#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/30/2103083.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103083_Fobs
loop_
_publ_author_name
'Albert, St\'ephanie'
'Pillet, S\'ebastien'
'Lecomte, Claude'
'Pradel, Annie'
'Ribes, Michel'
_publ_section_title
;
 Disorder in Ag~7~GeSe~5~I, a superionic conductor:
 temperature-dependent anharmonic structural study
;
_journal_coeditor_code           CK5029
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              1
_journal_page_last               11
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           216
_symmetry_space_group_name_Hall  'F -4 2 3'
_symmetry_space_group_name_H-M   'F -4 3 m'
_[local]_cod_data_source_file    ck5029150Ksup5.hkl
_[local]_cod_data_source_block   150K
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_intensity_meas
_refln_intensity_calc
_refln_intensity_sigma
_refln_observed_status
1 1 -1 249.3 200.7 15.0 o
2 0 0 14.7 2.8 1.6 o
2 2 2 13460.0 14167.6 154.9 o
2 2 0 143.1 223.4 2.5 o
2 2 -2 12940.0 12988.8 7.9 o
3 1 1 1020.0 1035.7 4.6 o
3 1 -1 941.9 999.9 6.4 o
3 3 3 4173.0 4195.0 4.8 o
3 3 1 1635.0 1559.7 7.0 o
3 3 -1 1752.0 1729.1 6.4 o
3 3 -3 4659.0 4636.6 18.3 o
4 0 0 1417.0 1479.5 12.9 o
4 2 2 758.6 774.5 4.7 o
4 2 0 107.7 84.4 1.6 o
4 2 -2 719.6 757.1 5.7 o
4 4 4 281.9 313.3 10.2 o
4 4 2 512.8 499.5 3.9 o
4 4 0 13460.0 13087.3 23.0 o
4 4 -2 507.2 489.5 7.5 o
4 4 -4 181.4 221.5 7.4 o
5 1 1 4702.0 4515.1 15.7 o
5 1 -1 4665.0 4488.5 14.8 o
5 3 3 496.6 519.5 4.5 o
5 3 1 889.4 836.8 4.2 o
5 3 -1 949.2 916.4 4.2 o
5 3 -3 520.3 514.9 5.2 o
5 5 5 2724.0 2677.2 10.4 o
5 5 3 1057.0 1070.5 7.5 o
5 5 1 313.3 339.4 5.4 o
5 5 -1 218.9 239.3 4.4 o
5 5 -3 1007.0 1017.6 9.0 o
5 5 -5 2753.0 2726.0 25.6 o
6 0 0 748.6 614.5 10.5 o
6 2 2 2354.0 2359.1 9.5 o
6 2 0 897.2 864.6 4.9 o
6 2 -2 2685.0 2693.9 7.2 o
6 4 4 41.8 49.3 2.1 o
6 4 2 143.3 151.8 2.4 o
6 4 0 4.2 1.1 1.2 o
6 4 -2 124.7 132.5 2.5 o
6 4 -4 39.5 56.8 3.0 o
6 6 6 1060.0 983.3 24.0 o
6 6 4 555.4 593.2 8.0 o
6 6 2 2825.0 2646.8 14.3 o
6 6 0 2294.0 2155.1 13.7 o
6 6 -2 2615.0 2495.0 17.6 o
6 6 -4 560.9 576.5 7.8 o
6 6 -6 1182.0 1114.8 14.9 o
7 1 1 1056.0 1120.5 8.3 o
7 1 -1 948.0 1001.5 9.0 o
7 3 3 1548.0 1613.6 8.7 o
7 3 1 58.2 67.4 1.9 o
7 3 -1 27.8 36.7 1.5 o
7 3 -3 1408.0 1449.0 9.5 o
7 5 5 351.3 411.1 6.2 o
7 5 3 890.9 921.1 5.8 o
7 5 1 388.6 388.6 4.4 o
7 5 -1 377.6 391.4 4.5 o
7 5 -3 890.9 953.1 8.0 o
7 5 -5 420.0 491.3 6.7 o
7 7 7 1535.0 1516.0 21.1 o
7 7 5 106.8 113.9 7.3 o
7 7 3 52.7 64.3 5.8 o
7 7 1 358.4 350.7 7.0 o
7 7 -1 356.1 386.2 6.8 o
7 7 -3 91.8 88.0 6.8 o
7 7 -5 87.0 80.2 5.4 o
7 7 -7 1391.0 1367.0 39.7 o
8 0 0 4624.0 4593.2 21.2 o
8 2 2 18.1 22.4 2.0 o
8 2 0 110.0 99.0 3.9 o
8 2 -2 35.8 28.9 3.3 o
8 4 4 3107.0 2936.8 15.6 o
8 4 2 570.3 624.5 6.1 o
8 4 0 340.0 332.7 5.3 o
8 4 -2 571.6 602.1 6.6 o
8 4 -4 3127.0 3014.9 17.1 o
8 6 6 39.6 45.9 5.6 o
8 6 4 99.2 78.5 3.3 o
8 6 2 6.4 0.7 1.6 o
8 6 0 9.4 0.2 1.8 o
8 6 -2 19.6 4.5 2.2 o
8 6 -4 95.1 67.8 3.9 o
8 6 -6 32.7 40.1 3.8 o
8 8 8 625.7 515.5 28.4 o
8 8 6 95.6 102.8 7.3 o
8 8 4 256.0 271.8 7.3 o
8 8 2 752.7 690.5 14.4 o
8 8 0 1164.0 1102.3 13.4 o
8 8 -2 763.1 688.4 9.8 o
8 8 -4 260.7 277.4 5.2 o
8 8 -6 82.8 94.7 6.1 o
8 8 -8 542.5 548.3 5.4 o
9 1 1 687.8 678.6 5.9 o
9 1 -1 520.7 566.4 4.4 o
9 3 3 201.9 224.3 6.9 o
9 3 1 510.9 532.7 5.2 o
9 3 -1 480.4 517.7 6.0 o
9 3 -3 281.8 283.9 5.1 o
9 5 5 340.3 452.2 7.7 o
9 5 3 327.2 338.6 4.7 o
9 5 1 390.9 402.7 6.0 o
9 5 -1 412.9 422.6 5.1 o
9 5 -3 390.7 375.0 5.8 o
9 5 -5 293.9 357.5 9.5 o
9 7 7 366.4 321.9 11.6 o
9 7 5 256.5 262.8 7.3 o
9 7 3 72.3 64.3 5.0 o
9 7 1 532.7 575.6 6.3 o
9 7 -1 548.3 591.9 7.3 o
9 7 -3 57.5 49.2 3.7 o
9 7 -5 251.1 251.2 6.0 o
9 7 -7 358.7 332.5 15.5 o
9 9 9 48.0 47.8 4.7 o
9 9 7 210.8 219.2 12.3 o
9 9 5 323.1 309.4 7.7 o
9 9 3 176.5 194.2 10.9 o
9 9 1 149.3 163.4 5.8 o
9 9 -1 144.2 149.0 6.3 o
9 9 -3 174.9 209.5 9.5 o
9 9 -5 356.2 339.1 11.5 o
9 9 -7 287.7 251.7 12.7 o
9 9 -9 61.2 29.4 14.8 o
10 0 0 13.7 3.4 2.5 o
10 2 2 1466.0 1401.9 14.0 o
10 2 0 285.7 277.3 4.5 o
10 2 -2 1339.0 1351.2 9.9 o
10 4 4 92.0 90.4 8.2 o
10 4 2 289.9 291.0 5.6 o
10 4 0 40.8 36.7 3.4 o
10 4 -2 270.2 277.7 4.8 o
10 4 -4 119.5 116.5 5.9 o
10 6 6 764.7 775.0 9.3 o
10 6 4 247.8 218.3 5.7 o
10 6 2 704.9 679.6 9.1 o
10 6 0 596.3 599.0 7.0 o
10 6 -2 719.2 674.3 9.4 o
10 6 -4 250.4 230.3 6.2 o
10 6 -6 825.8 793.4 11.4 o
10 8 8 75.5 50.9 5.6 o
10 8 6 105.8 92.2 5.3 o
10 8 4 17.9 0.8 3.1 o
10 8 2 68.6 59.1 4.8 o
10 8 0 8.2 0.8 2.0 o
10 8 -2 51.8 53.0 3.1 o
10 8 -4 9.9 1.6 1.7 o
10 8 -6 85.0 86.2 5.3 o
10 8 -8 52.1 42.1 7.3 o
10 10 8 105.9 80.0 31.4 o
10 10 6 199.9 171.8 12.6 o
10 10 4 249.8 244.9 8.7 o
10 10 2 318.5 358.5 9.5 o
10 10 0 375.2 297.7 11.1 o
10 10 -2 313.7 370.6 9.6 o
10 10 -4 275.6 263.9 9.9 o
10 10 -6 154.6 148.0 9.5 o
10 10 -8 32.4 88.4 32.1 <
11 1 1 78.2 73.8 2.4 o
11 1 -1 95.4 97.1 4.5 o
11 3 3 41.0 29.9 4.9 o
11 3 1 533.4 575.8 7.1 o
11 3 -1 601.0 590.6 8.5 o
11 3 -3 18.0 15.6 2.2 o
11 5 5 154.3 191.2 8.4 o
11 5 3 60.8 63.5 4.0 o
11 5 1 118.5 131.9 4.4 o
11 5 -1 149.1 152.5 4.6 o
11 5 -3 76.8 72.1 3.5 o
11 5 -5 178.7 196.2 4.2 o
11 7 7 13.0 12.5 4.3 o
11 7 5 214.4 203.5 6.5 o
11 7 3 418.1 490.2 8.8 o
11 7 1 63.1 86.9 5.2 o
11 7 -1 67.9 78.0 3.8 o
11 7 -3 402.2 466.8 7.8 o
11 7 -5 239.2 223.8 6.9 o
11 7 -7 14.6 3.9 3.3 o
11 9 7 21.4 27.4 4.1 o
11 9 5 226.2 226.5 7.7 o
11 9 3 237.9 227.6 8.5 o
11 9 1 137.4 126.7 4.6 o
11 9 -1 125.8 114.8 6.6 o
11 9 -3 210.1 217.4 5.6 o
11 9 -5 224.9 252.6 7.1 o
11 9 -7 24.4 25.0 4.6 o
11 11 5 74.5 65.1 38.4 <
11 11 3 29.6 15.3 6.3 o
11 11 1 49.2 56.4 6.2 o
11 11 -1 82.0 68.3 8.0 o
11 11 -3 19.5 12.7 3.7 o
12 0 0 134.1 112.7 6.6 o
12 2 2 152.1 151.7 5.9 o
12 2 0 300.1 286.5 5.2 o
12 2 -2 186.7 167.8 7.2 o
12 4 4 478.4 445.5 13.7 o
12 4 2 236.4 208.4 6.7 o
12 4 0 947.7 908.2 10.6 o
12 4 -2 218.4 200.6 4.7 o
12 4 -4 453.2 433.0 5.8 o
12 6 6 26.0 33.4 5.6 o
12 6 4 99.9 84.6 6.9 o
12 6 2 14.3 8.1 1.8 o
12 6 0 226.7 241.9 6.1 o
12 6 -2 14.0 4.3 2.3 o
12 6 -4 69.0 73.1 4.1 o
12 6 -6 21.5 31.4 5.2 o
12 8 8 291.5 260.1 55.4 o
12 8 6 133.7 133.3 7.3 o
12 8 4 344.8 321.8 5.9 o
12 8 2 220.9 191.1 7.3 o
12 8 0 291.6 245.8 7.4 o
12 8 -2 219.0 190.5 8.9 o
12 8 -4 299.0 310.1 8.6 o
12 8 -6 127.2 130.1 9.4 o
12 8 -8 226.6 236.9 49.1 o
12 10 4 28.4 20.0 5.1 o
12 10 2 17.4 4.5 4.1 o
12 10 0 12.4 8.8 3.5 o
12 10 -2 15.4 3.7 1.8 o
12 10 -4 27.5 16.9 2.0 o
13 1 1 79.5 127.3 4.9 o
13 1 -1 105.8 137.7 7.1 o
13 3 3 24.2 42.6 4.0 o
13 3 1 373.2 354.1 8.8 o
13 3 -1 338.5 343.1 7.5 o
13 3 -3 16.2 30.3 2.1 o
13 5 5 42.5 58.6 5.8 o
13 5 3 40.7 41.7 5.1 o
13 5 1 211.0 225.8 5.1 o
13 5 -1 205.6 214.6 4.3 o
13 5 -3 31.9 39.5 3.2 o
13 5 -5 40.3 68.5 3.9 o
13 7 7 16.3 30.7 5.0 o
13 7 5 158.5 181.6 7.0 o
13 7 3 264.8 258.9 9.9 o
13 7 1 17.3 1.8 3.1 o
13 7 -1 18.7 7.1 2.6 o
13 7 -3 296.9 277.4 7.6 o
13 7 -5 173.5 187.6 6.6 o
13 7 -7 29.3 26.2 29.7 <
13 9 3 91.8 121.4 8.5 o
13 9 1 37.1 44.1 8.5 o
13 9 -1 28.6 45.3 4.1 o
13 9 -3 110.0 117.3 12.6 o
13 9 -5 42.4 54.0 43.2 <
14 0 0 111.1 74.2 9.0 o
14 2 2 333.7 402.9 11.2 o
14 2 0 48.7 53.5 5.0 o
14 2 -2 419.7 445.2 12.1 o
14 4 4 21.6 12.7 3.6 o
14 4 2 69.0 104.5 6.9 o
14 4 0 10.9 5.1 3.0 o
14 4 -2 88.8 104.3 5.2 o
14 4 -4 11.6 18.6 2.0 o
14 6 6 176.9 147.8 68.5 o
14 6 4 85.4 63.4 5.8 o
14 6 2 322.1 317.3 10.3 o
14 6 0 23.0 28.0 3.2 o
14 6 -2 339.1 328.3 10.3 o
14 6 -4 78.3 64.4 5.4 o
14 6 -6 81.5 122.9 45.1 <
14 8 2 26.8 45.0 3.3 o
14 8 0 15.3 0.2 4.6 o
14 8 -2 28.4 43.9 5.7 o
14 8 -4 33.6 25.8 13.4 o
15 1 1 231.2 191.6 10.2 o
15 1 -1 195.5 206.9 9.6 o
15 3 3 112.3 114.7 3.3 o
15 3 1 23.0 17.2 3.8 o
15 3 -1 24.7 17.9 3.8 o
15 3 -3 119.1 102.5 10.5 o
15 5 3 57.3 77.0 13.6 o
15 5 1 150.5 157.9 6.8 o
15 5 -1 138.6 146.8 6.8 o
15 5 -3 42.2 65.5 6.2 o
15 5 -5 147.7 168.5 47.8 o
15 7 1 46.0 97.9 41.0 <
15 7 -1 91.3 95.0 7.8 o
16 2 2 46.0 20.9 11.6 o
16 2 0 81.8 90.8 6.6 o
16 2 -2 20.1 16.8 25.5 <
16 4 2 84.1 72.5 8.1 o
16 4 0 104.8 140.0 15.3 o