#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2102084.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102084_Fobs loop_ _publ_author_name 'Figgis, Brian N.' 'Sobolev, Alexandre N.' 'Simmons, Charles J.' 'Hitchman, Michael A.' 'Stratemeier, Horst' 'Riley, Mark J.' _publ_section_title ; Bonding effects and the crystal structures of (NH~4~)~2~[Cu(H~2~O)~6~](SO~4~)~2~ and its H~2~^18^O substituted form at 9.5K ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 438 _journal_page_last 443 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.295 _cell_angle_gamma 90.000 _cell_length_a 9.0964 _cell_length_b 12.2225 _cell_length_c 6.3447 _exptl_crystal_F_000 414.00 _reflns_d_resolution_high 0.7093 _[local]_cod_data_source_file ta0006snsup2.hkl _[local]_cod_data_source_block sn #BEGIN Tags that were not found in dictionaries: _shelx_title ' CuTS (normal) in P2(1)/a at 9.1K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 132.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8303.20 7471.97 392.03 o 4 0 0 272.86 227.68 1.80 o 6 0 0 57.90 60.17 2.08 o 8 0 0 7.40 5.56 2.12 o 10 0 0 995.83 1033.78 8.97 o 12 0 0 1953.57 1962.54 21.60 o 1 1 0 345.52 322.88 21.06 o 2 1 0 2816.13 3026.42 141.98 o 3 1 0 2533.58 2421.46 67.15 o 4 1 0 2664.69 2592.07 52.74 o 5 1 0 8088.05 7544.09 127.89 o 6 1 0 0.68 2.05 1.23 o 7 1 0 6637.10 6577.91 68.89 o 8 1 0 943.19 956.90 11.31 o 9 1 0 736.66 746.27 7.26 o 10 1 0 457.68 471.61 3.48 o 11 1 0 685.45 694.80 7.60 o 12 1 0 35.79 39.20 2.04 o 0 2 0 3344.13 4107.56 17.08 o 1 2 0 1429.45 1690.43 50.47 o 2 2 0 1586.32 1508.01 95.18 o 3 2 0 269.54 265.07 25.71 o 4 2 0 7310.43 7227.44 327.07 o 5 2 0 1795.79 1807.88 57.64 o 6 2 0 3525.51 3561.13 90.02 o 7 2 0 324.99 328.01 5.77 o 8 2 0 1087.77 1108.21 18.55 o 9 2 0 2150.57 2168.20 18.16 o 10 2 0 533.89 541.09 9.40 o 11 2 0 21.86 25.95 1.40 o 12 2 0 143.82 150.75 3.03 o 1 3 0 15505.48 16916.33 177.13 o 2 3 0 52.69 85.29 3.82 o 3 3 0 3570.97 3560.36 227.48 o 4 3 0 740.99 877.62 46.97 o 5 3 0 251.52 307.10 16.81 o 6 3 0 139.80 149.96 2.19 o 7 3 0 196.25 184.15 3.84 o 8 3 0 177.81 179.10 3.43 o 9 3 0 968.58 988.88 21.50 o 10 3 0 0.42 1.42 1.15 o 11 3 0 1214.05 1239.00 15.86 o 12 3 0 43.42 46.15 2.14 o 0 4 0 3837.33 3655.09 56.80 o 1 4 0 18.80 14.42 0.55 o 2 4 0 3999.92 4080.84 96.42 o 3 4 0 3821.42 4268.08 207.64 o 4 4 0 5046.10 5109.96 334.49 o 5 4 0 309.47 359.17 19.46 o 6 4 0 1316.05 1306.47 49.35 o 7 4 0 26.60 34.46 2.31 o 8 4 0 1801.43 1766.14 51.56 o 9 4 0 251.28 267.06 7.39 o 10 4 0 272.34 271.27 3.17 o 11 4 0 278.31 288.05 2.98 o 1 5 0 295.18 272.01 1.94 o 2 5 0 412.84 407.61 11.24 o 3 5 0 4655.20 4634.41 174.00 o 4 5 0 3286.34 3426.09 165.83 o 5 5 0 589.95 655.58 40.24 o 6 5 0 3.40 5.61 0.80 o 7 5 0 59.46 78.01 7.77 o 8 5 0 137.82 152.02 9.68 o 9 5 0 671.64 669.58 14.08 o 10 5 0 427.42 457.47 5.57 o 11 5 0 173.13 169.37 2.43 o 0 6 0 263.95 200.38 9.04 o 1 6 0 5.91 2.92 0.71 o 2 6 0 1973.93 1998.46 34.96 o 3 6 0 285.58 292.79 10.21 o 4 6 0 8.59 16.16 0.76 o 5 6 0 421.96 455.32 36.36 o 6 6 0 258.83 233.12 11.38 o 7 6 0 3.24 6.39 0.92 o 8 6 0 1140.87 1065.13 19.79 o 9 6 0 775.14 778.15 13.58 o 10 6 0 630.47 612.01 10.19 o 11 6 0 90.17 91.34 2.11 o 1 7 0 590.44 618.70 6.56 o 2 7 0 298.23 310.91 7.17 o 3 7 0 520.13 549.63 18.55 o 4 7 0 245.06 231.88 6.88 o 5 7 0 2935.17 3094.82 133.02 o 6 7 0 8.67 10.46 1.01 o 7 7 0 216.53 228.52 9.68 o 8 7 0 120.13 126.21 3.71 o 9 7 0 224.94 223.12 5.53 o 10 7 0 60.55 62.93 1.59 o 11 7 0 6.71 11.14 1.83 o 0 8 0 1585.62 1601.59 5.19 o 1 8 0 1.42 1.12 0.57 o 2 8 0 806.74 794.03 10.62 o 3 8 0 128.40 147.97 2.48 o 4 8 0 31.55 42.83 3.59 o 5 8 0 9.21 12.76 0.82 o 6 8 0 330.95 343.66 15.79 o 7 8 0 26.60 37.56 2.56 o 8 8 0 4.43 7.13 1.54 o 9 8 0 87.93 109.50 8.38 o 10 8 0 266.74 273.62 5.02 o 1 9 0 1806.40 1829.54 13.89 o 2 9 0 271.82 283.81 3.06 o 3 9 0 120.14 129.38 2.04 o 4 9 0 1834.79 1854.71 48.55 o 5 9 0 1398.86 1361.89 45.97 o 6 9 0 60.68 62.55 1.61 o 7 9 0 720.03 696.63 25.18 o 8 9 0 140.23 143.63 7.15 o 9 9 0 220.52 221.56 5.87 o 10 9 0 554.06 550.53 9.66 o 0 10 0 36.18 42.64 3.67 o 1 10 0 172.94 183.32 1.48 o 2 10 0 87.54 88.86 3.62 o 3 10 0 1383.24 1387.79 22.53 o 4 10 0 724.34 740.22 14.74 o 5 10 0 402.02 404.98 11.18 o 6 10 0 1781.19 1829.43 57.62 o 7 10 0 23.53 25.20 1.17 o 8 10 0 624.46 649.18 27.22 o 9 10 0 514.79 524.95 15.53 o 10 10 0 210.44 202.43 4.66 o 1 11 0 2971.49 3029.39 13.84 o 2 11 0 200.39 214.78 2.21 o 3 11 0 1009.96 1032.48 11.51 o 4 11 0 296.34 298.63 8.44 o 5 11 0 19.74 19.81 1.00 o 6 11 0 111.20 113.09 3.68 o 7 11 0 18.54 19.12 1.14 o 8 11 0 337.50 342.86 12.45 o 9 11 0 25.51 30.85 2.63 o 0 12 0 200.88 202.72 5.06 o 1 12 0 213.65 224.13 1.80 o 2 12 0 484.14 506.15 3.37 o 3 12 0 76.76 76.51 1.52 o 4 12 0 908.49 887.40 12.83 o 5 12 0 121.23 127.24 4.11 o 6 12 0 1013.06 1005.62 25.91 o 7 12 0 4.81 6.71 1.12 o 8 12 0 1403.78 1383.91 43.20 o 1 13 0 78.45 85.44 1.30 o 2 13 0 174.93 171.68 2.56 o 3 13 0 1992.65 1993.12 25.59 o 4 13 0 212.40 203.32 3.73 o 5 13 0 325.91 321.55 7.16 o 6 13 0 22.83 21.85 1.21 o 7 13 0 797.86 790.47 18.41 o 8 13 0 381.87 381.18 11.82 o 0 14 0 2315.83 2258.28 29.39 o 1 14 0 251.92 252.51 2.13 o 2 14 0 1805.92 1798.81 14.24 o 3 14 0 48.59 52.56 1.24 o 4 14 0 1085.65 1066.06 9.13 o 5 14 0 12.92 13.99 1.07 o 6 14 0 4.91 5.30 1.12 o 7 14 0 9.88 9.26 2.77 o 1 15 0 79.00 86.33 1.49 o 2 15 0 26.40 25.30 1.58 o 3 15 0 782.72 762.14 6.84 o 4 15 0 1.68 3.98 0.98 o 5 15 0 1054.34 1022.07 13.18 o 6 15 0 163.82 165.91 2.92 o 0 16 0 2529.52 2448.97 17.48 o 1 16 0 91.62 90.42 1.65 o 2 16 0 880.38 850.77 6.95 o 3 16 0 55.37 54.60 1.99 o 4 16 0 690.03 656.46 7.78 o 1 17 0 466.50 439.41 3.20 o 2 17 0 187.86 184.21 2.20 o -12 0 1 481.08 494.00 8.30 o -10 0 1 4.40 11.92 1.62 o -8 0 1 52.33 53.56 4.21 o -6 0 1 3025.57 2998.22 8.94 o -4 0 1 177.43 163.02 2.30 o -2 0 1 17555.31 21742.11 70.09 o 0 0 1 3723.46 3532.17 61.68 o 2 0 1 1715.74 1452.01 11.61 o 4 0 1 383.82 321.68 2.52 o 6 0 1 1494.91 1441.64 15.85 o 8 0 1 3558.57 3440.92 10.66 o 10 0 1 1855.54 1869.29 9.28 o -12 1 1 200.21 208.01 8.07 o -11 1 1 381.38 408.17 5.10 o -10 1 1 12.19 14.52 1.70 o -9 1 1 921.46 967.19 13.51 o -8 1 1 527.60 545.48 4.67 o -7 1 1 2864.67 3010.52 54.74 o -6 1 1 313.80 330.81 9.71 o -5 1 1 3111.86 3213.04 140.76 o -4 1 1 280.62 302.25 6.93 o -3 1 1 429.56 369.59 8.52 o -2 1 1 1483.83 1651.30 38.66 o -1 1 1 1576.30 1624.54 172.91 o 0 1 1 3021.62 3180.83 165.71 o 1 1 1 7681.39 6188.15 86.05 o 2 1 1 6929.27 5982.13 22.75 o 3 1 1 655.23 491.63 15.93 o 4 1 1 45.82 52.62 1.26 o 5 1 1 3396.35 3098.49 52.99 o 6 1 1 3978.92 3829.96 19.55 o 7 1 1 195.54 200.39 7.16 o 8 1 1 69.11 73.17 6.56 o 9 1 1 103.78 103.61 2.43 o 10 1 1 163.97 166.66 3.40 o 11 1 1 117.61 126.34 3.08 o -12 2 1 697.06 703.97 7.22 o -11 2 1 64.39 100.51 29.09 o -10 2 1 435.59 456.48 4.68 o -9 2 1 119.14 130.15 2.58 o -8 2 1 277.91 297.04 3.36 o -7 2 1 2567.80 2597.89 8.84 o -6 2 1 1153.38 1148.44 33.55 o -5 2 1 390.88 408.57 19.84 o -4 2 1 10.89 33.51 1.27 o -3 2 1 1527.52 1673.80 60.68 o -2 2 1 721.11 758.57 6.10 o -1 2 1 3668.24 3831.75 161.84 o 0 2 1 3576.45 3494.58 403.73 o 1 2 1 1875.47 1801.28 48.51 o 2 2 1 8763.56 7818.90 210.60 o 3 2 1 149.50 135.97 12.93 o 4 2 1 4986.88 4696.66 142.46 o 5 2 1 664.71 644.19 22.05 o 6 2 1 1181.47 1143.79 32.78 o 7 2 1 3890.14 3813.84 94.03 o 8 2 1 439.77 434.50 5.68 o 9 2 1 270.67 276.58 9.49 o 10 2 1 9.66 13.84 2.36 o 11 2 1 503.49 510.95 15.81 o -12 3 1 213.96 223.37 3.90 o -11 3 1 41.20 41.29 2.13 o -10 3 1 203.64 206.87 3.39 o -9 3 1 557.06 568.86 4.84 o -8 3 1 255.96 250.48 3.08 o -7 3 1 37.22 34.50 1.51 o -6 3 1 72.53 54.25 4.07 o -5 3 1 1928.02 1960.22 93.34 o -4 3 1 230.90 251.22 6.60 o -3 3 1 17011.89 18531.70 533.37 o -2 3 1 1072.20 1079.47 3.50 o -1 3 1 4078.36 3907.37 42.55 o 0 3 1 3010.23 3067.75 133.55 o 1 3 1 153.31 178.92 13.19 o 2 3 1 3413.93 3373.49 494.61 o 3 3 1 15.93 39.14 5.33 o 4 3 1 808.46 880.27 57.17 o 5 3 1 157.30 145.88 10.97 o 6 3 1 833.65 782.53 42.15 o 7 3 1 1260.12 1224.66 51.98 o 8 3 1 122.68 138.87 20.99 o 9 3 1 2439.85 2431.41 91.04 o 10 3 1 2.69 5.12 2.90 o 11 3 1 1641.41 1669.87 30.83 o -12 4 1 119.78 124.32 3.37 o -11 4 1 267.11 267.28 3.93 o -10 4 1 2103.06 2077.57 29.79 o -9 4 1 73.60 71.85 2.11 o -8 4 1 3399.59 3381.42 33.15 o -7 4 1 353.03 340.82 12.02 o -6 4 1 702.36 746.52 24.15 o -5 4 1 5.24 9.22 2.77 o -4 4 1 2071.33 2161.29 87.78 o -3 4 1 677.97 694.42 17.26 o -2 4 1 4.80 6.22 1.35 o -1 4 1 918.17 1076.61 19.93 o 0 4 1 41.01 26.15 5.60 o 1 4 1 2275.59 2309.05 65.75 o 2 4 1 9199.43 8187.44 582.98 o 3 4 1 1103.97 1199.31 181.81 o 4 4 1 3043.36 3045.94 331.47 o 5 4 1 91.17 113.24 6.00 o 6 4 1 1119.49 1091.07 78.94 o 7 4 1 12.04 7.40 4.43 o 8 4 1 270.72 265.95 18.93 o 9 4 1 86.27 86.27 2.33 o 10 4 1 18.11 22.40 3.06 o 11 4 1 494.32 509.72 17.93 o -12 5 1 623.19 655.19 12.68 o -11 5 1 184.63 187.42 3.42 o -10 5 1 45.44 45.87 2.08 o -9 5 1 385.81 392.91 4.14 o -8 5 1 19.64 22.26 1.44 o -7 5 1 269.80 272.75 6.07 o -6 5 1 1125.26 1254.40 71.20 o -5 5 1 1222.88 1226.67 67.77 o -4 5 1 1100.73 1163.29 49.46 o -3 5 1 5829.11 5760.25 205.64 o -2 5 1 1022.20 1204.28 9.43 o -1 5 1 602.24 636.90 19.14 o 0 5 1 1840.48 2162.96 57.01 o 1 5 1 1870.29 1774.42 63.28 o 2 5 1 1707.85 1798.38 114.76 o 3 5 1 4698.75 4915.13 570.91 o 4 5 1 291.82 332.16 41.65 o 5 5 1 621.88 695.89 47.01 o 6 5 1 1029.92 1051.30 88.40 o 7 5 1 1110.21 1072.42 98.13 o 8 5 1 191.15 203.86 12.79 o 9 5 1 547.12 537.51 28.53 o 10 5 1 70.21 73.40 2.70 o 11 5 1 277.35 286.62 8.44 o -11 6 1 600.22 595.01 10.14 o -10 6 1 755.06 737.95 7.56 o -9 6 1 32.86 40.98 8.50 o -8 6 1 846.66 818.52 27.90 o -7 6 1 217.76 214.67 11.02 o -6 6 1 28.22 89.39 36.26 o -5 6 1 386.57 398.92 13.21 o -4 6 1 5275.66 5454.81 216.88 o -3 6 1 1.24 -3.04 5.77 o -2 6 1 6014.28 6111.90 16.97 o -1 6 1 671.18 689.35 6.72 o 0 6 1 3349.88 3423.40 62.91 o 1 6 1 1001.37 1019.40 27.18 o 2 6 1 568.58 521.21 22.86 o 3 6 1 45.72 37.42 5.67 o 4 6 1 228.23 217.51 21.59 o 5 6 1 58.87 95.72 46.37 o 6 6 1 318.31 329.79 30.81 o 7 6 1 46.36 53.74 1.89 o 8 6 1 344.78 364.97 20.14 o 9 6 1 33.66 32.65 4.38 o 10 6 1 1501.88 1492.45 75.33 o 11 6 1 717.42 742.18 22.08 o -11 7 1 1866.64 1888.53 27.40 o -10 7 1 54.58 50.54 2.20 o -9 7 1 1237.71 1250.14 35.97 o -8 7 1 230.23 213.49 8.29 o -7 7 1 2851.33 2976.65 188.89 o -6 7 1 367.71 369.70 24.99 o -5 7 1 334.49 360.35 12.61 o -4 7 1 48.17 50.53 2.37 o -3 7 1 176.93 208.22 14.71 o -2 7 1 786.15 828.96 9.83 o -1 7 1 1297.37 1319.94 11.94 o 0 7 1 28.41 30.44 1.42 o 1 7 1 2128.33 2023.35 41.41 o 2 7 1 1.86 2.72 0.80 o 3 7 1 6539.48 6473.05 243.12 o 4 7 1 682.74 686.09 66.54 o 5 7 1 1791.36 1846.89 205.53 o 6 7 1 235.73 208.03 21.53 o 7 7 1 827.39 805.05 60.44 o 8 7 1 137.27 146.89 13.37 o 9 7 1 15.10 14.88 1.91 o 10 7 1 10.18 15.19 4.81 o -11 8 1 356.79 362.42 4.66 o -10 8 1 110.42 110.96 3.92 o -9 8 1 3.51 7.09 1.53 o -8 8 1 299.12 303.62 20.41 o -7 8 1 70.41 80.82 2.02 o -6 8 1 4083.89 4108.62 205.85 o -5 8 1 59.26 68.94 2.45 o -4 8 1 6534.15 6671.07 181.77 o -3 8 1 23.46 33.98 1.13 o -2 8 1 2305.28 2420.90 9.72 o -1 8 1 569.33 669.56 10.94 o 0 8 1 2105.33 2215.11 30.93 o 1 8 1 374.02 398.10 9.58 o 2 8 1 445.63 461.15 19.08 o 3 8 1 683.42 704.80 36.42 o 4 8 1 36.15 40.57 2.62 o 5 8 1 153.32 167.67 15.84 o 6 8 1 1006.63 1010.87 113.25 o 7 8 1 67.03 83.68 7.87 o 8 8 1 922.90 908.07 63.28 o 9 8 1 26.28 26.31 1.80 o 10 8 1 1712.28 1705.12 79.98 o -10 9 1 0.93 0.46 1.73 o -9 9 1 328.84 329.99 10.60 o -8 9 1 281.74 301.18 13.26 o -7 9 1 638.27 638.22 33.41 o -6 9 1 1045.94 1073.81 47.19 o -5 9 1 25.67 31.22 3.13 o -4 9 1 85.83 91.36 2.43 o -3 9 1 40.39 42.30 1.35 o -2 9 1 542.15 577.93 3.40 o -1 9 1 5023.62 5172.08 28.69 o 0 9 1 42.99 37.76 1.18 o 1 9 1 2008.24 2087.10 35.73 o 2 9 1 46.04 47.40 1.25 o 3 9 1 2445.41 2392.17 97.03 o 4 9 1 550.63 565.44 38.79 o 5 9 1 1313.16 1299.18 83.45 o 6 9 1 624.79 642.41 54.22 o 7 9 1 335.71 355.94 35.49 o 8 9 1 116.37 123.14 8.84 o 9 9 1 28.61 33.07 5.96 o 10 9 1 94.40 96.92 3.12 o -10 10 1 582.41 604.41 8.82 o -9 10 1 39.44 39.20 2.12 o -8 10 1 1101.21 1150.88 53.39 o -7 10 1 175.94 167.77 7.51 o -6 10 1 1464.56 1492.14 64.76 o -5 10 1 187.82 188.73 7.32 o -4 10 1 165.76 171.95 2.27 o -3 10 1 612.61 632.57 3.90 o -2 10 1 97.07 105.76 1.72 o -1 10 1 1261.11 1314.03 13.60 o 0 10 1 3083.22 3154.90 43.12 o 1 10 1 584.03 600.18 7.47 o 2 10 1 1696.46 1683.90 55.44 o 3 10 1 571.57 556.20 21.06 o 4 10 1 754.38 772.60 35.91 o 5 10 1 45.72 45.26 7.03 o 6 10 1 650.63 648.63 65.79 o 7 10 1 0.48 -0.78 1.49 o 8 10 1 135.01 130.94 14.24 o 9 10 1 5.06 7.43 1.84 o -9 11 1 12.00 14.11 3.15 o -8 11 1 55.30 54.40 2.15 o -7 11 1 614.18 617.94 35.51 o -6 11 1 129.02 127.80 5.04 o -5 11 1 3333.55 3403.37 74.16 o -4 11 1 173.65 177.30 3.00 o -3 11 1 3447.37 3531.10 9.47 o -2 11 1 24.44 24.90 1.17 o -1 11 1 785.93 845.42 7.03 o 0 11 1 696.03 730.05 13.42 o 1 11 1 20.21 28.76 3.61 o 2 11 1 0.03 3.18 0.98 o 3 11 1 12.49 14.81 1.21 o 4 11 1 482.82 496.78 25.15 o 5 11 1 290.17 286.63 22.51 o 6 11 1 1.04 0.33 2.22 o 7 11 1 1610.42 1577.70 117.89 o 8 11 1 41.52 45.02 5.60 o -9 12 1 548.14 564.08 33.76 o -8 12 1 1008.33 1025.01 41.48 o -7 12 1 1704.99 1697.46 51.10 o -6 12 1 10.11 13.40 1.39 o -5 12 1 8.09 9.80 1.31 o -4 12 1 52.46 58.24 2.43 o -3 12 1 106.29 105.27 2.00 o -2 12 1 382.93 400.18 5.85 o -1 12 1 443.89 427.52 10.27 o 0 12 1 505.09 518.80 8.02 o 1 12 1 75.63 74.63 1.69 o 2 12 1 2704.52 2667.13 48.75 o 3 12 1 36.46 39.62 1.50 o 4 12 1 1699.46 1645.90 52.81 o 5 12 1 1394.80 1360.79 52.36 o 6 12 1 451.48 450.04 25.48 o 7 12 1 777.85 759.69 41.56 o 8 12 1 54.20 54.77 3.08 o -8 13 1 291.94 296.86 6.42 o -7 13 1 64.66 70.63 2.52 o -6 13 1 421.44 424.77 10.09 o -5 13 1 331.06 323.24 3.61 o -4 13 1 3.34 5.95 1.19 o -3 13 1 1054.52 1075.11 5.84 o -2 13 1 1492.00 1504.64 12.78 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