#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/38/2103806.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103806_Fobs loop_ _publ_author_name 'Bowes, Katharine F.' 'Ferguson, George' 'Lough, Alan J.' 'Zakaria, Choudhury M.' 'Glidewell, Christopher' _publ_section_title ; Phosphonoacetic acid as a building block in supramolecular chemistry: salts with organic polyamines ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 87 _journal_page_last 99 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 96.926 _cell_angle_beta 109.414 _cell_angle_gamma 105.483 _cell_length_a 11.7486 _cell_length_b 13.3913 _cell_length_c 13.8206 _exptl_crystal_F_000 752.00 _reflns_d_resolution_high 0.7671 _[local]_cod_data_source_file bm0057IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 210 - SHELXL' _shelx_refln_list_code 4 _shelx_F_calc_maximum 156.46 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k 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16.72 14.54 o 11 1 0 41.84 38.85 20.01 o 12 1 0 9.76 18.47 25.24 o 13 1 0 1.20 108.09 36.41 o -14 2 0 2.10 34.00 41.60 o -13 2 0 165.44 143.72 23.84 o -12 2 0 182.48 142.86 24.83 o -11 2 0 64.45 54.92 18.54 o -10 2 0 241.42 247.07 24.54 o -9 2 0 63.72 83.70 25.03 o -8 2 0 35.22 32.45 19.69 o -7 2 0 199.12 201.19 22.36 o -6 2 0 706.54 665.43 39.11 o -5 2 0 110.00 172.35 25.11 o -4 2 0 907.01 856.89 38.98 o -3 2 0 176.50 117.34 15.80 o -2 2 0 59.04 62.43 10.71 o -1 2 0 348.75 280.22 33.83 o 1 2 0 143.09 212.78 21.12 o 2 2 0 955.90 608.40 29.46 o 3 2 0 2398.84 2167.03 92.40 o 4 2 0 179.31 191.88 17.76 o 5 2 0 457.79 539.49 32.10 o 6 2 0 323.43 333.45 18.27 o 7 2 0 620.91 631.35 38.55 o 8 2 0 169.70 171.49 19.83 o 9 2 0 186.53 181.33 19.06 o 10 2 0 14.98 17.64 19.49 o 11 2 0 178.15 124.34 21.21 o 12 2 0 94.52 49.49 30.95 o -14 3 0 7.05 96.80 46.44 o -13 3 0 199.94 172.13 25.57 o -12 3 0 234.03 290.84 32.78 o -11 3 0 2.77 0.27 20.94 o -10 3 0 110.66 132.46 22.29 o -9 3 0 60.91 77.97 18.19 o 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