#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2102085.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102085_Fobs loop_ _publ_author_name 'Figgis, Brian N.' 'Sobolev, Alexandre N.' 'Simmons, Charles J.' 'Hitchman, Michael A.' 'Stratemeier, Horst' 'Riley, Mark J.' _publ_section_title ; Bonding effects and the crystal structures of (NH~4~)~2~[Cu(H~2~O)~6~](SO~4~)~2~ and its H~2~^18^O substituted form at 9.5K ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 438 _journal_page_last 443 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.277 _cell_angle_gamma 90.000 _cell_length_a 9.0921 _cell_length_b 12.2195 _cell_length_c 6.3442 _exptl_crystal_F_000 414.00 _reflns_d_resolution_high 0.7093 _[local]_cod_data_source_file ta0006sosup3.hkl _[local]_cod_data_source_block so #BEGIN Tags that were not found in dictionaries: _shelx_title ' Z in P2(1)/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8375.37 9952.76 32.04 o 4 0 0 274.51 264.31 2.29 o 6 0 0 63.24 64.47 1.69 o 8 0 0 8.26 13.68 1.91 o 10 0 0 1017.16 969.58 6.79 o 12 0 0 2023.29 1897.99 10.69 o 1 1 0 332.37 305.57 0.90 o 2 1 0 2782.90 2666.89 9.45 o 3 1 0 2532.75 2462.65 18.93 o 4 1 0 2646.70 2715.59 16.81 o 5 1 0 8157.56 7485.70 21.10 o 6 1 0 0.43 0.90 0.60 o 7 1 0 6759.86 6610.49 23.48 o 8 1 0 955.72 957.91 7.86 o 9 1 0 761.43 756.37 4.04 o 10 1 0 477.33 465.23 3.34 o 11 1 0 714.87 679.07 4.22 o 12 1 0 41.58 38.79 1.47 o 0 2 0 3260.12 3848.06 39.20 o 1 2 0 1463.50 1465.82 18.83 o 2 2 0 1565.30 1362.25 6.48 o 3 2 0 265.57 242.74 4.04 o 4 2 0 7283.80 6550.71 8.31 o 5 2 0 1859.71 1896.72 4.58 o 6 2 0 3531.17 3621.81 7.06 o 7 2 0 315.97 323.59 7.44 o 8 2 0 1125.03 1121.33 4.42 o 9 2 0 2197.85 2164.23 21.47 o 10 2 0 554.02 541.73 3.58 o 11 2 0 23.84 21.61 1.09 o 12 2 0 151.56 144.22 2.84 o 1 3 0 15446.85 16245.52 283.56 o 2 3 0 57.91 81.20 0.75 o 3 3 0 3574.78 3199.57 27.20 o 4 3 0 773.83 879.19 15.71 o 5 3 0 251.50 304.13 8.39 o 6 3 0 134.56 145.11 1.87 o 7 3 0 196.19 191.80 1.78 o 8 3 0 182.65 178.21 1.84 o 9 3 0 970.63 976.12 7.60 o 10 3 0 0.32 -1.38 2.00 o 11 3 0 1239.87 1218.66 5.68 o 12 3 0 48.57 44.83 3.36 o 0 4 0 3772.18 3150.78 27.36 o 1 4 0 19.93 20.79 4.52 o 2 4 0 3960.04 3603.08 71.02 o 3 4 0 3792.15 3729.74 38.56 o 4 4 0 4969.63 4613.33 9.18 o 5 4 0 318.04 353.32 2.05 o 6 4 0 1327.16 1338.09 6.29 o 7 4 0 30.13 37.73 0.95 o 8 4 0 1826.36 1819.71 8.74 o 9 4 0 257.63 265.42 5.03 o 10 4 0 283.14 277.01 4.84 o 11 4 0 297.03 290.21 2.89 o 1 5 0 298.89 257.20 5.48 o 2 5 0 396.91 372.50 3.43 o 3 5 0 4587.99 4158.79 53.84 o 4 5 0 3244.56 3196.97 11.47 o 5 5 0 582.65 636.75 3.32 o 6 5 0 3.19 5.57 1.50 o 7 5 0 60.75 70.65 2.48 o 8 5 0 136.02 147.88 4.53 o 9 5 0 683.86 690.77 3.90 o 10 5 0 442.49 456.81 3.61 o 11 5 0 177.64 169.87 3.05 o 0 6 0 249.14 199.60 1.56 o 1 6 0 9.33 28.93 15.55 o 2 6 0 1971.11 1854.25 19.41 o 3 6 0 282.88 272.94 1.84 o 4 6 0 7.36 13.74 1.79 o 5 6 0 419.67 428.64 6.84 o 6 6 0 263.55 230.43 5.28 o 7 6 0 2.45 4.58 0.60 o 8 6 0 1134.00 1100.08 26.10 o 9 6 0 789.57 786.14 4.29 o 10 6 0 636.91 635.99 4.04 o 11 6 0 92.91 93.93 2.72 o 1 7 0 575.24 571.12 6.55 o 2 7 0 285.75 290.94 3.72 o 3 7 0 514.13 508.99 7.96 o 4 7 0 235.00 212.97 1.64 o 5 7 0 2918.07 2887.52 15.72 o 6 7 0 9.23 11.47 0.67 o 7 7 0 210.89 227.52 2.24 o 8 7 0 121.21 135.70 4.51 o 9 7 0 233.33 221.92 2.37 o 10 7 0 59.80 61.13 1.53 o 11 7 0 5.75 5.58 1.05 o 0 8 0 1549.32 1456.16 3.94 o 1 8 0 1.18 1.69 0.47 o 2 8 0 772.37 738.54 6.13 o 3 8 0 127.29 141.20 1.35 o 4 8 0 37.11 36.36 1.02 o 5 8 0 8.61 16.53 5.20 o 6 8 0 319.56 334.45 5.33 o 7 8 0 26.61 41.89 5.84 o 8 8 0 4.35 20.47 6.86 o 9 8 0 87.95 96.97 2.28 o 10 8 0 262.98 295.36 18.59 o 1 9 0 1737.01 1700.39 13.85 o 2 9 0 254.00 263.04 1.83 o 3 9 0 116.30 126.05 4.17 o 4 9 0 1803.22 1757.20 5.06 o 5 9 0 1347.92 1276.22 8.26 o 6 9 0 61.61 64.64 1.34 o 7 9 0 703.22 672.54 7.48 o 8 9 0 131.65 135.86 2.18 o 9 9 0 220.52 211.49 3.32 o 10 9 0 556.40 559.39 4.06 o 0 10 0 38.89 43.83 1.60 o 1 10 0 168.69 171.77 1.55 o 2 10 0 81.61 78.75 1.81 o 3 10 0 1317.17 1278.92 12.29 o 4 10 0 685.82 697.45 4.30 o 5 10 0 388.09 376.69 3.62 o 6 10 0 1723.71 1745.03 5.84 o 7 10 0 23.38 21.52 1.00 o 8 10 0 613.36 618.59 12.75 o 9 10 0 498.93 500.32 3.91 o 10 10 0 209.42 205.39 2.80 o 1 11 0 2822.02 2762.63 37.25 o 2 11 0 191.79 193.04 2.48 o 3 11 0 955.82 971.36 16.72 o 4 11 0 283.74 288.61 2.28 o 5 11 0 18.85 19.27 1.54 o 6 11 0 113.25 109.31 1.81 o 7 11 0 16.23 20.82 1.00 o 8 11 0 329.04 338.15 15.55 o 9 11 0 23.52 28.56 4.94 o 0 12 0 190.26 193.22 2.25 o 1 12 0 198.18 211.08 1.90 o 2 12 0 464.93 486.79 13.84 o 3 12 0 74.66 73.84 1.37 o 4 12 0 847.34 830.53 4.59 o 5 12 0 115.14 121.34 5.12 o 6 12 0 960.95 952.54 4.70 o 7 12 0 3.26 4.25 0.95 o 8 12 0 1338.79 1314.82 26.51 o 1 13 0 72.37 76.66 1.64 o 2 13 0 158.68 160.61 2.46 o 3 13 0 1870.71 1845.03 17.69 o 4 13 0 201.58 190.37 2.18 o 5 13 0 303.47 308.14 2.70 o 6 13 0 21.92 18.98 1.06 o 7 13 0 753.62 771.40 14.89 o 8 13 0 350.34 354.00 5.88 o 0 14 0 2121.65 2091.92 18.53 o 1 14 0 234.99 238.79 2.25 o 2 14 0 1665.22 1667.17 17.91 o 3 14 0 43.87 48.65 1.21 o 4 14 0 1006.50 988.70 18.39 o 5 14 0 11.35 14.48 1.54 o 6 14 0 4.30 8.32 2.29 o 7 14 0 9.57 12.00 2.48 o 1 15 0 72.95 82.09 1.52 o 2 15 0 25.17 25.79 3.86 o 3 15 0 711.76 717.84 4.13 o 4 15 0 1.05 2.79 0.78 o 5 15 0 965.91 949.28 10.67 o 6 15 0 154.99 162.63 2.33 o 0 16 0 2256.60 2269.71 22.91 o 1 16 0 81.46 85.40 2.77 o 2 16 0 783.43 790.21 12.93 o 3 16 0 50.12 51.79 1.38 o 4 16 0 620.30 592.86 4.07 o 1 17 0 416.13 411.17 3.35 o -12 0 1 496.73 478.10 5.25 o -10 0 1 4.36 5.17 1.20 o -8 0 1 49.85 49.02 1.50 o -6 0 1 3019.87 3045.14 8.83 o -4 0 1 176.46 125.21 1.66 o -2 0 1 17374.89 20597.39 51.72 o 0 0 1 3816.79 4982.24 24.28 o 2 0 1 1757.11 1621.56 4.67 o 4 0 1 406.39 389.27 2.85 o 6 0 1 1509.83 1538.52 6.54 o 8 0 1 3696.87 3620.54 11.60 o 10 0 1 1958.07 1850.24 9.42 o -12 1 1 207.39 204.08 2.86 o -11 1 1 380.04 371.71 3.37 o -10 1 1 11.72 12.88 1.35 o -9 1 1 910.23 910.85 4.18 o -8 1 1 539.03 540.09 3.02 o -7 1 1 2841.96 2972.81 17.08 o -6 1 1 320.98 334.02 2.13 o -5 1 1 3124.93 3244.34 21.38 o -4 1 1 287.01 309.42 2.93 o -3 1 1 424.59 365.16 6.09 o -2 1 1 1496.01 1481.37 29.74 o -1 1 1 1567.74 1501.03 2.31 o 0 1 1 3010.74 3122.11 269.14 o 1 1 1 7734.48 8401.04 81.92 o 2 1 1 7051.47 7732.93 42.50 o 3 1 1 698.31 544.84 6.88 o 4 1 1 42.38 46.38 0.84 o 5 1 1 3468.46 3392.46 22.29 o 6 1 1 4044.51 4079.72 12.72 o 7 1 1 212.58 224.34 1.95 o 8 1 1 73.20 87.73 10.07 o 9 1 1 113.62 111.58 1.65 o 10 1 1 166.07 158.64 2.08 o 11 1 1 124.47 120.16 1.97 o -12 2 1 708.06 673.72 12.83 o -11 2 1 63.91 68.18 1.54 o -10 2 1 436.68 438.25 3.19 o -9 2 1 122.75 134.93 13.63 o -8 2 1 274.93 293.80 3.74 o -7 2 1 2601.63 2688.84 6.37 o -6 2 1 1152.32 1182.56 8.24 o -5 2 1 394.37 411.90 7.95 o -4 2 1 8.88 25.85 0.64 o -3 2 1 1509.63 1563.66 23.18 o -2 2 1 718.55 714.42 6.86 o -1 2 1 3690.05 4272.67 91.22 o 0 2 1 3565.81 3039.85 227.61 o 1 2 1 1821.29 1738.65 7.14 o 2 2 1 8835.81 9650.46 31.33 o 3 2 1 143.73 134.82 1.15 o 4 2 1 5059.69 4827.57 14.62 o 5 2 1 664.83 708.10 28.87 o 6 2 1 1224.23 1249.44 39.27 o 7 2 1 4049.41 4030.28 22.20 o 8 2 1 456.23 446.13 2.92 o 9 2 1 293.03 296.65 2.56 o 10 2 1 10.00 10.79 1.42 o 11 2 1 530.39 505.04 3.77 o -12 3 1 221.88 215.70 5.51 o -11 3 1 41.65 38.57 1.31 o -10 3 1 202.12 204.50 3.74 o -9 3 1 570.05 568.32 3.39 o -8 3 1 266.55 258.97 2.20 o -7 3 1 39.42 36.81 0.89 o -6 3 1 68.89 57.01 1.17 o -5 3 1 1899.69 1919.31 9.75 o -4 3 1 218.18 247.01 4.87 o -3 3 1 16951.23 18178.74 316.47 o -2 3 1 1077.79 1019.06 12.15 o -1 3 1 4047.60 3503.51 44.54 o 0 3 1 2975.92 2776.29 12.82 o 1 3 1 158.39 183.29 2.41 o 2 3 1 3378.08 3048.51 9.97 o 3 3 1 19.91 42.66 1.65 o 4 3 1 825.34 895.03 15.89 o 5 3 1 155.62 148.33 1.42 o 6 3 1 838.04 825.04 3.49 o 7 3 1 1271.89 1277.16 4.63 o 8 3 1 126.15 125.77 2.34 o 9 3 1 2538.35 2542.27 36.27 o 10 3 1 2.17 2.51 1.83 o 11 3 1 1756.29 1688.49 6.89 o -12 4 1 124.03 124.52 4.21 o -11 4 1 264.23 260.78 2.71 o -10 4 1 2127.78 2092.55 10.56 o -9 4 1 75.42 70.66 2.43 o -8 4 1 3402.25 3498.50 72.04 o -7 4 1 345.18 342.46 2.32 o -6 4 1 701.40 731.39 3.12 o -5 4 1 5.77 6.75 0.55 o -4 4 1 2039.20 2036.11 16.75 o -3 4 1 651.50 664.55 8.08 o -2 4 1 5.31 5.83 0.44 o -1 4 1 892.70 997.20 13.21 o 0 4 1 39.91 24.87 2.02 o 1 4 1 2221.52 2236.30 23.54 o 2 4 1 9151.07 9118.15 24.46 o 3 4 1 1128.31 1135.76 11.24 o 4 4 1 3003.30 2907.89 12.53 o 5 4 1 92.75 112.66 1.26 o 6 4 1 1135.68 1137.00 9.33 o 7 4 1 12.87 12.25 3.03 o 8 4 1 280.15 285.87 2.45 o 9 4 1 83.57 85.44 1.57 o 10 4 1 19.76 21.01 1.19 o 11 4 1 513.70 508.15 3.83 o -12 5 1 639.19 644.18 4.41 o -11 5 1 186.71 182.53 2.34 o -10 5 1 42.68 42.33 1.27 o -9 5 1 386.63 408.55 2.95 o -8 5 1 21.24 25.94 0.91 o -7 5 1 273.65 282.12 2.15 o -6 5 1 1124.44 1224.81 4.09 o -5 5 1 1228.93 1183.71 3.74 o -4 5 1 1074.92 1105.65 3.34 o -3 5 1 5750.08 5165.48 178.39 o -2 5 1 961.00 1095.19 14.02 o -1 5 1 596.53 597.63 6.02 o 0 5 1 1804.47 2027.30 5.19 o 1 5 1 1861.51 1708.34 12.96 o 2 5 1 1699.85 1711.87 4.55 o 3 5 1 4614.48 4461.47 33.91 o 4 5 1 283.24 313.04 2.35 o 5 5 1 631.18 649.29 4.12 o 6 5 1 1019.02 1058.45 8.01 o 7 5 1 1127.86 1089.06 4.41 o 8 5 1 197.58 216.07 2.18 o 9 5 1 553.29 547.67 3.58 o 10 5 1 67.60 67.04 2.05 o 11 5 1 287.56 280.90 6.21 o -11 6 1 588.72 576.93 14.04 o -10 6 1 759.69 726.72 4.22 o -9 6 1 28.84 44.03 11.76 o -8 6 1 835.12 815.38 10.79 o -7 6 1 216.34 214.54 3.23 o -6 6 1 28.68 50.48 15.38 o -5 6 1 363.65 364.58 2.15 o -4 6 1 5190.23 4922.01 50.65 o -3 6 1 1.22 7.72 4.84 o -2 6 1 5909.15 5423.65 130.59 o -1 6 1 651.28 644.10 8.18 o 0 6 1 3282.57 3143.54 10.67 o 1 6 1 990.83 985.28 9.81 o 2 6 1 562.50 506.02 2.19 o 3 6 1 48.38 37.25 2.03 o 4 6 1 222.41 206.50 2.29 o 5 6 1 60.00 67.38 9.96 o 6 6 1 317.54 330.13 5.96 o 7 6 1 50.21 53.94 4.81 o 8 6 1 342.96 360.07 7.04 o 9 6 1 35.44 35.89 1.18 o 10 6 1 1559.24 1514.45 8.52 o 11 6 1 746.17 750.35 9.13 o -11 7 1 1900.44 1871.36 9.04 o -10 7 1 57.62 56.85 1.51 o -9 7 1 1223.38 1243.27 20.00 o -8 7 1 228.68 215.68 3.83 o -7 7 1 2787.43 2823.68 7.03 o -6 7 1 347.94 343.54 5.41 o -5 7 1 319.87 326.29 3.06 o -4 7 1 44.88 50.88 0.91 o -3 7 1 169.13 181.40 4.96 o -2 7 1 782.02 754.67 13.05 o -1 7 1 1277.01 1235.26 8.61 o 0 7 1 29.64 25.78 0.61 o 1 7 1 2040.09 1925.37 12.77 o 2 7 1 1.33 5.14 1.29 o 3 7 1 6518.07 6031.23 99.20 o 4 7 1 683.64 660.94 2.94 o 5 7 1 1778.15 1778.96 5.25 o 6 7 1 235.25 209.70 1.92 o 7 7 1 823.62 814.43 5.82 o 8 7 1 136.58 147.40 3.88 o 9 7 1 16.35 18.56 1.17 o 10 7 1 9.58 13.71 4.74 o -11 8 1 350.66 348.31 3.64 o -10 8 1 108.29 106.56 3.07 o -9 8 1 2.52 8.68 2.54 o -8 8 1 291.35 302.92 16.16 o -7 8 1 73.07 80.51 1.32 o -6 8 1 3990.45 3860.79 17.33 o -5 8 1 56.76 63.35 1.65 o -4 8 1 6349.78 6003.52 119.44 o -3 8 1 23.98 30.29 0.75 o -2 8 1 2252.74 2206.67 21.49 o -1 8 1 552.52 620.88 5.46 o 0 8 1 2019.07 2026.63 8.86 o 1 8 1 361.25 380.08 2.06 o 2 8 1 427.10 439.00 3.39 o 3 8 1 673.14 690.14 10.32 o 4 8 1 38.08 37.75 0.88 o 5 8 1 153.12 167.41 4.92 o 6 8 1 997.44 954.93 4.18 o 7 8 1 67.41 83.99 1.44 o 8 8 1 927.43 924.38 4.59 o 9 8 1 26.55 23.89 1.13 o 10 8 1 1746.48 1748.81 13.65 o -10 9 1 1.83 4.08 2.07 o -9 9 1 320.79 305.59 3.43 o -8 9 1 273.15 285.43 2.55 o -7 9 1 618.27 611.58 5.21 o -6 9 1 1002.63 1006.40 10.70 o -5 9 1 25.71 33.35 0.87 o -4 9 1 79.63 95.40 17.73 o -3 9 1 37.70 42.11 2.60 o -2 9 1 545.82 542.97 3.17 o -1 9 1 4863.68 4738.51 53.70 o 0 9 1 39.29 37.18 0.84 o 1 9 1 1933.38 1974.29 7.41 o 2 9 1 43.25 48.49 1.67 o 3 9 1 2386.44 2304.69 32.88 o 4 9 1 540.99 531.68 6.97 o 5 9 1 1289.31 1258.42 6.84 o 6 9 1 605.24 630.01 3.50 o 7 9 1 335.04 352.10 2.80 o 8 9 1 116.97 121.74 4.61 o 9 9 1 28.57 28.80 1.22 o 10 9 1 90.13 88.40 2.68 o -10 10 1 559.52 568.17 5.58 o -9 10 1 38.46 36.63 1.25 o -8 10 1 1064.27 1070.99 13.28 o -7 10 1 165.92 160.61 4.95 o -6 10 1 1382.40 1383.40 5.12 o -5 10 1 172.27 167.56 1.75 o -4 10 1 150.25 154.27 1.79 o -3 10 1 590.41 580.69 8.78 o -2 10 1 90.96 96.77 2.54 o -1 10 1 1188.73 1189.21 14.24 o 0 10 1 3001.79 2903.78 7.21 o 1 10 1 571.09 566.28 6.96 o 2 10 1 1632.18 1634.39 13.59 o 3 10 1 547.62 533.37 8.24 o 4 10 1 737.10 745.96 3.54 o 5 10 1 44.73 42.25 1.73 o 6 10 1 638.06 630.92 3.62 o 7 10 1 0.42 0.97 0.79 o 8 10 1 140.16 132.76 5.64 o 9 10 1 6.05 7.79 0.99 o -9 11 1 10.37 13.91 1.02 o -8 11 1 56.72 55.57 2.57 o -7 11 1 596.27 578.69 4.40 o -6 11 1 118.24 118.68 1.66 o -5 11 1 3164.49 3116.64 18.21 o -4 11 1 168.70 161.93 4.71 o -3 11 1 3245.13 3210.73 50.01 o -2 11 1 24.87 23.20 0.79 o -1 11 1 745.06 760.43 3.98 o 0 11 1 672.35 691.78 2.27 o 1 11 1 21.04 42.91 9.44 o 2 11 1 0.20 10.21 1.10 o 3 11 1 12.89 15.08 0.75 o 4 11 1 467.40 467.86 3.78 o 5 11 1 274.96 279.32 5.22 o 6 11 1 1.05 0.01 0.69 o 7 11 1 1574.49 1552.96 11.16 o 8 11 1 41.53 46.74 1.41 o -9 12 1 531.93 523.06 8.30 o -8 12 1 948.44 937.02 7.76 o -7 12 1 1601.68 1565.87 15.25 o -6 12 1 9.26 9.26 2.11 o -5 12 1 6.46 10.00 2.17 o -4 12 1 50.44 55.02 1.16 o -3 12 1 100.13 100.04 1.43 o -2 12 1 355.49 371.10 6.66 o -1 12 1 404.02 399.86 2.60 o 0 12 1 468.80 484.13 2.03 o 1 12 1 71.55 68.62 1.21 o 2 12 1 2543.78 2535.87 18.12 o 3 12 1 33.83 38.12 1.37 o 4 12 1 1623.01 1584.80 19.88 o 5 12 1 1333.53 1315.89 6.05 o 6 12 1 445.69 443.33 3.29 o 7 12 1 762.56 755.16 4.46 o 8 12 1 54.66 54.10 1.50 o -8 13 1 266.95 261.03 7.67 o -7 13 1 57.26 56.73 1.46 o -6 13 1 385.12 378.48 3.07 o -5 13 1 304.76 295.62 2.63 o -4 13 1 3.26 6.08 0.74 o -3 13 1 982.51 986.78 14.01 o -2 13 1 1376.06 1380.87 12.72 o -1 13 1 309.43 314.76 2.45 o 0 13 1 1741.43 1752.53 12.14 o 1 13 1 1697.33 1684.49 5.63 o 2 13 1 31.26 36.09 2.13 o 3 13 1 468.81 490.30 8.31 o 4 13 1 6.68 11.49 1.54 o 5 13 1 94.72 103.59 1.70 o 6 13 1 332.32 336.26 2.99 o 7 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