#------------------------------------------------------------------------------ #$Date: 2023-09-15 04:45:14 +0300 (Fri, 15 Sep 2023) $ #$Revision: 286351 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/28/2022861.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022861 loop_ _publ_author_name 'Meurer, Florian' 'Dimova, Tanya' 'Bodensteiner, Michael' 'Kolev, Iliyan' _publ_section_title ; 2,6-Dibromo-3,4,5-trimethoxybenzoic acid ; _journal_coeditor_code JY2033 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989023007831 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C10 H10 Br2 O5' _chemical_formula_moiety 'C10 H10 Br2 O5' _chemical_formula_sum 'C10 H10 Br2 O5' _chemical_formula_weight 369.995 _chemical_name_common ; 2,6-Dibromo-3,4,5-trimethoxybenzoic acid ; _chemical_name_systematic ; 2,6-Dibromo-3,4,5-trimethoxybenzoic acid ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.5-alpha (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _cell_angle_alpha 90 _cell_angle_beta 107.009(8) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.4047(9) _cell_length_b 7.1107(3) _cell_length_c 16.8997(13) _cell_measurement_reflns_used 1911 _cell_measurement_temperature 100.00(12) _cell_measurement_theta_max 28.8050 _cell_measurement_theta_min 3.1290 _cell_volume 1310.54(16) _computing_cell_refinement ; CrysAlisPro 1.171.43.36a (Rigaku OD, 2022) ; _computing_data_collection ; CrysAlisPro 1.171.43.36a (Rigaku OD, 2022) ; _computing_data_reduction ; CrysAlisPro 1.171.43.36a (Rigaku OD, 2022) ; _computing_molecular_graphics ; Olex2 1.5-alpha (Dolomanov et al., 2009) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; olex2.refine 1.5-alpha (Bourhis et al., 2015), NoSpherA2 (Kleemiss et al., 2021) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2015) ; _diffrn_ambient_temperature 100.00(12) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2548 _diffrn_measured_fraction_theta_full 0.9966 _diffrn_measured_fraction_theta_max 0.9966 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dualflex, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0835 _diffrn_reflns_av_unetI/netI 0.1336 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 18764 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 28.28 _diffrn_reflns_theta_min 3.13 _diffrn_source 'micro-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 6.190 _exptl_absorpt_correction_T_max 0.855 _exptl_absorpt_correction_T_min 0.749 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2022) ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_density_diffrn 1.875 _exptl_crystal_description block _exptl_crystal_F_000 718.856 _exptl_crystal_size_max 0.083 _exptl_crystal_size_mid 0.058 _exptl_crystal_size_min 0.032 _refine_diff_density_max 1.2481 _refine_diff_density_min -1.4830 _refine_ls_goodness_of_fit_ref 1.0578 _refine_ls_hydrogen_treatment refU _refine_ls_matrix_type full _refine_ls_number_constraints 4 _refine_ls_number_parameters 218 _refine_ls_number_reflns 3245 _refine_ls_number_restraints 63 _refine_ls_restrained_S_all 1.0470 _refine_ls_R_factor_all 0.0875 _refine_ls_R_factor_gt 0.0528 _refine_ls_shift/su_max 0.0002 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0395P)^2^+3.4625P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1066 _refine_ls_wR_factor_ref 0.1231 _reflns_number_gt 2254 _reflns_number_total 3245 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL br2ome3coohph_mo_a.res in P2(1)/n REM Old TITL br2ome3coohph_mo_a.res in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.193, Rweak 0.005, Alpha 0.033 REM 0.619 for 228 systematic absences, Orientation as input REM Formula found by SHELXT: C10 Br2 O5 CELL 0.71073 11.4047 7.1107 16.8997 90 107.009 90 ZERR 4 0.0009 0.0003 0.0013 0 0.008 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Br O UNIT 40 40 8 20 RIGU 0.01 0.01 O1 H003 ISOR 0.05 0.05 H003 RIGU C10 H00d H00e H00f RIGU C9 H00g H00h H00i RIGU C8 H00a H00b H00c L.S. 10 PLAN 20 SIZE 0.032 0.058 0.083 TEMP -173 CONF BOND FMAP 2 list 4 MORE -1 BOND $H ACTA SHEL 99 0.75 WGHT 0.039521 3.462542 FVAR 0.337472 Br1 3 0.86638 0.67372 0.45104 11.00000 0.03075 0.02070 0.03820 = -0.00465 -0.00914 0.00335 Br2 3 0.43161 0.68854 0.17096 11.00000 0.03818 0.01809 0.03123 = -0.00445 -0.00975 0.00315 O1 4 0.65580 0.98305 0.30322 11.00000 0.04334 0.02078 0.03831 = 0.00031 0.02415 -0.00142 AFIX 147 0.983 H003 2 0.69235 1.08099 0.27683 11.00000 0.07694 0.02538 0.04068 = -0.00566 0.03285 -0.02426 AFIX 0 O2 4 0.75699 0.79338 0.24098 11.00000 0.06107 0.01761 0.05571 = 0.00007 0.04721 0.00060 O3 4 0.72455 0.34803 0.50037 11.00000 0.08342 0.02885 0.03097 = 0.00715 0.02099 0.01037 O4 4 0.50370 0.19131 0.41312 11.00000 0.06811 0.02058 0.06245 = 0.00283 0.04812 0.00388 O5 4 0.36432 0.35756 0.26691 11.00000 0.02735 0.02592 0.08946 = -0.00728 0.01310 -0.00411 C4 1 0.63570 0.65858 0.31981 11.00000 0.02289 0.01524 0.02487 = -0.00071 0.01181 -0.00346 C5 1 0.70542 0.57732 0.39319 11.00000 0.03532 0.02207 0.02792 = 0.00006 0.01244 0.00391 C3 1 0.52345 0.58215 0.27727 11.00000 0.02581 0.01939 0.03979 = -0.00239 0.00922 -0.00205 C6 1 0.66060 0.42040 0.42617 11.00000 0.04923 0.02029 0.02825 = 0.00422 0.01771 0.00201 C2 1 0.47707 0.42389 0.30793 11.00000 0.02566 0.02355 0.04990 = -0.00094 0.01642 -0.00545 C7 1 0.68838 0.81844 0.28380 11.00000 0.03648 0.01439 0.03477 = -0.00121 0.02195 0.00260 C1 1 0.54512 0.34417 0.38272 11.00000 0.04332 0.01484 0.04022 = 0.00284 0.02555 -0.00053 C8 1 0.79109 0.18147 0.49369 11.00000 0.06807 0.02837 0.03926 = 0.00850 0.00637 0.00895 AFIX 137 1.077 H00a 2 0.85194 0.21046 0.45702 11.00000 0.06936 0.05161 0.04141 = 0.01200 0.00638 0.00490 H00b 2 0.84373 0.13614 0.55452 11.00000 0.07249 0.05029 0.04170 = 0.01388 0.00488 0.00619 H00c 2 0.72774 0.07225 0.46450 11.00000 0.06610 0.03101 0.04047 = 0.00780 0.00764 0.01099 AFIX 0 C10 1 0.36183 0.17525 0.23137 11.00000 0.05039 0.02786 0.07676 = -0.00881 0.01567 -0.00547 AFIX 137 1.077 H00d 2 0.26961 0.14238 0.19505 11.00000 0.05405 0.05897 0.08161 = -0.00292 0.01490 -0.01164 H00e 2 0.42139 0.17300 0.19231 11.00000 0.05342 0.04957 0.07816 = -0.00990 0.01639 -0.00834 H00f 2 0.39260 0.07264 0.27991 11.00000 0.06338 0.03599 0.07903 = -0.00743 0.01751 -0.00326 AFIX 0 C9 1 0.43302 0.23410 0.46789 11.00000 0.07564 0.03608 0.08111 = 0.01006 0.06308 0.00999 AFIX 137 1.077 H00g 2 0.35860 0.32620 0.43727 11.00000 0.08248 0.03833 0.08700 = 0.00816 0.05925 0.01199 H00h 2 0.39666 0.10603 0.48535 11.00000 0.08050 0.03339 0.07315 = 0.00257 0.06965 0.01239 H00i 2 0.49043 0.30237 0.52239 11.00000 0.09708 0.04090 0.09222 = 0.00746 0.05087 0.00819 AFIX 0 HKLF 4 END Q1 1 0.4 0.625 0.2 11 0.05 1.25 Q2 1 0.55 0.875 0.283333 11 0.05 1.09 Q3 1 0.475 0.625 0.15 11 0.05 0.99 Q4 1 0.825 0.708333 0.45 11 0.05 0.97 Q5 1 0.575 -0.083333 0.4 11 0.05 0.91 Q6 1 0.8 0.375 0.366667 11 0.05 0.91 Q7 1 0.4 0.708333 0.15 11 0.05 0.89 Q8 1 0.75 -0.166667 0.533333 11 0.05 0.86 Q9 1 0.525 0.25 0.233333 11 0.05 0.84 Q10 1 0.325 0.458333 0.133333 11 0.05 0.84 Q11 1 0.45 0.458333 0.233333 11 0.05 0.82 Q12 1 0.2 0.083333 0.266667 11 0.05 0.82 Q13 1 0.85 0 0.583333 11 0.05 0.82 Q14 1 0.8 0 0.416667 11 0.05 0.78 Q15 1 0.425 0.666667 0.3 11 0.05 0.77 Q16 1 0.2 0.291667 0.366667 11 0.05 0.75 Q17 1 0.75 0.875 0.466667 11 0.05 0.75 Q18 1 0.275 0.083333 0.35 11 0.05 0.73 Q19 1 0.375 -0.125 0.266667 11 0.05 0.73 Q20 1 0.975 0.666667 0.583333 11 0.05 0.72 REM The information below was added by Olex2. REM REM R1 = 0.0528 for 2254 Fo > 4sig(Fo) and 0.0875 for all 3245 data REM 218 parameters refined using 63 restraints REM Highest difference peak 1.2481, deepest hole -1.4830 REM Mean Shift 0.0000, Max Shift 0.0002. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0875 REM R1_gt = 0.0528 REM wR_ref = 0.1231 REM GOOF = 1.0578 REM Shift_max = 0.0002 REM Shift_mean = 0.0000 REM Reflections_all = 3245 REM Reflections_gt = 2254 REM Parameters = 218 REM Hole = -1.4830 REM Peak = 1.2481 REM Flack = n/a ; _cod_data_source_file jy2033sup1.cif _cod_data_source_block I _cod_database_code 2022861 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x+1/2,y+1/2,-z+1/2 3 -x,-y,-z 4 x-1/2,-y-1/2,z-1/2 loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy Br Br1 0.86638(5) 0.67372(7) 0.45104(4) 0.03398(18) Uani 1.000000 Br Br2 0.43161(5) 0.68854(7) 0.17096(3) 0.03341(18) Uani 1.000000 O O1 0.6558(4) 0.9831(5) 0.3032(2) 0.0315(9) Uani 1.000000 H H1 0.692(6) 1.0810(6) 0.277(4) 0.04(2) Uani 1.000000 O O2 0.7570(4) 0.7934(5) 0.2410(3) 0.0384(11) Uani 1.000000 O O3 0.7246(5) 0.3480(5) 0.5004(3) 0.0468(12) Uani 1.000000 O O4 0.5037(4) 0.1913(5) 0.4131(3) 0.0442(12) Uani 1.000000 O O5 0.3643(4) 0.3576(5) 0.2669(3) 0.0484(13) Uani 1.000000 C C4 0.6357(4) 0.6586(6) 0.3198(3) 0.0200(10) Uani 1.000000 C C5 0.7054(5) 0.5773(7) 0.3932(3) 0.0278(12) Uani 1.000000 C C3 0.5234(5) 0.5822(7) 0.2773(4) 0.0284(12) Uani 1.000000 C C6 0.6606(6) 0.4204(7) 0.4262(3) 0.0312(13) Uani 1.000000 C C2 0.4771(5) 0.4239(7) 0.3079(4) 0.0319(13) Uani 1.000000 C C7 0.6884(5) 0.8184(7) 0.2838(3) 0.0261(12) Uani 1.000000 C C1 0.5451(6) 0.3442(7) 0.3827(4) 0.0300(13) Uani 1.000000 C C8 0.7911(7) 0.1815(8) 0.4937(4) 0.0472(17) Uani 1.000000 H H00a 0.852(3) 0.2105(16) 0.457(2) 0.056(11) Uani 1.000000 H H00b 0.844(3) 0.136(3) 0.5545(5) 0.057(10) Uani 1.000000 H H00c 0.7277(7) 0.0722(18) 0.465(2) 0.048(10) Uani 1.000000 C C10 0.3618(7) 0.1753(8) 0.2314(5) 0.0523(19) Uani 1.000000 H H00d 0.2696(10) 0.142(3) 0.195(2) 0.066(11) Uani 1.000000 H H00e 0.421(3) 0.173(2) 0.192(2) 0.061(11) Uani 1.000000 H H00f 0.393(4) 0.0726(11) 0.2799(5) 0.060(11) Uani 1.000000 C C9 0.4330(7) 0.2341(9) 0.4679(5) 0.056(2) Uani 1.000000 H H00g 0.359(2) 0.326(5) 0.4373(10) 0.062(10) Uani 1.000000 H H00h 0.397(3) 0.1060(11) 0.485(2) 0.052(10) Uani 1.000000 H H00i 0.4904(11) 0.302(5) 0.5224(12) 0.072(11) Uani 1.000000 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Br1 0.0308(3) 0.0207(3) 0.0382(4) 0.0033(2) -0.0091(2) -0.0047(2) Br2 0.0382(4) 0.0181(3) 0.0312(3) 0.0032(2) -0.0097(2) -0.0045(2) O1 0.043(2) 0.0208(19) 0.038(2) -0.0014(17) 0.0242(19) 0.0003(16) H1 0.08(4) 0.03(3) 0.04(3) -0.024(13) 0.033(17) -0.006(13) O2 0.061(3) 0.0176(19) 0.056(3) 0.0006(18) 0.047(2) 0.0001(18) O3 0.083(4) 0.029(2) 0.031(2) 0.010(2) 0.021(2) 0.0072(18) O4 0.068(3) 0.021(2) 0.062(3) 0.0039(19) 0.048(3) 0.0028(19) O5 0.027(2) 0.026(2) 0.089(4) -0.0041(17) 0.013(2) -0.007(2) C4 0.023(3) 0.015(2) 0.025(3) -0.0035(19) 0.012(2) -0.0007(18) C5 0.035(3) 0.022(3) 0.028(3) 0.004(2) 0.012(2) 0.000(2) C3 0.026(3) 0.019(3) 0.040(3) -0.002(2) 0.009(2) -0.002(2) C6 0.049(4) 0.020(3) 0.028(3) 0.002(2) 0.018(3) 0.004(2) C2 0.026(3) 0.024(3) 0.050(4) -0.005(2) 0.016(3) -0.001(2) C7 0.036(3) 0.014(2) 0.035(3) 0.003(2) 0.022(2) -0.001(2) C1 0.043(3) 0.015(2) 0.040(3) -0.001(2) 0.026(3) 0.003(2) C8 0.068(5) 0.028(3) 0.039(4) 0.009(3) 0.006(3) 0.008(3) H00a 0.069(13) 0.05(3) 0.041(11) 0.005(8) 0.006(6) 0.012(7) H00b 0.072(15) 0.05(2) 0.042(7) 0.006(8) 0.005(5) 0.014(5) H00c 0.066(17) 0.031(15) 0.040(12) 0.011(8) 0.008(6) 0.008(6) C10 0.050(5) 0.028(3) 0.077(6) -0.005(3) 0.016(4) -0.009(3) H00d 0.054(7) 0.06(3) 0.082(14) -0.012(5) 0.015(5) -0.003(8) H00e 0.053(10) 0.05(3) 0.078(13) -0.008(7) 0.016(6) -0.010(8) H00f 0.063(13) 0.036(19) 0.079(14) -0.003(7) 0.018(6) -0.007(8) C9 0.076(6) 0.036(4) 0.081(6) 0.010(3) 0.063(5) 0.010(4) H00g 0.082(12) 0.038(11) 0.09(2) 0.012(5) 0.059(8) 0.008(6) H00h 0.081(17) 0.033(9) 0.073(19) 0.012(6) 0.070(8) 0.003(6) H00i 0.10(2) 0.041(12) 0.092(12) 0.008(6) 0.051(8) 0.007(6) loop_ _atom_type_symbol _atom_type_scat_dispersion_source _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Br 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' -0.28346 2.55990 'NoSpherA2: Chem.Sci. 2021, DOI:10.1039/D0SC05526C' C 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' 0.00347 0.00161 'NoSpherA2: Chem.Sci. 2021, DOI:10.1039/D0SC05526C' H 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' 0.00000 0.00000 'NoSpherA2: Chem.Sci. 2021, DOI:10.1039/D0SC05526C' O 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' 0.01158 0.00611 'NoSpherA2: Chem.Sci. 2021, DOI:10.1039/D0SC05526C' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l 0 0 -3 0 0 -3 0 0 -4 0 0 -6 0 0 -7 0 0 -8 0 0 -9 0 0 -10 0 0 -11 0 0 -12 0 0 -13 0 0 -14 0 0 -15 0 0 -16 0 0 -17 0 0 -18 0 0 19 0 0 -19 0 0 20 0 0 -20 0 0 21 0 0 -21 0 0 22 0 0 -22 0 0 23 0 0 -23 0 0 24 0 0 -24 0 0 25 0 0 -25 0 0 26 0 0 -26 0 1 0 0 -1 0 0 1 0 0 1 1 0 -1 -1 0 1 -1 0 -1 1 0 1 -2 0 -1 2 0 1 2 0 -1 -2 0 1 -2 0 1 3 0 -1 3 0 1 -3 0 -1 -3 0 -1 4 0 1 4 0 -1 -4 0 1 -4 0 -1 -4 0 1 -4 0 1 -5 0 -1 -5 0 -1 -6 0 1 -6 0 -1 -7 0 1 -7 0 -1 -8 0 1 -8 0 1 -9 0 -1 -9 0 1 -10 0 -1 -10 0 -1 -11 0 1 -11 0 1 -12 0 -1 -12 0 -1 -13 0 1 -13 0 -1 -14 0 1 -14 0 1 -15 0 -1 -15 0 1 -16 0 -1 -16 0 1 -17 0 -1 -17 0 1 -18 0 -1 -18 0 1 -19 0 -1 -19 0 1 19 0 -1 19 0 1 -20 0 -1 -20 0 1 20 0 -1 20 0 -1 -21 0 1 -21 0 1 21 0 -1 21 0 -1 22 0 1 22 0 -1 -22 0 1 -22 0 -1 23 0 1 23 0 -1 -23 0 1 -23 0 1 24 0 -1 24 0 -1 -24 0 1 -24 0 -1 25 0 1 25 0 -1 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4 -8 16 -4 -8 16 -4 -7 16 4 -7 16 -4 -7 16 4 -6 16 -4 -6 16 -4 -5 16 4 -5 16 -4 -5 16 4 -4 16 -4 -4 16 -4 -4 16 4 -3 16 -4 -3 16 -4 -3 16 4 -2 16 -4 -2 16 -4 -2 16 4 -1 16 -4 -1 16 -4 -1 16 4 0 16 -4 0 16 -4 0 16 4 1 16 -4 1 16 -4 1 16 4 2 16 -4 2 16 -4 2 16 4 3 16 -4 3 16 -4 3 16 -4 4 16 4 4 16 -4 4 16 4 5 16 -4 5 16 4 5 16 -4 5 16 -4 5 16 -4 6 16 -5 -18 16 5 -18 -16 5 18 -16 -5 18 16 -5 -17 16 5 -17 16 5 -16 16 -5 -16 16 5 -15 16 -5 -15 16 5 -14 16 -5 -14 16 5 -13 16 -5 -13 16 -5 -12 16 5 -12 16 5 -11 16 -5 -11 16 5 -10 16 -5 -10 16 5 -9 16 -5 -9 16 5 -8 16 -5 -8 16 -5 -7 16 5 -7 16 -5 -7 16 -5 -6 16 5 -6 16 -5 -6 16 5 -5 16 -5 -5 16 -5 -5 16 5 -4 16 -5 -4 16 -5 -4 16 5 -3 16 -5 -3 16 -5 -3 16 5 -2 16 -5 -2 16 -5 -1 16 5 -1 16 -5 -1 16 -5 0 16 5 0 16 -5 0 16 -5 1 16 5 1 16 -5 1 16 -5 2 16 5 2 16 -5 2 16 -5 3 16 5 3 16 -5 3 16 -5 4 16 5 4 16 5 4 16 -5 4 16 -6 -7 16 -6 -6 16 -6 -5 16 -6 -4 16 -6 -3 16 -6 -2 16 -6 -1 16 -6 0 -17 0 19 17 0 -19 -17 0 18 17 0 -18 -17 0 17 17 0 -17 -17 0 16 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-5 -15 17 5 -14 17 -5 -14 17 5 -13 17 -5 -13 17 5 -12 17 -5 -12 17 5 -11 17 -5 -11 17 5 -10 17 -5 -10 17 -5 -9 17 5 -9 17 5 -8 17 -5 -8 17 5 -7 17 -5 -7 17 5 -6 17 -5 -6 17 -5 -5 17 5 -5 17 -5 -5 17 5 -4 17 -5 -4 17 -5 -4 17 5 -3 17 -5 -3 17 -5 -3 17 -5 -2 17 -5 -2 17 5 -2 17 -5 -1 17 5 -1 17 -5 -1 17 -5 0 17 5 0 17 -5 0 18 0 -16 18 0 -15 18 0 -14 18 0 -13 18 0 -12 18 0 -11 18 0 -10 18 0 -9 18 0 -8 18 0 -7 18 0 -6 18 0 -5 18 0 -4 18 0 -3 18 0 -2 18 0 -1 18 0 0 18 1 -16 18 -1 -16 18 1 -15 18 -1 -15 18 1 -14 18 -1 -14 18 1 -13 18 -1 -13 18 1 -12 18 -1 -12 18 1 -11 18 -1 -11 18 1 -10 18 -1 -10 18 1 -9 18 -1 -9 18 1 -8 18 -1 -8 18 1 -7 18 -1 -7 18 1 -6 18 -1 -6 18 -1 -5 18 1 -5 18 1 -4 18 -1 -4 18 1 -3 18 -1 -3 18 1 -2 18 -1 -2 18 1 -1 18 -1 -1 18 1 0 18 -1 0 18 2 -15 18 -2 -15 18 2 -14 18 -2 -14 18 2 -13 18 -2 -13 18 2 -12 18 -2 -12 18 2 -11 18 -2 -11 18 2 -10 18 -2 -10 18 2 -9 18 -2 -9 18 2 -8 18 -2 -8 18 2 -7 18 -2 -7 18 2 -6 18 -2 -6 18 2 -5 18 -2 -5 18 2 -4 18 -2 -4 18 2 -3 18 -2 -3 18 2 -2 18 -2 -2 18 2 -1 18 -2 -1 18 -2 0 18 3 -14 18 -3 -14 18 3 -13 18 -3 -13 18 3 -12 18 -3 -12 18 3 -11 18 -3 -11 18 3 -10 18 -3 -10 18 3 -9 18 -3 -9 18 3 -8 18 -3 -8 18 3 -7 18 -3 -7 18 3 -6 18 -3 -6 18 3 -5 18 -3 -5 18 3 -4 18 -3 -4 18 -3 -3 18 3 -3 18 3 -2 18 -3 -2 18 4 -12 18 -4 -12 18 4 -11 18 -4 -11 18 -4 -10 18 4 -10 18 4 -9 18 -4 -9 18 4 -8 18 -4 -8 18 4 -7 18 -4 -7 18 4 -6 18 -4 -6 18 4 -5 18 -4 -5 18 4 -4 18 -4 -4 19 0 -9 19 0 -8 19 0 -7 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 1 0 -2 0.0212 2 2 1 0.0573 0 -1 2 0.0272 -2 -1 -2 0.0085 0 1 -2 0.0289 -2 1 -1 0.0057 1 -2 1 0.0408 1 0 0 0.0487 -13 5 10 0.0114 -12 1 20 0.0097 -8 -2 23 0.0097 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C1 C2 C3 119.3(5) C1 C2 O5 121.0(5) C1 C6 C5 119.2(5) C1 C6 O3 120.2(5) C10 O5 C2 115.5(5) C2 C1 C6 120.1(5) C2 C1 O4 120.6(6) C2 C3 C4 120.9(5) C2 C3 Br2 119.5(4) C3 C2 O5 119.6(5) C3 C4 C5 120.1(5) C4 C7 O2 122.1(4) C4 C7 O1 113.8(4) C4 C3 Br2 119.5(4) C4 C5 Br1 121.0(4) C5 C6 O3 120.5(6) C6 C1 O4 119.3(5) C6 C5 C4 120.3(5) C6 C5 Br1 118.8(4) C7 C4 C3 120.5(5) C7 C4 C5 119.1(5) C7 O1 H1 109.5 C8 O3 C6 113.4(5) C9 O4 C1 113.8(4) H00a C8 O3 109.5 H00b C8 H00a 109.5 H00b C8 O3 109.5 H00c C8 H00b 109.5 H00c C8 H00a 109.5 H00c C8 O3 109.5 H00d C10 O5 109.5 H00e C10 H00d 109.5 H00e C10 O5 109.5 H00f C10 H00e 109.5 H00f C10 H00d 109.5 H00f C10 O5 109.5 H00g C9 O4 109.5 H00h C9 H00g 109.5 H00h C9 O4 109.5 H00i C9 H00h 109.5 H00i C9 H00g 109.5 H00i C9 O4 109.5 O2 C7 O1 124.0(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Br1 C5 1.935(6) Br2 C3 1.948(6) O1 C7 1.299(6) O2 C7 1.224(6) O3 C6 1.354(7) O3 C8 1.429(7) O4 C1 1.346(6) O4 C9 1.427(7) O5 C2 1.355(7) O5 C10 1.425(7) C4 C5 1.388(7) C4 C3 1.383(7) C4 C7 1.496(7) C5 C6 1.408(7) C3 C2 1.405(7) C6 C1 1.415(8) C2 C1 1.395(8) C8 H00a 1.0770 C8 H00b 1.0770 C8 H00c 1.0770 C10 H00d 1.0770 C10 H00e 1.0770 C10 H00f 1.0770 C9 H00g 1.0770 C9 H00h 1.0770 C9 H00i 1.0770 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA O1 H1 O2 2_655 0.98(5) 1.68(3) 2.617(5) 160(5) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion Br1 C5 C4 C3 176.9(4) Br1 C5 C4 C7 2.2(5) Br1 C5 C6 O3 5.3(5) Br1 C5 C6 C1 -177.5(4) Br2 C3 C4 C5 -176.2(4) Br2 C3 C4 C7 -1.7(5) Br2 C3 C2 O5 -5.8(5) Br2 C3 C2 C1 177.8(4) O1 C7 C4 C5 -96.1(5) O1 C7 C4 C3 89.3(5) O2 C7 C4 C5 83.0(6) O2 C7 C4 C3 -91.5(6) O3 C6 C5 C4 -175.7(5) O3 C6 C1 O4 -4.6(6) O3 C6 C1 C2 177.3(5) O4 C1 C6 C5 178.3(5) O4 C1 C2 O5 4.4(6) O4 C1 C2 C3 -179.2(5) O5 C2 C3 C4 176.9(5) O5 C2 C1 C6 -177.5(5) C4 C5 C6 C1 1.4(6) C4 C3 C2 C1 0.5(6) C5 C6 C1 C2 0.2(6) C3 C2 C1 C6 -1.2(6) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma -15 0 3 o 46.274 3.737 90.001 -15 0 5 o 55.142 97.002 114.850 -15 0 7 o -120.997 13.971 113.972 -15 0 9 o 427.088 396.916 152.080 -15 1 4 o 75.122 50.401 54.762 -15 1 5 o 677.941 598.185 109.034 -15 1 6 o 17.266 50.253 87.894 -15 1 7 o -27.548 3.756 68.588 -15 1 8 o 143.607 4.867 85.001 -15 1 9 o 1.128 75.594 66.921 -14 0 -2 o 19.493 41.747 120.909 -14 0 0 o 1624.760 1327.820 276.589 -14 0 2 o -105.081 1.319 70.700 -14 0 4 o 537.216 417.397 110.516 -14 0 6 o -15.805 22.135 84.645 -14 0 8 o 431.917 434.375 161.738 -14 0 10 o 92.566 161.695 63.272 -14 0 12 o 306.933 328.706 95.329 -14 0 14 o 72.525 113.262 66.603 -14 1 -2 o 353.828 192.963 79.467 -14 1 -1 o 113.221 38.187 55.408 -14 1 0 o 324.758 214.962 111.726 -14 1 1 o 108.123 5.501 61.708 -14 1 2 o 69.392 44.699 55.045 -14 1 3 o 77.430 39.801 56.469 -14 1 4 o 478.087 399.412 89.570 -14 1 5 o 100.676 199.689 98.212 -14 1 6 o 13.976 58.877 156.953 -14 1 7 o 6.267 23.344 68.539 -14 1 8 o 84.376 128.941 191.417 -14 1 9 o 195.713 45.188 92.541 -14 1 10 o 49.386 0.410 49.951 -14 1 11 o -16.759 2.439 44.969 -14 1 12 o 91.339 137.588 50.457 -14 1 13 o 41.397 9.124 53.293 -14 1 14 o 310.926 223.865 72.717 -14 2 -1 o 23.463 42.921 63.922 -14 2 0 o 349.923 414.385 87.311 -14 2 1 o 555.053 644.791 150.867 -14 2 2 o 167.935 0.171 68.473 -14 2 3 o 385.907 333.449 84.203 -14 2 4 o 149.339 196.588 62.772 -14 2 5 o 65.474 2.243 52.896 -14 2 6 o 13.007 25.866 57.301 -14 2 7 o 88.719 95.185 54.373 -14 2 8 o 301.265 250.856 98.854 -14 2 9 o 139.023 22.357 66.243 -14 2 10 o -32.329 69.208 46.431 -14 2 11 o 103.751 153.017 62.187 -14 2 12 o -53.342 32.693 50.384 -14 2 13 o 7.915 0.408 48.017 -14 3 2 o 170.256 0.927 63.609 -14 3 3 o 24.613 101.453 51.210 -14 3 4 o -71.246 0.744 58.548 -14 3 5 o 113.713 146.349 63.477 -14 3 6 o -28.708 0.114 52.145 -14 3 7 o 558.124 525.625 98.096 -14 3 8 o 4.082 28.674 51.328 -14 3 9 o 22.663 4.467 71.088 -14 3 10 o 35.634 0.429 54.907 -13 0 -5 o 1275.120 1504.250 252.881 -13 0 -3 o 198.090 75.960 95.357 -13 0 -1 o 5.466 5.839 58.918 -13 0 1 o 102.877 140.476 45.684 -13 0 3 o 2819.870 2504.600 218.551 -13 0 5 o -21.688 99.177 90.352 -13 0 7 o 123.192 84.326 87.543 -13 0 9 o -39.765 11.421 58.077 -13 0 11 o 124.974 65.771 68.234 -13 0 13 o 21.852 102.683 64.693 -13 0 15 o 167.858 98.825 78.706 -13 1 -5 o 94.743 26.369 137.943 -13 1 -4 o 113.796 46.428 82.625 -13 1 -3 o -16.768 2.187 53.120 -13 1 -2 o 153.811 246.461 60.935 -13 1 -1 o 1674.990 1643.330 154.519 -13 1 0 o -52.157 15.508 53.735 -13 1 1 o 251.400 350.510 62.930 -13 1 2 o 118.600 187.603 55.708 -13 1 3 o 1.658 6.634 47.023 -13 1 4 o 126.146 17.724 63.092 -13 1 5 o 453.548 440.033 77.216 -13 1 6 o 204.548 130.940 63.239 -13 1 7 o 466.587 496.614 127.758 -13 1 8 o 96.499 72.327 37.739 -13 1 9 o 698.324 611.339 85.254 -13 1 10 o 234.605 221.058 64.325 -13 1 11 o 15.245 2.645 42.883 -13 1 12 o 343.274 285.736 73.258 -13 1 13 o 66.106 83.220 50.753 -13 1 14 o -53.441 58.304 53.511 -13 1 15 o -32.119 8.314 47.372 -13 1 16 o 12.332 44.965 53.546 -13 2 -4 o 365.273 432.179 149.533 -13 2 -3 o -37.139 0.749 56.839 -13 2 -2 o 166.385 185.136 79.678 -13 2 -1 o 48.293 9.689 67.945 -13 2 0 o 311.253 232.367 80.848 -13 2 1 o 127.487 88.996 57.289 -13 2 2 o 703.473 769.354 107.799 -13 2 3 o 787.713 744.621 105.575 -13 2 4 o 83.719 0.135 56.084 -13 2 5 o 40.229 48.888 46.512 -13 2 6 o 123.642 121.570 50.206 -13 2 7 o 25.292 10.857 44.200 -13 2 8 o 57.568 0.044 97.772 -13 2 9 o 88.596 49.094 46.103 -13 2 10 o 500.288 458.011 75.038 -13 2 11 o -21.212 14.821 38.293 -13 2 12 o 47.903 65.000 50.117 -13 2 13 o 170.760 134.542 59.514 -13 2 14 o 128.661 0.469 51.350 -13 2 15 o -41.831 41.978 46.061 -13 3 -3 o 88.802 12.166 60.346 -13 3 -2 o 1185.460 1227.510 137.380 -13 3 -1 o 226.747 97.959 89.585 -13 3 0 o 301.542 351.244 79.642 -13 3 1 o -3.843 0.897 61.292 -13 3 2 o 28.183 167.867 64.076 -13 3 3 o 113.866 87.327 69.348 -13 3 4 o 129.587 127.300 102.676 -13 3 5 o 99.718 125.925 79.128 -13 3 6 o 744.143 933.312 105.490 -13 3 7 o 13.191 25.564 54.309 -13 3 8 o 134.101 76.224 86.422 -13 3 9 o 85.082 21.407 169.378 -13 3 10 o 120.384 146.478 47.063 -13 3 11 o 33.608 11.511 46.916 -13 3 12 o 90.966 35.301 70.085 -13 3 13 o 108.761 0.219 66.638 -13 3 14 o 189.539 121.946 75.396 -13 4 0 o 184.409 197.125 71.757 -13 4 1 o -14.018 0.996 62.049 -13 4 2 o 276.769 352.069 73.387 -13 4 3 o 222.196 134.295 70.701 -13 4 4 o -79.862 4.701 58.962 -13 4 5 o -42.294 1.559 55.556 -13 4 6 o 54.932 133.858 56.854 -13 4 7 o 247.455 166.641 79.498 -13 4 8 o 38.424 11.462 57.679 -13 4 9 o 15.640 1.409 52.632 -13 4 10 o 389.779 410.954 117.001 -13 4 11 o 32.268 16.751 41.385 -13 4 12 o 186.729 124.316 48.361 -12 0 -8 o -73.142 7.703 102.645 -12 0 -6 o 921.347 957.941 209.593 -12 0 -4 o 477.049 904.314 155.768 -12 0 -2 o 1529.840 1386.590 230.227 -12 0 0 o 568.942 431.762 104.502 -12 0 2 o 56.842 135.227 133.816 -12 0 4 o 3130.480 2834.850 228.032 -12 0 6 o 137.592 5.566 86.225 -12 0 8 o 10.124 69.607 46.919 -12 0 10 o 491.618 398.467 101.592 -12 0 12 o 1321.550 1560.530 166.636 -12 0 14 o 76.150 77.591 61.369 -12 0 16 o 8.511 50.565 92.767 -12 0 18 o -33.829 1.331 73.025 -12 1 -7 o 40.039 301.947 114.587 -12 1 -6 o 1710.020 1566.720 292.569 -12 1 -5 o 107.166 0.076 89.123 -12 1 -4 o 68.088 70.209 101.723 -12 1 -3 o 101.523 56.661 72.404 -12 1 -2 o 704.010 682.863 112.001 -12 1 -1 o 33.615 23.937 44.548 -12 1 0 o 1632.400 1622.370 115.182 -12 1 1 o 891.562 756.642 90.081 -12 1 2 o 530.007 565.632 69.587 -12 1 3 o 18.255 4.476 35.291 -12 1 4 o 194.244 196.894 71.790 -12 1 5 o 85.067 95.929 45.419 -12 1 6 o 93.084 81.831 50.869 -12 1 7 o 16.086 7.513 34.843 -12 1 8 o 681.788 894.806 87.233 -12 1 9 o 135.269 1.834 49.698 -12 1 10 o 30.563 2.778 39.523 -12 1 11 o 82.557 11.655 45.304 -12 1 12 o 57.721 44.865 40.639 -12 1 13 o 166.752 149.925 54.192 -12 1 14 o 79.062 25.825 54.662 -12 1 15 o -39.168 40.218 48.846 -12 1 16 o 259.927 199.066 70.917 -12 1 17 o 27.242 6.453 53.496 -12 1 18 o 130.816 175.975 79.527 -12 2 -7 o 36.615 10.893 92.899 -12 2 -6 o 205.466 306.500 131.182 -12 2 -5 o 186.236 227.758 120.470 -12 2 -4 o 145.055 211.966 120.558 -12 2 -3 o 1562.770 1970.750 270.003 -12 2 -2 o 503.442 503.884 95.175 -12 2 -1 o 112.884 96.001 50.641 -12 2 0 o 116.187 88.644 58.676 -12 2 1 o 191.033 94.899 63.342 -12 2 2 o 42.229 75.769 62.770 -12 2 3 o 49.309 108.893 46.880 -12 2 4 o 901.774 812.399 106.970 -12 2 5 o 713.178 987.440 93.404 -12 2 6 o 119.386 74.999 71.740 -12 2 7 o 450.263 360.784 83.413 -12 2 8 o 234.864 183.441 55.250 -12 2 9 o 17.224 3.184 40.146 -12 2 10 o 65.707 28.485 82.480 -12 2 11 o 14.938 100.991 37.491 -12 2 12 o 130.864 162.098 49.440 -12 2 13 o 85.481 1.192 44.470 -12 2 14 o 13.746 55.065 42.873 -12 2 15 o 234.146 238.740 63.344 -12 2 16 o 407.941 270.884 75.108 -12 2 17 o 58.883 1.406 49.361 -12 3 -6 o 455.976 182.025 200.373 -12 3 -5 o 11.415 14.483 116.431 -12 3 -4 o -39.776 31.155 103.962 -12 3 -3 o 105.943 160.271 55.779 -12 3 -2 o 9.776 0.321 46.886 -12 3 -1 o 204.944 134.970 68.591 -12 3 0 o 134.307 24.890 66.567 -12 3 1 o 1730.630 1973.070 154.981 -12 3 2 o 93.407 50.115 57.063 -12 3 3 o 263.459 205.540 80.167 -12 3 4 o 10.861 5.258 55.761 -12 3 5 o 49.533 13.414 43.316 -12 3 6 o 103.396 0.360 56.758 -12 3 7 o 188.934 229.980 60.652 -12 3 8 o 40.230 29.697 36.903 -12 3 9 o 247.161 191.572 55.230 -12 3 10 o 139.675 40.769 50.896 -12 3 11 o 508.935 366.781 72.876 -12 3 12 o 132.691 97.877 45.531 -12 3 13 o 57.920 8.725 45.331 -12 3 14 o -14.062 9.123 36.286 -12 3 15 o 297.153 233.637 66.852 -12 3 16 o 19.232 26.391 46.733 -12 4 -4 o 46.770 0.474 70.705 -12 4 -3 o 2051.350 2313.760 175.456 -12 4 -2 o -94.600 6.830 83.705 -12 4 -1 o 52.015 8.481 53.277 -12 4 0 o 208.050 154.114 65.221 -12 4 1 o 102.771 33.047 84.327 -12 4 2 o 79.507 18.621 47.588 -12 4 3 o 990.746 781.683 117.640 -12 4 4 o 131.898 39.138 55.547 -12 4 5 o 2278.130 1802.850 171.478 -12 4 6 o 98.563 15.830 60.960 -12 4 7 o 147.057 144.525 70.238 -12 4 8 o 13.196 0.558 45.293 -12 4 9 o 120.127 112.074 42.014 -12 4 10 o -38.467 7.064 41.805 -12 4 11 o 68.630 121.512 38.063 -12 4 12 o 240.734 141.872 60.159 -12 4 13 o 41.700 24.016 43.692 -12 4 14 o 39.270 53.281 44.017 -12 5 -1 o -8.074 12.312 65.797 -12 5 0 o 48.424 138.426 111.935 -12 5 1 o 871.490 952.561 118.951 -12 5 2 o 9.102 14.752 104.357 -12 5 3 o 13.409 73.284 48.076 -12 5 4 o -79.473 1.180 55.437 -12 5 5 o 6.954 46.986 74.647 -12 5 6 o 259.467 119.548 76.623 -12 5 7 o 155.505 255.352 60.969 -12 5 8 o 367.425 316.186 78.706 -12 5 9 o 616.144 578.446 103.113 -12 5 10 o -27.559 5.707 74.240 -12 5 11 o 22.634 45.767 37.937 -11 0 -9 o 538.302 824.223 113.060 -11 0 -7 o 62.693 79.380 95.621 -11 0 -5 o 383.624 365.762 156.207 -11 0 -3 o 1215.940 1057.470 208.978 -11 0 -1 o 3988.140 4036.590 340.336 -11 0 1 o 31.964 21.638 47.443 -11 0 3 o 382.893 314.957 84.683 -11 0 5 o 81.944 103.267 43.954 -11 0 7 o 2145.680 2146.840 184.863 -11 0 9 o 872.612 829.918 124.030 -11 0 11 o 336.946 249.639 135.397 -11 0 13 o 365.996 299.836 92.944 -11 0 15 o 20.550 4.098 58.453 -11 0 17 o 175.298 179.274 82.476 -11 0 19 o 15.774 10.139 67.993 -11 1 -9 o 28.247 78.337 41.160 -11 1 -8 o 652.022 488.196 118.402 -11 1 -7 o 1462.170 1320.890 141.153 -11 1 -6 o -7.244 15.240 55.148 -11 1 -5 o 2487.370 2984.230 212.147 -11 1 -4 o 192.810 256.845 91.406 -11 1 -3 o 116.199 86.210 63.067 -11 1 -2 o 215.318 87.605 98.738 -11 1 -1 o 744.724 624.119 110.036 -11 1 0 o 89.491 96.381 39.960 -11 1 1 o 83.550 90.742 48.413 -11 1 2 o 486.628 531.410 60.746 -11 1 3 o 1378.560 1554.250 98.404 -11 1 4 o -7.853 36.763 43.233 -11 1 5 o 454.151 489.531 72.287 -11 1 6 o -20.737 1.526 33.038 -11 1 7 o 100.259 93.537 35.629 -11 1 8 o 49.654 12.219 33.877 -11 1 9 o 1761.370 1659.110 155.906 -11 1 10 o 873.722 767.913 91.446 -11 1 11 o 413.315 451.737 61.844 -11 1 12 o 150.638 103.927 48.694 -11 1 13 o 315.273 309.495 67.862 -11 1 14 o 57.468 17.552 42.049 -11 1 15 o -20.595 14.688 42.024 -11 1 16 o -11.995 0.715 61.810 -11 1 17 o 111.020 110.043 45.698 -11 1 18 o 82.240 41.552 46.160 -11 1 19 o 1.542 3.211 55.955 -11 2 -9 o 324.919 416.219 62.328 -11 2 -8 o 1009.010 914.200 103.010 -11 2 -7 o 304.511 253.158 155.065 -11 2 -6 o -57.162 51.737 127.670 -11 2 -5 o 187.992 157.975 132.148 -11 2 -4 o 1367.660 1386.220 261.662 -11 2 -3 o 80.869 211.925 80.255 -11 2 -2 o 753.814 776.451 201.954 -11 2 -1 o 1640.940 1904.270 145.586 -11 2 0 o 1580.250 1590.650 139.929 -11 2 1 o 66.069 18.677 50.241 -11 2 2 o 28.838 35.534 49.831 -11 2 3 o 71.101 44.321 44.035 -11 2 4 o 754.052 716.620 93.788 -11 2 5 o 171.410 155.635 64.403 -11 2 6 o 873.624 1027.490 99.358 -11 2 7 o 2440.930 2291.370 127.953 -11 2 8 o 100.527 89.147 42.485 -11 2 9 o 7.446 2.420 42.723 -11 2 10 o 142.082 81.308 49.798 -11 2 11 o 92.009 58.740 42.935 -11 2 12 o 48.661 0.037 40.688 -11 2 13 o 112.691 80.934 51.651 -11 2 14 o 228.286 303.717 56.256 -11 2 15 o 14.922 6.093 44.901 -11 2 16 o 181.191 52.255 59.055 -11 2 17 o -6.254 25.777 41.589 -11 2 18 o 26.456 0.264 51.987 -11 3 -8 o 1331.770 1271.550 142.404 -11 3 -7 o 37.757 25.040 108.704 -11 3 -6 o 296.872 90.470 151.377 -11 3 -5 o 366.326 139.451 180.529 -11 3 -4 o 1497.350 1726.010 280.715 -11 3 -3 o 305.038 164.838 135.221 -11 3 -2 o 58.359 84.838 51.100 -11 3 -1 o 46.402 118.972 83.644 -11 3 0 o 266.074 342.099 62.052 -11 3 1 o 80.428 113.296 67.966 -11 3 2 o 2748.180 2770.630 178.851 -11 3 3 o 305.717 276.016 67.022 -11 3 4 o 642.234 550.595 91.858 -11 3 5 o 117.658 3.752 56.337 -11 3 6 o 0.881 1.734 58.798 -11 3 7 o 24.067 16.075 34.180 -11 3 8 o 101.469 176.344 35.171 -11 3 9 o 65.350 23.692 39.548 -11 3 10 o 1676.990 1712.380 121.895 -11 3 11 o 84.059 85.168 42.270 -11 3 12 o 137.259 80.845 50.905 -11 3 13 o -88.592 4.554 39.553 -11 3 14 o 49.084 34.055 52.216 -11 3 15 o 75.109 13.038 44.104 -11 3 16 o 46.047 44.694 44.815 -11 3 17 o 77.026 1.202 47.631 -11 4 -7 o 139.859 39.989 62.793 -11 4 -6 o -208.276 6.588 175.436 -11 4 -5 o -36.440 0.486 146.811 -11 4 -4 o 1862.710 1445.120 333.136 -11 4 -3 o 13.708 56.787 50.457 -11 4 -2 o 478.663 526.633 89.899 -11 4 -1 o 151.752 97.133 70.558 -11 4 0 o 671.146 633.507 96.228 -11 4 1 o 6.237 7.964 42.216 -11 4 2 o 230.249 157.966 70.454 -11 4 3 o 201.473 274.286 75.903 -11 4 4 o 805.722 701.254 102.659 -11 4 5 o -23.786 0.961 47.764 -11 4 6 o 1465.430 1547.460 145.297 -11 4 7 o -2.372 2.415 43.519 -11 4 8 o 13.834 3.127 33.583 -11 4 9 o 37.285 20.879 33.708 -11 4 10 o 139.732 182.969 48.033 -11 4 11 o 261.915 132.825 58.069 -11 4 12 o 91.428 55.559 44.609 -11 4 13 o -4.926 2.285 39.683 -11 4 14 o 432.363 402.684 69.275 -11 4 15 o -44.365 8.348 46.365 -11 4 16 o 106.904 77.236 55.054 -11 5 -4 o 977.663 916.201 121.219 -11 5 -3 o 74.380 4.082 114.695 -11 5 -2 o 88.557 0.974 58.773 -11 5 -1 o 217.978 260.254 66.165 -11 5 0 o 92.707 198.700 65.921 -11 5 1 o 136.618 54.595 63.169 -11 5 2 o 938.043 848.262 113.618 -11 5 3 o 433.131 479.478 80.624 -11 5 4 o 116.210 212.999 133.169 -11 5 5 o 356.731 301.895 58.629 -11 5 6 o -2.037 35.383 46.555 -11 5 7 o -14.847 26.705 41.622 -11 5 8 o 20.900 4.731 80.404 -11 5 9 o 86.514 135.966 66.932 -11 5 10 o 208.867 259.130 51.197 -11 5 11 o -14.704 60.909 44.526 -11 5 12 o 128.693 89.561 78.361 -11 5 13 o 262.329 223.322 54.554 -11 5 14 o 263.838 211.746 57.918 -11 6 -1 o 937.590 974.683 184.506 -11 6 0 o 871.084 640.415 112.113 -11 6 1 o -31.170 44.524 59.907 -11 6 2 o 23.713 4.619 86.840 -11 6 3 o 241.744 247.422 68.328 -11 6 4 o -14.947 7.292 47.399 -11 6 5 o 55.321 32.778 50.311 -11 6 6 o 154.946 204.876 54.024 -11 6 7 o 889.604 864.501 90.485 -11 6 8 o 85.285 34.168 42.379 -11 6 9 o 40.020 23.619 40.268 -11 6 10 o 219.847 138.527 73.409 -10 0 -8 o 313.291 265.899 118.099 -10 0 -6 o 2754.820 2626.200 300.911 -10 0 -4 o 110.196 44.119 92.635 -10 0 -2 o 2395.700 2885.220 259.818 -10 0 0 o 2388.040 2571.760 180.062 -10 0 2 o 3253.780 3120.600 204.939 -10 0 4 o 189.286 164.940 51.469 -10 0 6 o 1183.840 1162.460 131.572 -10 0 8 o 2981.500 2917.430 230.447 -10 0 10 o -43.488 1.258 46.206 -10 0 12 o 35.815 2.997 46.898 -10 0 14 o 59.776 40.731 154.670 -10 0 16 o 655.409 794.516 121.055 -10 0 18 o 73.428 25.191 75.645 -10 0 20 o 64.350 74.547 68.825 -10 1 -9 o -51.477 11.986 41.437 -10 1 -8 o -9.049 28.009 148.655 -10 1 -7 o 22.668 27.051 54.219 -10 1 -6 o 3258.570 3113.770 228.334 -10 1 -5 o 599.043 614.957 86.552 -10 1 -4 o 3.891 72.349 79.289 -10 1 -3 o 886.875 1031.770 155.241 -10 1 -2 o 3443.110 3408.060 213.825 -10 1 -1 o 126.065 0.203 75.645 -10 1 0 o -37.786 24.593 32.071 -10 1 1 o 406.328 412.247 57.204 -10 1 2 o 2708.850 2766.490 135.454 -10 1 3 o -2.491 13.061 30.049 -10 1 4 o 2916.190 2745.500 164.994 -10 1 5 o 971.219 915.517 76.741 -10 1 6 o 496.822 462.637 56.507 -10 1 7 o 88.312 126.405 33.291 -10 1 8 o 56.852 69.553 29.818 -10 1 9 o 61.255 56.314 31.942 -10 1 10 o 443.666 531.775 60.129 -10 1 11 o 48.102 118.035 39.571 -10 1 12 o 1233.910 1258.830 102.076 -10 1 13 o 329.682 364.034 74.281 -10 1 14 o 17.143 12.708 41.134 -10 1 15 o 14.242 4.387 39.716 -10 1 16 o 53.876 30.385 41.301 -10 1 17 o 10.719 0.929 48.025 -10 1 18 o 178.023 119.564 82.354 -10 1 19 o -14.907 23.683 43.861 -10 1 20 o -11.318 60.752 45.292 -10 2 -9 o 2275.130 2066.990 144.105 -10 2 -8 o 192.364 197.164 71.789 -10 2 -7 o 642.097 717.126 149.226 -10 2 -6 o 704.623 720.334 96.047 -10 2 -5 o 31.544 6.220 49.762 -10 2 -4 o 7.909 12.514 68.357 -10 2 -3 o -31.772 21.404 41.164 -10 2 -2 o 958.995 976.199 109.692 -10 2 -1 o 853.836 788.077 95.819 -10 2 0 o 500.428 569.456 53.642 -10 2 1 o 1900.970 1953.790 100.454 -10 2 2 o 794.408 761.430 109.413 -10 2 3 o 168.177 178.056 57.154 -10 2 4 o 3.509 2.886 34.294 -10 2 5 o 59.214 75.646 52.188 -10 2 6 o 117.876 163.365 29.204 -10 2 7 o 2359.340 2212.330 119.737 -10 2 8 o 330.004 359.679 56.925 -10 2 9 o 1083.220 1104.600 92.817 -10 2 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811.145 63.253 0 1 6 o 5301.530 5369.120 166.569 0 1 7 o 1316.090 1446.980 91.819 0 1 8 o 155.920 182.188 34.230 0 1 9 o 306.020 234.617 58.581 0 1 10 o 4391.120 4177.990 202.103 0 1 11 o 2301.410 2098.590 155.773 0 1 12 o 2143.470 1923.850 159.603 0 1 13 o 172.531 89.349 63.029 0 1 14 o 5013.860 5119.800 264.088 0 1 15 o 78.767 58.477 55.028 0 1 16 o -7.452 7.712 55.845 0 1 17 o 70.727 43.749 63.433 0 1 18 o 1108.860 1057.700 157.191 0 1 19 o 119.777 69.323 60.020 0 1 20 o 78.756 114.890 51.818 0 1 21 o 159.341 162.309 57.533 0 2 0 o 42084.900 44187.100 324.613 0 2 1 o 8044.130 7254.890 127.229 0 2 2 o 955.268 1065.490 19.965 0 2 3 o 7752.930 8041.630 103.954 0 2 4 o 768.923 957.694 26.902 0 2 5 o 309.779 221.564 64.054 0 2 6 o 1743.750 1533.130 95.954 0 2 7 o 16239.800 16528.900 333.136 0 2 8 o 1721.030 1595.280 110.955 0 2 9 o 16.142 33.375 35.649 0 2 10 o 3964.830 3837.100 187.966 0 2 11 o 1167.290 1081.610 110.206 0 2 12 o 854.409 816.285 104.963 0 2 13 o 418.565 386.874 80.642 0 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541.811 56.753 0 5 16 o 93.050 34.760 36.547 0 5 17 o 33.843 32.376 35.417 0 5 18 o 234.906 200.134 51.391 0 6 0 o 15531.400 15431.300 618.680 0 6 1 o 1707.250 1599.750 109.451 0 6 2 o 277.987 224.998 54.543 0 6 3 o 862.500 783.425 82.261 0 6 4 o 184.990 250.273 55.979 0 6 5 o 287.510 346.166 29.011 0 6 6 o 1025.740 1096.280 57.627 0 6 7 o 1374.590 1420.110 63.601 0 6 8 o 2462.120 2503.580 82.789 0 6 9 o 73.531 15.245 20.810 0 6 10 o 1107.030 1105.870 66.824 0 6 11 o 692.427 751.191 59.365 0 6 12 o 73.111 1.378 29.680 0 6 13 o 417.902 287.047 60.091 0 6 14 o 769.019 748.221 70.803 0 6 15 o 157.865 115.091 69.605 0 6 16 o 209.025 112.743 43.100 0 7 1 o 609.045 673.996 75.010 0 7 2 o 76.079 101.919 37.253 0 7 3 o 61.243 25.076 44.598 0 7 4 o 5352.110 4870.710 249.039 0 7 5 o 191.499 193.521 80.430 0 7 6 o 1930.090 2125.400 201.978 0 7 7 o 501.080 406.404 109.162 0 7 8 o 41.141 16.251 77.607 0 7 9 o 318.384 455.847 143.036 0 7 10 o 1077.470 1015.600 214.949 0 7 11 o 127.670 11.774 108.879 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113.840 1 1 1 o 1695.790 1768.660 25.977 1 1 2 o 248.023 232.319 14.474 1 1 3 o 2385.380 2176.080 47.984 1 1 4 o 986.884 1229.550 43.377 1 1 5 o 30331.400 30001.500 254.459 1 1 6 o 1921.660 1599.660 71.591 1 1 7 o 7536.640 8486.560 270.774 1 1 8 o 1024.340 1096.540 88.801 1 1 9 o 3175.390 3353.050 164.371 1 1 10 o 44.389 3.013 43.105 1 1 11 o -1.741 1.049 53.781 1 1 12 o 954.185 823.758 108.228 1 1 13 o 9649.190 9573.740 351.222 1 1 14 o 411.403 222.366 119.153 1 1 15 o 1217.620 1195.740 143.014 1 1 16 o 650.054 547.975 108.239 1 1 17 o 246.182 367.370 86.565 1 1 18 o 125.513 27.466 78.097 1 1 19 o 344.680 307.476 103.479 1 1 20 o 322.940 237.489 101.321 1 2 1 o 6569.180 6053.650 62.583 1 2 2 o 30835.300 29574.000 159.755 1 2 3 o 7556.140 7532.820 72.699 1 2 4 o 111.282 198.659 14.851 1 2 5 o 70.787 40.216 18.927 1 2 6 o 491.115 514.308 37.112 1 2 7 o 27.544 31.862 25.667 1 2 8 o 1129.070 1049.320 93.161 1 2 9 o 10060.900 10223.700 384.063 1 2 10 o 4930.810 4881.590 213.878 1 2 11 o 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298.902 42.484 1 5 16 o 829.528 936.825 75.201 1 5 17 o 23.841 17.471 33.648 1 6 1 o 2899.090 2792.420 140.234 1 6 2 o 6185.100 6376.120 204.116 1 6 3 o 1268.620 1224.600 112.594 1 6 4 o 1296.990 1277.110 117.920 1 6 5 o 151.542 177.279 16.345 1 6 6 o 64.448 75.433 17.461 1 6 7 o 1747.570 1762.470 66.846 1 6 8 o 1283.310 1317.250 62.605 1 6 9 o 4236.370 4423.140 120.066 1 6 10 o 773.626 759.327 57.329 1 6 11 o 272.413 254.350 40.319 1 6 12 o 153.902 133.680 45.077 1 6 13 o 314.031 322.985 45.786 1 6 14 o 251.329 268.782 43.775 1 6 15 o 23.224 18.700 30.753 1 6 16 o 216.282 166.943 48.934 1 7 1 o 94.243 168.511 39.568 1 7 2 o 7.318 0.045 36.882 1 7 3 o 652.902 570.580 109.746 1 7 4 o 82.022 174.079 43.653 1 7 5 o 5418.610 5486.300 335.246 1 7 6 o 521.109 289.447 121.526 1 7 7 o 2087.090 1980.950 219.092 1 7 8 o 823.116 625.343 152.056 1 7 9 o 608.495 671.265 152.343 1 7 10 o -9.307 166.186 97.816 1 7 11 o -52.157 0.104 107.211 1 7 12 o -68.928 28.584 103.787 1 7 13 o 2744.640 2626.320 369.838 1 7 14 o 72.791 12.409 128.636 1 8 1 o 1225.600 1212.110 111.829 1 8 2 o 582.665 507.576 104.409 1 8 3 o 1728.780 1655.860 159.863 1 8 4 o 671.969 593.043 156.558 1 8 5 o 225.939 216.624 86.290 1 8 6 o 136.354 99.093 73.229 1 8 7 o 141.872 112.866 84.864 1 8 8 o 184.329 178.048 75.114 1 8 9 o 2978.780 2897.570 284.437 1 8 10 o 13.172 72.405 217.056 1 8 11 o -8.404 1.593 77.817 1 9 1 o 37.858 79.654 70.039 1 9 2 o 43.939 3.917 84.845 1 9 3 o 119.661 37.959 67.254 1 9 4 o 154.774 7.213 91.420 1 9 5 o 786.654 879.148 167.986 1 9 6 o 1041.370 1112.110 189.663 2 0 2 o 60.175 165.963 13.348 2 0 4 o 87797.100 92653.800 872.527 2 0 6 o 227.769 247.207 60.762 2 0 8 o 7290.520 7378.170 335.331 2 0 10 o 5560.590 5891.820 450.752 2 0 12 o 6326.770 5945.650 392.405 2 0 14 o 745.121 885.804 152.870 2 0 16 o 15.542 45.037 78.323 2 0 18 o 1640.740 1843.300 259.115 2 0 20 o -12.205 85.709 82.450 2 1 2 o 654.109 656.798 26.384 2 1 3 o 31.111 34.961 16.623 2 1 4 o 9.866 51.032 11.982 2 1 5 o 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2 2 17 o 277.618 244.775 82.440 2 2 18 o 561.495 644.070 114.757 2 2 19 o 1045.970 996.742 159.104 2 2 20 o -2.623 15.929 67.011 2 3 2 o 2517.050 2755.800 54.432 2 3 3 o 385.938 396.329 22.500 2 3 4 o 13.232 1.421 13.871 2 3 5 o 8087.490 8022.070 131.120 2 3 6 o 42.873 46.662 17.127 2 3 7 o 9887.450 9444.890 164.211 2 3 8 o 923.288 966.750 54.466 2 3 9 o 650.736 649.934 64.456 2 3 10 o 12.857 15.478 28.849 2 3 11 o 276.530 321.067 49.305 2 3 12 o 291.585 290.735 67.837 2 3 13 o 15.652 5.635 32.946 2 3 14 o 723.407 773.211 86.165 2 3 15 o 3446.850 3580.190 184.654 2 3 16 o -41.555 47.492 41.873 2 3 17 o 563.064 498.071 89.453 2 3 18 o 165.211 113.020 60.037 2 3 19 o 102.056 79.085 54.648 2 4 2 o 1622.900 1713.510 35.492 2 4 3 o 11553.700 11643.200 132.512 2 4 4 o 304.839 277.053 23.890 2 4 5 o 5107.630 5102.580 105.065 2 4 6 o 1496.640 1602.540 83.906 2 4 7 o 63.161 76.571 29.117 2 4 8 o 166.821 181.787 37.375 2 4 9 o 130.306 109.294 35.968 2 4 10 o 4.354 22.206 31.124 2 4 11 o 9268.790 9177.040 262.032 2 4 12 o -14.907 7.319 35.182 2 4 13 o 69.268 23.169 39.375 2 4 14 o 120.385 39.643 49.933 2 4 15 o 344.754 213.284 67.433 2 4 16 o 111.768 74.138 63.560 2 4 17 o 395.801 278.025 79.164 2 4 18 o 99.136 42.830 54.823 2 5 2 o 684.598 707.668 22.642 2 5 3 o 40.827 50.370 13.734 2 5 4 o 85.320 55.771 18.743 2 5 5 o 795.457 783.708 58.135 2 5 6 o 97.408 66.748 26.224 2 5 7 o 4932.330 5026.450 161.063 2 5 8 o 1602.650 1739.050 96.771 2 5 9 o 2168.610 2103.850 120.029 2 5 10 o 430.926 391.898 60.336 2 5 11 o 229.379 229.288 48.995 2 5 12 o 428.303 328.940 68.643 2 5 13 o 91.094 93.822 42.562 2 5 14 o 758.886 532.577 94.241 2 5 15 o 2216.560 2153.620 157.699 2 5 16 o 372.602 168.178 82.133 2 5 17 o 80.530 90.971 37.297 2 6 2 o 84.042 97.204 100.249 2 6 3 o 972.196 1094.850 55.885 2 6 4 o 17626.500 17401.400 202.016 2 6 5 o 527.856 584.470 43.603 2 6 6 o 565.522 569.002 50.250 2 6 7 o 74.463 53.834 21.319 2 6 8 o 411.759 401.687 50.945 2 6 9 o 68.644 108.363 27.309 2 6 10 o 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