#------------------------------------------------------------------------------ #$Date: 2023-10-04 04:57:10 +0300 (Wed, 04 Oct 2023) $ #$Revision: 286650 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/28/2022868.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022868 _cell_angle_alpha 95.746 _cell_angle_beta 91.156 _cell_angle_gamma 115.002 _cell_length_a 6.8537 _cell_length_b 7.0873 _cell_length_c 14.5145 _exptl_crystal_F_000 426.00 _reflns_d_resolution_high 0.7259 _cod_data_source_file wm5697Isup2.hkl _cod_data_source_block I _shelx_title ' shi_5164_igfr_auto_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 277.81 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6573.97 6703.65 57.84 o 2 0 0 65.97 59.45 5.83 o 3 0 0 475.37 523.92 20.20 o 4 0 0 51.29 48.12 28.37 o 5 0 0 39.96 29.50 24.62 o 6 0 0 13.61 -19.80 38.18 o 7 0 0 191.21 164.31 60.39 o -8 1 0 143.16 176.27 61.20 o -7 1 0 146.78 178.05 42.39 o -6 1 0 13.59 43.91 34.10 o -5 1 0 128.04 100.62 17.75 o -4 1 0 320.55 281.31 32.40 o -3 1 0 38.04 26.91 10.60 o -2 1 0 1737.08 1795.17 41.08 o -1 1 0 2964.72 2942.29 43.97 o 0 1 0 3324.24 3468.47 59.48 o 1 1 0 254.45 268.58 9.70 o 2 1 0 5087.35 5131.96 63.72 o 3 1 0 177.87 164.46 17.70 o 4 1 0 53.27 84.10 23.37 o 5 1 0 426.60 391.19 44.24 o 6 1 0 27.58 20.30 22.69 o 7 1 0 19.14 21.44 33.24 o -8 2 0 84.47 141.48 46.44 o -7 2 0 311.13 272.61 38.01 o -6 2 0 2.94 22.50 18.95 o -5 2 0 2225.48 2211.28 97.95 o -4 2 0 3355.12 3295.05 89.29 o -3 2 0 274.54 233.48 16.99 o -2 2 0 4244.58 4231.32 72.61 o -1 2 0 2766.88 2852.50 57.32 o 0 2 0 25637.08 25069.39 573.92 o 1 2 0 2099.80 2136.76 38.08 o 2 2 0 286.12 322.05 18.11 o 3 2 0 1439.37 1448.44 51.68 o 4 2 0 1545.20 1588.09 60.78 o 5 2 0 188.09 183.19 23.97 o 6 2 0 3.59 26.86 40.68 o -8 3 0 80.92 102.79 47.29 o -7 3 0 122.12 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