#------------------------------------------------------------------------------ #$Date: 2023-08-30 04:48:26 +0300 (Wed, 30 Aug 2023) $ #$Revision: 285905 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/28/2022847.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022847 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.9774 _cell_length_b 18.3039 _cell_length_c 18.2877 _exptl_crystal_F_000 2200.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file qf3061Isup2.hkl _cod_data_source_block I _shelx_title ' _PLATINUM_DPPM_S_(R)DMANSBF6 OLEX2: imported from CIF' _shelx_refln_list_code 4 _shelx_f_calc_maximum 532.00 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 107332.44 104766.16 1587.33 o 4 0 0 27746.50 28188.41 789.12 o 6 0 0 139785.44 146293.61 3865.70 o 8 0 0 1547.97 1998.23 257.26 o 10 0 0 11910.02 12321.32 787.27 o 12 0 0 1766.45 1884.53 578.09 o 14 0 0 334.25 657.82 307.47 o 16 0 0 1217.23 1455.77 603.57 o 2 1 0 14123.63 14635.98 228.01 o 3 1 0 15026.96 14282.44 294.62 o 4 1 0 2920.37 3371.57 152.85 o 5 1 0 4409.02 4819.01 191.08 o 6 1 0 23093.54 22891.85 611.06 o 7 1 0 11229.13 11585.86 423.82 o 8 1 0 26978.81 27300.63 833.03 o 9 1 0 801.13 590.69 138.33 o 10 1 0 9.95 136.92 218.04 o 11 1 0 1376.47 1463.39 225.74 o 12 1 0 9279.05 8930.39 527.67 o 13 1 0 1508.95 1778.96 278.67 o 14 1 0 4575.99 4253.00 433.02 o 15 1 0 581.65 779.53 295.09 o 16 1 0 244.91 345.68 216.21 o 2 2 0 53375.35 57709.30 659.54 o 3 2 0 10569.04 11521.09 253.93 o 4 2 0 25218.23 25079.18 507.97 o 5 2 0 27615.10 27382.01 616.65 o 6 2 0 26329.86 26157.79 656.51 o 7 2 0 13217.76 13884.04 450.36 o 8 2 0 4430.18 4248.81 258.47 o 9 2 0 1877.56 1889.94 227.33 o 10 2 0 2798.41 2348.18 256.61 o 11 2 0 8836.50 8094.94 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5 23 712.93 590.98 408.63 o 2 5 23 821.48 474.99 626.25 o