#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103089.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103089_Fobs
loop_
_publ_author_name
'Albert, St\'ephanie'
'Pillet, S\'ebastien'
'Lecomte, Claude'
'Pradel, Annie'
'Ribes, Michel'
_publ_section_title
;
 Disorder in Ag~7~GeSe~5~I, a superionic conductor:
 temperature-dependent anharmonic structural study
;
_journal_coeditor_code           CK5029
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              1
_journal_page_last               11
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           216
_symmetry_space_group_name_Hall  'F -4 2 3'
_symmetry_space_group_name_H-M   'F -4 3 m'
_[local]_cod_data_source_file    ck5029475Ksup11.hkl
_[local]_cod_data_source_block   475K
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_intensity_meas
_refln_intensity_calc
_refln_intensity_sigma
_refln_observed_status
1 1 1 259.6 243.0 2.5 o
2 0 0 3.4 6.1 0.3 o
2 2 -2 13240.0 13398.2 25.0 o
2 2 0 121.6 165.1 1.6 o
2 2 2 14360.0 14614.1 47.6 o
3 1 -1 1046.0 1047.3 2.9 o
3 1 1 1130.0 1090.0 2.9 o
3 3 -3 4178.0 3991.9 47.2 o
3 3 -1 1113.0 1129.6 2.7 o
3 3 1 1002.0 995.6 2.9 o
3 3 3 3536.0 3582.8 6.6 o
4 0 0 1747.0 1782.9 3.0 o
4 2 -2 1253.0 1263.2 3.2 o
4 2 0 92.7 87.6 0.9 o
4 2 2 1238.0 1272.3 3.6 o
4 4 -4 137.7 149.9 2.5 o
4 4 -2 214.2 205.6 1.7 o
4 4 0 13740.0 13711.4 14.2 o
4 4 2 217.0 207.8 2.1 o
4 4 4 205.4 223.0 4.1 o
5 1 -1 4189.0 4114.5 5.1 o
5 1 1 4133.0 4171.7 5.3 o
5 3 -3 643.0 637.5 2.3 o
5 3 -1 737.9 715.2 1.9 o
5 3 1 677.6 663.3 1.6 o
5 3 3 623.6 599.6 2.8 o
5 5 -5 1025.0 1023.6 6.1 o
5 5 -3 613.3 616.8 4.7 o
5 5 -1 95.3 90.6 1.4 o
5 5 1 141.9 147.9 2.1 o
5 5 3 633.5 658.1 3.7 o
5 5 5 1082.0 1050.5 4.2 o
6 0 0 626.2 618.6 2.8 o
6 2 -2 2248.0 2204.5 4.5 o
6 2 0 737.0 740.2 1.8 o
6 2 2 1947.0 1933.7 5.5 o
6 4 -4 14.6 9.1 1.5 o
6 4 -2 190.4 190.2 1.2 o
6 4 0 82.6 81.5 0.9 o
6 4 2 200.7 203.4 1.3 o
6 4 4 8.8 8.3 1.3 o
6 6 -6 632.3 667.1 9.5 o
6 6 -4 319.0 328.4 3.5 o
6 6 -2 1554.0 1606.6 6.1 o
6 6 0 801.0 817.8 4.8 o
6 6 2 1652.0 1713.3 5.7 o
6 6 4 340.2 344.8 2.8 o
6 6 6 548.8 571.8 4.7 o
7 1 -1 727.6 693.5 2.9 o
7 1 1 781.1 760.3 2.7 o
7 3 -3 363.8 339.5 3.0 o
7 3 -1 114.0 118.1 1.4 o
7 3 1 130.5 141.4 1.6 o
7 3 3 410.4 403.3 3.3 o
7 5 -5 219.9 244.7 3.0 o
7 5 -3 430.2 445.9 3.0 o
7 5 -1 248.4 245.7 1.9 o
7 5 1 254.0 244.2 1.9 o
7 5 3 422.4 437.2 2.3 o
7 5 5 210.4 232.7 3.5 o
7 7 -7 118.7 94.0 4.5 o
7 7 -5 48.8 57.8 2.5 o
7 7 -3 57.0 52.3 2.6 o
7 7 -1 149.3 167.3 2.5 o
7 7 1 133.0 150.1 2.0 o
7 7 3 38.6 35.8 1.2 o
7 7 5 58.6 58.7 2.1 o
7 7 7 128.7 111.4 6.2 o
8 0 0 3360.0 3321.7 8.8 o
8 2 -2 300.4 292.9 3.5 o
8 2 0 21.3 19.4 0.9 o
8 2 2 288.0 289.0 2.8 o
8 4 -4 2258.0 2188.2 9.5 o
8 4 -2 104.5 114.3 1.5 o
8 4 0 68.9 81.5 1.4 o
8 4 2 113.2 119.9 1.6 o
8 4 4 2204.0 2137.7 7.1 o
8 6 -6 34.9 32.8 1.9 o
8 6 -4 47.9 37.7 1.5 o
8 6 -2 96.2 83.0 1.8 o
8 6 0 4.9 0.2 0.7 o
8 6 2 79.7 79.3 1.4 o
8 6 4 54.2 40.5 1.2 o
8 6 6 33.1 34.3 2.5 o
8 8 -8 328.4 395.4 38.6 o
8 8 -6 3.2 3.3 1.0 o
8 8 -4 28.2 38.8 2.2 o
8 8 -2 110.2 103.1 2.3 o
8 8 0 800.0 835.4 5.7 o
8 8 2 118.7 99.6 2.2 o
8 8 4 31.4 47.5 1.8 o
8 8 6 8.9 4.3 1.4 o
8 8 8 320.3 378.1 8.5 o
9 1 -1 274.9 306.6 2.7 o
9 1 1 331.6 350.6 2.6 o
9 3 -3 96.7 116.9 2.2 o
9 3 -1 395.6 382.8 2.3 o
9 3 1 413.7 392.9 2.2 o
9 3 3 103.9 117.5 1.9 o
9 5 -5 67.9 88.7 3.1 o
9 5 -3 162.1 187.2 2.1 o
9 5 -1 186.3 213.2 2.3 o
9 5 1 183.4 211.3 2.6 o
9 5 3 154.4 173.3 1.9 o
9 5 5 88.1 108.8 2.7 o
9 7 -7 112.5 104.4 6.1 o
9 7 -5 60.6 63.7 2.3 o
9 7 -3 67.8 79.4 1.9 o
9 7 -1 212.7 230.1 2.5 o
9 7 1 208.8 224.0 2.8 o
9 7 3 64.2 74.4 1.7 o
9 7 5 67.3 70.3 1.7 o
9 7 7 96.4 105.7 2.5 o
9 9 -9 22.6 12.4 19.6 <
9 9 -7 82.5 61.5 3.6 o
9 9 -5 28.7 24.9 2.3 o
9 9 -3 42.7 52.3 2.0 o
9 9 -1 56.5 59.8 1.9 o
9 9 1 69.5 62.2 3.0 o
9 9 3 47.6 49.8 2.5 o
9 9 5 18.9 24.8 2.5 o
9 9 7 51.3 57.8 5.8 o
9 9 9 1.6 16.9 10.0 <
10 0 0 68.3 44.0 3.5 o
10 2 -2 643.1 626.3 4.9 o
10 2 0 209.7 172.9 2.0 o
10 2 2 664.1 658.6 3.9 o
10 4 -4 31.8 33.1 2.5 o
10 4 -2 140.1 146.9 2.0 o
10 4 0 3.7 4.2 0.5 o
10 4 2 145.7 154.1 2.3 o
10 4 4 30.9 30.2 1.8 o
10 6 -6 253.7 275.2 4.8 o
10 6 -4 53.5 49.4 2.9 o
10 6 -2 252.9 269.1 3.7 o
10 6 0 198.9 193.4 2.4 o
10 6 2 235.3 257.9 2.8 o
10 6 4 54.4 50.3 1.8 o
10 6 6 259.7 287.2 4.1 o
10 8 -8 16.4 13.9 3.6 o
10 8 -6 26.6 23.0 2.0 o
10 8 -4 4.9 0.5 1.2 o
10 8 -2 28.4 31.6 1.6 o
10 8 0 19.3 16.5 1.4 o
10 8 2 27.1 32.0 1.4 o
10 8 4 6.3 0.4 0.7 o
10 8 6 22.8 24.9 2.0 o
10 8 8 8.9 14.5 2.1 o
10 10 -6 68.1 60.0 5.8 o
10 10 -4 46.4 54.0 5.0 o
10 10 -2 102.0 111.0 4.5 o
10 10 0 16.4 23.2 2.2 o
10 10 2 123.3 115.2 4.3 o
10 10 4 42.9 55.2 1.6 o
10 10 6 41.4 53.4 3.2 o
11 1 -1 44.4 52.0 2.7 o
11 1 1 37.0 45.6 1.9 o
11 3 -3 14.8 30.7 1.3 o
11 3 -1 148.4 178.2 1.9 o
11 3 1 152.6 168.9 2.5 o
11 3 3 15.0 29.0 1.7 o
11 5 -5 38.4 37.6 3.1 o
11 5 -3 42.9 47.1 1.9 o
11 5 -1 123.2 135.5 2.1 o
11 5 1 127.4 136.2 2.3 o
11 5 3 35.3 43.6 1.5 o
11 5 5 41.1 37.5 2.3 o
11 7 -7 8.2 5.4 2.0 o
11 7 -5 63.0 62.3 3.3 o
11 7 -3 49.2 45.6 2.4 o
11 7 -1 26.5 38.8 1.9 o
11 7 1 33.8 41.0 1.7 o
11 7 3 60.2 48.2 2.0 o
11 7 5 55.1 59.6 2.4 o
11 7 7 14.6 5.7 3.5 o
11 9 -7 18.5 11.9 4.8 o
11 9 -5 66.5 62.6 5.6 o
11 9 -3 69.4 66.8 3.8 o
11 9 -1 16.0 26.2 2.3 o
11 9 1 20.4 29.1 2.0 o
11 9 3 70.2 68.3 4.0 o
11 9 5 56.0 61.2 3.3 o
11 9 7 7.2 10.1 0.3 o
11 11 -3 6.2 11.8 15.3 <
11 11 -1 10.9 14.2 3.6 o
11 11 1 12.6 13.8 3.4 o
11 11 3 17.4 11.9 3.0 o
12 0 0 75.8 64.3 2.3 o
12 2 -2 29.7 39.4 1.9 o
12 2 0 44.3 30.3 1.5 o
12 2 2 28.6 36.3 2.2 o
12 4 -4 66.6 56.6 2.1 o
12 4 -2 37.1 40.7 1.8 o
12 4 0 387.1 388.2 3.6 o
12 4 2 38.4 40.9 1.6 o
12 4 4 78.5 63.2 3.6 o
12 6 -6 20.1 27.9 3.4 o
12 6 -4 9.6 4.1 0.7 o
12 6 -2 13.8 15.7 2.2 o
12 6 0 37.9 40.6 2.3 o
12 6 2 9.7 15.3 1.2 o
12 6 4 11.1 5.0 0.9 o
12 6 6 22.0 27.5 4.0 o
12 8 -6 22.9 17.3 2.8 o
12 8 -4 142.2 150.8 5.0 o
12 8 -2 12.4 15.6 1.8 o
12 8 0 21.4 33.3 1.8 o
12 8 2 17.0 17.1 2.1 o
12 8 4 128.6 146.7 4.4 o
12 8 6 17.4 17.6 3.0 o
12 10 -4 15.7 9.3 9.9 <
12 10 -2 6.1 9.1 3.7 <
12 10 0 8.0 0.3 2.3 o
12 10 2 7.3 9.0 2.4 o
12 10 4 20.4 9.5 16.1 <
13 1 -1 39.1 52.8 3.1 o
13 1 1 33.1 50.9 2.3 o
13 3 -3 31.9 37.1 2.5 o
13 3 -1 81.5 88.6 2.3 o
13 3 1 78.9 84.3 2.3 o
13 3 3 20.0 36.3 2.6 o
13 5 -5 6.3 6.8 2.4 o
13 5 -3 16.4 15.6 2.2 o
13 5 -1 55.5 54.5 2.6 o
13 5 1 55.4 55.3 1.9 o
13 5 3 23.7 16.4 2.3 o
13 5 5 6.7 6.2 2.7 o
13 7 -5 35.2 40.2 3.0 o
13 7 -3 54.6 52.1 3.3 o
13 7 -1 7.8 11.6 1.4 o
13 7 1 15.2 12.0 2.2 o
13 7 3 58.3 52.6 4.4 o
13 7 5 36.8 38.4 3.8 o
13 9 -3 23.8 22.3 6.7 o
13 9 -1 28.6 0.9 4.3 o
13 9 1 8.7 0.9 3.3 o
13 9 3 22.0 22.8 2.9 o
14 0 0 3.4 0.4 0.4 o
14 2 -2 91.5 83.9 4.2 o
14 2 0 33.4 41.0 1.9 o
14 2 2 98.9 84.0 2.2 o
14 4 -4 6.8 2.0 1.5 o
14 4 -2 24.2 24.0 2.1 o
14 4 0 15.5 11.7 1.9 o
14 4 2 20.6 24.6 2.7 o
14 4 4 17.0 2.0 5.8 o
14 6 -4 12.9 20.0 2.0 o
14 6 -2 66.7 71.7 2.8 o
14 6 0 16.1 10.9 3.1 o
14 6 2 74.0 70.9 3.0 o
14 6 4 14.7 21.6 3.6 o
14 8 0 5.2 0.0 13.3 <
14 8 2 12.9 12.2 13.2 <
15 1 -1 42.7 42.2 3.0 o
15 1 1 34.3 43.6 4.3 o
15 3 -3 17.2 20.0 0.3 o
15 3 -1 10.0 13.2 2.5 o
15 3 1 15.1 12.5 2.0 o
15 3 3 26.9 20.0 5.9 o
15 5 -3 21.4 22.7 5.2 o
15 5 -1 23.0 14.0 16.7 <
15 5 1 10.8 14.8 6.8 <
15 5 3 23.4 23.0 3.2 o
16 0 0 75.6 72.5 0.2 o
16 2 0 11.0 10.4 2.4 o
16 2 2 22.8 4.5 21.3 <