#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:58:34 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180878 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/18/2101841.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2101841_Fobs loop_ _publ_author_name 'Ferguson, G.' 'Bell, W.' 'Coupar, P. I.' 'Glidewell, C.' _publ_section_title ; Crystal Engineering Using Trisphenols. Three-Dimensional Hydrogen-Bonding Networks in 1,1,1-Tris(4-hydroxyphenyl)ethane, its Hydrated Adduct with 1,4-Diazabicyclo[2.2.2]octane (1/1/1) and its Adduct with Piperazine (4/3) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 534 _journal_page_last 543 _journal_volume 53 _journal_year 1997 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'I -2ya' _symmetry_space_group_name_H-M 'I 1 a 1' _exptl_crystal_F_000 648.00 _cod_data_source_file ab03621sup2.hkl _cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' ME-C-TRIOL in Ia' _shelx_refln_list_code 4 _shelx_f_calc_maximum 151.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 -13 19.48 41.73 39.80 o 2 1 -13 2.96 40.57 29.37 o 1 2 -13 17.79 40.96 37.48 o 3 2 -13 13.47 41.35 39.80 o 2 3 -13 52.82 44.83 30.92 o 1 4 -13 5.84 41.73 42.89 o 0 0 -12 57.01 37.10 51.01 o 2 0 -12 26.71 36.32 73.81 o 4 0 -12 11.18 37.87 63.76 o 1 1 -12 58.52 48.69 29.76 o 3 1 -12 7.75 36.71 36.32 o 5 1 -12 18.67 40.19 39.80 o 0 2 -12 68.87 106.66 31.30 o 2 2 -12 95.31 107.83 31.69 o 4 2 -12 16.32 38.25 39.80 o 1 3 -12 28.88 67.24 40.96 o 3 3 -12 7.33 37.48 25.89 o 5 3 -12 91.23 62.22 48.70 o 0 4 -12 76.45 38.26 43.28 o 2 4 -12 109.58 100.88 34.79 o 4 4 -12 55.14 83.47 29.37 o 1 5 -12 85.70 65.32 26.28 o 3 5 -12 37.84 38.26 38.26 o 5 5 -12 3.90 41.73 41.34 o 0 6 -12 33.63 61.83 27.82 o 2 6 -12 140.39 71.51 32.86 o 4 6 -12 32.49 40.19 30.91 o 1 7 -12 39.07 75.35 25.50 o 3 7 -12 18.60 39.80 39.80 o 0 8 -12 68.28 71.49 27.83 o 2 8 -12 62.12 64.92 42.90 o 1 9 -12 95.23 66.09 29.37 o 0 1 -11 205.70 199.89 25.90 o 2 1 -11 323.72 321.79 28.23 o 4 1 -11 12.74 34.39 35.94 o 6 1 -11 30.70 62.99 44.05 o 1 2 -11 181.17 207.22 25.13 o 3 2 -11 10.14 33.23 37.48 o 5 2 -11 36.18 36.71 35.17 o 0 3 -11 115.59 112.48 24.74 o 2 3 -11 86.92 86.96 28.21 o 4 3 -11 19.83 34.78 32.46 o 6 3 -11 31.33 39.80 40.57 o 1 4 -11 588.06 534.93 35.22 o 3 4 -11 269.34 318.25 30.16 o 5 4 -11 42.83 37.48 40.58 o 0 5 -11 108.27 66.87 29.37 o 2 5 -11 143.16 136.07 31.70 o 4 5 -11 161.54 158.49 28.22 o 6 5 -11 87.56 40.58 51.02 o 1 6 -11 88.94 72.66 32.08 o 3 6 -11 196.10 162.76 33.64 o 5 6 -11 64.95 38.65 40.96 o 0 7 -11 98.92 124.07 23.96 o 2 7 -11 152.46 151.14 27.45 o 4 7 -11 30.96 55.26 27.05 o 1 8 -11 20.98 36.32 27.05 o 3 8 -11 25.62 45.21 27.44 o 5 8 -11 97.95 60.29 34.40 o 0 9 -11 32.56 38.26 41.73 o 2 9 -11 25.56 66.08 24.73 o 4 9 -11 62.39 68.02 40.96 o 1 10 -11 83.82 143.00 31.69 o 3 10 -11 48.88 100.86 27.82 o 0 11 -11 48.02 44.05 36.33 o 2 11 -11 40.22 55.26 27.44 o 1 12 -11 6.00 41.34 38.25 o 0 0 -10 97.57 107.06 27.06 o 2 0 -10 1049.88 1091.48 52.73 o 4 0 -10 111.40 67.64 54.11 o 6 0 -10 21.79 35.94 51.78 o 1 1 -10 253.17 213.85 25.14 o 3 1 -10 129.12 138.39 28.22 o 5 1 -10 21.06 33.23 40.19 o 7 1 -10 38.59 39.80 47.53 o 0 2 -10 249.15 295.44 25.52 o 2 2 -10 220.93 178.26 24.75 o 4 2 -10 53.28 68.79 25.89 o 6 2 -10 73.91 71.11 28.60 o 1 3 -10 753.46 802.58 35.25 o 3 3 -10 11.30 29.75 22.80 o 5 3 -10 24.58 33.62 36.32 o 7 3 -10 37.62 76.13 44.05 o 0 4 -10 226.91 174.00 26.29 o 2 4 -10 928.98 946.02 38.37 o 4 4 -10 185.84 194.47 26.29 o 6 4 -10 34.22 37.10 40.57 o 1 5 -10 306.73 330.30 26.69 o 3 5 -10 328.72 345.79 29.78 o 5 5 -10 72.19 34.78 37.87 o 7 5 -10 48.83 40.96 43.28 o 0 6 -10 184.73 242.79 22.81 o 2 6 -10 71.49 84.64 20.87 o 4 6 -10 312.11 322.55 30.17 o 6 6 -10 12.40 38.25 34.00 o 1 7 -10 400.34 355.53 30.95 o 3 7 -10 90.85 93.15 24.35 o 5 7 -10 157.19 161.97 27.06 o 0 8 -10 11.09 33.23 23.96 o 2 8 -10 152.20 151.15 25.51 o 4 8 -10 55.21 67.63 20.87 o 6 8 -10 5.34 40.19 43.28 o 1 9 -10 127.87 157.71 23.19 o 3 9 -10 136.19 150.75 24.74 o 5 9 -10 47.73 38.26 42.89 o 0 10 -10 83.06 71.89 51.79 o 2 10 -10 22.94 46.76 26.28 o 4 10 -10 33.97 58.35 27.05 o 1 11 -10 120.82 179.73 32.08 o 3 11 -10 102.75 136.82 30.92 o 5 11 -10 47.18 64.15 32.07 o 0 12 -10 8.15 38.25 50.23 o 2 12 -10 28.31 37.87 28.60 o 4 12 -10 10.74 40.19 29.75 o 1 13 -10 35.75 54.10 27.82 o 3 13 -10 2.65 40.18 35.16 o 0 14 -10 46.26 41.74 38.64 o 2 14 -10 28.88 40.96 41.35 o 0 1 -9 191.62 223.87 22.04 o 2 1 -9 277.68 259.14 23.59 o 4 1 -9 425.08 413.26 29.02 o 6 1 -9 172.74 175.90 25.13 o 8 1 -9 57.37 105.89 34.01 o 1 2 -9 642.09 637.48 30.21 o 3 2 -9 77.16 87.35 25.12 o 5 2 -9 372.59 321.08 28.24 o 7 2 -9 8.72 37.09 42.12 o 0 3 -9 738.69 809.66 32.15 o 2 3 -9 281.79 244.44 23.59 o 4 3 -9 214.64 228.13 23.20 o 6 3 -9 29.75 45.21 29.37 o 8 3 -9 29.77 41.73 49.08 o 1 4 -9 45.79 43.28 22.03 o 3 4 -9 963.03 961.43 36.05 o 5 4 -9 37.24 30.91 27.05 o 7 4 -9 18.04 37.87 30.91 o 0 5 -9 198.30 198.35 22.43 o 2 5 -9 900.00 882.95 34.50 o 4 5 -9 336.84 368.63 27.85 o 6 5 -9 214.38 214.58 33.64 o 1 6 -9 206.49 209.18 22.81 o 3 6 -9 808.98 765.18 34.09 o 5 6 -9 46.51 32.46 41.35 o 7 6 -9 0.40 39.03 35.93 o 0 7 -9 77.98 59.91 23.96 o 2 7 -9 176.40 191.76 21.65 o 4 7 -9 254.02 279.20 25.91 o 6 7 -9 42.63 36.33 43.28 o 1 8 -9 38.72 56.42 22.03 o 3 8 -9 668.51 677.63 34.46 o 5 8 -9 223.72 270.26 31.32 o 7 8 -9 9.35 44.05 43.66 o 0 9 -9 72.62 78.46 29.76 o 2 9 -9 140.39 168.54 22.42 o 4 9 -9 30.68 65.69 26.66 o 6 9 -9 7.73 38.25 41.34 o 1 10 -9 151.01 149.22 27.83 o 3 10 -9 74.49 69.95 24.35 o 5 10 -9 65.24 36.33 44.06 o 0 11 -9 118.59 80.78 57.21 o 2 11 -9 267.01 276.10 27.84 o 4 11 -9 238.67 208.41 27.84 o 6 11 -9 40.34 40.96 44.05 o 1 12 -9 59.55 34.39 42.51 o 3 12 -9 2.33 35.55 34.00 o 5 12 -9 28.88 86.17 22.80 o 0 13 -9 350.68 315.99 40.61 o 2 13 -9 55.59 63.76 27.82 o 4 13 -9 25.59 75.74 23.18 o 1 14 -9 2.45 37.87 27.82 o 3 14 -9 6.66 38.64 42.50 o 0 15 -9 71.16 40.19 62.61 o 2 15 -9 26.52 39.80 28.21 o 1 16 -9 2.49 41.34 39.80 o 0 0 -8 167.36 142.67 26.68 o 2 0 -8 2982.66 3064.09 73.12 o 4 0 -8 157.27 148.85 29.38 o 6 0 -8 430.01 396.98 43.72 o 8 0 -8 91.71 39.04 66.09 o 1 1 -8 30.63 21.64 21.25 o 3 1 -8 354.52 364.09 24.76 o 5 1 -8 47.29 52.56 19.32 o 7 1 -8 74.44 34.40 47.54 o 0 2 -8 1.52 22.41 25.12 o 2 2 -8 466.56 459.11 24.39 o 4 2 -8 0.80 42.12 27.05 o 6 2 -8 19.18 30.91 25.89 o 8 2 -8 0.79 39.41 40.96 o 1 3 -8 139.48 133.77 18.56 o 3 3 -8 1543.95 1544.15 39.64 o 5 3 -8 111.38 96.63 25.12 o 7 3 -8 111.19 113.64 33.63 o 0 4 -8 100.60 95.09 20.87 o 2 4 -8 292.61 279.68 22.82 o 4 4 -8 109.06 111.71 20.87 o 6 4 -8 66.92 31.69 37.87 o 8 4 -8 225.32 225.01 36.34 o 1 5 -8 44.18 45.60 30.92 o 3 5 -8 90.82 119.43 18.94 o 5 5 -8 67.46 52.17 40.97 o 7 5 -8 89.45 88.12 39.04 o 0 6 -8 20.54 24.73 21.64 o 2 6 -8 247.30 237.46 21.66 o 4 6 -8 389.26 384.97 27.47 o 6 6 -8 48.09 66.08 30.14 o 8 6 -8 10.96 121.72 40.57 o 1 7 -8 134.96 163.52 20.88 o 3 7 -8 215.36 223.50 22.81 o 5 7 -8 230.81 198.75 26.29 o 7 7 -8 62.16 49.85 40.58 o 0 8 -8 52.17 26.67 46.38 o 2 8 -8 134.53 140.71 20.87 o 4 8 -8 433.53 460.07 29.41 o 6 8 -8 103.86 113.25 24.35 o 1 9 -8 494.34 476.45 28.25 o 3 9 -8 406.70 394.26 26.31 o 5 9 -8 258.92 212.68 28.23 o 7 9 -8 10.44 39.80 29.37 o 0 10 -8 172.16 200.26 35.57 o 2 10 -8 392.43 408.17 27.08 o 4 10 -8 257.05 239.37 27.07 o 6 10 -8 34.32 37.10 40.57 o 1 11 -8 76.47 80.00 24.35 o 3 11 -8 210.94 155.04 25.13 o 5 11 -8 34.46 52.17 26.28 o 0 12 -8 116.53 146.49 33.63 o 2 12 -8 311.71 300.90 27.85 o 4 12 -8 45.99 34.39 24.73 o 6 12 -8 18.77 39.80 41.73 o 1 13 -8 27.38 32.85 41.73 o 3 13 -8 104.38 90.06 32.85 o 5 13 -8 22.02 60.67 27.82 o 0 14 -8 31.06 35.16 52.55 o 2 14 -8 5.04 34.78 38.25 o 4 14 -8 72.10 106.66 29.37 o 1 15 -8 104.13 99.33 25.12 o 3 15 -8 113.45 87.74 48.31 o 5 15 -8 95.37 42.90 42.90 o 0 16 -8 25.68 39.03 30.91 o 2 16 -8 1.93 50.62 42.12 o 4 16 -8 4.97 41.34 39.03 o 1 17 -8 62.98 40.58 48.69 o 3 17 -8 27.86 41.73 44.44 o 0 1 -7 69.48 21.64 27.44 o 2 1 -7 289.50 291.33 20.89 o 4 1 -7 14.20 41.35 28.21 o 6 1 -7 133.23 89.30 27.83 o 8 1 -7 7.96 37.09 47.53 o 1 2 -7 1503.90 1549.15 34.62 o 3 2 -7 130.13 117.14 17.78 o 5 2 -7 231.25 218.49 25.14 o 7 2 -7 60.67 32.85 34.01 o 0 3 -7 65.68 76.53 18.17 o 2 3 -7 1084.80 1134.82 31.84 o 4 3 -7 161.54 160.07 20.49 o 6 3 -7 87.35 93.53 26.67 o 8 3 -7 191.97 192.91 27.83 o 1 4 -7 193.83 218.88 17.40 o 3 4 -7 0.48 29.75 27.43 o 5 4 -7 289.06 269.98 25.53 o 7 4 -7 65.36 61.06 39.81 o 0 5 -7 268.25 255.30 18.95 o 2 5 -7 247.79 264.57 20.11 o 4 5 -7 610.45 580.53 28.66 o 6 5 -7 115.74 93.93 31.70 o 8 5 -7 194.98 188.27 32.47 o 1 6 -7 136.82 122.94 21.26 o 3 6 -7 178.35 169.74 20.11 o 5 6 -7 222.53 253.66 23.97 o 7 6 -7 122.78 127.55 27.44 o 0 7 -7 155.42 198.73 26.68 o 2 7 -7 129.28 122.55 18.17 o 4 7 -7 547.34 567.56 29.04 o 6 7 -7 49.45 73.81 27.44 o 8 7 -7 72.32 96.23 35.17 o 1 8 -7 179.09 182.12 20.11 o 3 8 -7 329.43 326.51 25.15 o 5 8 -7 248.12 252.13 26.30 o 7 8 -7 43.92 60.67 36.33 o 0 9 -7 206.08 199.14 32.48 o 2 9 -7 396.04 412.88 26.70 o 4 9 -7 952.40 974.51 37.60 o 6 9 -7 9.52 33.62 40.19 o 1 10 -7 381.02 382.27 25.15 o 3 10 -7 909.41 888.37 35.27 o 5 10 -7 45.81 65.70 26.66 o 7 10 -7 21.96 62.21 22.41 o 0 11 -7 537.09 553.55 40.26 o 2 11 -7 613.58 533.56 30.20 o 4 11 -7 25.50 36.32 29.75 o 6 11 -7 43.40 36.33 42.89 o 1 12 -7 946.03 857.37 34.50 o 3 12 -7 201.45 172.05 25.90 o 5 12 -7 123.27 34.40 46.38 o 7 12 -7 39.37 41.73 32.46 o 0 13 -7 117.13 97.41 32.08 o 2 13 -7 89.03 68.80 26.28 o 4 13 -7 351.99 356.24 30.56 o 6 13 -7 1.78 39.41 41.34 o 1 14 -7 53.43 58.35 24.35 o 3 14 -7 35.66 33.62 39.80 o 5 14 -7 3.31 37.87 32.84 o 0 15 -7 28.43 34.39 62.60 o 2 15 -7 94.46 150.35 22.80 o 4 15 -7 185.84 140.72 29.77 o 1 16 -7 64.49 35.94 42.12 o 3 16 -7 8.75 37.48 25.12 o 5 16 -7 28.98 62.60 40.19 o 0 17 -7 47.48 38.26 68.40 o 2 17 -7 17.19 38.25 40.19 o 4 17 -7 81.42 105.89 31.69 o 1 18 -7 9.36 40.19 27.82 o 3 18 -7 43.51 41.73 42.89 o 0 0 -6 915.77 899.96 34.55 o 2 0 -6 2781.58 2761.17 57.22 o 4 0 -6 1474.34 1499.83 51.33 o 6 0 -6 38.56 42.51 52.56 o 8 0 -6 20.03 85.78 60.67 o 1 1 -6 823.68 805.67 22.90 o 3 1 -6 166.86 190.26 17.40 o 5 1 -6 88.14 84.65 25.51 o 7 1 -6 26.87 36.32 35.55 o 9 1 -6 50.74 46.76 45.60 o 0 2 -6 605.51 637.99 21.32 o 2 2 -6 44.10 70.34 12.37 o 4 2 -6 38.40 45.60 17.39 o 6 2 -6 109.32 149.59 22.81 o 8 2 -6 144.70 66.10 36.34 o 1 3 -6 193.30 204.60 15.08 o 3 3 -6 103.44 109.79 16.62 o 5 3 -6 212.08 197.22 22.43 o 7 3 -6 322.33 293.18 30.17 o 9 3 -6 3.82 41.73 50.62 o 0 4 -6 1563.89 1606.84 32.32 o 2 4 -6 264.28 260.37 17.80 o 4 4 -6 360.87 359.49 23.61 o 6 4 -6 525.07 529.14 31.74 o 8 4 -6 24.67 36.71 35.16 o 1 5 -6 836.07 815.85 25.60 o 3 5 -6 481.64 472.78 22.85 o 5 5 -6 292.97 312.93 25.53 o 7 5 -6 159.83 165.46 25.13 o 0 6 -6 278.70 303.70 27.47 o 2 6 -6 389.69 421.52 22.06 o 4 6 -6 32.33 22.80 31.69 o 6 6 -6 553.70 522.96 32.52 o 8 6 -6 46.88 64.54 33.23 o 1 7 -6 288.35 261.92 20.12 o 3 7 -6 89.06 99.72 17.01 o 5 7 -6 777.83 724.52 32.55 o 7 7 -6 596.38 553.13 35.22 o 0 8 -6 24.61 53.71 38.26 o 2 8 -6 277.04 292.45 20.50 o 4 8 -6 511.01 488.93 27.87 o 6 8 -6 458.83 404.36 31.73 o 8 8 -6 97.44 133.73 33.62 o 1 9 -6 28.31 22.03 20.48 o 3 9 -6 775.64 758.00 31.39 o 5 9 -6 813.73 779.91 34.87 o 7 9 -6 47.07 35.94 32.46 o 0 10 -6 54.65 37.10 42.90 o 2 10 -6 203.76 225.83 22.04 o 4 10 -6 474.56 517.84 28.64 o 6 10 -6 126.22 115.57 24.74 o 1 11 -6 13.72 24.73 31.30 o 3 11 -6 211.01 230.46 22.81 o 5 11 -6 232.43 258.30 27.84 o 7 11 -6 2.13 38.64 28.98 o 0 12 -6 188.49 230.83 32.48 o 2 12 -6 192.37 135.33 22.81 o 4 12 -6 84.16 83.48 21.64 o 6 12 -6 12.94 35.94 40.19 o 1 13 -6 226.19 196.44 24.36 o 3 13 -6 85.97 95.46 21.26 o 5 13 -6 19.59 34.39 30.14 o 7 13 -6 22.90 41.35 44.05 o 0 14 -6 103.75 76.92 52.57 o 2 14 -6 37.68 30.14 36.32 o 4 14 -6 560.30 561.59 35.61 o 6 14 -6 29.86 39.41 40.57 o 1 15 -6 13.69 50.62 24.73 o 3 15 -6 368.51 391.46 30.17 o 5 15 -6 231.80 271.42 31.70 o 0 16 -6 8.72 34.00 51.00 o 2 16 -6 34.48 34.01 40.58 o 4 16 -6 71.09 37.10 42.90 o 1 17 -6 54.31 47.92 37.49 o 3 17 -6 185.47 164.69 28.61 o 5 17 -6 207.70 186.34 33.25 o 0 18 -6 16.76 38.25 54.48 o 2 18 -6 43.16 38.26 45.60 o 4 18 -6 327.08 417.66 33.26 o 1 19 -6 36.26 40.19 42.12 o 0 1 -5 1565.38 1673.34 28.48 o 2 1 -5 1272.97 1258.69 25.70 o 4 1 -5 638.40 593.73 24.03 o 6 1 -5 55.35 63.38 35.94 o 8 1 -5 56.02 62.61 47.15 o 1 2 -5 369.92 373.34 16.65 o 3 2 -5 380.64 427.82 18.58 o 5 2 -5 804.87 763.30 30.63 o 7 2 -5 80.15 42.51 40.19 o 9 2 -5 61.25 88.11 51.01 o 0 3 -5 177.11 186.44 13.54 o 2 3 -5 1447.07 1510.38 28.83 o 4 3 -5 624.89 635.49 25.96 o 6 3 -5 934.77 952.53 35.67 o 8 3 -5 3.62 35.16 42.89 o 1 4 -5 91.01 98.58 12.76 o 3 4 -5 98.39 120.61 14.30 o 5 4 -5 20.85 22.41 33.23 o 7 4 -5 104.01 126.39 28.99 o 9 4 -5 29.41 40.96 47.14 o 0 5 -5 1728.34 1875.91 45.63 o 2 5 -5 1751.91 1740.70 31.98 o 4 5 -5 53.38 65.31 17.01 o 6 5 -5 447.45 407.89 30.19 o 8 5 -5 38.43 65.31 34.01 o 1 6 -5 117.28 131.84 14.31 o 3 6 -5 347.61 333.61 20.90 o 5 6 -5 2182.12 2126.65 47.14 o 7 6 -5 30.89 57.19 30.91 o 0 7 -5 257.86 289.00 25.53 o 2 7 -5 82.58 73.83 14.69 o 4 7 -5 209.70 231.64 21.27 o 6 7 -5 370.12 380.68 29.79 o 8 7 -5 97.79 107.06 34.78 o 1 8 -5 562.61 517.96 22.86 o 3 8 -5 402.43 375.44 23.61 o 5 8 -5 665.83 619.69 31.37 o 7 8 -5 41.06 33.62 40.19 o 0 9 -5 161.03 182.89 24.75 o 2 9 -5 44.04 58.74 14.30 o 4 9 -5 304.59 287.80 24.37 o 6 9 -5 155.85 171.26 25.13 o 8 9 -5 104.29 50.24 49.09 o 1 10 -5 12.85 21.25 18.16 o 3 10 -5 154.06 152.33 20.49 o 5 10 -5 694.38 669.23 33.31 o 7 10 -5 83.35 35.94 47.92 o 0 11 -5 203.96 192.19 28.62 o 2 11 -5 127.67 119.84 19.33 o 4 11 -5 63.21 68.02 25.12 o 6 11 -5 67.15 52.56 30.92 o 1 12 -5 49.92 24.35 33.24 o 3 12 -5 188.55 185.59 22.43 o 5 12 -5 186.37 189.05 25.90 o 7 12 -5 52.04 99.32 30.14 o 0 13 -5 10.08 26.28 42.89 o 2 13 -5 157.97 155.41 20.49 o 4 13 -5 69.41 70.73 24.35 o 6 13 -5 19.45 36.32 41.35 o 1 14 -5 19.63 43.66 21.64 o 3 14 -5 144.19 138.01 26.29 o 5 14 -5 21.89 34.39 42.51 o 0 15 -5 154.51 147.67 32.47 o 2 15 -5 140.22 161.97 23.58 o 4 15 -5 20.01 33.62 39.03 o 6 15 -5 22.05 39.80 45.98 o 1 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149.21 34.02 o 1 6 7 33.68 74.20 19.32 o 3 6 7 191.30 227.35 22.04 o 5 6 7 8.94 34.78 39.41 o 0 7 7 155.59 161.61 27.06 o 2 7 7 53.81 59.90 22.80 o 4 7 7 147.13 69.97 32.47 o 6 7 7 6.44 40.19 45.59 o 1 8 7 79.33 58.75 34.01 o 3 8 7 138.10 129.50 27.83 o 5 8 7 10.19 37.09 42.12 o 0 9 7 205.94 197.21 32.48 o 2 9 7 34.50 32.07 22.80 o 4 9 7 61.16 85.02 27.83 o 1 10 7 82.34 68.80 23.58 o 3 10 7 39.77 85.79 26.28 o 5 10 7 29.30 43.67 24.34 o 0 11 7 536.87 538.45 39.87 o 2 11 7 74.89 30.53 36.72 o 4 11 7 84.71 82.71 25.51 o 1 12 7 10.50 30.14 32.84 o 3 12 7 102.36 152.28 28.21 o 5 12 7 56.45 62.60 27.05 o 0 13 7 117.25 54.50 52.57 o 2 13 7 88.09 71.50 30.15 o 4 13 7 21.60 39.41 44.44 o 1 14 7 0.78 33.62 35.16 o 3 14 7 112.33 157.31 25.51 o 0 15 7 28.40 34.39 60.28 o 2 15 7 4.09 42.89 25.12 o 1 16 7 0.41 37.48 39.03 o 3 16 7 21.98 109.35 27.82 o 0 17 7 47.47 44.05 34.78 o 2 17 7 14.89 41.35 40.19 o 1 18 7 16.23 41.73 44.05 o 2 0 8 388.54 456.58 36.37 o 4 0 8 13.03 31.69 44.44 o 6 0 8 117.44 87.35 39.81 o 1 1 8 2.96 23.57 30.53 o 3 1 8 41.19 28.21 35.94 o 5 1 8 65.72 57.20 30.53 o 2 2 8 186.87 163.17 22.04 o 4 2 8 35.12 32.07 37.10 o 6 2 8 22.73 40.96 44.05 o 1 3 8 360.86 366.02 23.99 o 3 3 8 31.25 71.10 22.03 o 5 3 8 95.58 60.68 31.31 o 2 4 8 868.99 808.45 32.94 o 4 4 8 117.71 93.93 24.74 o 6 4 8 65.20 100.48 35.55 o 1 5 8 105.58 89.68 20.87 o 3 5 8 38.44 29.76 35.94 o 5 5 8 23.19 64.14 39.80 o 2 6 8 137.81 138.78 20.87 o 4 6 8 9.42 34.00 35.16 o 1 7 8 78.39 62.23 19.32 o 3 7 8 42.83 31.69 36.71 o 5 7 8 10.03 39.03 47.53 o 0 8 8 52.21 26.67 42.90 o 2 8 8 26.35 29.75 35.55 o 4 8 8 4.47 35.93 34.78 o 1 9 8 2.21 28.98 32.46 o 3 9 8 3.97 33.62 34.78 o 5 9 8 0.84 40.96 39.80 o 0 10 8 172.56 153.10 33.63 o 2 10 8 0.53 32.07 32.84 o 4 10 8 25.40 38.26 40.57 o 1 11 8 76.73 31.69 40.97 o 3 11 8 61.88 62.22 24.35 o 0 12 8 116.68 75.37 35.17 o 2 12 8 12.50 34.78 23.57 o 4 12 8 64.60 75.75 31.69 o 1 13 8 82.89 128.31 23.19 o 3 13 8 92.69 109.76 25.89 o 0 14 8 31.16 83.47 30.14 o 2 14 8 0.26 38.25 39.41 o 1 15 8 5.79 38.25 32.84 o 0 16 8 25.62 53.33 32.85 o 2 1 9 11.28 28.98 30.91 o 4 1 9 23.04 35.16 37.87 o 1 2 9 78.76 28.21 26.28 o 3 2 9 10.45 32.07 38.25 o 5 2 9 67.09 39.81 41.74 o 2 3 9 154.67 148.83 20.88 o 4 3 9 14.60 35.94 27.05 o 1 4 9 350.30 339.65 25.53 o 3 4 9 21.23 32.85 38.26 o 5 4 9 19.52 40.57 38.25 o 2 5 9 400.42 388.04 28.24 o 4 5 9 2.12 36.71 35.93 o 1 6 9 261.64 229.71 24.75 o 3 6 9 43.55 69.17 23.57 o 5 6 9 3.57 41.73 40.18 o 2 7 9 19.80 32.07 37.10 o 4 7 9 6.85 38.25 31.30 o 1 8 9 132.42 148.82 23.19 o 3 8 9 7.74 35.94 43.66 o 0 9 9 72.78 30.92 49.08 o 2 9 9 10.45 52.94 22.02 o 4 9 9 32.23 40.57 38.64 o 1 10 9 15.48 33.62 32.84 o 3 10 9 30.02 38.26 29.37 o 0 11 9 118.54 67.26 58.75 o 2 11 9 11.08 36.71 35.94 o 1 12 9 0.28 36.32 35.16 o 3 12 9 22.36 40.96 42.12 o 0 13 9 350.62 328.76 46.80 o 2 13 9 9.55 39.80 40.19 o 1 14 9 60.56 58.74 27.44 o 0 15 9 71.10 48.31 52.17 o 2 0 10 159.03 217.26 32.47 o 4 0 10 1.22 39.03 31.68 o 1 1 10 96.84 98.17 26.28 o 3 1 10 0.09 35.55 24.73 o 2 2 10 20.53 32.85 26.28 o 4 2 10 9.68 39.41 27.05 o 1 3 10 91.34 81.94 24.35 o 3 3 10 19.50 36.32 36.71 o 2 4 10 9.05 33.62 35.16 o 4 4 10 39.34 40.19 30.91 o 1 5 10 3.75 32.07 35.16 o 3 5 10 16.27 37.10 42.12 o 2 6 10 52.45 35.17 26.28 o 4 6 10 6.98 41.34 43.28 o 1 7 10 66.92 33.62 26.67 o 3 7 10 34.74 49.46 26.28 o 2 8 10 5.21 36.71 40.57 o 1 9 10 84.80 69.95 41.35 o 3 9 10 6.05 40.57 37.87 o 0 10 10 82.79 56.43 35.94 o 2 10 10 9.73 39.03 41.73 o 1 11 10 80.15 38.26 49.08 o 0 12 10 8.15 38.25 52.55 o 2 12 10 12.34 45.60 38.64 o 1 13 10 32.59 41.35 40.96 o 0 14 10 46.37 67.24 72.26 o 2 1 11 53.56 36.71 42.12 o 1 2 11 93.69 139.52 23.58 o 3 2 11 8.80 39.80 40.19 o 2 3 11 20.10 37.48 42.12 o 1 4 11 15.34 35.55 32.07 o 3 4 11 3.40 49.07 31.68 o 2 5 11 36.20 49.85 38.64 o 1 6 11 46.27 99.32 22.80 o 2 7 11 9.73 39.80 46.75 o 1 8 11 30.43 38.64 28.60 o 1 10 11 24.30 40.96 40.96 o 0 11 11 48.10 40.58 57.97 o 2 0 12 140.44 49.86 64.55 o 1 1 12 37.70 58.74 36.71 o 2 2 12 11.47 68.39 39.80 o 1 3 12 40.02 39.42 38.64 o 1 5 12 9.33 40.57 35.94 o