#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103087.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103087_Fobs
loop_
_publ_author_name
'Albert, St\'ephanie'
'Pillet, S\'ebastien'
'Lecomte, Claude'
'Pradel, Annie'
'Ribes, Michel'
_publ_section_title
;
 Disorder in Ag~7~GeSe~5~I, a superionic conductor:
 temperature-dependent anharmonic structural study
;
_journal_coeditor_code           CK5029
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              1
_journal_page_last               11
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           216
_symmetry_space_group_name_Hall  'F -4 2 3'
_symmetry_space_group_name_H-M   'F -4 3 m'
_[local]_cod_data_source_file    ck5029375Ksup9.hkl
_[local]_cod_data_source_block   375K
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_intensity_meas
_refln_intensity_calc
_refln_intensity_sigma
_refln_observed_status
1 1 1 336.0 267.5 4.8 o
2 0 0 10.8 15.7 0.7 o
2 2 -2 16620.0 15879.3 232.6 o
2 2 0 145.7 184.2 1.7 o
2 2 2 16870.0 17310.6 106.5 o
3 1 -1 1207.0 1183.0 3.0 o
3 1 1 1258.0 1228.4 4.7 o
3 3 -3 5252.0 5065.8 11.0 o
3 3 -1 1516.0 1533.8 5.3 o
3 3 1 1353.0 1370.9 3.8 o
3 3 3 4298.0 4558.1 13.8 o
4 0 0 2280.0 2329.7 4.7 o
4 2 -2 1271.0 1282.5 2.7 o
4 2 0 128.9 125.7 1.1 o
4 2 2 1261.0 1299.4 3.9 o
4 4 -4 242.1 263.3 5.1 o
4 4 -2 291.3 293.2 2.3 o
4 4 0 16270.0 16291.7 13.4 o
4 4 2 302.5 299.7 2.5 o
4 4 4 304.2 352.7 6.2 o
5 1 -1 5368.0 5102.4 12.9 o
5 1 1 5137.0 5166.1 7.0 o
5 3 -3 736.0 709.5 4.3 o
5 3 -1 946.1 921.9 2.4 o
5 3 1 860.2 850.7 2.2 o
5 3 3 697.3 680.9 3.7 o
5 5 -5 1734.0 1607.5 37.8 o
5 5 -3 838.4 834.9 4.6 o
5 5 -1 147.4 144.8 1.8 o
5 5 1 215.7 225.9 2.4 o
5 5 3 877.5 884.9 3.7 o
5 5 5 1747.0 1630.9 11.3 o
6 0 0 770.8 770.8 1.4 o
6 2 -2 2935.0 2896.2 6.3 o
6 2 0 883.9 888.2 2.1 o
6 2 2 2540.0 2534.9 5.3 o
6 4 -4 15.9 17.4 1.6 o
6 4 -2 205.9 193.8 1.7 o
6 4 0 66.0 71.4 1.3 o
6 4 2 222.2 211.9 1.9 o
6 4 4 14.7 16.3 1.3 o
6 6 -6 960.4 928.9 4.6 o
6 6 -4 410.2 377.2 6.2 o
6 6 -2 2180.0 2193.0 7.1 o
6 6 0 1248.0 1284.9 5.1 o
6 6 2 2359.0 2347.8 6.4 o
6 6 4 427.7 402.2 3.6 o
6 6 6 785.9 786.8 7.1 o
7 1 -1 939.1 912.4 3.4 o
7 1 1 1011.0 1006.4 5.7 o
7 3 -3 665.2 626.9 3.7 o
7 3 -1 112.6 116.2 1.4 o
7 3 1 133.5 144.8 1.8 o
7 3 3 730.7 725.0 6.1 o
7 5 -5 328.0 342.4 4.6 o
7 5 -3 647.1 663.9 3.5 o
7 5 -1 318.3 321.6 2.8 o
7 5 1 318.7 315.4 2.4 o
7 5 3 635.1 646.1 3.3 o
7 5 5 293.9 316.6 4.0 o
7 7 -7 266.5 262.6 10.2 o
7 7 -5 66.1 59.9 2.1 o
7 7 -3 58.5 72.2 2.9 o
7 7 -1 225.1 261.7 4.6 o
7 7 1 214.3 235.7 4.2 o
7 7 3 38.8 47.5 2.0 o
7 7 5 65.8 61.9 1.5 o
7 7 7 336.3 305.7 9.1 o
8 0 0 4467.0 4489.9 10.3 o
8 2 -2 273.4 275.9 4.2 o
8 2 0 32.7 33.3 1.3 o
8 2 2 254.6 270.5 3.6 o
8 4 -4 3058.0 3027.1 12.5 o
8 4 -2 190.1 200.9 2.1 o
8 4 0 112.2 118.9 1.6 o
8 4 2 192.7 208.4 2.4 o
8 4 4 2946.0 2956.1 12.1 o
8 6 -6 52.4 43.8 3.2 o
8 6 -4 74.8 54.9 3.1 o
8 6 -2 70.6 66.1 1.8 o
8 6 0 4.0 0.0 0.6 o
8 6 2 68.8 59.1 2.0 o
8 6 4 72.2 62.2 2.0 o
8 6 6 45.3 46.9 3.1 o
8 8 -8 489.6 642.3 51.3 o
8 8 -6 11.8 10.9 2.1 o
8 8 -4 70.8 78.0 2.5 o
8 8 -2 220.2 228.7 2.7 o
8 8 0 1163.0 1167.6 6.6 o
8 8 2 214.5 226.4 3.9 o
8 8 4 75.1 94.2 2.7 o
8 8 6 9.7 13.5 1.3 o
8 8 8 487.7 600.7 35.8 o
9 1 -1 409.9 438.8 3.8 o
9 1 1 478.3 509.4 4.4 o
9 3 -3 137.4 136.5 2.2 o
9 3 -1 551.5 536.1 3.9 o
9 3 1 559.2 551.4 2.8 o
9 3 3 130.0 131.6 3.9 o
9 5 -5 126.8 122.9 3.0 o
9 5 -3 242.9 285.1 3.2 o
9 5 -1 309.3 315.6 3.7 o
9 5 1 295.2 308.1 3.2 o
9 5 3 224.6 262.1 2.3 o
9 5 5 155.4 157.9 3.2 o
9 7 -7 186.2 180.9 6.9 o
9 7 -5 101.2 110.0 3.1 o
9 7 -3 83.5 75.4 2.8 o
9 7 -1 337.0 331.9 3.4 o
9 7 1 329.8 321.8 3.4 o
9 7 3 78.8 71.2 1.9 o
9 7 5 109.6 121.1 1.9 o
9 7 7 178.7 180.0 3.7 o
9 9 -9 44.0 25.0 26.2 <
9 9 -7 89.5 105.3 9.1 o
9 9 -5 67.2 72.9 4.2 o
9 9 -3 86.5 65.0 4.8 o
9 9 -1 76.1 107.2 3.7 o
9 9 1 93.2 101.0 3.9 o
9 9 3 84.3 58.9 3.1 o
9 9 5 61.0 71.0 2.8 o
9 9 7 89.0 96.8 6.5 o
10 0 0 58.8 39.9 2.6 o
10 2 -2 956.8 926.9 5.3 o
10 2 0 283.6 250.8 2.5 o
10 2 2 1022.0 974.3 7.5 o
10 4 -4 50.4 56.9 3.3 o
10 4 -2 196.2 176.2 2.6 o
10 4 0 4.9 15.7 0.7 o
10 4 2 205.4 188.0 3.4 o
10 4 4 41.7 47.1 2.3 o
10 6 -6 455.1 504.1 5.6 o
10 6 -4 90.8 121.0 3.2 o
10 6 -2 400.2 403.0 4.4 o
10 6 0 305.2 303.5 3.8 o
10 6 2 379.6 388.8 4.0 o
10 6 4 95.7 123.3 2.5 o
10 6 6 459.5 519.6 5.3 o
10 8 -8 24.4 18.2 4.7 o
10 8 -6 27.9 21.7 2.6 o
10 8 -4 7.0 2.5 1.4 o
10 8 -2 42.1 40.5 2.8 o
10 8 0 15.7 21.4 1.4 o
10 8 2 46.3 43.5 2.0 o
10 8 4 6.0 2.1 1.1 o
10 8 6 37.0 27.0 2.9 o
10 8 8 25.1 19.9 3.2 o
10 10 -6 94.2 97.3 6.9 o
10 10 -4 96.8 88.8 7.8 o
10 10 -2 206.1 195.4 5.9 o
10 10 0 64.9 76.4 3.5 o
10 10 2 204.9 200.0 7.7 o
10 10 4 98.8 89.8 4.0 o
10 10 6 73.9 83.9 7.2 o
11 1 -1 64.3 60.0 3.5 o
11 1 1 50.3 48.1 4.3 o
11 3 -3 13.9 33.9 1.8 o
11 3 -1 277.6 312.1 3.8 o
11 3 1 252.5 296.3 3.2 o
11 3 3 17.7 35.7 1.9 o
11 5 -5 64.8 64.4 3.9 o
11 5 -3 59.4 60.4 2.6 o
11 5 -1 176.2 176.9 3.3 o
11 5 1 177.8 177.2 2.8 o
11 5 3 53.2 56.6 2.4 o
11 5 5 64.7 64.3 2.7 o
11 7 -7 6.6 8.9 1.7 o
11 7 -5 99.6 89.6 4.4 o
11 7 -3 111.4 84.8 3.1 o
11 7 -1 46.7 93.6 2.0 o
11 7 1 48.9 97.8 2.0 o
11 7 3 117.9 86.5 2.5 o
11 7 5 99.9 85.4 2.4 o
11 7 7 10.1 9.2 2.8 o
11 9 -7 25.6 11.2 5.3 o
11 9 -5 112.4 112.2 5.5 o
11 9 -3 107.6 114.1 3.8 o
11 9 -1 40.5 47.7 2.9 o
11 9 1 50.0 53.7 2.8 o
11 9 3 111.3 117.9 3.4 o
11 9 5 109.5 107.2 4.4 o
11 9 7 18.2 8.6 21.2 <
11 11 -3 5.2 49.6 11.6 <
11 11 -1 11.8 6.6 3.7 o
11 11 1 18.1 10.2 5.0 o
11 11 3 57.2 47.4 0.3 o
12 0 0 125.6 168.5 5.8 o
12 2 -2 43.2 51.0 3.8 o
12 2 0 86.3 74.7 2.2 o
12 2 2 28.3 42.8 2.2 o
12 4 -4 138.0 155.4 5.3 o
12 4 -2 72.6 91.5 2.5 o
12 4 0 608.0 529.4 5.5 o
12 4 2 71.3 94.1 2.4 o
12 4 4 149.4 170.0 4.2 o
12 6 -6 23.7 49.6 3.3 o
12 6 -4 14.2 14.8 1.8 o
12 6 -2 12.4 17.2 1.2 o
12 6 0 77.6 66.9 2.9 o
12 6 2 11.6 14.6 1.6 o
12 6 4 18.8 17.4 2.2 o
12 6 6 11.5 45.4 2.5 o
12 8 -6 33.2 34.2 3.1 o
12 8 -4 236.6 239.2 5.7 o
12 8 -2 53.3 39.2 5.1 o
12 8 0 75.8 88.1 3.4 o
12 8 2 43.5 41.9 3.0 o
12 8 4 231.4 231.7 6.8 o
12 8 6 40.1 36.3 4.6 o
12 10 -4 5.1 11.9 11.1 <
12 10 -2 14.2 11.5 7.3 <
12 10 0 10.1 0.0 2.4 o
12 10 2 15.6 10.9 4.8 o
12 10 4 10.7 13.9 4.2 o
13 1 -1 74.3 88.8 3.7 o
13 1 1 67.3 82.9 4.0 o
13 3 -3 25.3 46.5 2.1 o
13 3 -1 140.6 126.0 4.0 o
13 3 1 128.9 120.5 3.2 o
13 3 3 26.2 47.0 2.0 o
13 5 -5 11.3 5.1 1.1 o
13 5 -3 23.5 20.8 2.3 o
13 5 -1 101.4 125.0 3.5 o
13 5 1 102.9 123.5 3.0 o
13 5 3 27.1 20.3 3.4 o
13 5 5 20.2 3.4 2.7 o
13 7 -5 79.6 65.3 3.8 o
13 7 -3 90.8 89.1 4.1 o
13 7 -1 12.5 9.2 1.9 o
13 7 1 10.6 7.9 1.5 o
13 7 3 97.5 86.5 6.8 o
13 7 5 61.1 63.4 4.8 o
13 9 -3 37.0 45.1 5.0 o
13 9 -1 13.7 4.3 7.0 <
13 9 1 5.2 6.9 3.3 <
13 9 3 30.2 53.7 23.6 <
14 0 0 14.5 10.3 2.5 o
14 2 -2 154.3 135.7 6.3 o
14 2 0 59.2 75.0 3.2 o
14 2 2 180.5 143.6 13.4 o
14 4 -4 5.9 14.6 1.8 o
14 4 -2 44.7 51.5 3.7 o
14 4 0 15.5 22.0 2.1 o
14 4 2 47.6 53.0 4.1 o
14 4 4 3.1 14.6 0.9 o
14 6 -4 32.2 27.8 4.9 o
14 6 -2 158.9 147.1 7.3 o
14 6 0 12.1 17.4 2.2 o
14 6 2 151.4 140.8 5.3 o
14 6 4 32.2 32.2 5.1 o
14 8 0 4.7 0.8 13.7 <
15 1 -1 80.9 74.0 5.3 o
15 1 1 69.8 75.9 6.5 o
15 3 -3 55.8 58.3 6.1 o
15 3 -1 13.3 26.5 1.4 o
15 3 1 11.3 25.9 2.5 o
15 3 3 32.1 53.1 5.3 o
15 5 -3 27.6 23.0 1.3 o
15 5 -1 15.5 36.9 1.3 o
15 5 1 29.5 37.8 9.1 o
15 5 3 58.3 24.0 22.1 o
16 0 0 135.0 98.4 10.5 o
16 2 0 63.2 34.0 27.7 o