 79 |
| Journal issue | 8 |
| Pages of publication | 762 - 766 |
| a | 4.4717 ± 0.0001 Å |
| b | 11.9367 ± 0.0002 Å |
| c | 20.1382 ± 0.0003 Å |
| α | 90° |
| β | 95.689 ± 0.002° |
| γ | 90° |
| Cell volume | 1069.63 ± 0.03 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0403 |
| Residual factor for significantly intense reflections | 0.0383 |
| Weighted residual factors for significantly intense reflections | 0.1083 |
| Weighted residual factors for all reflections included in the refinement | 0.1111 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.084 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 285386 (current) | 2023-07-29 | cif/ hkl/ Adding structures of 2022830, 2022831 via cif-deposit CGI script. |
2022830.cif 2022830.hkl |
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Users of the data should acknowledge the original authors of the
structural data.