#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/34/2103480.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103480_Fobs loop_ _publ_author_name 'Saraswathi, N. T.' 'Vijayan, M.' _publ_section_title ; X-ray studies on crystalline complexes involving amino acids and peptides. XL. Conformational variability, recurring and new features of aggregation, and effect of chirality in the malonic acid complexes of DL- and L-arginine ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 1051 _journal_page_last 1056 _journal_volume 58 _journal_year 2002 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.553 _cell_angle_gamma 90.000 _cell_length_a 19.5587 _cell_length_b 5.0296 _cell_length_c 28.4071 _exptl_crystal_F_000 1264.00 _reflns_d_resolution_high .8905 _[local]_cod_data_source_file de0019DLsup2.hkl _[local]_cod_data_source_block DL #BEGIN Tags that were not found in dictionaries: _shelx_title ' DL-arginine complexed with malonic acid' _shelx_refln_list_code 4 _shelx_F_calc_maximum 259.52 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 404.49 428.72 14.93 o 4 0 0 59997.74 66310.63 685.27 o 6 0 0 451.83 462.20 46.13 o 8 0 0 31054.57 32758.68 502.40 o 10 0 0 13.66 .00 46.90 o 12 0 0 2196.42 2310.72 105.33 o 14 0 0 623.21 654.16 77.44 o 16 0 0 5842.58 5613.96 196.41 o 18 0 0 59.17 62.62 93.48 o 20 0 0 287.81 114.45 187.61 o 1 1 0 2397.93 2382.44 41.13 o 3 1 0 5109.54 5109.89 92.39 o 5 1 0 22033.12 23818.68 144.55 o 7 1 0 1435.91 1432.29 48.10 o 9 1 0 301.56 368.82 38.51 o 11 1 0 379.80 352.27 41.69 o 13 1 0 1583.70 1516.97 68.30 o 15 1 0 5.95 59.10 51.09 o 17 1 0 15.37 111.49 60.13 o 19 1 0 188.60 334.92 102.41 o 21 1 0 35.80 97.46 91.15 o 0 2 0 3689.30 4070.92 102.92 o 2 2 0 694.81 561.20 34.26 o 4 2 0 3487.40 3537.73 66.73 o 6 2 0 245.16 263.14 28.63 o 8 2 0 1938.19 2016.39 59.17 o 10 2 0 16.87 68.69 34.45 o 12 2 0 1334.80 1317.66 83.34 o 14 2 0 2.71 35.73 55.29 o 16 2 0 419.17 423.21 75.77 o 18 2 0 6.08 56.65 74.77 o 20 2 0 114.47 188.99 94.03 o 1 3 0 690.27 739.75 44.77 o 3 3 0 .31 62.31 29.59 o 5 3 0 351.54 385.69 36.98 o 7 3 0 210.05 255.38 42.90 o 9 3 0 5.38 8.20 46.88 o 11 3 0 .07 38.93 59.56 o 13 3 0 .03 .00 67.22 o 15 3 0 981.12 836.22 105.14 o 17 3 0 2.33 152.91 81.57 o 0 4 0 870.21 911.34 99.05 o 2 4 0 15.21 44.89 32.60 o 4 4 0 803.41 851.14 60.13 o 6 4 0 181.13 278.64 54.69 o 8 4 0 .44 .00 61.34 o 10 4 0 170.93 .00 69.26 o 12 4 0 69.94 87.99 76.81 o 14 4 0 199.01 169.63 85.94 o 1 5 0 52.11 110.90 66.80 o 3 5 0 52.68 34.52 62.25 o 5 5 0 130.03 181.38 78.64 o 7 5 0 30.89 128.09 76.40 o 9 5 0 30.13 68.53 87.35 o -21 1 1 22.25 132.34 94.30 o -19 1 1 5.54 93.59 72.20 o -17 1 1 114.09 98.82 62.11 o -15 1 1 3867.09 3449.00 128.83 o -13 1 1 256.15 171.99 45.32 o -11 1 1 1794.47 1847.31 66.30 o -9 1 1 138.89 173.68 35.11 o -7 1 1 10584.26 11621.52 128.68 o -5 1 1 26829.12 26938.51 177.95 o -3 1 1 15037.18 15067.69 139.84 o -1 1 1 19664.02 20933.24 133.03 o 1 1 1 529.16 398.27 22.34 o 3 1 1 242.99 216.15 20.71 o 5 1 1 5720.16 5627.49 102.34 o 7 1 1 1534.70 1652.31 47.29 o 9 1 1 6633.51 6657.36 112.89 o 11 1 1 1989.59 1992.97 66.51 o 13 1 1 2183.69 2128.13 76.35 o 15 1 1 278.83 320.13 63.40 o 17 1 1 1060.80 1078.27 85.34 o 19 1 1 31.24 165.40 76.89 o 21 1 1 13.30 103.92 91.69 o -20 2 1 .02 164.58 92.04 o -18 2 1 648.48 741.75 104.43 o -16 2 1 237.96 271.22 71.58 o -14 2 1 5.80 89.34 54.95 o -12 2 1 2.05 78.31 51.22 o -10 2 1 18652.75 19228.22 285.59 o -8 2 1 3.94 54.19 30.49 o -6 2 1 4880.55 5367.84 86.34 o -4 2 1 912.51 856.08 38.01 o -2 2 1 641.01 776.51 38.06 o 0 2 1 1071.73 1096.55 41.95 o 2 2 1 184.27 189.55 27.12 o 4 2 1 906.60 1036.19 41.97 o 6 2 1 4254.75 4684.78 94.16 o 8 2 1 44.99 43.44 28.45 o 10 2 1 115.28 146.38 32.22 o 12 2 1 711.82 718.97 71.52 o 14 2 1 36.73 40.70 53.48 o 16 2 1 125.80 184.17 67.97 o 18 2 1 239.21 275.16 83.92 o 20 2 1 183.66 301.88 95.30 o -17 3 1 61.03 93.57 82.24 o -15 3 1 11.55 119.22 77.89 o -13 3 1 190.50 213.30 74.13 o -11 3 1 406.72 447.63 74.14 o -9 3 1 354.74 400.43 61.26 o -7 3 1 15.42 56.31 34.26 o -5 3 1 1623.09 1638.22 59.41 o -3 3 1 17.09 58.08 25.63 o -1 3 1 1397.22 1380.67 57.05 o 1 3 1 28.16 52.43 28.44 o 3 3 1 533.34 511.37 41.00 o 5 3 1 955.13 978.97 48.03 o 7 3 1 168.67 119.95 37.55 o 9 3 1 268.08 288.21 57.50 o 11 3 1 114.06 135.26 52.18 o 13 3 1 84.98 68.13 59.94 o 15 3 1 181.31 243.60 80.57 o 17 3 1 65.03 206.47 81.27 o -14 4 1 221.43 236.43 84.91 o -12 4 1 26.45 24.20 78.83 o -10 4 1 98.86 89.42 73.58 o -8 4 1 7.73 3.07 57.77 o -6 4 1 .24 41.98 52.58 o -4 4 1 31.90 124.80 39.68 o -2 4 1 194.65 201.33 38.15 o 0 4 1 176.48 240.85 38.14 o 2 4 1 9.58 81.96 37.70 o 4 4 1 86.58 87.34 40.27 o 6 4 1 763.58 737.81 64.53 o 8 4 1 2.19 .00 59.25 o 10 4 1 12.76 19.20 65.76 o 12 4 1 30.12 51.53 76.99 o 14 4 1 35.50 58.06 80.07 o -9 5 1 5.40 89.47 85.44 o -7 5 1 217.51 314.74 90.09 o -5 5 1 210.65 274.62 81.89 o -3 5 1 76.86 190.71 76.41 o -1 5 1 1445.91 1483.03 108.91 o 1 5 1 259.04 200.58 68.24 o 3 5 1 218.17 251.27 68.49 o 5 5 1 205.66 228.24 72.03 o 7 5 1 379.13 404.13 88.76 o 9 5 1 44.87 157.88 80.09 o -20 0 2 3313.97 2818.45 228.68 o -18 0 2 1062.31 953.74 122.02 o -16 0 2 311.46 273.41 90.83 o -14 0 2 7.38 3.49 75.00 o -12 0 2 596.50 688.40 80.54 o -10 0 2 5253.83 5508.03 139.09 o -8 0 2 890.66 988.56 63.92 o -6 0 2 5352.98 5943.71 119.66 o -4 0 2 16591.33 15691.21 150.33 o -2 0 2 3971.43 4127.53 85.11 o 0 0 2 931.13 614.90 166.66 o 2 0 2 9319.94 9001.50 150.31 o 4 0 2 938.53 964.81 36.69 o 6 0 2 23295.83 25017.91 816.94 o 8 0 2 19225.85 20509.50 608.82 o 10 0 2 3694.90 3314.57 107.90 o 12 0 2 1181.22 1205.09 80.15 o 14 0 2 1682.60 1632.11 100.62 o 16 0 2 4092.76 3987.89 191.91 o 18 0 2 478.47 592.06 108.01 o 20 0 2 6.05 94.53 203.30 o -21 1 2 295.18 302.45 111.79 o -19 1 2 14.82 136.44 77.52 o -17 1 2 631.41 640.03 75.40 o -15 1 2 1166.05 1063.61 75.94 o -13 1 2 135.68 157.46 45.51 o -11 1 2 4862.19 4843.94 98.70 o -9 1 2 7813.41 8391.08 115.75 o -7 1 2 218.18 219.53 32.69 o -5 1 2 2557.93 2676.93 55.21 o -3 1 2 4195.13 3912.05 56.73 o -1 1 2 7588.77 7160.32 76.78 o 1 1 2 319.74 151.43 16.03 o 3 1 2 16963.71 17195.59 267.98 o 5 1 2 10526.35 10001.75 184.65 o 7 1 2 5775.69 5567.32 87.70 o 9 1 2 235.87 282.98 33.38 o 11 1 2 797.93 861.91 50.25 o 13 1 2 2689.29 2650.10 92.04 o 15 1 2 671.95 743.22 73.88 o 17 1 2 66.43 142.62 59.50 o 19 1 2 68.32 106.77 74.86 o 21 1 2 12.77 66.33 91.43 o -20 2 2 287.00 229.37 100.67 o -18 2 2 2.21 47.59 80.43 o -16 2 2 1737.29 1529.21 122.47 o -14 2 2 75.06 151.75 64.53 o -12 2 2 1284.23 1245.93 81.47 o -10 2 2 385.19 425.92 43.81 o -8 2 2 200.34 230.95 34.99 o -6 2 2 4122.50 4379.70 84.63 o -4 2 2 3380.23 3725.01 69.74 o -2 2 2 .13 17.51 20.47 o 0 2 2 14.19 99.96 24.69 o 2 2 2 5842.94 5983.61 87.65 o 4 2 2 156.43 215.92 27.22 o 6 2 2 5836.87 5857.06 104.13 o 8 2 2 1782.20 1456.45 55.86 o 10 2 2 985.16 998.40 64.91 o 12 2 2 380.37 319.83 59.26 o 14 2 2 196.08 248.91 62.27 o 16 2 2 186.23 205.51 70.94 o 18 2 2 104.67 152.81 72.85 o 20 2 2 125.46 243.01 91.61 o -17 3 2 1.39 57.91 83.43 o -15 3 2 124.86 206.87 81.57 o -13 3 2 303.01 378.86 98.51 o -11 3 2 7.62 26.37 64.40 o -9 3 2 881.93 915.77 65.12 o -7 3 2 379.62 392.55 40.91 o -5 3 2 10148.90 9594.62 138.60 o -3 3 2 216.69 187.71 30.02 o -1 3 2 1164.85 1044.67 47.38 o 1 3 2 715.76 746.65 44.92 o 3 3 2 6156.89 6057.81 127.84 o 5 3 2 335.61 459.36 40.18 o 7 3 2 3013.42 2790.93 85.52 o 9 3 2 521.17 468.04 54.55 o 11 3 2 715.46 709.83 71.66 o 13 3 2 172.64 299.58 71.31 o 15 3 2 49.05 112.42 78.75 o 17 3 2 124.68 130.13 79.81 o -14 4 2 494.49 538.08 99.20 o -12 4 2 33.27 72.30 74.68 o -10 4 2 191.23 244.93 80.47 o -8 4 2 .05 69.14 66.18 o -6 4 2 87.64 102.78 51.94 o -4 4 2 600.65 653.76 52.09 o -2 4 2 447.30 519.95 45.81 o 0 4 2 93.33 131.36 36.56 o 2 4 2 270.51 304.49 47.22 o 4 4 2 152.82 129.17 43.82 o 6 4 2 .01 59.22 44.67 o 8 4 2 15.77 .00 44.46 o 10 4 2 .00 71.72 70.70 o 12 4 2 351.75 373.99 83.06 o 14 4 2 80.74 130.41 87.54 o -9 5 2 53.71 75.42 87.21 o -7 5 2 .26 75.31 81.48 o -5 5 2 244.66 266.34 88.23 o -3 5 2 240.01 274.13 71.03 o -1 5 2 138.10 227.98 81.33 o 1 5 2 29.68 66.37 57.44 o 3 5 2 1995.70 1630.24 139.52 o 5 5 2 240.67 261.72 67.33 o 7 5 2 519.64 451.51 83.79 o 9 5 2 5.64 113.08 88.13 o -21 1 3 330.79 217.03 119.38 o -19 1 3 23.02 154.46 76.94 o -17 1 3 18.19 47.61 67.05 o -15 1 3 1090.79 972.85 68.43 o -13 1 3 6.11 61.00 43.01 o -11 1 3 507.14 625.46 48.69 o -9 1 3 945.67 852.66 47.92 o -7 1 3 2299.47 2002.52 56.09 o -5 1 3 3288.12 3157.77 58.95 o -3 1 3 927.11 632.66 32.10 o -1 1 3 8333.74 8609.58 135.84 o 1 1 3 1576.07 1485.27 35.40 o 3 1 3 55593.39 58142.45 581.96 o 5 1 3 4947.31 4650.85 91.68 o 7 1 3 12299.32 12413.99 286.21 o 9 1 3 .09 2.64 31.76 o 11 1 3 2594.02 2565.63 85.66 o 13 1 3 863.40 802.05 62.24 o 15 1 3 562.49 582.84 69.63 o 17 1 3 .01 8.37 57.35 o 19 1 3 1771.59 1781.31 122.78 o 21 1 3 103.15 256.24 99.66 o -20 2 3 8.41 113.71 94.59 o -18 2 3 12.67 122.01 84.62 o -16 2 3 750.29 557.96 93.72 o -14 2 3 410.80 380.47 73.29 o -12 2 3 2031.01 1900.35 74.32 o -10 2 3 228.36 221.99 38.99 o -8 2 3 1291.39 1426.36 55.91 o -6 2 3 54.09 52.07 29.28 o -4 2 3 6197.03 6158.73 91.71 o -2 2 3 2867.04 3020.80 61.77 o 0 2 3 43.46 34.36 20.46 o 2 2 3 50.65 23.57 18.47 o 4 2 3 209.98 279.98 27.87 o 6 2 3 5991.47 6108.01 115.62 o 8 2 3 1025.90 921.82 56.43 o 10 2 3 51.83 23.48 44.11 o 12 2 3 49.84 62.47 43.93 o 14 2 3 917.44 938.67 83.34 o 16 2 3 67.61 107.51 61.37 o 18 2 3 145.17 303.27 78.79 o 20 2 3 41.44 71.53 89.24 o -17 3 3 20.56 113.63 80.64 o -15 3 3 2.56 47.33 76.02 o -13 3 3 1593.86 1368.69 117.71 o -11 3 3 .14 26.88 63.89 o -9 3 3 1.23 13.28 49.45 o -7 3 3 626.07 665.94 48.59 o -5 3 3 5454.69 5627.14 102.99 o -3 3 3 288.13 249.98 34.11 o -1 3 3 203.97 247.56 31.59 o 1 3 3 298.78 293.08 31.92 o 3 3 3 336.87 428.32 44.11 o 5 3 3 164.44 155.12 32.66 o 7 3 3 20.23 89.04 47.90 o 9 3 3 7.70 45.61 44.02 o 11 3 3 1219.76 1326.86 86.84 o 13 3 3 114.54 178.88 54.86 o 15 3 3 107.91 217.72 72.57 o 17 3 3 212.29 319.22 88.99 o -14 4 3 1.42 76.05 79.86 o -12 4 3 1128.10 915.41 113.57 o -10 4 3 89.13 114.26 70.52 o -8 4 3 343.52 288.86 77.56 o -6 4 3 75.44 153.46 59.33 o -4 4 3 3.35 84.65 43.24 o -2 4 3 38.30 109.97 38.20 o 0 4 3 104.99 152.84 38.45 o 2 4 3 18.27 68.88 41.02 o 4 4 3 30.90 71.95 44.46 o 6 4 3 7.48 73.97 45.30 o 8 4 3 248.49 198.29 53.54 o 10 4 3 1.46 .00 67.75 o 12 4 3 119.09 93.20 79.54 o 14 4 3 21.69 25.91 85.35 o -9 5 3 .16 60.21 91.74 o -7 5 3 278.23 301.96 88.87 o -5 5 3 18.15 2.82 76.94 o -3 5 3 .11 75.79 82.73 o -1 5 3 172.80 239.68 88.71 o 1 5 3 848.76 847.44 81.05 o 3 5 3 53.68 65.36 68.50 o 5 5 3 190.26 133.94 65.43 o 7 5 3 468.42 418.97 85.31 o 9 5 3 19.09 84.64 88.26 o -20 0 4 .33 .00 124.19 o -18 0 4 693.85 471.65 94.70 o -16 0 4 .51 5.71 73.77 o -14 0 4 1173.61 1124.22 100.87 o -12 0 4 5452.15 5301.78 161.73 o -10 0 4 12.56 11.61 53.08 o -8 0 4 5870.67 5855.92 132.30 o -6 0 4 12814.39 13879.89 173.58 o -4 0 4 1.14 35.15 38.20 o -2 0 4 10519.19 9780.92 245.92 o 0 0 4 4277.00 4800.81 108.86 o 2 0 4 15273.41 15677.12 514.84 o 4 0 4 23694.89 24877.03 740.94 o 6 0 4 39373.74 39491.41 1522.40 o 8 0 4 1402.49 1496.04 64.64 o 10 0 4 4304.56 4343.37 229.22 o 12 0 4 1819.45 1690.11 89.93 o 14 0 4 831.81 914.61 80.82 o 16 0 4 34.79 .00 88.60 o 18 0 4 82.35 44.40 119.80 o 20 0 4 4.90 152.08 125.10 o -21 1 4 812.81 878.57 141.67 o -19 1 4 .96 79.78 127.05 o -17 1 4 21.26 85.58 61.57 o -15 1 4 403.59 537.67 59.66 o -13 1 4 2652.29 2497.99 85.11 o -11 1 4 200.80 214.56 41.14 o -9 1 4 3751.84 3740.70 81.40 o -7 1 4 789.73 865.62 42.17 o -5 1 4 1430.80 1396.36 43.05 o -3 1 4 4449.33 4552.89 81.71 o -1 1 4 182.70 197.43 24.85 o 1 1 4 67353.03 67823.02 522.76 o 3 1 4 4499.47 3670.61 76.29 o 5 1 4 26442.15 28293.38 397.63 o 7 1 4 20308.71 21315.93 583.99 o 9 1 4 2433.19 2616.94 69.77 o 11 1 4 1772.94 1770.44 66.85 o 13 1 4 1362.34 1491.13 74.86 o 15 1 4 1737.32 1849.82 98.71 o 17 1 4 299.50 276.85 64.94 o 19 1 4 194.25 326.52 84.09 o 21 1 4 150.86 358.93 100.13 o -20 2 4 4.47 41.14 91.62 o -18 2 4 190.83 199.35 86.18 o -16 2 4 188.59 321.02 83.34 o -14 2 4 80.42 98.52 69.34 o -12 2 4 339.44 315.60 51.34 o -10 2 4 206.43 287.19 41.87 o -8 2 4 1420.92 1502.60 57.72 o -6 2 4 6827.13 7493.89 105.95 o -4 2 4 1096.14 1059.93 43.87 o -2 2 4 15837.00 17016.11 195.08 o 0 2 4 1301.55 1277.45 45.29 o 2 2 4 169.77 180.67 22.89 o 4 2 4 274.60 295.55 35.63 o 6 2 4 2048.88 1855.75 61.86 o 8 2 4 666.39 722.70 60.76 o 10 2 4 2165.52 1887.37 81.87 o 12 2 4 243.90 249.22 52.33 o 14 2 4 2569.80 2396.27 112.65 o 16 2 4 172.57 115.36 60.11 o 18 2 4 312.78 411.40 73.54 o 20 2 4 7.15 219.42 92.15 o -17 3 4 27.36 99.59 86.62 o -15 3 4 180.38 193.43 85.63 o -13 3 4 1911.17 1837.65 131.11 o -11 3 4 664.50 565.57 87.01 o -9 3 4 10.92 .00 41.49 o -7 3 4 741.04 866.60 54.36 o -5 3 4 186.87 233.81 38.55 o -3 3 4 1794.08 1715.02 62.80 o -1 3 4 228.44 263.29 34.70 o 1 3 4 469.31 502.88 38.57 o 3 3 4 2105.91 1822.01 62.21 o 5 3 4 145.73 166.57 38.66 o 7 3 4 202.26 295.78 54.24 o 9 3 4 1191.47 1255.31 82.72 o 11 3 4 128.04 147.06 51.35 o 13 3 4 18.46 40.30 53.86 o 15 3 4 52.84 111.55 69.57 o 17 3 4 17.15 140.71 83.71 o -14 4 4 75.07 61.59 81.90 o -12 4 4 41.36 .00 73.32 o -10 4 4 502.54 393.69 86.90 o -8 4 4 191.03 199.13 95.44 o -6 4 4 669.52 708.51 79.17 o -4 4 4 2466.22 2347.36 102.65 o -2 4 4 333.56 441.22 49.44 o 0 4 4 115.29 214.68 41.53 o 2 4 4 .51 67.10 41.73 o 4 4 4 309.13 389.28 58.48 o 6 4 4 2538.22 2531.24 127.07 o 8 4 4 460.75 424.31 59.89 o 10 4 4 844.24 768.43 85.10 o 12 4 4 345.11 416.41 89.88 o 14 4 4 81.66 72.85 75.01 o -9 5 4 5.35 47.17 85.51 o -7 5 4 95.26 64.36 81.85 o -5 5 4 65.30 201.54 87.22 o -3 5 4 91.64 143.02 81.10 o -1 5 4 117.70 264.52 83.53 o 1 5 4 6.06 83.03 71.41 o 3 5 4 3.94 31.67 64.00 o 5 5 4 78.51 101.40 57.58 o 7 5 4 26.46 95.51 67.50 o 9 5 4 6.82 107.01 76.90 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184.04 116.24 o -11 1 25 82.00 186.40 85.63 o -9 1 25 3.02 12.07 72.31 o -7 1 25 252.77 265.67 85.46 o -5 1 25 525.09 601.90 73.01 o -3 1 25 166.21 190.76 60.67 o -1 1 25 633.69 638.66 76.18 o 1 1 25 525.08 564.99 71.02 o 3 1 25 45.58 67.11 72.33 o 5 1 25 1241.10 1309.31 101.81 o 7 1 25 .04 128.02 64.98 o 9 1 25 1.52 152.55 86.08 o 11 1 25 208.93 353.16 93.57 o -10 2 25 275.46 259.02 78.14 o -8 2 25 548.83 598.56 78.37 o -6 2 25 954.08 962.93 87.84 o -4 2 25 14.26 58.34 59.00 o -2 2 25 53.73 178.90 60.95 o 0 2 25 .08 16.97 67.93 o 2 2 25 68.16 9.63 78.92 o 4 2 25 55.95 19.89 74.18 o 6 2 25 34.08 124.22 77.29 o 8 2 25 221.26 350.20 94.38 o 10 2 25 134.99 207.23 92.90 o -7 3 25 96.05 111.05 69.34 o -5 3 25 .90 47.59 67.13 o -3 3 25 136.98 170.67 78.67 o -1 3 25 156.34 223.89 74.51 o 1 3 25 91.59 180.52 76.21 o 3 3 25 .34 174.00 86.94 o 5 3 25 78.20 135.75 87.60 o -12 0 26 125.24 358.77 403.77 o -10 0 26 509.78 466.00 139.12 o -8 0 26 524.21 605.61 140.89 o -6 0 26 878.75 804.99 147.00 o 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286.85 84.42 o 3 3 26 2.80 46.95 83.46 o -11 1 27 83.87 238.89 93.24 o -9 1 27 53.69 165.33 81.56 o -7 1 27 9.32 6.94 73.94 o -5 1 27 101.77 56.88 75.06 o -3 1 27 195.83 235.96 73.09 o -1 1 27 217.27 225.03 66.93 o 1 1 27 77.86 197.36 63.86 o 3 1 27 1.89 50.59 79.02 o 5 1 27 46.89 100.58 80.99 o 7 1 27 50.87 93.53 84.74 o 9 1 27 1.75 100.53 84.95 o -8 2 27 387.37 482.48 89.91 o -6 2 27 1432.68 1378.92 102.27 o -4 2 27 31.87 70.56 60.74 o -2 2 27 149.84 213.15 70.73 o 0 2 27 120.86 304.98 93.57 o 2 2 27 16.04 .00 79.73 o 4 2 27 82.39 119.77 81.37 o 6 2 27 622.25 530.59 101.45 o 8 2 27 198.28 411.49 106.15 o -1 3 27 163.32 307.73 88.51 o -10 0 28 64.23 31.53 104.73 o -8 0 28 70.87 152.56 125.92 o -6 0 28 128.19 102.78 112.02 o -4 0 28 2780.07 2288.08 208.69 o -2 0 28 50.76 134.79 103.68 o 0 0 28 2391.48 2514.70 214.83 o 2 0 28 796.17 516.37 113.39 o 4 0 28 136.48 184.88 118.05 o 6 0 28 758.04 771.22 157.28 o 8 0 28 32.71 .00 115.69 o 10 0 28 140.52 269.25 208.88 o -9 1 28 492.36 463.67 94.59 o -7 1 28 311.53 342.25 89.82 o -5 1 28 166.17 253.90 83.60 o -3 1 28 196.98 249.28 83.93 o -1 1 28 364.24 414.58 75.83 o 1 1 28 305.34 384.85 92.63 o 3 1 28 705.61 730.19 104.13 o 5 1 28 816.80 849.36 174.89 o 7 1 28 98.56 200.49 87.17 o 9 1 28 9.75 177.51 103.31 o -6 2 28 72.08 179.90 66.09 o -4 2 28 39.23 136.07 65.42 o -2 2 28 46.73 83.54 77.56 o 0 2 28 90.82 238.52 87.47 o 2 2 28 146.54 95.44 83.42 o 4 2 28 21.62 34.45 91.46 o 6 2 28 237.25 210.07 90.80 o -7 1 29 26.78 38.10 76.18 o -5 1 29 403.15 452.24 91.52 o -3 1 29 .66 64.07 78.22 o -1 1 29 35.58 36.93 71.00 o 1 1 29 347.56 366.55 94.45 o 3 1 29 30.58 206.52 91.16 o 5 1 29 72.45 139.42 111.15 o 7 1 29 251.22 300.71 108.62 o -4 2 29 169.24 322.19 75.76 o -2 2 29 .48 57.19 96.81 o 0 2 29 343.31 391.69 97.90 o 2 2 29 115.89 121.35 88.42 o 4 2 29 193.38 132.46 90.47 o -6 0 30 389.54 399.09 124.55 o -4 0 30 173.73 329.72 126.84 o -2 0 30 .87 129.01 108.99 o 0 0 30 432.90 435.50 134.93 o 2 0 30 24.89 .00 125.20 o 6 0 30 107.94 408.59 183.12 o -5 1 30 120.77 176.72 80.51 o -3 1 30 4.53 116.60 81.61 o -1 1 30 282.99 336.74 90.72 o 1 1 30 26.91 .00 97.85 o 3 1 30 467.62 628.47 107.05 o 5 1 30 814.75 818.54 132.90 o -3 1 31 13.42 152.52 79.60 o -1 1 31 378.07 392.56 108.32 o 1 1 31 162.48 302.09 106.33 o 3 1 31 561.23 628.98 108.68 o