#------------------------------------------------------------------------------ #$Date: 2023-08-24 04:44:14 +0300 (Thu, 24 Aug 2023) $ #$Revision: 285855 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/28/2022843.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022843 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.6013 _cell_length_b 17.2644 _cell_length_c 8.1099 _exptl_crystal_F_000 1608.00 _reflns_d_resolution_high 0.7506 _cod_data_source_file ex2074IIsup3.hkl _cod_data_source_block II _shelx_title ' shi_6071_yala_autored_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 692.63 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 363305.31 341438.19 1651.71 o 6 0 0 45379.35 48812.36 762.63 o 8 0 0 34157.20 33817.15 742.45 o 10 0 0 13979.14 13391.33 600.29 o 12 0 0 1276.76 1295.38 208.10 o 14 0 0 3876.32 4138.21 404.84 o 16 0 0 1349.88 1137.63 237.01 o 18 0 0 243.47 546.16 189.05 o 20 0 0 5593.06 5568.58 606.96 o 2 1 0 79946.95 84891.15 659.82 o 4 1 0 11288.65 11812.20 212.59 o 6 1 0 1847.62 2113.03 145.37 o 8 1 0 9624.50 10053.99 427.36 o 10 1 0 10382.57 10282.35 334.08 o 12 1 0 41647.65 41052.88 827.49 o 14 1 0 915.74 837.16 149.95 o 16 1 0 8592.35 8327.56 448.14 o 18 1 0 122.93 114.25 87.96 o 20 1 0 1168.28 1151.49 272.05 o 0 2 0 55459.86 58795.65 287.91 o 2 2 0 148751.80 154191.44 744.87 o 4 2 0 90723.48 94580.24 860.09 o 6 2 0 53805.05 56448.96 429.47 o 8 2 0 10991.66 12497.07 797.28 o 10 2 0 27853.59 28397.87 688.73 o 12 2 0 189.74 301.49 101.70 o 14 2 0 1874.62 1798.63 193.45 o 16 2 0 15.71 45.52 60.95 o 18 2 0 4825.72 4605.03 387.51 o 20 2 0 400.54 818.66 240.00 o 2 3 0 6514.89 6465.56 168.18 o 4 3 0 121942.96 124790.66 553.33 o 6 3 0 82688.86 83144.38 619.17 o 8 3 0 22858.88 21904.92 220.48 o 10 3 0 54980.00 54950.48 1545.20 o 12 3 0 762.09 868.87 93.30 o 14 3 0 85.39 138.58 61.10 o 16 3 0 79.68 11.44 61.97 o 18 3 0 89.72 89.82 74.98 o 20 3 0 20.42 112.84 117.85 o 0 4 0 48047.53 52603.29 403.25 o 2 4 0 58491.17 61504.40 797.48 o 4 4 0 8846.56 8990.09 207.66 o 6 4 0 293124.91 295142.12 2733.69 o 8 4 0 10240.90 10662.16 168.71 o 10 4 0 48817.52 49049.84 1266.87 o 12 4 0 7710.89 8074.51 264.39 o 14 4 0 35055.69 34098.22 832.61 o 16 4 0 1568.90 1449.17 184.15 o 18 4 0 8478.72 8088.39 572.28 o 20 4 0 48.04 -84.67 112.57 o 2 5 0 4112.46 4490.52 104.99 o 4 5 0 47383.43 47580.32 1545.72 o 6 5 0 83386.23 83874.27 530.36 o 8 5 0 22653.58 22325.57 322.16 o 10 5 0 19416.46 19804.54 241.17 o 12 5 0 1406.12 1415.93 153.82 o 14 5 0 555.60 492.43 114.78 o 16 5 0 175.08 123.49 73.08 o 18 5 0 1293.73 1177.52 190.04 o 20 5 0 17.04 201.85 130.37 o 0 6 0 243926.95 251421.23 2016.55 o 2 6 0 47304.00 48857.14 395.05 o 4 6 0 102761.20 104950.46 1299.16 o 6 6 0 38571.75 39121.49 415.84 o 8 6 0 1537.33 1805.60 96.03 o 10 6 0 13296.10 13571.43 202.71 o 12 6 0 1826.34 1782.21 114.84 o 14 6 0 214.25 220.49 65.92 o 16 6 0 143.56 105.36 65.25 o 18 6 0 1518.22 1186.69 184.91 o 20 6 0 393.69 624.42 187.38 o 2 7 0 91332.78 89909.18 656.06 o 4 7 0 10376.29 11177.84 197.12 o 6 7 0 3843.64 3642.97 200.83 o 8 7 0 18564.57 18394.54 292.89 o 10 7 0 7619.82 7543.83 198.97 o 12 7 0 27251.45 27860.78 389.90 o 14 7 0 57.47 41.54 48.25 o 16 7 0 13084.56 12973.40 600.35 o 18 7 0 565.57 658.58 149.81 o 0 8 0 479740.31 486514.50 2306.82 o 2 8 0 4760.34 5477.82 126.16 o 4 8 0 128259.96 127183.80 1192.27 o 6 8 0 19899.34 20450.64 284.12 o 8 8 0 11236.71 11263.26 236.53 o 10 8 0 5515.73 5440.36 176.20 o 12 8 0 1263.23 1265.09 88.71 o 14 8 0 542.23 603.97 116.17 o 16 8 0 126.42 167.17 207.47 o 18 8 0 51.91 70.56 100.78 o 2 9 0 41142.30 41521.25 249.52 o 4 9 0 4387.40 4183.56 223.08 o 6 9 0 4355.58 4276.43 127.06 o 8 9 0 1676.86 1639.02 93.49 o 10 9 0 8546.66 8727.44 230.01 o 12 9 0 21387.29 21571.10 379.06 o 14 9 0 2779.31 2763.80 236.07 o 16 9 0 2195.70 2136.73 356.52 o 0 10 0 43919.89 44161.91 740.47 o 2 10 0 31847.89 31991.15 361.94 o 4 10 0 17845.08 18092.35 475.39 o 6 10 0 28060.07 27730.24 446.38 o 8 10 0 6765.56 6308.06 256.21 o 10 10 0 8889.99 9001.76 239.80 o 12 10 0 292.14 254.91 44.60 o 14 10 0 1411.84 1434.90 284.72 o 16 10 0 127.30 94.88 89.84 o 2 11 0 17305.37 16713.30 303.98 o 4 11 0 47496.15 45592.17 789.24 o 6 11 0 50864.96 50194.81 623.44 o 8 11 0 21755.13 21680.22 464.29 o 10 11 0 25889.98 26603.37 568.07 o 12 11 0 3791.11 4068.57 336.16 o 14 11 0 13.36 40.54 75.64 o 16 11 0 158.12 -7.88 86.12 o 0 12 0 16223.42 15538.58 551.92 o 2 12 0 16706.63 16501.71 267.14 o 4 12 0 930.48 868.15 60.70 o 6 12 0 84614.45 82913.70 963.43 o 8 12 0 5290.16 5373.36 231.98 o 10 12 0 22390.68 22573.12 509.85 o 12 12 0 999.32 1069.81 113.77 o 14 12 0 8932.99 8976.05 702.51 o 16 12 0 616.64 500.93 198.73 o 2 13 0 207.85 238.10 58.08 o 4 13 0 13253.84 13079.59 175.71 o 6 13 0 8655.66 8299.53 272.53 o 8 13 0 1556.07 1773.60 134.19 o 10 13 0 2733.08 2681.69 168.99 o 12 13 0 3055.29 2714.52 188.64 o 14 13 0 2.80 111.14 98.43 o 16 13 0 0.91 -166.73 167.50 o 0 14 0 67338.41 65608.24 1584.49 o 2 14 0 9497.66 9059.25 236.30 o 4 14 0 28861.85 28366.94 486.70 o 6 14 0 9512.45 9156.73 294.16 o 8 14 0 14.87 25.86 40.55 o 10 14 0 776.51 695.55 110.32 o 12 14 0 183.28 139.66 38.05 o 14 14 0 64.98 265.28 142.67 o 2 15 0 32562.80 31089.41 1148.96 o 4 15 0 2138.49 2085.33 136.74 o 6 15 0 2082.67 2315.98 152.46 o 8 15 0 4505.73 4455.24 223.04 o 10 15 0 2105.68 1867.61 150.11 o 12 15 0 7693.66 8110.61 384.81 o 14 15 0 30.99 4.30 119.67 o 0 16 0 72575.17 72462.12 1804.57 o 2 16 0 1695.00 1747.72 202.60 o 4 16 0 25154.12 24027.30 710.07 o 6 16 0 1592.41 1396.19 173.11 o 8 16 0 813.01 763.03 120.88 o 10 16 0 1697.04 1495.47 139.81 o 12 16 0 48.21 3.88 49.08 o 14 16 0 884.99 1044.59 208.57 o 2 17 0 4247.13 4342.90 329.75 o 4 17 0 1160.87 924.97 153.53 o 6 17 0 4179.34 4387.18 223.29 o 8 17 0 107.80 179.60 67.57 o 10 17 0 2255.43 2362.01 178.58 o 12 17 0 3589.18 3375.56 309.69 o 14 17 0 1063.19 853.35 191.02 o 0 18 0 6490.90 5500.47 546.68 o 2 18 0 3837.62 3688.33 348.35 o 4 18 0 95.71 27.96 61.60 o 6 18 0 10983.38 11148.49 464.67 o 8 18 0 2587.01 2696.08 235.28 o 10 18 0 2270.50 2341.20 181.40 o 12 18 0 886.08 793.58 170.67 o 2 19 0 2567.51 2970.49 292.77 o 4 19 0 9636.59 9336.04 685.68 o 6 19 0 5826.75 6371.05 434.84 o 8 19 0 2162.72 2897.15 250.76 o 10 19 0 5486.87 5517.14 425.35 o 0 20 0 1196.65 981.04 240.90 o 2 20 0 4641.56 4370.50 366.71 o 4 20 0 54.70 136.32 87.52 o 6 20 0 9009.03 9110.30 532.15 o 8 20 0 1532.06 1330.25 175.85 o 10 20 0 3593.37 3251.77 324.12 o 2 21 0 426.15 496.43 237.09 o 4 21 0 2560.92 2756.01 307.89 o 6 21 0 871.74 992.39 186.71 o 1 0 1 53211.58 51591.51 441.61 o 3 0 1 3160.61 3391.29 73.88 o 4 0 1 61683.43 65344.75 426.42 o 5 0 1 30943.72 32003.71 400.76 o 6 0 1 25.91 90.58 23.35 o 7 0 1 22.99 81.62 27.53 o 8 0 1 152384.84 153685.84 1094.82 o 9 0 1 3847.39 4298.00 149.34 o 10 0 1 783.35 946.73 176.42 o 11 0 1 26079.39 24938.43 881.43 o 12 0 1 93133.62 91826.08 1787.75 o 13 0 1 2550.69 2626.62 322.23 o 14 0 1 4727.22 4804.45 446.79 o 15 0 1 38.12 55.56 60.83 o 16 0 1 15667.12 15349.32 611.30 o 17 0 1 1993.06 1885.69 330.13 o 18 0 1 666.10 745.53 155.30 o 19 0 1 110.73 169.44 89.45 o 20 0 1 668.67 782.31 168.60 o 0 1 1 59634.83 58213.33 644.97 o 1 1 1 35722.88 37039.42 252.60 o 2 1 1 230.05 239.46 17.55 o 3 1 1 38.83 82.22 10.92 o 4 1 1 47622.39 47845.55 222.50 o 5 1 1 8679.85 8799.93 103.92 o 6 1 1 17267.85 16667.52 167.41 o 7 1 1 8101.23 8625.62 94.40 o 8 1 1 12122.54 12308.21 164.15 o 9 1 1 318.28 380.19 38.03 o 10 1 1 29633.64 29318.45 457.28 o 11 1 1 1095.32 1328.89 330.91 o 12 1 1 7656.22 7609.94 363.22 o 13 1 1 57.51 164.15 77.74 o 14 1 1 2782.23 2662.05 238.27 o 15 1 1 515.82 531.81 81.07 o 16 1 1 2583.21 2268.56 169.61 o 17 1 1 2105.40 2223.87 175.11 o 18 1 1 615.74 826.72 115.70 o 19 1 1 527.56 478.67 95.61 o 20 1 1 297.09 431.21 169.64 o 1 2 1 18609.20 19370.15 126.27 o 2 2 1 37958.53 39442.79 236.62 o 3 2 1 14310.05 14275.55 128.46 o 4 2 1 10529.32 11654.64 112.94 o 5 2 1 1988.97 2118.52 53.46 o 6 2 1 43933.31 44059.56 247.99 o 7 2 1 36686.89 37982.97 300.65 o 8 2 1 37131.85 38517.14 265.68 o 9 2 1 7504.13 7297.36 120.33 o 10 2 1 3082.46 3024.17 130.20 o 11 2 1 3425.67 3404.35 175.96 o 12 2 1 24466.12 24745.47 653.92 o 13 2 1 8236.43 8724.44 409.78 o 14 2 1 2912.32 2996.22 369.49 o 15 2 1 239.00 219.39 54.68 o 16 2 1 1622.01 1582.41 144.17 o 17 2 1 123.11 136.52 55.41 o 18 2 1 1532.12 1428.56 144.41 o 19 2 1 688.80 573.89 94.07 o 20 2 1 136.49 -97.31 97.31 o 0 3 1 12948.51 13175.94 163.34 o 1 3 1 57057.88 58062.31 189.15 o 2 3 1 366.56 395.89 20.40 o 3 3 1 506.19 586.03 26.70 o 4 3 1 54037.29 54430.74 248.94 o 5 3 1 28003.70 28574.07 200.18 o 6 3 1 17296.88 17573.45 174.97 o 7 3 1 5201.37 5094.82 113.49 o 8 3 1 11785.30 12009.59 202.25 o 9 3 1 1938.72 2010.87 69.00 o 10 3 1 9757.02 10067.83 174.05 o 11 3 1 217.21 228.77 17.41 o 12 3 1 4218.61 4219.37 262.60 o 13 3 1 366.09 323.17 89.05 o 14 3 1 7628.17 8277.11 416.36 o 15 3 1 439.49 391.28 68.34 o 16 3 1 4647.29 4764.16 242.34 o 17 3 1 945.83 871.35 115.35 o 18 3 1 10279.19 10275.38 384.61 o 19 3 1 885.22 966.68 125.02 o 20 3 1 601.40 445.61 129.79 o 1 4 1 1525.34 1730.60 35.16 o 2 4 1 437936.44 439785.22 2784.32 o 3 4 1 5028.85 5364.52 82.42 o 4 4 1 3854.56 3665.59 62.28 o 5 4 1 64526.43 65790.75 379.84 o 6 4 1 168095.00 169911.39 1130.69 o 7 4 1 805.79 950.53 60.52 o 8 4 1 134.72 282.12 49.07 o 9 4 1 16.64 51.45 22.98 o 10 4 1 10056.84 10118.04 223.27 o 11 4 1 15120.59 15574.03 163.62 o 12 4 1 401.82 432.50 27.05 o 13 4 1 549.78 550.72 155.49 o 14 4 1 6271.07 6628.70 298.98 o 15 4 1 723.70 636.69 90.00 o 16 4 1 1576.38 1697.92 144.42 o 17 4 1 1014.57 1050.87 134.85 o 18 4 1 8095.44 8288.45 347.43 o 19 4 1 169.89 89.88 62.28 o 20 4 1 1096.59 1301.54 204.01 o 0 5 1 13896.31 14089.63 144.29 o 1 5 1 22098.00 22146.16 130.49 o 2 5 1 8527.04 8864.61 88.64 o 3 5 1 1621.21 1910.33 49.48 o 4 5 1 9319.77 9141.46 143.61 o 5 5 1 4412.78 4310.48 82.69 o 6 5 1 8805.19 8550.33 129.35 o 7 5 1 16715.67 17204.71 212.75 o 8 5 1 1225.87 1430.15 107.45 o 9 5 1 1.93 26.95 17.20 o 10 5 1 1843.81 1899.02 112.88 o 11 5 1 405.56 425.32 39.40 o 12 5 1 4463.08 4371.58 98.04 o 13 5 1 32.66 56.33 19.60 o 14 5 1 5274.57 5400.88 272.02 o 15 5 1 0.91 62.35 43.63 o 16 5 1 6944.56 7048.40 295.58 o 17 5 1 3651.83 3830.22 228.73 o 18 5 1 4836.92 5282.24 276.08 o 19 5 1 252.00 264.06 104.32 o 20 5 1 302.34 306.02 108.86 o 1 6 1 1292.84 1348.08 47.71 o 2 6 1 19750.35 21180.67 168.34 o 3 6 1 19439.55 19822.73 216.82 o 4 6 1 4387.81 4500.01 103.70 o 5 6 1 1121.24 1205.82 62.99 o 6 6 1 16544.66 16823.61 250.65 o 7 6 1 16696.23 17148.92 254.44 o 8 6 1 33439.46 34099.94 298.04 o 9 6 1 3114.19 3120.85 119.52 o 10 6 1 1022.00 1105.07 82.99 o 11 6 1 3927.07 3821.70 117.06 o 12 6 1 20662.26 20571.99 314.94 o 13 6 1 7370.64 7655.71 180.90 o 14 6 1 4953.99 5197.45 264.63 o 15 6 1 778.18 824.79 97.68 o 16 6 1 3387.06 3566.50 259.14 o 17 6 1 183.52 283.54 68.21 o 18 6 1 1517.86 1466.16 148.39 o 19 6 1 210.77 126.42 80.80 o 0 7 1 73581.52 72682.55 324.85 o 1 7 1 28726.69 29278.17 204.68 o 2 7 1 512.72 595.58 48.73 o 3 7 1 416.78 457.09 23.38 o 4 7 1 49405.08 48563.80 269.19 o 5 7 1 10404.72 10227.92 157.91 o 6 7 1 24111.66 23380.84 349.80 o 7 7 1 336.72 405.23 42.70 o 8 7 1 12271.41 12394.12 171.56 o 9 7 1 2461.80 2605.22 87.57 o 10 7 1 31869.70 32558.47 829.20 o 11 7 1 238.87 268.46 37.41 o 12 7 1 7320.27 7370.66 185.63 o 13 7 1 446.85 502.51 59.66 o 14 7 1 5097.30 5528.28 239.29 o 15 7 1 2036.52 1904.93 146.56 o 16 7 1 1850.58 2064.49 163.24 o 17 7 1 309.79 352.34 74.24 o 18 7 1 190.64 104.02 45.90 o 1 8 1 3944.95 3957.34 72.79 o 2 8 1 5350.18 5138.37 82.60 o 3 8 1 225.55 283.00 16.92 o 4 8 1 38610.85 39305.29 287.07 o 5 8 1 17248.82 17479.66 210.21 o 6 8 1 214.19 283.38 42.89 o 7 8 1 942.37 948.61 83.09 o 8 8 1 81362.23 81362.67 660.53 o 9 8 1 363.07 434.85 52.44 o 10 8 1 1458.90 1526.84 102.33 o 11 8 1 11448.39 11297.84 234.84 o 12 8 1 64564.15 64627.05 571.08 o 13 8 1 1087.18 1095.68 91.38 o 14 8 1 1967.87 1922.93 143.47 o 15 8 1 126.68 129.09 50.04 o 16 8 1 9389.36 9982.25 349.24 o 17 8 1 1000.88 1147.06 127.70 o 18 8 1 215.34 167.68 215.89 o 0 9 1 28221.11 28558.69 324.51 o 1 9 1 21381.98 21578.41 168.26 o 2 9 1 691.53 734.31 37.39 o 3 9 1 53.61 92.14 13.97 o 4 9 1 3463.43 3384.01 69.16 o 5 9 1 5159.35 5150.72 96.93 o 6 9 1 1292.95 1253.23 89.92 o 7 9 1 5649.40 5640.44 194.38 o 8 9 1 1096.27 1262.28 131.02 o 9 9 1 19.54 2.33 24.42 o 10 9 1 5889.75 5924.48 155.43 o 11 9 1 1160.08 1307.46 70.64 o 12 9 1 2550.36 2700.00 121.84 o 13 9 1 347.15 378.31 53.43 o 14 9 1 637.87 585.78 81.29 o 15 9 1 2.39 112.81 48.75 o 16 9 1 574.75 516.19 209.25 o 17 9 1 1811.68 2198.06 268.76 o 1 10 1 1103.10 1112.08 48.47 o 2 10 1 47986.01 47111.57 336.95 o 3 10 1 3273.08 3098.99 77.51 o 4 10 1 431.89 494.79 28.61 o 5 10 1 2476.02 2481.66 64.46 o 6 10 1 27544.39 27595.37 290.21 o 7 10 1 10192.42 10260.75 221.52 o 8 10 1 11992.89 12325.42 261.16 o 9 10 1 1199.60 1177.28 96.88 o 10 10 1 4822.77 4903.89 161.58 o 11 10 1 2585.34 2581.08 109.88 o 12 10 1 5711.48 5824.12 170.85 o 13 10 1 4643.63 4493.08 174.14 o 14 10 1 1002.60 1056.93 172.37 o 15 10 1 132.94 44.64 65.03 o 16 10 1 12.17 -36.41 116.24 o 17 10 1 85.15 192.75 90.87 o 0 11 1 28358.47 27520.95 377.55 o 1 11 1 7309.29 7130.31 139.74 o 2 11 1 4198.66 3968.18 107.72 o 3 11 1 2630.49 2520.09 81.35 o 4 11 1 18410.74 17542.03 189.03 o 5 11 1 5305.00 5069.04 94.35 o 6 11 1 4110.90 3909.27 85.70 o 7 11 1 4865.56 4545.44 129.67 o 8 11 1 7578.84 7748.02 193.05 o 9 11 1 1133.00 1196.22 85.68 o 10 11 1 3416.65 3330.76 126.17 o 11 11 1 1090.23 1037.83 78.99 o 12 11 1 813.70 912.43 72.89 o 13 11 1 999.01 1081.44 135.09 o 14 11 1 5205.49 5249.89 378.94 o 15 11 1 336.58 574.42 148.06 o 16 11 1 3144.64 3097.14 311.51 o 17 11 1 466.36 575.65 154.77 o 1 12 1 273.76 288.88 26.63 o 2 12 1 77015.00 77302.18 1288.81 o 3 12 1 137.44 169.69 29.33 o 4 12 1 1039.41 1133.40 66.74 o 5 12 1 11373.04 11112.46 149.95 o 6 12 1 43464.51 43511.56 502.17 o 7 12 1 895.38 874.38 71.23 o 8 12 1 39.08 7.50 38.03 o 9 12 1 336.05 384.50 53.60 o 10 12 1 3617.99 3841.58 150.23 o 11 12 1 4665.33 4986.40 173.48 o 12 12 1 58.28 63.35 26.58 o 13 12 1 343.15 286.36 106.73 o 14 12 1 2878.14 3122.17 294.39 o 15 12 1 101.48 155.83 82.31 o 16 12 1 391.51 451.03 140.37 o 0 13 1 658.54 682.69 67.17 o 1 13 1 7741.85 7203.42 170.63 o 2 13 1 758.51 845.21 66.04 o 3 13 1 4.74 4.36 15.96 o 4 13 1 2044.69 1956.28 117.25 o 5 13 1 1074.75 1245.80 78.84 o 6 13 1 2451.38 2434.68 121.81 o 7 13 1 2662.77 2462.29 125.96 o 8 13 1 1.52 15.97 35.87 o 9 13 1 5.03 -3.49 26.17 o 10 13 1 74.77 25.33 29.43 o 11 13 1 1590.52 1493.82 95.47 o 12 13 1 2726.13 2522.49 130.99 o 13 13 1 92.37 107.97 78.66 o 14 13 1 727.71 513.51 121.76 o 15 13 1 49.77 45.36 126.06 o 16 13 1 3138.65 3688.85 351.60 o 1 14 1 43.43 58.93 23.40 o 2 14 1 514.34 645.91 91.39 o 3 14 1 2108.34 2222.22 270.24 o 4 14 1 3166.10 2897.29 125.40 o 5 14 1 2312.08 2412.32 120.31 o 6 14 1 2156.57 2315.51 121.31 o 7 14 1 2080.04 1884.92 114.07 o 8 14 1 8939.46 8489.31 211.32 o 9 14 1 491.64 557.55 56.80 o 10 14 1 499.83 412.24 49.69 o 11 14 1 1557.41 1527.73 94.26 o 12 14 1 11153.35 11376.00 286.36 o 13 14 1 1414.49 1522.62 179.28 o 14 14 1 2360.09 2358.33 641.21 o 15 14 1 7.13 -26.77 96.75 o 0 15 1 22919.96 20930.80 1490.62 o 1 15 1 6999.95 6318.11 249.52 o 2 15 1 391.02 370.89 57.93 o 3 15 1 1.13 29.23 32.07 o 4 15 1 13078.89 12617.18 285.88 o 5 15 1 3701.52 3709.38 152.58 o 6 15 1 7254.59 6973.91 215.30 o 7 15 1 156.82 134.15 30.19 o 8 15 1 3465.59 3453.34 139.41 o 9 15 1 1091.29 970.91 76.97 o 10 15 1 11193.43 11531.08 263.53 o 11 15 1 2.03 45.29 34.41 o 12 15 1 2509.48 2720.13 158.28 o 13 15 1 106.88 71.49 63.13 o 14 15 1 3381.14 3611.14 259.87 o 15 15 1 818.02 961.03 160.92 o 1 16 1 475.34 323.38 97.25 o 2 16 1 264.46 245.66 49.68 o 3 16 1 568.08 486.43 162.77 o 4 16 1 4164.30 4140.42 224.07 o 5 16 1 962.38 1024.49 88.55 o 6 16 1 0.24 9.69 24.28 o 7 16 1 1288.18 1269.84 86.61 o 8 16 1 20525.87 20491.89 368.40 o 9 16 1 44.91 52.18 32.62 o 10 16 1 56.83 134.89 31.90 o 11 16 1 2175.63 2126.47 120.02 o 12 16 1 11942.92 12801.38 350.25 o 13 16 1 1209.63 1073.00 136.73 o 14 16 1 317.53 254.02 107.46 o 0 17 1 1645.88 1927.54 317.52 o 1 17 1 3045.41 2927.42 274.95 o 2 17 1 3.09 68.29 117.28 o 3 17 1 33.09 45.64 69.84 o 4 17 1 141.25 189.62 60.32 o 5 17 1 494.80 392.92 56.42 o 6 17 1 435.99 493.90 56.88 o 7 17 1 2140.03 1856.92 105.14 o 8 17 1 65.98 159.10 37.01 o 9 17 1 16.63 -10.69 26.15 o 10 17 1 1237.05 1116.55 86.10 o 11 17 1 225.15 199.91 57.09 o 12 17 1 43.65 10.36 35.46 o 13 17 1 124.68 224.00 60.72 o 1 18 1 0.42 72.28 46.96 o 2 18 1 10659.09 10905.07 380.14 o 3 18 1 202.37 188.17 61.45 o 4 18 1 2.07 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3040.97 3099.52 103.74 o 9 1 2 528.45 476.21 37.48 o 10 1 2 0.83 5.84 14.64 o 11 1 2 20187.33 20247.25 224.80 o 12 1 2 3120.06 3211.88 110.01 o 13 1 2 10419.25 10468.88 364.11 o 14 1 2 6244.47 6290.98 378.35 o 15 1 2 551.09 404.98 119.69 o 16 1 2 6422.77 7447.16 443.37 o 17 1 2 2101.43 2010.73 240.65 o 18 1 2 2469.70 1982.64 200.60 o 19 1 2 20.81 19.74 47.38 o 0 2 2 52320.14 52783.99 862.26 o 1 2 2 59923.22 59125.62 460.64 o 2 2 2 679.34 758.84 40.79 o 3 2 2 290.83 392.44 29.08 o 4 2 2 8699.13 9103.11 136.18 o 5 2 2 23175.82 23869.79 208.15 o 6 2 2 42047.15 42791.57 311.43 o 7 2 2 6847.22 6920.05 108.11 o 8 2 2 18968.15 19037.17 189.92 o 9 2 2 41.88 102.56 16.55 o 10 2 2 11698.71 11862.35 160.81 o 11 2 2 71.50 51.06 17.05 o 12 2 2 6270.97 7071.77 237.02 o 13 2 2 1435.34 1511.20 142.62 o 14 2 2 9559.82 8546.89 440.24 o 15 2 2 360.76 381.86 105.37 o 16 2 2 1529.89 1388.45 198.38 o 17 2 2 2028.26 2130.82 250.04 o 18 2 2 155.38 188.32 67.59 o 19 2 2 1555.24 1776.69 168.91 o 20 2 2 647.98 676.01 162.19 o 1 3 2 12589.97 12796.47 200.78 o 2 3 2 61848.25 61545.59 354.78 o 3 3 2 430.19 527.51 44.41 o 4 3 2 11777.44 11481.12 142.21 o 5 3 2 50511.38 50081.45 456.83 o 6 3 2 19971.62 18783.54 229.17 o 7 3 2 19081.64 18410.28 189.68 o 8 3 2 39414.16 38745.43 297.88 o 9 3 2 5543.68 5401.46 114.40 o 10 3 2 7239.63 7473.10 121.94 o 11 3 2 12098.48 12396.71 294.06 o 12 3 2 18335.15 18730.62 383.14 o 13 3 2 3069.08 3176.56 302.58 o 14 3 2 3986.23 3720.38 462.61 o 15 3 2 6.11 20.23 55.41 o 16 3 2 1270.21 1306.42 191.36 o 17 3 2 684.00 727.97 238.02 o 18 3 2 1.11 6.36 63.97 o 19 3 2 526.46 462.51 92.60 o 20 3 2 275.53 164.03 113.60 o 0 4 2 36383.86 36240.75 514.53 o 1 4 2 18495.09 17903.76 168.24 o 2 4 2 49833.59 50657.23 461.63 o 3 4 2 1700.87 1762.46 68.24 o 4 4 2 1109.00 1426.97 51.51 o 5 4 2 4172.57 4209.37 91.36 o 6 4 2 52657.29 53095.79 337.52 o 7 4 2 19215.70 18685.70 217.08 o 8 4 2 7782.53 7693.65 153.39 o 9 4 2 119.34 173.51 24.84 o 10 4 2 115045.08 114258.02 807.87 o 11 4 2 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47.37 o 4 6 2 6389.97 6272.63 117.36 o 5 6 2 30602.84 32273.37 311.71 o 6 6 2 22884.44 23485.26 228.12 o 7 6 2 4358.27 4372.18 113.95 o 8 6 2 18408.42 18302.07 336.53 o 9 6 2 1.11 1.24 17.88 o 10 6 2 7744.68 7857.99 213.85 o 11 6 2 60.76 56.24 40.82 o 12 6 2 772.35 989.21 80.42 o 13 6 2 1325.26 1403.46 128.68 o 14 6 2 3246.49 3492.25 488.63 o 15 6 2 225.77 282.69 101.11 o 16 6 2 952.07 817.84 154.40 o 17 6 2 1882.43 1821.06 184.73 o 18 6 2 280.96 384.28 78.54 o 19 6 2 838.16 919.22 212.96 o 1 7 2 16.75 49.21 12.46 o 2 7 2 52034.38 50751.66 491.26 o 3 7 2 175.58 201.16 23.97 o 4 7 2 2284.79 2228.88 62.29 o 5 7 2 4051.84 4429.38 104.59 o 6 7 2 23042.64 23148.21 283.24 o 7 7 2 17740.67 17307.00 262.90 o 8 7 2 998.15 937.25 73.40 o 9 7 2 330.23 221.37 46.26 o 10 7 2 1305.84 1420.57 96.88 o 11 7 2 11247.86 11566.46 372.59 o 12 7 2 5370.78 5847.12 276.08 o 13 7 2 10628.88 10734.62 351.71 o 14 7 2 6261.55 6282.62 377.82 o 15 7 2 393.92 552.41 127.41 o 16 7 2 3691.95 3659.99 245.80 o 17 7 2 1714.11 1887.68 221.55 o 18 7 2 809.05 678.49 154.51 o 0 8 2 112262.21 111905.89 901.58 o 1 8 2 42308.19 42301.00 292.03 o 2 8 2 801.12 948.87 54.76 o 3 8 2 6127.03 6489.63 139.86 o 4 8 2 158536.22 159917.22 1163.37 o 5 8 2 11203.04 11249.74 170.68 o 6 8 2 6563.15 6740.63 144.88 o 7 8 2 28.07 37.39 21.81 o 8 8 2 15717.67 16041.99 627.58 o 9 8 2 15.15 44.69 21.42 o 10 8 2 261.37 228.66 73.38 o 11 8 2 3623.79 3335.71 373.85 o 12 8 2 15.87 73.42 112.27 o 13 8 2 0.30 200.49 132.95 o 14 8 2 1977.41 2305.70 231.29 o 15 8 2 634.09 632.35 102.42 o 16 8 2 6837.12 7092.67 339.91 o 17 8 2 1100.54 1147.40 132.45 o 1 9 2 195.97 252.42 20.64 o 2 9 2 7324.29 7047.20 162.37 o 3 9 2 3.93 43.01 20.22 o 4 9 2 1329.90 1363.35 50.05 o 5 9 2 10928.91 10905.25 150.32 o 6 9 2 7092.22 7175.00 128.16 o 7 9 2 7260.78 6996.32 135.02 o 8 9 2 2629.06 2716.18 218.91 o 9 9 2 49.86 67.42 62.99 o 10 9 2 1898.93 1932.77 199.35 o 11 9 2 11678.26 11835.50 720.54 o 12 9 2 1.29 113.32 88.66 o 13 9 2 2531.07 2494.41 361.48 o 14 9 2 2035.21 2047.36 209.66 o 15 9 2 269.13 488.73 336.03 o 16 9 2 3203.07 2997.56 446.65 o 17 9 2 574.06 670.38 168.17 o 0 10 2 7022.39 7586.38 140.81 o 1 10 2 14098.36 13967.83 183.38 o 2 10 2 21.30 57.13 18.30 o 3 10 2 285.06 220.15 25.96 o 4 10 2 579.19 677.93 48.98 o 5 10 2 5802.87 5420.15 106.64 o 6 10 2 19173.05 19211.15 227.29 o 7 10 2 4798.92 4760.85 133.45 o 8 10 2 1307.99 1373.78 96.82 o 9 10 2 67.97 82.56 23.13 o 10 10 2 11957.20 12524.16 514.25 o 11 10 2 7.39 -8.70 72.51 o 12 10 2 5195.74 5160.87 504.03 o 13 10 2 681.17 662.13 117.36 o 14 10 2 7362.80 7962.92 673.88 o 15 10 2 56.77 32.31 87.41 o 16 10 2 1829.33 2056.19 261.54 o 17 10 2 1791.69 2078.08 273.68 o 1 11 2 6122.21 6043.60 105.88 o 2 11 2 17843.71 17685.53 249.42 o 3 11 2 34.73 123.77 20.34 o 4 11 2 3253.45 3109.56 95.27 o 5 11 2 10745.51 10277.76 146.26 o 6 11 2 13848.27 13773.71 160.24 o 7 11 2 9440.92 9122.31 179.42 o 8 11 2 29244.07 28843.34 297.42 o 9 11 2 1767.46 2090.19 208.25 o 10 11 2 1284.48 1375.84 176.41 o 11 11 2 4630.28 4908.70 474.24 o 12 11 2 6851.95 7753.19 620.51 o 13 11 2 1700.05 1528.97 171.50 o 14 11 2 3835.14 3793.60 474.24 o 15 11 2 33.76 123.68 131.72 o 16 11 2 1682.76 1795.82 247.62 o 0 12 2 6120.64 5869.29 287.60 o 1 12 2 7337.35 6973.04 114.04 o 2 12 2 4771.30 4719.18 116.81 o 3 12 2 1385.90 1577.31 54.97 o 4 12 2 536.36 494.07 29.04 o 5 12 2 4777.59 4904.59 162.08 o 6 12 2 20716.10 20800.45 305.45 o 7 12 2 5521.31 5412.31 136.82 o 8 12 2 825.47 856.91 80.39 o 9 12 2 5.12 151.90 52.26 o 10 12 2 37100.95 37822.85 1719.01 o 11 12 2 160.20 113.48 120.85 o 12 12 2 163.23 83.94 92.74 o 13 12 2 685.56 826.05 220.09 o 14 12 2 7853.48 8728.85 718.07 o 15 12 2 10.22 7.83 90.67 o 16 12 2 650.18 687.85 238.71 o 1 13 2 0.27 39.71 30.13 o 2 13 2 1947.44 2079.08 71.03 o 3 13 2 132.35 77.32 18.53 o 4 13 2 3256.04 3320.30 145.77 o 5 13 2 7634.23 7488.86 195.45 o 6 13 2 330.49 335.64 43.22 o 7 13 2 3376.45 3218.86 150.41 o 8 13 2 2202.57 2109.25 126.99 o 9 13 2 103.13 119.75 49.30 o 10 13 2 1468.58 1406.56 168.32 o 11 13 2 3920.14 4309.31 341.70 o 12 13 2 4361.06 4719.06 325.57 o 13 13 2 1875.41 1773.31 325.30 o 14 13 2 80.11 12.99 81.70 o 15 13 2 0.64 61.96 156.29 o 0 14 2 20790.44 21636.93 594.26 o 1 14 2 11611.32 11366.50 304.36 o 2 14 2 9.35 40.42 18.13 o 3 14 2 448.15 415.58 60.02 o 4 14 2 15609.79 15567.53 322.52 o 5 14 2 4182.16 4159.41 150.95 o 6 14 2 911.92 797.24 75.28 o 7 14 2 604.63 619.72 78.50 o 8 14 2 6559.70 6823.96 252.42 o 9 14 2 5.24 49.48 34.90 o 10 14 2 975.84 1026.66 115.76 o 11 14 2 522.13 580.94 117.36 o 12 14 2 32.05 5.36 42.38 o 13 14 2 21.10 9.10 54.51 o 14 14 2 140.37 144.31 67.91 o 15 14 2 192.23 291.70 94.84 o 1 15 2 121.97 94.29 56.58 o 2 15 2 17481.55 17666.70 390.09 o 3 15 2 983.98 1214.69 98.04 o 4 15 2 2436.08 2580.78 176.97 o 5 15 2 272.78 428.76 94.35 o 6 15 2 7349.07 7068.44 295.54 o 7 15 2 3535.88 3368.85 178.89 o 8 15 2 721.19 794.34 90.99 o 9 15 2 179.89 159.91 59.87 o 10 15 2 1141.88 1193.95 114.97 o 11 15 2 3427.98 3284.44 170.19 o 12 15 2 2743.08 2685.78 176.77 o 13 15 2 3230.88 3295.32 237.24 o 14 15 2 1951.28 1849.17 184.55 o 15 15 2 190.33 236.09 99.20 o 0 16 2 21372.05 22589.02 1046.25 o 1 16 2 5459.31 6039.77 388.43 o 2 16 2 101.76 84.69 62.88 o 3 16 2 31.45 90.88 69.30 o 4 16 2 16325.02 16995.26 558.59 o 5 16 2 2059.77 2039.04 198.15 o 6 16 2 23.70 18.13 56.69 o 7 16 2 316.75 277.81 69.09 o 8 16 2 3594.69 3435.16 166.07 o 9 16 2 181.65 197.77 76.90 o 10 16 2 71.08 62.83 41.85 o 11 16 2 222.50 176.16 41.64 o 12 16 2 239.84 103.33 55.68 o 13 16 2 71.75 34.66 72.19 o 14 16 2 176.13 176.88 87.21 o 1 17 2 0.48 61.89 59.54 o 2 17 2 673.93 637.26 134.55 o 3 17 2 170.54 286.44 127.89 o 4 17 2 341.79 257.64 84.05 o 5 17 2 2081.13 2174.23 190.86 o 6 17 2 275.84 277.57 75.06 o 7 17 2 1391.37 1581.31 143.31 o 8 17 2 55.48 71.01 43.70 o 9 17 2 18.77 48.74 32.45 o 10 17 2 623.90 686.85 71.57 o 11 17 2 2888.50 2878.46 165.51 o 12 17 2 57.54 23.37 53.51 o 13 17 2 430.55 458.74 160.04 o 0 18 2 21.50 46.54 80.05 o 1 18 2 2431.22 2484.79 270.68 o 2 18 2 291.42 439.91 116.75 o 3 18 2 72.50 54.19 56.46 o 4 18 2 88.95 85.87 84.24 o 5 18 2 739.68 939.96 144.99 o 6 18 2 1927.92 2048.78 212.73 o 7 18 2 1298.14 1276.10 172.18 o 8 18 2 31.81 21.00 44.93 o 9 18 2 88.50 47.54 31.21 o 10 18 2 3957.27 3764.54 176.75 o 11 18 2 2.08 54.76 37.86 o 12 18 2 1005.88 628.57 137.14 o 1 19 2 677.72 566.08 142.73 o 2 19 2 4667.85 5202.71 398.49 o 3 19 2 55.62 38.54 66.75 o 4 19 2 1708.04 2083.70 258.69 o 5 19 2 3230.25 3060.59 309.14 o 6 19 2 1795.18 2346.49 235.80 o 7 19 2 1575.04 1500.37 139.06 o 8 19 2 5525.62 5249.58 260.35 o 9 19 2 710.14 820.44 103.52 o 10 19 2 733.76 624.35 97.70 o 11 19 2 538.20 663.54 205.78 o 0 20 2 262.52 198.01 153.12 o 1 20 2 1505.55 1602.38 237.43 o 2 20 2 159.04 39.99 80.43 o 3 20 2 164.93 231.20 132.72 o 4 20 2 203.69 188.46 103.95 o 5 20 2 895.97 1060.95 132.91 o 6 20 2 3468.41 3522.73 234.97 o 7 20 2 838.31 688.76 96.80 o 8 20 2 7.38 17.47 52.16 o 9 20 2 16.42 22.48 58.54 o 1 21 2 37.79 34.68 58.05 o 2 21 2 0.95 -4.03 53.81 o 3 21 2 154.46 255.82 80.63 o 4 21 2 140.62 283.99 256.50 o 1 0 3 4208.86 4381.42 160.49 o 2 0 3 360.34 261.06 36.11 o 3 0 3 2590.70 2326.89 103.34 o 4 0 3 130013.92 130100.12 841.80 o 5 0 3 8274.41 8564.42 240.44 o 6 0 3 45787.29 45450.43 631.30 o 7 0 3 18586.94 18398.29 459.79 o 8 0 3 90846.17 89142.87 1449.64 o 9 0 3 169.83 171.33 68.42 o 10 0 3 16831.07 17000.20 575.55 o 11 0 3 3837.61 3584.18 241.48 o 12 0 3 12093.67 11567.39 452.47 o 13 0 3 8896.65 8543.14 629.80 o 14 0 3 795.83 829.98 230.40 o 15 0 3 6650.97 7022.68 392.55 o 16 0 3 7871.28 7484.53 646.25 o 17 0 3 1012.73 1061.94 262.04 o 18 0 3 424.66 476.12 177.71 o 19 0 3 395.75 227.65 169.91 o 0 1 3 9453.03 10384.64 310.57 o 1 1 3 34882.79 34122.57 273.10 o 2 1 3 24582.16 24196.23 256.83 o 3 1 3 13631.79 13754.47 193.22 o 4 1 3 5362.30 5149.47 113.58 o 5 1 3 19155.05 19218.40 290.95 o 6 1 3 62749.61 60955.43 735.63 o 7 1 3 333.95 440.64 58.91 o 8 1 3 25126.39 23820.30 358.18 o 9 1 3 7096.98 7109.45 181.77 o 10 1 3 8852.66 8571.23 253.65 o 11 1 3 8.43 8.68 19.68 o 12 1 3 1821.41 1769.78 100.79 o 13 1 3 1195.83 1094.32 105.32 o 14 1 3 1101.37 1240.71 113.84 o 15 1 3 111.97 122.47 48.83 o 16 1 3 435.28 430.59 119.44 o 17 1 3 66.76 172.54 89.28 o 18 1 3 1260.44 1047.14 299.70 o 19 1 3 620.01 335.96 225.56 o 1 2 3 117.04 90.22 39.08 o 2 2 3 57056.19 57354.76 586.12 o 3 2 3 29910.27 31911.50 370.09 o 4 2 3 44738.03 44537.62 337.10 o 5 2 3 8420.39 7808.19 188.26 o 6 2 3 67.85 60.29 24.61 o 7 2 3 4873.74 4973.04 152.63 o 8 2 3 5165.46 4959.94 165.75 o 9 2 3 2525.02 2574.11 121.67 o 10 2 3 6250.14 6342.23 141.90 o 11 2 3 16052.95 15869.88 254.88 o 12 2 3 24.24 35.76 28.80 o 13 2 3 52.14 52.03 33.16 o 14 2 3 82.28 39.91 30.19 o 15 2 3 369.44 216.31 83.52 o 16 2 3 124.33 287.04 110.79 o 17 2 3 1923.93 1982.54 242.18 o 18 2 3 191.38 76.85 74.27 o 19 2 3 243.98 135.03 144.12 o 0 3 3 166594.27 155900.64 2434.64 o 1 3 3 6042.31 6091.70 164.04 o 2 3 3 22852.84 23298.10 317.22 o 3 3 3 780.49 753.70 49.89 o 4 3 3 62281.81 59477.78 734.80 o 5 3 3 18856.44 19117.97 304.46 o 6 3 3 7023.35 7058.71 209.63 o 7 3 3 2722.77 2495.60 114.75 o 8 3 3 523.96 543.65 41.32 o 9 3 3 5902.31 5777.11 134.15 o 10 3 3 5802.75 5695.88 145.44 o 11 3 3 4461.16 4071.66 114.88 o 12 3 3 1138.78 1121.21 73.85 o 13 3 3 2977.89 2828.34 162.81 o 14 3 3 5393.72 5791.31 242.22 o 15 3 3 3050.17 2976.43 221.51 o 16 3 3 67.45 84.81 102.41 o 17 3 3 2220.43 1962.30 242.93 o 18 3 3 531.37 754.13 186.69 o 19 3 3 616.53 675.71 225.46 o 1 4 3 51230.76 50847.98 977.85 o 2 4 3 232104.80 225367.89 1739.20 o 3 4 3 1874.36 2019.18 103.66 o 4 4 3 4739.86 4771.82 164.98 o 5 4 3 11440.52 11505.74 210.81 o 6 4 3 15340.43 15025.36 244.23 o 7 4 3 18229.29 17404.07 244.24 o 8 4 3 1756.56 1828.52 81.13 o 9 4 3 16635.50 15672.34 239.15 o 10 4 3 154.75 153.70 22.78 o 11 4 3 251.90 303.90 33.76 o 12 4 3 16571.34 16137.37 329.21 o 13 4 3 226.46 298.75 57.98 o 14 4 3 851.21 752.91 88.10 o 15 4 3 984.61 1061.94 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