#------------------------------------------------------------------------------ #$Date: 2023-09-09 04:36:17 +0300 (Sat, 09 Sep 2023) $ #$Revision: 286283 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/28/2022854.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022854 _cell_angle_alpha 90.000 _cell_angle_beta 91.317 _cell_angle_gamma 90.000 _cell_length_a 8.8072 _cell_length_b 17.7950 _cell_length_c 16.2222 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.7857 _cod_data_source_file hb8074Isup2.hkl _cod_data_source_block I _shelx_title ' shelxt_a.res in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.87 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -22 0 488.74 585.79 73.11 o 1 -22 0 31.21 12.24 23.85 o 2 -22 0 40.76 48.31 26.65 o 1 -21 0 38.33 23.87 20.82 o 2 -21 0 9.55 3.29 21.01 o 3 -21 0 14.92 -21.03 22.58 o 4 -21 0 34.95 56.92 41.61 o 0 -20 0 1177.88 1400.84 126.70 o 1 -20 0 277.51 347.93 35.56 o 2 -20 0 61.75 96.31 21.98 o 3 -20 0 117.30 136.45 25.26 o 4 -20 0 358.35 285.25 60.49 o 5 -20 0 2.94 39.10 29.94 o 1 -19 0 23.74 51.22 25.95 o 2 -19 0 52.99 45.23 21.86 o 3 -19 0 622.77 727.55 53.27 o 4 -19 0 28.61 49.92 21.25 o 5 -19 0 56.50 57.47 31.92 o 6 -19 0 23.32 35.02 62.37 o 0 -18 0 128.51 177.89 35.38 o 1 -18 0 25.02 60.96 17.60 o 2 -18 0 1443.59 1955.45 123.44 o 3 -18 0 28.96 41.24 18.20 o 4 -18 0 351.34 338.77 74.10 o 5 -18 0 72.16 43.32 27.10 o 6 -18 0 54.09 49.27 34.99 o 1 -17 0 388.61 522.36 42.00 o 2 -17 0 211.85 196.49 26.31 o 3 -17 0 241.59 288.05 29.94 o 4 -17 0 306.07 246.67 41.03 o 5 -17 0 114.51 75.99 28.33 o 6 -17 0 24.93 32.72 30.43 o 7 -17 0 11.78 34.32 43.80 o 0 -16 0 3742.87 4723.99 375.34 o 1 -16 0 39.66 18.43 12.55 o 2 -16 0 194.47 246.99 25.70 o 3 -16 0 72.59 90.94 22.64 o 4 -16 0 77.48 79.42 22.48 o 5 -16 0 728.87 562.98 54.02 o 6 -16 0 21.92 -5.74 24.61 o 7 -16 0 57.93 101.37 47.25 o 1 -15 0 2004.59 2647.59 149.42 o 2 -15 0 46.82 48.51 13.62 o 3 -15 0 670.72 766.99 64.72 o 4 -15 0 846.75 952.49 100.67 o 5 -15 0 32.67 48.22 21.73 o 6 -15 0 51.63 49.07 25.12 o 7 -15 0 183.98 240.87 42.76 o 8 -15 0 133.07 174.39 48.36 o 0 -14 0 16.52 11.15 13.58 o 1 -14 0 212.33 277.08 26.31 o 2 -14 0 142.60 156.30 19.54 o 3 -14 0 982.25 1052.10 75.28 o 4 -14 0 98.57 56.09 22.31 o 5 -14 0 1152.72 1164.29 84.05 o 6 -14 0 141.23 32.72 28.85 o 7 -14 0 254.05 219.84 53.53 o 8 -14 0 253.79 367.83 74.68 o 1 -13 0 1035.01 1178.44 69.39 o 2 -13 0 837.29 907.53 60.63 o 3 -13 0 1940.39 1754.14 149.89 o 4 -13 0 1154.79 1313.47 117.94 o 5 -13 0 230.69 232.69 32.56 o 6 -13 0 215.46 228.37 32.66 o 7 -13 0 220.29 305.31 44.37 o 8 -13 0 164.65 244.73 44.54 o 9 -13 0 88.45 75.87 59.96 o 0 -12 0 82.37 70.90 17.29 o 1 -12 0 159.65 186.28 19.16 o 2 -12 0 499.85 545.44 41.44 o 3 -12 0 1130.45 1100.91 75.75 o 4 -12 0 6.66 2.51 15.02 o 5 -12 0 71.24 82.43 22.69 o 6 -12 0 224.36 312.37 78.60 o 7 -12 0 248.28 267.92 41.37 o 8 -12 0 108.49 242.54 44.12 o 9 -12 0 120.29 209.88 58.40 o 1 -11 0 462.47 479.44 36.48 o 2 -11 0 54.40 92.67 16.02 o 3 -11 0 299.25 289.86 28.70 o 4 -11 0 18.15 -0.43 14.75 o 5 -11 0 205.94 214.81 31.97 o 6 -11 0 111.30 141.70 43.01 o 7 -11 0 388.62 458.07 49.58 o 8 -11 0 88.98 335.80 46.56 o 9 -11 0 145.02 181.63 48.35 o 0 -10 0 17.84 27.05 10.88 o 1 -10 0 150.22 155.98 16.02 o 2 -10 0 945.69 1124.82 80.21 o 3 -10 0 1517.90 1632.67 117.96 o 4 -10 0 363.38 436.75 36.10 o 5 -10 0 424.51 462.16 68.02 o 7 -10 0 153.39 247.37 35.60 o 8 -10 0 98.73 184.82 37.10 o 9 -10 0 42.62 86.03 38.50 o 10 -10 0 52.66 141.18 97.42 o 1 -9 0 35.20 49.05 9.80 o 2 -9 0 103.36 108.50 14.47 o 3 -9 0 41.95 41.59 12.02 o 4 -9 0 6.65 0.19 10.75 o 5 -9 0 574.16 556.16 46.60 o 6 -9 0 408.23 409.89 59.47 o 7 -9 0 82.98 132.07 27.62 o 8 -9 0 222.97 273.07 41.25 o 9 -9 0 44.97 109.91 34.35 o 10 -9 0 64.25 70.23 56.03 o 0 -8 0 92.06 139.75 19.72 o 1 -8 0 157.37 196.83 17.51 o 2 -8 0 810.59 933.00 84.45 o 3 -8 0 61.60 68.69 15.14 o 4 -8 0 61.64 70.24 14.71 o 5 -8 0 9.39 6.43 23.00 o 6 -8 0 40.89 17.01 15.71 o 7 -8 0 244.29 269.70 37.47 o 8 -8 0 19.27 37.95 28.28 o 9 -8 0 288.99 454.35 54.60 o 10 -8 0 23.90 63.42 53.48 o 1 -7 0 11.21 8.73 5.56 o 2 -7 0 0.80 5.61 6.51 o 3 -7 0 425.26 449.70 37.21 o 4 -7 0 602.09 539.58 38.79 o 5 -7 0 465.32 422.87 39.29 o 6 -7 0 18.15 23.83 16.46 o 7 -7 0 207.92 515.28 105.43 o 8 -7 0 127.50 234.39 44.02 o 9 -7 0 140.68 360.52 69.45 o 10 -7 0 78.29 43.51 75.44 o 0 -6 0 271.16 262.78 26.24 o 1 -6 0 471.80 544.38 36.65 o 2 -6 0 791.24 907.08 73.18 o 3 -6 0 1301.40 1276.43 125.89 o 4 -6 0 78.35 82.37 15.19 o 5 -6 0 367.62 334.16 27.80 o 6 -6 0 431.74 430.86 40.87 o 7 -6 0 26.36 23.45 20.36 o 8 -6 0 112.25 342.52 42.93 o 9 -6 0 195.14 252.69 38.95 o 10 -6 0 92.29 183.67 56.46 o 1 -5 0 3675.46 4472.34 300.98 o 3 -5 0 1424.75 1348.52 111.68 o 4 -5 0 168.03 160.53 23.57 o 5 -5 0 84.91 72.50 12.51 o 6 -5 0 733.46 689.70 48.87 o 7 -5 0 106.94 144.46 26.24 o 8 -5 0 245.87 774.83 69.27 o 9 -5 0 125.05 216.15 39.32 o 10 -5 0 159.39 155.37 47.36 o 0 -4 0 205.81 275.43 23.76 o 1 -4 0 6233.62 7446.45 564.73 o 2 -4 0 7338.98 7487.74 1110.46 o 3 -4 0 1675.29 1382.55 113.95 o 4 -4 0 161.88 167.39 18.01 o 5 -4 0 3786.40 2850.18 179.58 o 6 -4 0 526.46 1102.77 130.82 o 7 -4 0 332.25 388.60 34.25 o 8 -4 0 220.52 299.39 30.52 o 9 -4 0 131.04 153.89 39.72 o 10 -4 0 35.42 54.21 32.27 o 11 -4 0 55.59 -22.54 95.08 o 1 -3 0 70.13 98.76 11.40 o 2 -3 0 340.76 275.77 34.41 o 3 -3 0 2249.09 2013.79 165.71 o 4 -3 0 612.91 446.63 33.63 o 5 -3 0 281.59 260.78 27.52 o 6 -3 0 680.92 784.63 67.11 o 7 -3 0 158.65 324.17 39.63 o 8 -3 0 171.79 235.99 27.78 o 9 -3 0 296.29 522.13 50.31 o 10 -3 0 78.95 107.18 37.71 o 11 -3 0 129.68 43.20 95.17 o 1 -2 0 2286.59 2505.39 198.88 o 2 -2 0 424.92 392.15 35.11 o 3 -2 0 6225.43 4431.66 461.70 o 4 -2 0 2442.38 1931.05 118.59 o 5 -2 0 1521.89 1221.61 81.67 o 6 -2 0 1103.35 1141.84 71.17 o 7 -2 0 118.38 191.43 23.00 o 8 -2 0 111.09 273.51 34.36 o 9 -2 0 227.66 319.06 35.34 o 10 -2 0 112.36 115.41 27.23 o 11 -2 0 48.47 -75.96 89.22 o 1 -1 0 14176.64 9038.40 1351.83 o 2 -1 0 12908.40 8324.37 571.94 o 3 -1 0 2194.41 1473.93 109.12 o 4 -1 0 1454.69 1152.68 75.53 o 5 -1 0 1705.96 1504.21 95.01 o 6 -1 0 139.37 122.28 24.79 o 7 -1 0 69.26 80.08 25.00 o 8 -1 0 151.63 319.49 34.30 o 9 -1 0 354.16 526.37 51.37 o 10 -1 0 203.78 362.25 83.45 o 11 -1 0 26.56 25.34 81.66 o 1 0 0 29.15 17.27 10.13 o 2 0 0 4082.94 4485.20 430.30 o 3 0 0 103.77 91.87 11.86 o 4 0 0 125.12 171.68 19.85 o 5 0 0 484.52 450.63 37.64 o 6 0 0 234.49 397.86 37.44 o 7 0 0 4.40 0.12 12.81 o 8 0 0 863.63 1190.56 76.73 o 9 0 0 61.50 98.28 27.67 o 10 0 0 334.68 330.36 66.94 o 11 0 0 32.62 -41.34 71.20 o 2 1 0 12908.12 8792.29 660.74 o 3 1 0 2193.76 1702.45 110.53 o 4 1 0 1454.90 1197.36 84.73 o 5 1 0 1707.12 1388.73 123.46 o 6 1 0 139.22 209.71 40.93 o 7 1 0 69.30 60.35 18.51 o 8 1 0 151.41 360.71 38.75 o 9 1 0 354.00 673.04 120.28 o 10 1 0 203.89 294.49 72.18 o 11 1 0 26.49 -26.15 41.48 o 1 2 0 2286.65 2599.19 198.26 o 2 2 0 425.27 393.62 34.48 o 3 2 0 6224.94 5020.87 376.13 o 4 2 0 2442.19 1889.39 118.69 o 5 2 0 1520.90 1239.52 91.43 o 6 2 0 1103.06 1180.48 77.98 o 7 2 0 118.60 170.82 40.25 o 8 2 0 111.23 199.82 29.77 o 9 2 0 227.57 316.40 56.96 o 10 2 0 112.20 103.54 42.18 o 11 2 0 48.20 4.15 107.00 o 1 3 0 70.10 106.84 15.10 o 2 3 0 341.04 313.12 27.18 o 3 3 0 2248.22 2106.55 164.21 o 4 3 0 612.59 473.69 38.13 o 5 3 0 281.93 281.41 32.23 o 6 3 0 681.56 642.63 69.44 o 7 3 0 158.64 349.58 39.04 o 8 3 0 171.20 214.26 35.52 o 9 3 0 296.18 471.64 85.38 o 10 3 0 78.84 37.02 37.29 o 11 3 0 129.55 303.87 114.70 o 0 4 0 205.76 218.39 41.13 o 1 4 0 6234.35 6664.99 976.82 o 2 4 0 7339.08 8025.22 731.67 o 3 4 0 1675.52 1373.37 134.31 o 4 4 0 162.01 160.73 20.79 o 5 4 0 3786.54 2903.05 200.86 o 6 4 0 525.98 1286.14 106.21 o 7 4 0 332.31 375.94 39.64 o 8 4 0 220.67 262.69 47.56 o 9 4 0 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810.67 1062.79 73.34 o 3 8 0 61.57 61.06 14.06 o 4 8 0 61.61 43.53 13.70 o 5 8 0 9.55 -0.95 6.69 o 6 8 0 40.88 53.47 17.51 o 7 8 0 244.26 235.30 31.23 o 8 8 0 19.21 4.54 16.79 o 9 8 0 289.11 359.64 95.14 o 10 8 0 23.76 -30.19 39.79 o 1 9 0 35.25 40.67 12.04 o 2 9 0 103.43 116.40 17.85 o 3 9 0 41.84 26.43 12.08 o 4 9 0 6.68 9.91 13.15 o 5 9 0 574.00 585.74 74.84 o 6 9 0 408.84 347.82 39.85 o 7 9 0 83.00 110.61 22.89 o 8 9 0 223.42 176.67 27.85 o 9 9 0 44.93 73.36 37.19 o 10 9 0 64.01 113.79 44.00 o 0 10 0 17.72 35.11 19.71 o 1 10 0 150.35 182.64 33.61 o 2 10 0 945.75 1020.56 78.73 o 3 10 0 1517.88 1621.76 135.00 o 4 10 0 363.08 335.65 51.99 o 5 10 0 424.41 332.69 58.49 o 6 10 0 373.73 321.13 86.74 o 7 10 0 153.64 137.19 47.41 o 8 10 0 98.96 53.86 37.79 o 9 10 0 42.61 37.03 23.21 o 10 10 0 52.55 142.15 125.80 o 1 11 0 462.72 504.73 52.66 o 2 11 0 54.51 66.71 16.56 o 3 11 0 298.88 298.68 44.56 o 4 11 0 18.22 39.36 16.41 o 5 11 0 206.14 189.11 44.88 o 6 11 0 111.50 123.95 47.33 o 7 11 0 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90.89 o 5 15 0 32.61 32.12 32.83 o 6 15 0 51.71 48.60 30.93 o 7 15 0 183.97 189.78 56.19 o 8 15 0 132.90 79.34 67.29 o 0 16 0 3742.96 4509.30 652.77 o 1 16 0 39.68 21.99 24.04 o 2 16 0 194.28 237.49 41.74 o 3 16 0 72.55 95.66 26.12 o 4 16 0 77.66 57.91 23.87 o 5 16 0 728.55 393.71 52.04 o 6 16 0 21.95 -0.41 32.80 o 7 16 0 58.13 102.77 100.59 o 1 17 0 388.30 492.63 82.42 o 2 17 0 211.70 159.55 41.95 o 3 17 0 241.22 230.03 57.39 o 4 17 0 306.20 156.01 33.76 o 5 17 0 114.60 80.91 27.81 o 6 17 0 25.06 -12.29 31.71 o 7 17 0 11.80 21.86 44.92 o 0 18 0 128.89 213.92 76.76 o 1 18 0 25.26 40.00 32.49 o 2 18 0 1443.89 1648.54 196.36 o 3 18 0 29.05 11.32 25.89 o 4 18 0 351.40 278.03 40.86 o 5 18 0 72.28 35.69 35.01 o 6 18 0 53.93 39.87 37.51 o 1 19 0 23.79 25.50 26.61 o 2 19 0 52.96 66.08 37.91 o 3 19 0 622.88 675.58 85.95 o 4 19 0 28.63 6.48 31.53 o 5 19 0 56.49 -4.25 32.58 o 0 20 0 1177.57 1480.73 226.48 o 1 20 0 277.60 220.11 89.32 o 2 20 0 61.69 74.32 73.92 o 3 20 0 117.16 105.46 39.91 o 4 20 0 358.21 309.78 58.24 o 1 21 0 38.31 37.83 37.02 o 2 21 0 9.54 -4.91 33.03 o 3 21 0 14.95 -13.25 42.68 o 0 22 0 488.70 528.68 137.85 o 1 22 0 31.26 13.05 34.67 o 2 22 0 40.72 7.00 38.74 o -2 -22 1 53.93 82.49 29.49 o -1 -22 1 28.67 22.67 23.01 o 0 -22 1 62.66 152.36 29.91 o 1 -22 1 41.95 -7.32 25.23 o 2 -22 1 105.50 107.76 32.20 o -4 -21 1 57.69 29.61 38.81 o -3 -21 1 240.97 129.27 28.42 o -2 -21 1 91.68 69.22 24.23 o -1 -21 1 20.33 12.78 19.96 o 0 -21 1 24.53 51.89 20.01 o 1 -21 1 11.50 5.08 20.60 o 2 -21 1 129.55 124.68 26.85 o 3 -21 1 188.54 156.46 29.79 o 4 -21 1 90.00 -0.52 80.89 o -5 -20 1 253.94 166.44 36.24 o -4 -20 1 11.73 8.04 21.56 o -3 -20 1 71.98 70.92 22.85 o -2 -20 1 143.18 177.57 27.90 o -1 -20 1 129.62 119.93 22.89 o 0 -20 1 114.03 188.52 31.74 o 1 -20 1 65.42 78.41 26.03 o 2 -20 1 168.37 232.46 35.51 o 3 -20 1 27.60 28.50 20.87 o 4 -20 1 9.80 -18.12 23.14 o 5 -20 1 291.53 241.27 128.59 o -6 -19 1 33.65 -10.51 54.85 o -5 -19 1 83.19 78.02 31.74 o -4 -19 1 12.72 -10.28 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