#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103086.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103086_Fobs
loop_
_publ_author_name
'Albert, St\'ephanie'
'Pillet, S\'ebastien'
'Lecomte, Claude'
'Pradel, Annie'
'Ribes, Michel'
_publ_section_title
;
 Disorder in Ag~7~GeSe~5~I, a superionic conductor:
 temperature-dependent anharmonic structural study
;
_journal_coeditor_code           CK5029
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              1
_journal_page_last               11
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           216
_symmetry_space_group_name_Hall  'F -4 2 3'
_symmetry_space_group_name_H-M   'F -4 3 m'
_[local]_cod_data_source_file    ck5029325Ksup8.hkl
_[local]_cod_data_source_block   325K
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_intensity_meas
_refln_intensity_calc
_refln_intensity_sigma
_refln_observed_status
1 1 1 362.5 280.1 362.5 <
2 0 0 10.9 8.3 0.9 o
2 2 -2 17670.0 18394.2 142.5 o
2 2 0 165.9 250.8 3.0 o
2 2 2 17960.0 20030.8 52.3 o
3 1 -1 1293.0 1385.2 5.1 o
3 1 1 1414.0 1424.4 6.9 o
3 3 -3 5948.0 5802.8 27.3 o
3 3 -1 1804.0 1734.7 6.1 o
3 3 1 1593.0 1542.1 4.6 o
3 3 3 4828.0 5229.6 55.5 o
4 0 0 2493.0 2522.9 6.6 o
4 2 -2 1264.0 1305.0 5.1 o
4 2 0 150.5 131.2 1.1 o
4 2 2 1261.0 1320.5 4.6 o
4 4 -4 298.1 326.9 8.4 o
4 4 -2 357.9 368.6 2.1 o
4 4 0 18090.0 17939.8 20.1 o
4 4 2 357.6 374.3 3.0 o
4 4 4 358.5 427.2 7.4 o
5 1 -1 5827.0 5668.1 9.6 o
5 1 1 5830.0 5722.6 6.6 o
5 3 -3 766.7 796.7 3.7 o
5 3 -1 1089.0 1074.2 3.1 o
5 3 1 993.6 990.0 2.8 o
5 3 3 734.3 773.7 4.0 o
5 5 -5 2206.0 2113.6 26.2 o
5 5 -3 1010.0 1058.1 5.3 o
5 5 -1 181.3 189.3 2.8 o
5 5 1 272.1 286.8 3.2 o
5 5 3 1060.0 1118.0 5.3 o
5 5 5 2158.0 2125.8 13.2 o
6 0 0 865.6 820.6 3.4 o
6 2 -2 3344.0 3283.4 8.9 o
6 2 0 1012.0 993.9 2.9 o
6 2 2 2901.0 2862.6 7.0 o
6 4 -4 24.3 32.5 2.1 o
6 4 -2 212.9 217.8 1.9 o
6 4 0 50.3 30.9 1.3 o
6 4 2 233.2 241.0 2.3 o
6 4 4 27.6 29.6 2.3 o
6 6 -6 1151.0 1082.8 18.1 o
6 6 -4 479.1 456.3 3.9 o
6 6 -2 2637.0 2544.4 11.8 o
6 6 0 1580.0 1534.5 8.3 o
6 6 2 2813.0 2733.8 12.4 o
6 6 4 473.3 486.2 4.2 o
6 6 6 938.7 916.8 10.1 o
7 1 -1 1086.0 1111.3 4.5 o
7 1 1 1177.0 1239.2 6.5 o
7 3 -3 872.3 906.1 5.5 o
7 3 -1 102.6 89.3 1.8 o
7 3 1 127.4 127.8 1.6 o
7 3 3 1002.0 1041.5 5.7 o
7 5 -5 385.6 459.4 7.7 o
7 5 -3 796.8 816.2 4.2 o
7 5 -1 380.6 394.6 3.0 o
7 5 1 374.4 397.7 3.1 o
7 5 3 780.2 790.9 3.8 o
7 5 5 346.7 423.2 4.2 o
7 7 -7 456.1 463.7 16.1 o
7 7 -5 62.0 64.0 4.1 o
7 7 -3 61.3 100.3 3.2 o
7 7 -1 307.8 315.2 5.2 o
7 7 1 269.2 279.1 5.5 o
7 7 3 42.2 62.6 2.6 o
7 7 5 81.0 76.2 2.3 o
7 7 7 517.4 528.8 10.6 o
8 0 0 5240.0 5237.5 11.2 o
8 2 -2 234.0 238.5 3.4 o
8 2 0 40.4 53.2 1.7 o
8 2 2 221.7 227.4 2.9 o
8 4 -4 3622.0 3586.0 14.9 o
8 4 -2 262.9 320.1 2.8 o
8 4 0 167.5 191.0 2.6 o
8 4 2 276.9 334.4 3.2 o
8 4 4 3487.0 3479.0 12.7 o
8 6 -6 53.8 40.5 3.0 o
8 6 -4 82.2 66.3 3.2 o
8 6 -2 59.9 60.6 2.4 o
8 6 0 4.1 0.0 0.7 o
8 6 2 53.0 55.6 2.0 o
8 6 4 89.0 73.8 2.4 o
8 6 6 60.8 43.3 3.1 o
8 8 -8 722.3 622.2 41.4 o
8 8 -6 21.2 15.3 2.3 o
8 8 -4 105.7 77.1 7.0 o
8 8 -2 308.2 268.5 5.7 o
8 8 0 1355.0 1310.4 7.1 o
8 8 2 304.4 267.0 6.3 o
8 8 4 114.9 88.2 3.6 o
8 8 6 20.6 18.5 1.9 o
8 8 8 598.1 595.9 35.4 o
9 1 -1 499.0 548.5 5.7 o
9 1 1 586.6 649.0 8.6 o
9 3 -3 149.7 154.5 3.5 o
9 3 -1 619.3 646.9 4.5 o
9 3 1 633.2 667.1 4.0 o
9 3 3 137.4 140.9 2.5 o
9 5 -5 165.5 156.7 5.8 o
9 5 -3 291.3 280.9 4.1 o
9 5 -1 377.3 385.8 4.3 o
9 5 1 369.7 380.2 3.6 o
9 5 3 264.6 254.3 2.8 o
9 5 5 210.5 209.3 2.9 o
9 7 -7 244.4 227.9 10.0 o
9 7 -5 144.1 142.3 4.3 o
9 7 -3 74.4 84.7 3.2 o
9 7 -1 427.0 444.9 4.1 o
9 7 1 422.2 429.5 3.8 o
9 7 3 75.2 81.5 1.8 o
9 7 5 154.0 154.0 3.1 o
9 7 7 241.2 226.8 4.8 o
9 9 -7 158.2 168.5 9.1 o
9 9 -5 130.8 149.4 9.4 o
9 9 -3 113.4 117.8 7.2 o
9 9 -1 94.1 114.4 4.8 o
9 9 1 99.0 120.6 2.8 o
9 9 3 114.5 113.9 4.0 o
9 9 5 109.2 141.3 4.1 o
9 9 7 115.9 150.4 8.5 o
9 9 9 37.1 22.0 26.7 <
10 0 0 37.8 34.2 3.4 o
10 2 -2 1171.0 1213.4 8.5 o
10 2 0 316.0 281.5 3.3 o
10 2 2 1235.0 1258.0 8.9 o
10 4 -4 58.0 58.5 4.2 o
10 4 -2 225.8 216.0 3.8 o
10 4 0 6.5 6.7 1.0 o
10 4 2 243.5 229.8 3.1 o
10 4 4 47.0 46.5 2.0 o
10 6 -6 614.8 571.1 12.7 o
10 6 -4 137.3 111.5 4.0 o
10 6 -2 512.2 503.2 6.0 o
10 6 0 398.7 371.7 4.4 o
10 6 2 488.6 476.7 4.1 o
10 6 4 124.5 111.3 2.7 o
10 6 6 614.4 597.6 6.7 o
10 8 -8 30.8 26.6 13.2 o
10 8 -6 45.3 34.5 2.5 o
10 8 -4 2.6 3.3 1.3 <
10 8 -2 57.9 37.6 3.7 o
10 8 0 19.3 15.6 1.8 o
10 8 2 53.5 40.4 2.2 o
10 8 4 7.8 2.3 1.1 o
10 8 6 49.1 38.6 2.7 o
10 8 8 66.1 28.9 10.5 o
10 10 -6 118.5 115.6 0.9 o
10 10 -4 118.2 93.9 5.3 o
10 10 -2 264.6 268.5 6.1 o
10 10 0 107.5 72.5 7.9 o
10 10 2 271.2 279.4 5.7 o
10 10 4 123.7 93.4 8.1 o
10 10 6 88.1 109.7 7.0 o
11 1 -1 83.8 76.8 3.7 o
11 1 1 62.7 53.8 3.2 o
11 3 -3 8.8 13.5 1.8 o
11 3 -1 366.5 386.3 5.1 o
11 3 1 342.6 368.6 3.5 o
11 3 3 20.1 22.1 2.4 o
11 5 -5 77.2 96.5 3.3 o
11 5 -3 68.0 55.6 2.5 o
11 5 -1 203.1 203.6 3.3 o
11 5 1 205.2 208.0 4.1 o
11 5 3 73.6 50.1 3.1 o
11 5 5 83.6 99.4 2.5 o
11 7 -7 5.2 1.0 1.2 o
11 7 -5 163.3 155.5 5.4 o
11 7 -3 176.8 190.2 4.8 o
11 7 -1 50.1 65.3 3.7 o
11 7 1 59.9 72.4 2.5 o
11 7 3 190.2 202.2 3.8 o
11 7 5 132.5 143.7 3.8 o
11 7 7 10.2 0.2 1.9 o
11 9 -7 16.0 14.1 0.9 o
11 9 -5 158.7 163.0 6.0 o
11 9 -3 159.5 145.5 6.4 o
11 9 -1 60.1 47.2 5.1 o
11 9 1 61.7 52.6 3.1 o
11 9 3 160.2 149.2 5.2 o
11 9 5 157.0 153.7 7.2 o
11 9 7 28.2 12.0 22.7 <
11 11 -1 52.1 40.8 10.9 o
11 11 1 41.8 36.2 5.7 o
11 11 3 26.0 8.8 5.6 o
12 0 0 144.2 101.0 3.7 o
12 2 -2 48.2 50.7 3.4 o
12 2 0 125.1 129.9 2.6 o
12 2 2 29.8 37.4 2.8 o
12 4 -4 215.4 185.4 6.9 o
12 4 -2 108.2 91.9 3.6 o
12 4 0 752.9 749.3 6.3 o
12 4 2 100.9 94.3 3.4 o
12 4 4 225.0 194.6 4.0 o
12 6 -6 20.4 27.6 5.8 o
12 6 -4 23.3 17.2 2.9 o
12 6 -2 7.9 5.7 1.7 o
12 6 0 122.1 114.8 4.5 o
12 6 2 12.2 5.9 1.5 o
12 6 4 32.0 21.2 2.8 o
12 6 6 23.9 26.7 4.7 o
12 8 -6 45.5 47.3 6.7 o
12 8 -4 315.8 296.3 8.6 o
12 8 -2 63.8 52.7 6.0 o
12 8 0 109.0 93.4 4.4 o
12 8 2 62.9 55.6 4.1 o
12 8 4 287.6 293.6 7.5 o
12 8 6 47.1 48.5 4.4 o
12 10 -2 41.0 11.5 27.8 <
12 10 0 22.2 2.9 5.3 o
12 10 2 8.4 10.7 2.4 o
12 10 4 17.3 21.9 8.6 o
13 1 -1 105.4 111.6 3.3 o
13 1 1 79.3 105.0 5.2 o
13 3 -3 28.2 47.9 4.0 o
13 3 -1 188.1 170.7 3.7 o
13 3 1 177.7 162.7 2.8 o
13 3 3 33.0 49.2 3.7 o
13 5 -5 33.9 38.6 6.8 o
13 5 -3 32.8 38.4 4.4 o
13 5 -1 117.5 118.9 3.7 o
13 5 1 129.6 126.4 4.9 o
13 5 3 40.1 39.7 2.8 o
13 5 5 16.3 34.7 3.6 o
13 7 -5 98.3 102.4 8.8 o
13 7 -3 131.7 128.4 6.0 o
13 7 -1 16.8 16.0 3.9 o
13 7 1 10.9 16.8 1.6 o
13 7 3 127.0 126.9 7.4 o
13 7 5 100.1 96.8 6.6 o
13 9 -1 13.0 12.9 18.9 <
13 9 3 44.9 51.9 4.1 o
14 0 0 16.4 27.7 2.1 o
14 2 -2 228.1 254.7 6.3 o
14 2 0 73.6 57.3 4.1 o
14 2 2 243.9 246.3 10.3 o
14 4 -4 13.7 11.0 6.8 o
14 4 -2 81.3 60.3 5.9 o
14 4 0 15.7 7.1 2.4 o
14 4 2 60.9 60.3 4.4 o
14 4 4 11.7 9.8 4.7 o
14 6 -4 52.6 36.6 3.3 o
14 6 -2 203.9 173.2 7.7 o
14 6 0 16.4 12.0 2.7 o
14 6 2 199.9 171.0 7.4 o
14 6 4 33.5 38.1 4.7 o
14 8 0 5.5 0.0 18.5 <
15 1 -1 114.3 117.1 11.2 o
15 1 1 120.6 114.9 9.3 o
15 3 -3 50.4 56.6 6.4 o
15 3 -1 11.7 11.8 1.5 o
15 3 1 15.3 11.8 3.5 o
15 3 3 63.0 62.1 8.8 o
15 5 -3 40.9 49.9 7.9 o
15 5 -1 33.7 32.7 8.2 o
15 5 1 30.5 36.3 12.9 o
15 5 3 65.4 50.6 25.2 o
16 0 0 190.8 167.9 21.6 o
16 2 0 49.9 40.5 4.8 o